CN113230187A - 一种黑小米淀粉皮克林乳液及其制备方法 - Google Patents
一种黑小米淀粉皮克林乳液及其制备方法 Download PDFInfo
- Publication number
- CN113230187A CN113230187A CN202110591313.9A CN202110591313A CN113230187A CN 113230187 A CN113230187 A CN 113230187A CN 202110591313 A CN202110591313 A CN 202110591313A CN 113230187 A CN113230187 A CN 113230187A
- Authority
- CN
- China
- Prior art keywords
- black millet
- millet starch
- oil
- black
- emulsion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 244000062793 Sorghum vulgare Species 0.000 title claims abstract description 175
- 235000019713 millet Nutrition 0.000 title claims abstract description 175
- 229920002472 Starch Polymers 0.000 title claims abstract description 151
- 235000019698 starch Nutrition 0.000 title claims abstract description 151
- 239000008107 starch Substances 0.000 title claims abstract description 151
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 238000001484 Pickering emulsion method Methods 0.000 title description 2
- 239000000839 emulsion Substances 0.000 claims abstract description 91
- 239000008187 granular material Substances 0.000 claims abstract description 71
- 239000002245 particle Substances 0.000 claims abstract description 60
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 33
- 238000002156 mixing Methods 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 4
- 239000003921 oil Substances 0.000 claims description 37
- 235000019198 oils Nutrition 0.000 claims description 37
- 239000000341 volatile oil Substances 0.000 claims description 29
- 238000000227 grinding Methods 0.000 claims description 24
- 238000003756 stirring Methods 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 13
- 239000004570 mortar (masonry) Substances 0.000 claims description 12
- 239000002285 corn oil Substances 0.000 claims description 11
- 235000005687 corn oil Nutrition 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 11
- VFLDPWHFBUODDF-FCXRPNKRSA-N curcumin Chemical compound C1=C(O)C(OC)=CC(\C=C\C(=O)CC(=O)\C=C\C=2C=C(OC)C(O)=CC=2)=C1 VFLDPWHFBUODDF-FCXRPNKRSA-N 0.000 claims description 10
- 239000000126 substance Substances 0.000 claims description 9
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 claims description 8
- 230000000975 bioactive effect Effects 0.000 claims description 8
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 claims description 8
- 230000002209 hydrophobic effect Effects 0.000 claims description 7
- 239000008157 edible vegetable oil Substances 0.000 claims description 6
- 235000005976 Citrus sinensis Nutrition 0.000 claims description 5
- 240000002319 Citrus sinensis Species 0.000 claims description 5
- 244000178870 Lavandula angustifolia Species 0.000 claims description 5
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims description 5
- 235000019501 Lemon oil Nutrition 0.000 claims description 5
- 244000178231 Rosmarinus officinalis Species 0.000 claims description 5
- OENHQHLEOONYIE-UKMVMLAPSA-N all-trans beta-carotene Natural products CC=1CCCC(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C OENHQHLEOONYIE-UKMVMLAPSA-N 0.000 claims description 5
- 235000013734 beta-carotene Nutrition 0.000 claims description 5
- 239000011648 beta-carotene Substances 0.000 claims description 5
- TUPZEYHYWIEDIH-WAIFQNFQSA-N beta-carotene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2=CCCCC2(C)C TUPZEYHYWIEDIH-WAIFQNFQSA-N 0.000 claims description 5
- 229960002747 betacarotene Drugs 0.000 claims description 5
- 235000012754 curcumin Nutrition 0.000 claims description 5
- 239000004148 curcumin Substances 0.000 claims description 5
- 229940109262 curcumin Drugs 0.000 claims description 5
- VFLDPWHFBUODDF-UHFFFAOYSA-N diferuloylmethane Natural products C1=C(O)C(OC)=CC(C=CC(=O)CC(=O)C=CC=2C=C(OC)C(O)=CC=2)=C1 VFLDPWHFBUODDF-UHFFFAOYSA-N 0.000 claims description 5
- 239000001102 lavandula vera Substances 0.000 claims description 5
- 235000018219 lavender Nutrition 0.000 claims description 5
- 239000010501 lemon oil Substances 0.000 claims description 5
- 239000010502 orange oil Substances 0.000 claims description 5
- OENHQHLEOONYIE-JLTXGRSLSA-N β-Carotene Chemical compound CC=1CCCC(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C OENHQHLEOONYIE-JLTXGRSLSA-N 0.000 claims description 5
- 239000001100 (2S)-5,7-dihydroxy-2-(3-hydroxy-4-methoxyphenyl)chroman-4-one Substances 0.000 claims description 4
- KJPRLNWUNMBNBZ-QPJJXVBHSA-N (E)-cinnamaldehyde Chemical compound O=C\C=C\C1=CC=CC=C1 KJPRLNWUNMBNBZ-QPJJXVBHSA-N 0.000 claims description 4
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 claims description 4
- 239000005770 Eugenol Substances 0.000 claims description 4
- QUQPHWDTPGMPEX-UHFFFAOYSA-N Hesperidine Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(OC3C(C(O)C(O)C(COC4C(C(O)C(O)C(C)O4)O)O3)O)=CC(O)=C2C(=O)C1 QUQPHWDTPGMPEX-UHFFFAOYSA-N 0.000 claims description 4
- 240000002262 Litsea cubeba Species 0.000 claims description 4
- 235000012854 Litsea cubeba Nutrition 0.000 claims description 4
- 235000019483 Peanut oil Nutrition 0.000 claims description 4
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 claims description 4
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 claims description 4
- 235000019484 Rapeseed oil Nutrition 0.000 claims description 4
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 claims description 4
- LUKBXSAWLPMMSZ-OWOJBTEDSA-N Trans-resveratrol Chemical compound C1=CC(O)=CC=C1\C=C\C1=CC(O)=CC(O)=C1 LUKBXSAWLPMMSZ-OWOJBTEDSA-N 0.000 claims description 4
- QUQPHWDTPGMPEX-UTWYECKDSA-N aurantiamarin Natural products COc1ccc(cc1O)[C@H]1CC(=O)c2c(O)cc(O[C@@H]3O[C@H](CO[C@@H]4O[C@@H](C)[C@H](O)[C@@H](O)[C@H]4O)[C@@H](O)[C@H](O)[C@H]3O)cc2O1 QUQPHWDTPGMPEX-UTWYECKDSA-N 0.000 claims description 4
- 229940117916 cinnamic aldehyde Drugs 0.000 claims description 4
- KJPRLNWUNMBNBZ-UHFFFAOYSA-N cinnamic aldehyde Natural products O=CC=CC1=CC=CC=C1 KJPRLNWUNMBNBZ-UHFFFAOYSA-N 0.000 claims description 4
- APSNPMVGBGZYAJ-GLOOOPAXSA-N clematine Natural products COc1cc(ccc1O)[C@@H]2CC(=O)c3c(O)cc(O[C@@H]4O[C@H](CO[C@H]5O[C@@H](C)[C@H](O)[C@@H](O)[C@H]5O)[C@@H](O)[C@H](O)[C@H]4O)cc3O2 APSNPMVGBGZYAJ-GLOOOPAXSA-N 0.000 claims description 4
- 229960002217 eugenol Drugs 0.000 claims description 4
- 229940025878 hesperidin Drugs 0.000 claims description 4
- VUYDGVRIQRPHFX-UHFFFAOYSA-N hesperidin Natural products COc1cc(ccc1O)C2CC(=O)c3c(O)cc(OC4OC(COC5OC(O)C(O)C(O)C5O)C(O)C(O)C4O)cc3O2 VUYDGVRIQRPHFX-UHFFFAOYSA-N 0.000 claims description 4
- QUQPHWDTPGMPEX-QJBIFVCTSA-N hesperidin Chemical compound C1=C(O)C(OC)=CC=C1[C@H]1OC2=CC(O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]4[C@@H]([C@H](O)[C@@H](O)[C@H](C)O4)O)O3)O)=CC(O)=C2C(=O)C1 QUQPHWDTPGMPEX-QJBIFVCTSA-N 0.000 claims description 4
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 claims description 4
- 235000012680 lutein Nutrition 0.000 claims description 4
- 229960005375 lutein Drugs 0.000 claims description 4
- 239000001656 lutein Substances 0.000 claims description 4
- KBPHJBAIARWVSC-RGZFRNHPSA-N lutein Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\[C@H]1C(C)=C[C@H](O)CC1(C)C KBPHJBAIARWVSC-RGZFRNHPSA-N 0.000 claims description 4
- ORAKUVXRZWMARG-WZLJTJAWSA-N lutein Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=CC(O)CC2(C)C)C ORAKUVXRZWMARG-WZLJTJAWSA-N 0.000 claims description 4
- ARGKVCXINMKCAZ-UHFFFAOYSA-N neohesperidine Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(OC3C(C(O)C(O)C(CO)O3)OC3C(C(O)C(O)C(C)O3)O)=CC(O)=C2C(=O)C1 ARGKVCXINMKCAZ-UHFFFAOYSA-N 0.000 claims description 4
- 239000000312 peanut oil Substances 0.000 claims description 4
- 229960001285 quercetin Drugs 0.000 claims description 4
- 235000005875 quercetin Nutrition 0.000 claims description 4
- KBPHJBAIARWVSC-XQIHNALSSA-N trans-lutein Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC2C(=CC(O)CC2(C)C)C KBPHJBAIARWVSC-XQIHNALSSA-N 0.000 claims description 4
- 235000018991 trans-resveratrol Nutrition 0.000 claims description 4
- FJHBOVDFOQMZRV-XQIHNALSSA-N xanthophyll Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC2C=C(C)C(O)CC2(C)C FJHBOVDFOQMZRV-XQIHNALSSA-N 0.000 claims description 4
- 240000007594 Oryza sativa Species 0.000 claims description 3
- 235000007164 Oryza sativa Nutrition 0.000 claims description 3
- 238000000265 homogenisation Methods 0.000 claims description 3
- 235000009566 rice Nutrition 0.000 claims description 3
- 239000003549 soybean oil Substances 0.000 claims description 3
- 235000012424 soybean oil Nutrition 0.000 claims description 3
- 238000009210 therapy by ultrasound Methods 0.000 claims description 3
- 235000013628 Lantana involucrata Nutrition 0.000 claims description 2
- 235000006677 Monarda citriodora ssp. austromontana Nutrition 0.000 claims description 2
- 240000007673 Origanum vulgare Species 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 17
- 235000013305 food Nutrition 0.000 abstract description 3
- 239000002537 cosmetic Substances 0.000 abstract description 2
- 230000001804 emulsifying effect Effects 0.000 abstract description 2
- 238000001035 drying Methods 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- 235000013339 cereals Nutrition 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 235000011203 Origanum Nutrition 0.000 description 3
- 241001529744 Origanum Species 0.000 description 3
- 239000003995 emulsifying agent Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 230000020477 pH reduction Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 230000032798 delamination Effects 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 201000001320 Atherosclerosis Diseases 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 241000209504 Poaceae Species 0.000 description 1
- 235000005775 Setaria Nutrition 0.000 description 1
- 241000232088 Setaria <nematode> Species 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 208000007502 anemia Diseases 0.000 description 1
- 229910001566 austenite Inorganic materials 0.000 description 1
- 229920002988 biodegradable polymer Polymers 0.000 description 1
- 239000004621 biodegradable polymer Substances 0.000 description 1
- 230000009141 biological interaction Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 230000001914 calming effect Effects 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 238000013270 controlled release Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 235000021474 generally recognized As safe (food) Nutrition 0.000 description 1
- 235000021472 generally recognized as safe Nutrition 0.000 description 1
- 235000021473 generally recognized as safe (food ingredients) Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003839 salts Chemical group 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 235000020238 sunflower seed Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Mycology (AREA)
- Botany (AREA)
- Dermatology (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Molecular Biology (AREA)
- Biotechnology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Microbiology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Medicinal Preparation (AREA)
- Cosmetics (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
Abstract
本发明涉及一种黑小米淀粉皮克林乳液及其制备方法，所述乳液由黑小米淀粉颗粒、油相成分和水相成分组成，所述黑小米淀粉颗粒的颗粒浓度为0.001‑0.25g/mL，所述油相成分的体积分数为0.1‑50％，其余为水相成分。制备方法具体包括以下步骤：(a)取黑小米原料进行粉碎得到黑小米淀粉，再经预处理得到微细化黑小米淀粉颗粒；(b)按比例取步骤(a)得到的微细化黑小米淀粉颗粒、油相成分和水相成分混合，得到乳液。与现有技术相比，本发明制得的皮克林乳液的稳定性和乳化性能较为优异，可应用于食品、化妆品等领域，而且乳液的制备工艺简单，可量产。
Description
技术领域
本发明涉及乳液领域，具体涉及一种黑小米淀粉皮克林乳液及其制备方法。
背景技术
目前，皮克林乳液已在医学、食品、材料、化工等领域广泛应用。与传统的表面活性剂不同，皮克林乳液是一种以固体颗粒为乳化剂制成的乳液，它的稳定性与作为乳化剂的固体颗粒的浓度、湿润性、粒径大小等密切相关，这些固体颗粒具有明确的粒径分布以及可控的表面特性，可在油水界面上产生不可逆吸附作用，可以消除传统乳液采用的表面活性剂所带来的刺激性、发泡、空气截留、生物相互作用等不利影响，具有抗絮凝、聚集、奥氏熟化等优点，同时还可以实现多种生物活性物质的包埋作用，如β-胡萝卜素、姜黄素、植物甾醇等，对其功能成分起到保护、递送、控释等作用。
淀粉是一种天然、可生物降解的聚合物，其来源广泛，种类较多，价格低廉。淀粉颗粒具有一定的亲水性且颗粒大小适中。同时，淀粉是GRAS物质(一般认为是安全的)，不会引起过敏。淀粉作为乳化剂制备的皮克林乳液日益受到关注。由于淀粉是亲水性的，因此它主要用来稳定O/W型乳液。
黑小米是禾本科、狗尾草属，是小米众多品种中的一种，被誉为“谷中之王”。黑小米容易烹饪，易被人体消化吸，且营养丰富，含有蛋白质、脂肪、碳水化合物、钙、磷、铁、维生素等，丰富的营养元素，决定了黑小米的功能特性。研究表明，黑色作物具有治疗贫血，抗动脉粥样硬化，镇静和改善睡眠等功效，而黑小米同样具有良好的抗氧化性和稳定性，因此黑小米也具有营养保健和治疗的功效。
发明内容
本发明的目的就是提供一种黑小米淀粉皮克林乳液及其制备方法。
本发明的目的通过以下技术方案实现：
一种黑小米淀粉皮克林乳液，所述乳液由黑小米淀粉颗粒、油相成分和水相成分组成，所述黑小米淀粉颗粒的颗粒浓度为0.001-0.25g/mL，所述油相成分的体积分数为0.1-50％，其余为水相成分。
优选地，所述黑小米淀粉颗粒的颗粒浓度为0.001-0.25g/mL，所述油相成分的体积分数为1-50％，其余为水相成分。当油相成分的体积含量超过1％，便可以稳定乳液。
所述黑小米淀粉颗粒的粒径为100nm-5μm。
所述油相成分选自食用油、精油或疏水性生物活性物质中的一种或多种混合。
所述食用油选自玉米油、大豆油、花生油、米油或菜籽油中的一种或多种混合。
所述精油选自薰衣草精油、柠檬油、甜橙油、山苍子精油、迷迭香精油或牛至精油中的一种或多种混合。
所述疏水性生物活性物质选自反式白藜芦醇、姜黄素、丁香酚、肉桂醛、β-胡萝卜素、叶黄素、橙皮苷或槲皮素中的一种或多种混合。
一种黑小米淀粉皮克林乳液的制备方法，具体包括以下步骤：
(a)取黑小米原料进行粉碎得到黑小米淀粉，再经预处理得到微细化黑小米淀粉颗粒；
(b)按比例取步骤(a)得到的微细化黑小米淀粉颗粒、油相成分和水相成分混合，得到乳液。
步骤(a)中，预处理过程具体为：使用研钵研磨黑小米淀粉0.5-4h，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm。
步骤(a)中，预处理过程具体为：对黑小米淀粉依次进行酸化水解、干燥和研磨，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm。
步骤(a)中，预处理过程具体为：对黑小米淀粉进行细胞粉碎，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm。
步骤(a)中，预处理过程具体为：对将黑小米淀粉依次进行糊化、干燥和研磨，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm。研磨、细胞粉碎、糊化这些操作都是实现微细化黑小米淀粉颗粒粒径调控的方式，任一选择即可。
步骤(b)中，采用搅拌、超声或均质使三者均匀混合，三种方式择一选择即可，对乳液的稳定性基本没有影响。
本发明中通过对黑小米淀粉进行预处理，减小淀粉颗粒的粒径及形状，使其粒径、形状等达到要求，实现稳定Pickering乳液的属性，并且调整各组分的含量，最终制得的皮克林乳液的稳定性和乳化性能较为优异，静置48h后也不会出现分层，可改善乳液和膏体的外观，减少油腻感和人体器官刺激性，可应用于食品、化妆品等领域，而且乳液的制备工艺简单，可量产。
附图说明
图1为实施例1中得到的五份乳液静置后的效果图；
图2为实施例1中研磨1h得到的乳液静置两天后的显微镜照片(为20μm)。
具体实施方式
下面结合附图和具体实施例对本发明进行详细说明。
一种黑小米淀粉皮克林乳液，乳液由黑小米淀粉颗粒、油相成分和水相成分组成，黑小米淀粉颗粒的颗粒浓度为0.001-0.25g/mL，油相成分的体积分数为0.1-50％，其余为水相成分。
油相成分选自食用油、精油或疏水性生物活性物质中的一种或多种混合，食用油选自玉米油、大豆油、花生油、米油或菜籽油中的一种或多种混合；精油选自薰衣草精油、柠檬油、甜橙油、山苍子精油、迷迭香精油或牛至精油中的一种或多种混合；疏水性生物活性物质选自反式白藜芦醇、姜黄素、丁香酚、肉桂醛、β-胡萝卜素、叶黄素、橙皮苷或槲皮素中的一种或多种混合。
一种黑小米淀粉皮克林乳液的制备方法，具体包括以下步骤：
(a)取黑小米原料进行粉碎得到黑小米淀粉，再经预处理得到微细化黑小米淀粉颗粒，预处理过程具体为：使用研钵研磨黑小米淀粉0.5-4h，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm；或预处理过程具体为：对黑小米淀粉依次进行酸化水解、干燥和研磨，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm；或预处理过程具体为：对黑小米淀粉进行细胞粉碎，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm；或预处理过程具体为：对将黑小米淀粉依次进行糊化、干燥和研磨，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm；
(b)按比例取步骤(a)得到的微细化黑小米淀粉颗粒、油相成分和水相成分采用搅拌、超声或均质使三者均匀混合，得到乳液。
本发明着重于乳液的稳定性能，采用“静置48小时后的分层情况”作为判断依据，以下实施例的静置参数均为：稳定48h，温度范围为0-80℃，pH为3-11，电解质为食盐，用量为0-8％，占比为水的重量。
实施案例1
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为陕西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用研钵研磨0min、10min、0.5h、1h和2h，分别制得粒径为100nm-5μm的微细化黑小米淀粉颗粒。
3.分别取五份1.2g黑小米淀粉颗粒，五份8mL玉米油，五份8mL水混合，均质制得五份乳液，黑小米淀粉颗粒的颗粒浓度均为0.075g/mL，油相的体积分数均为50％。这五份乳液均静置48h，静置的情况如图1所示，可看到，研磨0.5h及以上的乳液在底部都没有发现水的析出，即未出现分层的情况，而研磨0和10min的乳液在底部发现水的析出，即出现分层的情况，对静置两天后的研磨1h得到的乳液进行观察，如图2所示，可看到，乳液液滴具有清晰的油水界面。乳液液滴大小不等。
实施案例2
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为山西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用研钵研磨0.5h，制得粒径为1-5μm xx的微细化黑小米淀粉颗粒。
3.取0.01g黑小米淀粉颗粒，1mL玉米油，9mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.001g/mL，油相的体积分数为10％。该乳液静置2天不分层。
实施案例3
1.选取产地为陕西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用细胞粉碎机对黑小米淀粉进行颗粒粉碎，制得粒径为1-5μm的微细化黑小米淀粉颗粒。
3.取0.01g黑小米淀粉颗粒，1mL玉米油，9mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.001g/mL，油相的体积分数为10％。该乳液静置2天不分层。
实施案例4
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为山西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用细胞粉碎0.5h，制得粒径为1-5μm的微细化黑小米淀粉颗粒。
3.取2g黑小米淀粉颗粒，4mL玉米油，4mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.25g/mL，油相的体积分数为50％。该乳液静置2天不分层。
实施案例5
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为陕西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用盐酸调整pH为4，60℃加热1h对黑小米淀粉进行酸化水解，之后干燥12h，再研磨0.5h，制得粒径为100nm-5μm的微细化黑小米淀粉颗粒。
3.取0.2g黑小米淀粉颗粒，2mL玉米油，8mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.02g/mL，油相的体积分数为20％。该乳液静置2天不分层。
实施案例6
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为山西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用醋酸调整pH为3，在50℃对黑小米淀粉进行酸化水解，干燥12h，研磨0.5h，制得粒径为100nm-5μm的微细化黑小米淀粉颗粒。
3.取1g黑小米淀粉颗粒，1mL玉米油，9mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.1g/mL，油相的体积分数为10％。该乳液静置2天不分层。
实施案例7
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为陕西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.将黑小米淀粉加热至70℃糊化2h，之后干燥12h，研磨0.5h，制得粒径为100nm-5μm的微细化黑小米淀粉颗粒。
3.取0.5g黑小米淀粉颗粒，1mL玉米油，9mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.05g/mL，油相的体积分数为10％。该乳液静置2天不分层。
实施案例8
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为山西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.将黑小米淀粉加热至90℃糊化0.5h，之后干燥12h，研磨0.5h，制得粒径为100nm-5μm的微细化黑小米淀粉颗粒。
3.取0.4g黑小米淀粉颗粒，1mL玉米油，9mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.04g/mL，油相的体积分数为10％。该乳液静置2天不分层。
实施案例9
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为陕西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用研钵研磨0.5h，制得粒径为1-5μm的微细化黑小米淀粉颗粒。
3.取0.1g黑小米淀粉颗粒，5mL橄榄油，5mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.01g/mL，油相的体积分数为50％。该乳液静置2天不分层。
实施案例10
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为陕西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用研钵研磨0.5h，制得粒径为1-5μm的微细化黑小米淀粉颗粒。
3.取0.1g黑小米淀粉颗粒，5mL葵花籽油，5mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.01g/mL，油相的体积分数为50％。该乳液静置2天不分层。
实施案例11
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为山西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用研钵研磨0.5h，制得粒径为1-5μm的微细化黑小米淀粉颗粒。
3.取0.1g黑小米淀粉颗粒，5mL菜籽油，5mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.01g/mL，油相的体积分数为50％。该乳液静置2天不分层。
实施案例12
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为山西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用研钵研磨0.5h，制得粒径为1-5μm的微细化黑小米淀粉颗粒。
3.取0.1g黑小米淀粉颗粒，5mL花生油，5mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.01g/mL，油相的体积分数为50％。该乳液静置2天不分层。
实施案例13
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为山西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用研钵研磨20min，制得粒径为1-5μm的微细化黑小米淀粉颗粒。
3.取0.1g黑小米淀粉颗粒，5mL精油(从薰衣草精油、柠檬油、甜橙油、山苍子精油、迷迭香精油、牛至精油中任意选择一种精油作为油相)，5mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.01g/mL，油相的体积分数为50％。该乳液静置2天不分层。
实施案例14
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为山西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用研钵研磨20min，制得粒径为1-5μm的微细化黑小米淀粉颗粒。
3.取0.1g黑小米淀粉颗粒，0.1mL精油(从薰衣草精油、柠檬油、甜橙油、山苍子精油、迷迭香精油、牛至精油中任意选择一种精油作为油相)，10mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.01g/mL，油相的体积分数为1％。该乳液静置2天不分层。
实施案例15
一种黑小米淀粉皮克林乳液，采用以下步骤制备得到：
1.选取产地为山西的黑小米，使用粉碎机粉碎，得到黑小米淀粉。
2.使用研钵研磨20min，制得粒径为1-5μm的微细化黑小米淀粉颗粒。
3.取0.1g黑小米淀粉颗粒，5mL疏水性生物活性物质(从反式白藜芦醇、姜黄素、丁香酚、肉桂醛、β-胡萝卜素、叶黄素、橙皮苷、槲皮素中任意选择一种精油作为油相)，5mL水混合，搅拌制得乳液，黑小米淀粉颗粒的颗粒浓度为0.01g/mL，油相的体积分数为50％。该乳液静置2天不分层。
上述的对实施例的描述是为便于该技术领域的普通技术人员能理解和使用发明。熟悉本领域技术的人员显然可以容易地对这些实施例做出各种修改，并把在此说明的一般原理应用到其他实施例中而不必经过创造性的劳动。因此，本发明不限于上述实施例，本领域技术人员根据本发明的揭示，不脱离本发明范畴所做出的改进和修改都应该在本发明的保护范围之内。
Claims (10)
1.一种黑小米淀粉皮克林乳液，其特征在于，所述乳液由黑小米淀粉颗粒、油相成分和水相成分组成，所述黑小米淀粉颗粒的颗粒浓度为0.001-0.25g/mL，所述油相成分的体积分数为0.1-50％，其余为水相成分。
2.根据权利要求1所述的一种黑小米淀粉皮克林乳液，其特征在于，所述油相成分选自食用油、精油或疏水性生物活性物质中的一种或多种混合。
3.根据权利要求2所述的一种黑小米淀粉皮克林乳液，其特征在于，所述食用油选自玉米油、大豆油、花生油、米油或菜籽油中的一种或多种混合。
4.根据权利要求2所述的一种黑小米淀粉皮克林乳液，其特征在于，所述精油选自薰衣草精油、柠檬油、甜橙油、山苍子精油、迷迭香精油或牛至精油中的一种或多种混合。
5.根据权利要求2所述的一种黑小米淀粉皮克林乳液，其特征在于，所述疏水性生物活性物质选自反式白藜芦醇、姜黄素、丁香酚、肉桂醛、β-胡萝卜素、叶黄素、橙皮苷或槲皮素中的一种或多种混合。
6.一种如权利要求1-5任一项所述的黑小米淀粉皮克林乳液的制备方法，其特征在于，所述制备方法具体包括以下步骤：
(a)取黑小米原料进行粉碎得到黑小米淀粉，再经预处理得到微细化黑小米淀粉颗粒；
(b)按比例取步骤(a)得到的微细化黑小米淀粉颗粒、油相成分和水相成分混合，得到乳液。
7.根据权利要求6所述的一种黑小米淀粉皮克林乳液的制备方法，其特征在于，步骤(a)中，预处理过程具体为：使用研钵研磨黑小米淀粉0.5-4h，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm。
8.根据权利要求6所述的一种黑小米淀粉皮克林乳液的制备方法，其特征在于，步骤(a)中，预处理过程具体为：对黑小米淀粉进行细胞粉碎，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm。
9.根据权利要求6所述的一种黑小米淀粉皮克林乳液的制备方法，其特征在于，步骤(a)中，预处理过程具体为：对将黑小米淀粉依次进行糊化、干燥和研磨，使微细化黑小米淀粉颗粒的粒径达到100nm-5μm。
10.根据权利要求6所述的一种黑小米淀粉皮克林乳液的制备方法，其特征在于，步骤(b)中，采用搅拌、超声或均质使三者均匀混合。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110591313.9A CN113230187A (zh) | 2021-05-28 | 2021-05-28 | 一种黑小米淀粉皮克林乳液及其制备方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110591313.9A CN113230187A (zh) | 2021-05-28 | 2021-05-28 | 一种黑小米淀粉皮克林乳液及其制备方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN113230187A true CN113230187A (zh) | 2021-08-10 |
Family
ID=77135597
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110591313.9A Pending CN113230187A (zh) | 2021-05-28 | 2021-05-28 | 一种黑小米淀粉皮克林乳液及其制备方法 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN113230187A (zh) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114190537A (zh) * | 2021-11-12 | 2022-03-18 | 上海应用技术大学 | 一种稳定的百里香精油可食用乳液的制备方法 |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012082065A1 (en) * | 2010-12-15 | 2012-06-21 | Speximo Ab | New particle stabilized emulsions and foams |
| CN104546539A (zh) * | 2014-12-03 | 2015-04-29 | 华南理工大学 | 一种含微细淀粉颗粒保湿霜及其制备方法 |
| WO2020104553A1 (en) * | 2018-11-20 | 2020-05-28 | Johan Engblom | Stabilized oil-in-water emulsion |
| US20200297589A1 (en) * | 2017-12-14 | 2020-09-24 | Firmenich Sa | Process for releasing an active ingredient |
| CN111971069A (zh) * | 2018-04-16 | 2020-11-20 | 斯博西莫公司 | 用于化妆品和健康用途的粉末组合物 |
| WO2021008172A1 (zh) * | 2019-07-17 | 2021-01-21 | 华南理工大学 | 一种淀粉基高稳定Pickering乳液及其制备方法 |
-
2021
- 2021-05-28 CN CN202110591313.9A patent/CN113230187A/zh active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012082065A1 (en) * | 2010-12-15 | 2012-06-21 | Speximo Ab | New particle stabilized emulsions and foams |
| CN103402370A (zh) * | 2010-12-15 | 2013-11-20 | 斯博西莫公司 | 新的粒子稳定型乳液和泡沫 |
| CN104546539A (zh) * | 2014-12-03 | 2015-04-29 | 华南理工大学 | 一种含微细淀粉颗粒保湿霜及其制备方法 |
| US20200297589A1 (en) * | 2017-12-14 | 2020-09-24 | Firmenich Sa | Process for releasing an active ingredient |
| CN111971069A (zh) * | 2018-04-16 | 2020-11-20 | 斯博西莫公司 | 用于化妆品和健康用途的粉末组合物 |
| WO2020104553A1 (en) * | 2018-11-20 | 2020-05-28 | Johan Engblom | Stabilized oil-in-water emulsion |
| WO2021008172A1 (zh) * | 2019-07-17 | 2021-01-21 | 华南理工大学 | 一种淀粉基高稳定Pickering乳液及其制备方法 |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114190537A (zh) * | 2021-11-12 | 2022-03-18 | 上海应用技术大学 | 一种稳定的百里香精油可食用乳液的制备方法 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE69531674T2 (de) | Nicht-trennbare stärke-öl-zusammensetzungen | |
| CN108752603B (zh) | 一种淀粉基Pickering乳液凝胶的制备方法 | |
| KR20120024570A (ko) | 수중유 에멀전의 농축된 크림형 내지 고형 건조 조성물, 이들의 제조 방법, 및 감각적 측면 및 영양 생리학 관점에서 개선된 식품을 제조하기 위한 이들의 용도 | |
| CN102972671A (zh) | 一种基于多糖-蛋白质复合聚集体的纳米尺度食品载体制备方法 | |
| Chen et al. | Development of anti-photo and anti-thermal high internal phase emulsions stabilized by biomass lignin as a nutraceutical delivery system | |
| Ashfaq et al. | Protein-based functional colloids and their potential applications in food: A review | |
| CN106173420A (zh) | 动物饲料组合物及生产方法 | |
| CN113230187A (zh) | 一种黑小米淀粉皮克林乳液及其制备方法 | |
| JPH04500301A (ja) | 油中水エマルション用エマルション | |
| CN108498694A (zh) | 一种中药饮片及其制备方法 | |
| Baqeri et al. | The effect of gelatin and thymol‐loaded nanostructured lipid carrier on physicochemical, rheological, and sensory properties of sesame paste/date syrup blends as a snack bar | |
| CN113966830A (zh) | 一种新型负载活性物的植物蛋白-多糖复合乳液凝胶的制备方法 | |
| Verdalet-Guzmán et al. | Characterization of new sources of derivative starches as wall materials of essential oil by spray drying | |
| CN113336966B (zh) | 一种糯米淀粉皮克林乳液及其制备方法 | |
| Safian et al. | Utilization of lignocellulosic biomass: A practical journey towards the development of emulsifying agent | |
| CN108064976A (zh) | 一种利用Pickering乳液制备多糖乳液凝胶的方法 | |
| Fu et al. | Research advances in plant protein-based products: Protein sources, processing technology, and food applications | |
| Mohd-Setapar et al. | Omega-3 emulsion of rubber (Hevea brasiliensis) seed oil | |
| CN106993811A (zh) | 乳状液微聚集体及其制备方法 | |
| CN108113008A (zh) | 一种减少脂肪消化的乳液及其制备方法和用途 | |
| CN113100417B (zh) | 一种花粉粒子稳定的食品级Pickering乳液及其制备方法 | |
| CN109645370B (zh) | 一种淡奶油专用脂肪替代品及其制备方法 | |
| Liu et al. | Cereal protein-based emulsion gels for edible oil structuring | |
| CN113057332A (zh) | 胶囊挤压式功能性食品3d打印材料及制备方法和用途 | |
| Hastarini et al. | Characteristics of Instant Mushroom Cream Soup Enriched with Catfish Oil Microcapsules |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210810 |
|
| RJ01 | Rejection of invention patent application after publication |