CN113215416B - Titanium lump uniform feeding device for titanium sponge reduction - Google Patents

Titanium lump uniform feeding device for titanium sponge reduction Download PDF

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Publication number
CN113215416B
CN113215416B CN202110389177.5A CN202110389177A CN113215416B CN 113215416 B CN113215416 B CN 113215416B CN 202110389177 A CN202110389177 A CN 202110389177A CN 113215416 B CN113215416 B CN 113215416B
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China
Prior art keywords
side wall
fixedly connected
outer side
titanium
box body
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CN202110389177.5A
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CN113215416A (en
Inventor
王俊博
梁军
韩志强
周可心
马勇
唐帅
杨志波
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Baotai Huashen Titanium Industry Co Ltd
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Baotai Huashen Titanium Industry Co Ltd
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Publication of CN113215416A publication Critical patent/CN113215416A/en
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1263Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
    • C22B34/1277Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using other metals, e.g. Al, Si, Mn
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00General methods of reducing to metals
    • C22B5/02Dry methods smelting of sulfides or formation of mattes
    • C22B5/04Dry methods smelting of sulfides or formation of mattes by aluminium, other metals or silicon
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D3/00Charging; Discharging; Manipulation of charge
    • F27D3/14Charging or discharging liquid or molten material

Abstract

The utility model discloses a titanium lump uniform feeding device for titanium sponge reduction, which comprises a box body, wherein a heat-insulating layer is fixedly connected inside the box body, and a feeding pipe is fixedly connected at the top of the box body in a penetrating manner, the reduction efficiency is ensured and the reaction time is saved.

Description

Titanium lump uniform feeding device for titanium sponge reduction
Technical Field
The utility model relates to the technical field of titanium sponge reduction, in particular to a titanium lump uniform feeding device for titanium sponge reduction.
Background
Titanium sponge, which is a raw material of titanium processing materials; generally light gray particles, clean in surface, free of visible inclusions, and also includes defective titanium sponge chunks, such as over-fired titanium sponge chunks, oxidized titanium sponge chunks having a pronounced dark yellow and bright yellow coloration, oxidized and nitrogen-enriched titanium sponge chunks having traces of dark yellow and bright yellow coloration, titanium sponge chunks having a pronounced chloride residue, titanium sponge chunks having debris, and the like.
Through the retrieval, chinese patent is CN 203768433U's utility model patent discloses an even distributing device of titanium tetrachloride of magnesium method production titanium sponge, distributing device includes main filling tube and tripper, and wherein, the export of main filling tube is connected with the feed inlet of tripper, evenly arranges a plurality of discharge gates on the bottom plate of tripper, the tripper is located the bell top or the bell below of reacting furnace, through the titanium tetrachloride evenly distributed that a plurality of discharge gates flow is on the magnesium liquid level in the reacting furnace. The uniform material distribution device has a simple structure, is convenient to clean and not easy to block, avoids the quality problem that the center part of the titanium sponge lump generates a hard core due to the concentrated reaction at the center part in the furnace when titanium tetrachloride enters, effectively reduces the bulk density of the titanium sponge, and improves the application performance of the titanium sponge;
however, the device does not accomplish the titanium sponge reduction in-process, to the ration interpolation of liquid magnesium and raw materials, this can influence the inside reduction efficiency of device, and traditional device still does effectual vibration for the raw materials of accomplishing to the inside interpolation of device and makes its good evenly distributed at the surface of liquid magnesium, can cause the raw materials to appear piling up of certain degree for reduction efficiency descends, brings unnecessary trouble, for this reason we propose a titanium lump even feeding device for the titanium sponge reduction and solve above-mentioned problem.
Disclosure of Invention
The utility model aims to solve the problems that quantitative addition of raw materials and uniform distribution of the raw materials in a feeding device cannot be realized in the prior art, and provides a titanium lump uniform feeding device for titanium sponge reduction.
In order to achieve the purpose, the utility model adopts the following technical scheme:
the titanium lump uniform feeding device for the reduction of the titanium sponge comprises a box body, wherein a heat-insulating layer is fixedly connected inside the box body, a charging pipe is fixedly connected to the top of the box body in a penetrating manner, a liquid adding pipe is fixedly connected to the top of the box body in a penetrating manner, a liquid outlet is formed in the bottom of the liquid adding pipe in a penetrating manner, an impeller is connected to the inner side wall of the liquid adding pipe in a rotating and sealing manner, a rotating shaft is fixedly connected to the end part of the impeller, the end part of the rotating shaft is fixedly connected with the inner side wall of the box body in a penetrating manner, a gear is meshed with the outer side wall of the rotating shaft in a penetrating manner, a rotating rod is fixedly connected to the inner side wall of the charging pipe in a penetrating manner, the end part of the rotating rod is rotatably connected with the inner side wall of the box body, and a feeding head is fixedly connected to the outer side wall of the rotating rod in a penetrating manner, the outer side wall of the feeding head is connected with the inner side wall of the feeding pipe in a sliding and sealing mode, the outer side wall of the rotating rod penetrates through a fixedly connected rotating extrusion mechanism, a fixed plate is fixedly connected to the inner side wall of the box body, and an elastic reset mechanism is arranged at the bottom of the fixed plate.
Preferably, the rotating and extruding mechanism comprises a connecting block which penetrates through the outer side wall of the rotating rod and is fixedly connected with the outer side wall of the rotating rod, the outer side wall of the connecting block is rotatably connected with a connecting rod, the outer side wall of the connecting block is fixedly connected with a connecting spring, the end part of the connecting spring is fixedly connected with the outer side wall of the connecting rod, the end part of the connecting rod is connected with a compression plate in a sliding and sealing mode, and the top part of the compression plate is fixedly connected with the top part of the inner side wall of the box body.
Preferably, the elastic reset mechanism comprises a chute formed in the bottom of the fixing plate, a reset spring is fixedly connected to the top of the inner side wall of the chute, a connector is fixedly connected to the bottom of the reset spring, a filter screen plate is fixedly connected to the bottom of the connector, and the outer side wall of the connector is connected with the inner side wall of the chute in a sliding and sealing mode.
Preferably, the end of the liquid feeding pipe is semicircular, the bottom of the liquid feeding pipe is obliquely arranged, and the liquid feeding pipe is cuboid.
Preferably, the outer side wall of the rotating shaft is provided with threads, and the threads arranged on the outer side wall of the rotating shaft are matched with the teeth arranged on the outer side wall of the gear.
Preferably, the rotating shaft, the gear and the rotating rod form a transmission mechanism to provide power for the operation of the device.
Preferably, the connecting rods are arranged in an arc shape, and the connecting rods and the connecting springs are arranged in an annular array.
Preferably, the spout sets up to cylindrically, reset spring is stainless steel material, reset spring is in tensile state, the connector sets up to cylindrically, filter plate sets up to cylindrically.
Compared with the prior art, the utility model has the beneficial effects that:
1. add required liquid magnesium through the liquid feeding pipe, the rotation of impact drive impeller through liquid magnesium, the rotation through the pivot drives liquid magnesium to liquid outlet department discharge, prevent to use the device liquid magnesium to cause the influence to the inside wall of liquid feeding pipe for a long time, the rotation through the impeller drives the rotation of pivot, and then drive the rotation of gear, the rotation of gear will make the bull stick rotate, and then make reinforced head rotate, make the titanium that the filling pipe inside wall adds in stick together the inside that gets into the box through the rotation of adding the stub bar, when having realized evenly feeding together titanium, liquid magnesium and the proportion that titanium sticks together have been guaranteed, the reaction efficiency of titanium stick together and liquid magnesium in the box has been improved, save reaction time when having guaranteed reduction efficiency.
2. The rotation of the connecting block is driven by the rotation of the rotating rod, the rotation of the connecting rod is driven by the rotation of the connecting block, when the connecting rod rotates to the bottom of the compression plate, the connecting rod can extend under the action of the connecting spring, and further the connecting rod can impact the filter screen plate, so that the filter screen plate can move downwards under the action of the reset spring, when the connecting rod rotates to the bottom of the compression plate, due to the arrangement of the connecting spring and the rotation connection with the connecting block, the connecting rod can enter the compression plate, the outer surface of the connecting rod is cleaned by the end part of the compression plate, when the connecting rod rotates to the top of the compression plate, the filter screen plate can move upwards under the action of the reset spring, so that the filter screen plate vibrates, titanium lumps at the top of the filter screen plate are uniformly distributed, liquid magnesium and titanium lumps can fully react, the reaction efficiency is ensured, and the reaction is prevented, the quality of the produced product is low due to the uneven distribution of the titanium lumps, and the quality of the product is ensured.
Drawings
FIG. 1 is a schematic structural view in cross section of the front side of a titanium lump uniform feeding device for titanium sponge reduction, which is provided by the utility model;
FIG. 2 is an enlarged schematic structural view of a part A in FIG. 1 of a titanium lump uniform feeding device for titanium sponge reduction according to the present invention;
FIG. 3 is a schematic side structure view of a transmission mechanism of a titanium lump uniform feeding device for titanium sponge reduction, which is provided by the utility model;
FIG. 4 is a schematic side sectional structural view of a feeding mechanism of the titanium lump uniform feeding device for titanium sponge reduction, which is provided by the utility model;
FIG. 5 is a schematic side structure view of a vibrating mechanism of a titanium lump uniform feeding device for titanium sponge reduction, which is provided by the utility model;
fig. 6 is a schematic view of a three-dimensional structure of a charging head of the titanium lump uniform charging device for titanium sponge reduction provided by the utility model.
In the figure: the device comprises a box body 1, a heat preservation layer 2, a liquid adding pipe 3, a liquid outlet 4, an impeller 5, a rotating shaft 6, a gear 7, a rotating rod 8, a connecting block 9, a connecting rod 10, a connecting spring 11, a compression plate 12, a feeding head 13, a feeding pipe 14, a fixing plate 15, a sliding chute 16, a return spring 17, a connector 18 and a filter screen plate 19.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Referring to fig. 1-6, a titanium lump uniform feeding device for sponge titanium reduction comprises a box body 1, a heat preservation layer 2 is fixedly connected inside the box body 1, a feed pipe 14 is fixedly connected on the top of the box body 1 in a penetrating manner, a liquid feeding pipe 3 is fixedly connected on the top of the box body 1 in a penetrating manner, the end part of the liquid feeding pipe 3 is arranged in a semicircular manner, the bottom of the liquid feeding pipe 3 is arranged in an inclined manner, the feed pipe 14 is arranged in a cuboid shape, a liquid outlet 4 is arranged on the bottom of the liquid feeding pipe 3 in a penetrating manner, an impeller 5 is connected on the inner side wall of the liquid feeding pipe 3 in a rotating and sealing manner, a rotating shaft 6 is fixedly connected on the end part of the impeller 5, the end part of the rotating shaft 6 is fixedly connected with the inner side wall of the box body 1, the outer side wall of the rotating shaft 6 is connected with the side wall of the liquid feeding pipe 3 in a penetrating and sealing manner, a gear 7 is meshed with the outer side wall of the rotating shaft 6, a thread is arranged on the outer side wall of the rotating shaft 6, a thread is matched with a tooth arranged on the outer side wall of the gear 7, the inner side wall of the gear 7 is fixedly connected with a rotating rod 8 in a penetrating manner, the rotating shaft 6, the gear 7 and the rotating rod 8 form a transmission mechanism to provide power for the operation of the device, the outer side wall of the rotating rod 8 is connected with the side wall of the charging pipe 14 in a penetrating and sealing manner, the end part of the rotating rod 8 is connected with the inner side wall of the box body 1 in a rotating manner, the outer side wall of the rotating rod 8 is fixedly connected with a feeding head 13 in a penetrating manner, and the outer side wall of the feeding head 13 is connected with the inner side wall of the charging pipe 14 in a sliding and sealing manner;
after the materials are completely added, the impeller 5 and the inner side wall of the liquid adding pipe 3 form a sealing state, and the outer side wall of the material adding head 13 and the inner side wall of the feeding pipe 14 form a sealing state, so that the toxic substances generated inside are prevented from being discharged into the nature to influence the health and safety of personnel when the reduction reaction is carried out inside the box body 1, and the health and safety of the personnel are protected to a certain degree;
the required liquid magnesium is added through the liquid adding pipe 3, the impeller 5 is driven to rotate through the impact of the liquid magnesium, the liquid magnesium is driven to the liquid outlet 4 to be discharged through the rotation of the rotating shaft 5, the influence of the liquid magnesium on the inner side wall of the liquid adding pipe 3 due to long-term use is prevented, the rotating shaft 6 is driven to rotate through the rotation of the impeller 5, the gear 7 is driven to rotate, the rotating rod 8 can rotate through the rotation of the gear 7, the feeding head 13 can rotate, titanium lumps added into the inner side wall of the feeding pipe 14 can enter the box body 1 through the rotation of the feeding head 13, the uniform feeding of the titanium lumps is realized, the proportion of the liquid magnesium and the titanium lumps is ensured, the reaction efficiency of the titanium lumps and the liquid magnesium in the box body 1 is improved, and the reaction time is saved while the reduction efficiency is ensured;
the outer side wall of the rotating rod 8 is fixedly connected with a rotating extrusion mechanism in a penetrating mode, the rotating extrusion mechanism comprises a connecting block 9 fixedly connected with the outer side wall of the rotating rod 8 in a penetrating mode, the outer side wall of the connecting block 9 is connected with a connecting rod 10 in a rotating mode, the outer side wall of the connecting block 9 is fixedly connected with a connecting spring 11, the connecting rod 10 is arranged in an arc shape, the connecting rod 10 and the connecting spring 11 are arranged in an annular array mode, the end portion of the connecting spring 11 is fixedly connected with the outer side wall of the connecting rod 10, the end portion of the connecting rod 10 is connected with a compression plate 12 in a sliding and sealing mode, and the top of the compression plate 12 is fixedly connected with the top of the inner side wall of the box body 1;
the inner side wall of the box body 1 is fixedly connected with a fixing plate 15, the bottom of the fixing plate 15 is provided with an elastic reset mechanism, the elastic reset mechanism comprises a sliding chute 16 arranged at the bottom of the fixing plate 15, the top of the inner side wall of the sliding chute 16 is fixedly connected with a reset spring 17, the bottom of the reset spring 17 is fixedly connected with a connector 18, the bottom of the connector 18 is fixedly connected with a filter screen plate 19, the sliding chute 16 is arranged to be cylindrical, the reset spring 17 is made of stainless steel, the reset spring 17 is in a stretching state, the connector 18 is arranged to be cylindrical, the filter screen plate 19 is arranged to be cylindrical, and the outer side wall of the connector 18 is connected with the inner side wall of the sliding chute 16 in a sliding and sealing manner;
the rotation of the rotating rod 8 drives the connecting block 9 to rotate, the rotation of the connecting block 9 drives the connecting rod 10 to rotate, when the connecting rod 10 rotates to the bottom of the compression plate 12, the connecting rod 10 extends under the action of the connecting spring 11, and then the connecting rod 10 impacts the filter screen plate 19, so that the filter screen plate 19 moves downwards under the action of the return spring 17, when the connecting rod 10 rotates to the bottom of the compression plate 12, because the connecting spring 11 is arranged and is connected with the connecting block 9 in a rotating way, the connecting rod 10 enters the compression plate 12, the outer surface of the connecting rod 10 is cleaned by the end part of the compression plate 12, when the connecting rod 10 rotates to the top of the compression plate 12, the filter screen plate 19 moves upwards under the action of the return spring 17, so that the filter screen plate 19 vibrates, and titanium on the top of the filter screen plate 19 is uniformly distributed, so that liquid magnesium and titanium are fully reacted, the reaction efficiency is ensured, the quality of the produced product caused by uneven distribution of the titanium lump is prevented from being lower during the reaction, and the quality of the product is ensured.
In the utility model, when the device is used, required liquid magnesium is added through the liquid adding pipe 3, the impeller 5 is driven to rotate by the impact of the liquid magnesium, the liquid magnesium is driven to the liquid outlet 4 to be discharged by the rotation of the rotating shaft 5, the rotating shaft 6 is driven to rotate by the rotation of the impeller 5, and then the gear 7 is driven to rotate, the rotating rod 8 is driven to rotate by the rotation of the gear 7, so that the feeding head 13 rotates, and the titanium lumps added into the inner side wall of the feeding pipe 14 enter the box body 1 by the rotation of the feeding head 13;
the rotation of the rotating rod 8 can also drive the connecting block 9 to rotate, the rotation of the connecting rod 10 is driven by the rotation of the connecting block 9, when the connecting rod 10 rotates to the bottom of the compression plate 12, the connecting rod 10 can extend under the action of the connecting spring 11, and then the connecting rod 10 can collide with the filter screen plate 19, so that the filter screen plate 19 can move downwards under the action of the return spring 17, when the connecting rod 10 rotates to the bottom of the compression plate 12, because the connecting spring 11 is arranged and is connected with the connecting block 9 in a rotating manner, the connecting rod 10 can enter the compression plate 12, the outer surface of the connecting rod 10 can be cleaned by the end part of the compression plate 12, when the connecting rod 10 rotates to the top of the compression plate 12, the filter screen plate 19 can move upwards under the action of the return spring 17, so that the filter screen plate 19 vibrates, and the titanium lumps at the top of the filter screen plate 19 are uniformly distributed, and the liquid magnesium and the titanium lumps can fully react, the operation is simple and quick, and the use by personnel is convenient.
In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", and the like, indicate orientations and positional relationships based on those shown in the drawings, and are used only for convenience of description and simplicity of description, and do not indicate or imply that the equipment or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be considered as limiting the present invention.
Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include one or more of that feature. In the description of the present invention, "a plurality" means two or more unless specifically defined otherwise.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (6)

1. The titanium lump uniform feeding device for titanium sponge reduction comprises a box body (1) and is characterized in that a heat preservation layer (2) is fixedly connected inside the box body (1), a feeding pipe (14) is fixedly connected to the top of the box body (1) in a penetrating mode, a liquid feeding pipe (3) is fixedly connected to the top of the box body (1) in a penetrating mode, a liquid outlet (4) is formed in the bottom of the liquid feeding pipe (3) in a penetrating mode, an impeller (5) is connected to the inner side wall of the liquid feeding pipe (3) in a rotating and sealing mode, a rotating shaft (6) is fixedly connected to the end portion of the impeller (5), the end portion of the rotating shaft (6) is fixedly connected with the inner side wall of the box body (1), the outer side wall of the rotating shaft (6) is connected with the side wall of the liquid feeding pipe (3) in a penetrating and sealing mode, gears (7) are meshed with each other on the outer side wall of the rotating shaft (6), and a rotating rod (8) is fixedly connected to the inner side wall of the gears (7), the outer side wall of the rotating rod (8) is connected with the side wall of the feeding pipe (14) in a penetrating, sealing and rotating mode, the end portion of the rotating rod (8) is connected with the inner side wall of the box body (1) in a rotating mode, the outer side wall of the rotating rod (8) is fixedly connected with a feeding head (13) in a penetrating mode, the outer side wall of the feeding head (13) is connected with the inner side wall of the feeding pipe (14) in a sliding and sealing mode, the outer side wall of the rotating rod (8) is fixedly connected with a rotating extrusion mechanism in a penetrating mode, the inner side wall of the box body (1) is fixedly connected with a fixing plate (15), and an elastic reset mechanism is arranged at the bottom of the fixing plate (15);
the rotary extrusion mechanism comprises a connecting block (9) which is fixedly connected with the outer side wall of the rotating rod (8) in a penetrating manner, the outer side wall of the connecting block (9) is rotatably connected with a connecting rod (10), the outer side wall of the connecting block (9) is fixedly connected with a connecting spring (11), the end part of the connecting spring (11) is fixedly connected with the outer side wall of the connecting rod (10), the end part of the connecting rod (10) is connected with a compression plate (12) in a sliding and sealing manner, and the top part of the compression plate (12) is fixedly connected with the top part of the inner side wall of the box body (1);
elasticity canceling release mechanical system includes spout (16) that fixed plate (15) bottom was seted up, the inside wall top fixedly connected with reset spring (17) of spout (16), the bottom fixedly connected with connector (18) of reset spring (17), the bottom fixedly connected with filter plate (19) of connector (18), the lateral wall of connector (18) and the inside wall sliding seal of spout (16) are connected.
2. The titanium lump uniform feeding device for titanium sponge reduction according to claim 1, wherein the end of the feeding tube (3) is semicircular, the bottom of the feeding tube (3) is inclined, and the feeding tube (14) is rectangular.
3. The titanium lump uniform feeding device for titanium sponge reduction according to claim 1, wherein threads are arranged on the outer side wall of the rotating shaft (6), and the threads arranged on the outer side wall of the rotating shaft (6) are matched with teeth arranged on the outer side wall of the gear (7).
4. The titanium lump uniform feeding device for titanium sponge reduction according to claim 1, wherein the rotating shaft (6), the gear (7) and the rotating rod (8) form a transmission mechanism to provide power for the operation of the device.
5. The titanium lump uniform feeding device for titanium sponge reduction according to claim 1, wherein the connecting rods (10) are arranged in an arc shape, and the connecting rods (10) and the connecting springs (11) are arranged in an annular array.
6. The titanium lump uniform feeding device for titanium sponge reduction according to claim 1, wherein the chute (16) is cylindrical, the return spring (17) is made of stainless steel, the return spring (17) is in a stretching state, the connector (18) is cylindrical, and the screen plate (19) is cylindrical.
CN202110389177.5A 2021-04-12 2021-04-12 Titanium lump uniform feeding device for titanium sponge reduction Active CN113215416B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110389177.5A CN113215416B (en) 2021-04-12 2021-04-12 Titanium lump uniform feeding device for titanium sponge reduction

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Application Number Priority Date Filing Date Title
CN202110389177.5A CN113215416B (en) 2021-04-12 2021-04-12 Titanium lump uniform feeding device for titanium sponge reduction

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CN113215416B true CN113215416B (en) 2022-04-26

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Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3821746B2 (en) * 2002-04-19 2006-09-13 新日本製鐵株式会社 Batch type sponge titanium manufacturing method
CN1962906A (en) * 2006-11-23 2007-05-16 遵义钛业股份有限公司 Process for charging titanium tetrachloride for use in preparation of titanium sponge by magnesium method
CN201614395U (en) * 2009-10-26 2010-10-27 遵义钛业股份有限公司 Reduction unit for titanium sponge preparation using magnesium reduction process
CN201678718U (en) * 2010-04-27 2010-12-22 四川恒为制钛科技有限公司 Reactor sieve plate used for producing titanium sponge
CN203768433U (en) * 2014-01-16 2014-08-13 攀钢集团攀枝花钢铁研究院有限公司 Uniform titanium tetrachloride distributing device for producing titanium sponge through magnesium method
CN112280998B (en) * 2020-11-19 2022-04-29 宝钛华神钛业有限公司 Closed cycle method titanium sponge production facility of easy operation

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