CN113118458A - Prediction method for tensile property of metal component formed by selective laser melting - Google Patents
Prediction method for tensile property of metal component formed by selective laser melting Download PDFInfo
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B33—ADDITIVE MANUFACTURING TECHNOLOGY
- B33Y—ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
A prediction method for tensile property of a laser selective melting formed metal component comprises the following steps: (1) 3D printing is carried out on the metal powder in a selective laser area to obtain metal components with different process parameters of laser power P, scanning speed v, scanning interval t and powder layer spreading thickness h; (2) the obtained different metal components are subjected to tensile property test to obtain the yield strength sigma thereofyAnd an elongation δ; (3) with vth/P value as abscissa and sigma respectivelyyAnd δ is the ordinate plotting σy-vth/P and δ -vth/P relationship maps; and the slope k of the fitting curve is obtained by linear fitting1、k2And intercept b of fitted curve1、b2(ii) a (4) Curve fitting by stepLine further predicts the maximum value of tensile properties sigma of metal memberyAnd δ; and calculating to obtain a predicted value of the tensile property. The 3D printing formed part obtained by the method is uniform and compact, and has high strong plasticity; the method can simply and conveniently realize the high-efficiency prediction of the tensile property.
Description
Technical Field
The invention relates to a prediction method for tensile property of a metal component formed by selective laser melting, belonging to the technical field of 3D printing.
Background
The 316L stainless steel has good corrosion resistance and oxidation resistance, and is widely applied to the fields of petroleum pipelines, nuclear power stations, marine equipment and the like. The selective laser melting technology is one of the main means of metal additive manufacturing, and has the advantage of finely forming metal parts with complex structures, but the process parameters in the selective laser melting forming process influence internal defects, thereby having great influence on the performance of formed parts. Wherein, the tensile property (including yield strength, elongation and the like) is the basic property of the structural material, which not only affects other static mechanical properties such as hardness, toughness and the like, but also directly affects the service performance of the material in final use.
In view of the fundamental importance of tensile properties, on the one hand, the evaluation of tensile properties during the development of engineering materials is indispensable and, on the other hand, the combined improvement of tensile strength and plasticity is often targeted. Therefore, accurate evaluation of tensile properties plays an important role in engineering material development and application. However, at present, the prediction of the tensile property of 3D printing metal materials is very deficient, so that a direct quantitative relationship between the tensile property and laser process parameters is established, the rapid prediction of the tensile property is realized, and the problem to be solved in the field of 3D printing at present is urgently solved.
Disclosure of Invention
The invention aims to establish the relation between a laser process and tensile property and improve the strong plasticity of the molten and formed stainless steel in a laser selection area.
The technical scheme of the invention is as follows, a prediction method of tensile property of a metal component formed by selective laser melting comprises the following steps:
(1) 3D printing is carried out on the metal powder in a selective laser area to obtain metal components with different process parameters of laser power P, scanning speed v, scanning interval t and powder layer spreading thickness h;
(2) the obtained different metal components are subjected to tensile property test to obtain the yield strength sigma thereofyAnd an elongation δ;
(3) by using process and performance data, with vth/P value as abscissa and sigma respectivelyyAnd δ is the ordinate plotting σy-vth/P and δ -vth/P relationship maps; and the parameter k is obtained through linear fitting1,k2,b1And b2Wherein k is1And k2As the slope of the fitted curve, b1And b2Is the intercept of the fitted curve;
(4) further predicting the maximum value sigma of the tensile property of the metal member through the curve fitted in the step (3)yAnd δ; or the process parameters P, v, t, h and the parameter value k1,k2,b1And b2Directly into the following equation:
σy=k1(vth/P)+b1
δ=k2(vth/P)+b2
and calculating to obtain a predicted value of the tensile property.
The metal powder is 316 stainless steel, and comprises, by mass, 16.0-18.0% of Cr, 10.0-14.0% of Ni, 2.0-3.0% of Mo, 2.00% of Mn, 1.00% of Si, and the balance of Fe.
The protective gas in the 3D printing process in the step (1) is high-purity argon; pre-laying a layer of stainless steel powder before printing, wherein the particle size of the powder is controlled to be 25-53 mu m; preheating the substrate to 80 ℃; the scraper is a steel scraper.
In the step (1), the laser power is 200-300W, the scanning speed is 800-1000mm/s, the scanning distance is 0.1mm, and the thickness of the powder layer is 0.02-0.04 mm.
And (2) carrying out tensile property test on the series metal members under the same experimental conditions.
And (3) fitting the data by adopting professional data processing software, wherein the restriction correlation degree is not lower than 0.95.
The method has the beneficial effects that the 3D printing formed part obtained by the method is uniform and compact, and has high strong plasticity; the method can simply and conveniently realize the high-efficiency prediction of the tensile property.
Drawings
FIG. 1 is a flow chart of a method for predicting tensile properties of a laser selective melting formed metal component;
FIG. 2 is a graph of tensile engineering stress-strain curves of selective laser melting 316L stainless steel under different laser process parameters eta ═ vth/P;
FIG. 3 is ay- (vth/P) linear relationship diagram;
FIG. 4 is a graph of the delta- (vth/P) linear relationship;
FIG. 5 shows selective laser melting at 0.009mm3Tensile fracture morphology scan at/J;
FIG. 6 shows selective laser melting at 0.012mm3Tensile fracture morphology scan at/J;
FIG. 7 shows selective laser melting at 0.013mm3Tensile fracture morphology scan at/J;
FIG. 8 shows selective laser melting at 0.016mm3Tensile fracture morphology scan at/J;
FIG. 9 shows selective laser melting at 0.018mm3Tensile fracture morphology scan at/J;
FIG. 10 is the result of prediction of tensile properties, and the selective laser melting is 0.020mm3Tensile fracture morphology scan at/J.
Detailed Description
A specific embodiment of the present invention is shown in fig. 1.
The embodiment of the method for predicting the tensile property of the laser selective melting forming metal component comprises the following steps:
(1) melting metal powder in a laser selective area for 3D printing to obtain metal components with different process parameters such as laser power P, scanning speed v, scanning interval t, powder layer spreading thickness h and the like;
the protective gas in the 3D printing process is high-purity argon; pre-laying a layer of stainless steel powder before printing, wherein the particle size of the powder is controlled to be 25-53 mu m; preheating the substrate to 80 ℃; the scraper is a steel scraper.
The tensile engineering stress-strain curve of the selective laser melting 316L stainless steel of the embodiment under different laser process parameters eta ═ vth/P is shown in FIG. 2.
(2) The tensile property of the metal component is tested to obtain the yield strength sigmayAnd an elongation δ.
(3) By using process and performance data, with vth/P value as abscissa and sigma respectivelyyAnd δ is the ordinate plotting σy- (vth/P) and delta- (vth/P) maps, and by linear fitting, ay2151.96 × vth/P +629.98 and δ 1782.50 × vth/P + 12.27. As shown in fig. 3 and 4.
The larger η ═ vth/P is, the smaller the melt pool size becomes, the lower the internal defects become, and the more excellent the tensile properties become, where η represents the energy dispersion.
When the formula is substituted by P200W, the scanning speed v 1000mm/s, the scanning distance t 0.1mm and the powder layer thickness h 0.04mm, eta 0.020 mm/P3J, can yield σy673MPa and δ 47.9%, which is very close to the tensile test results, with minimal fracture defects, as shown in fig. 10.
FIG. 5 shows the selective laser melting at 0.009mm for this example3Tensile fracture morphology scan at/J; the laser power P is 300W, the scanning speed v is 900mm/s, the scanning distance t is 0.1mm and the powder layer thickness h is 0.03mm, at this time, the yield strength is 652MPa, the plasticity is 28.54%, and at this time, the fracture defects are the most.
FIG. 6 shows that the laser selective melting is performed at 0.012mm in the present embodiment3Tensile fracture morphology scan at/J; the laser power P is 300W, the scanning speed v is 900mm/s,the scanning distance t was 0.1mm and the powder coating thickness h was 0.04mm, and the yield strength was 653MPa and the plasticity was 33.8%.
FIG. 7 shows that the laser of this embodiment is selectively melted to 0.013mm3Tensile fracture morphology scan at/J; the laser power P was 250W, the scanning speed v was 800mm/s, the scanning pitch t was 0.1mm, and the powder coating thickness h was 0.04mm, at which time the yield strength was 658MPa and the plasticity was 35.9%.
FIG. 8 shows that the laser selective melting is performed at 0.016mm in the present embodiment3Tensile fracture morphology scan at/J; the laser power P is 250W, the scanning speed v is 1000mm/s, the scanning distance t is 0.1mm and the powder layer thickness h is 0.04mm, at which time the yield strength is 669MPa and the plasticity is 39.8%.
FIG. 9 shows the selective laser melting at 0.018mm for this example3Tensile fracture morphology scan at/J; the laser power P is 200W, the scanning speed v is 900mm/s, the scanning distance t is 0.1mm and the powder coating thickness h is 0.04mm, the yield strength is 670MPa and the plasticity is 45.2%.
Claims (6)
1. A method for predicting tensile properties of a laser selective melting formed metal member, the method comprising the steps of:
(1) 3D printing is carried out on the metal powder in a selective laser area to obtain metal components with different process parameters of laser power P, scanning speed v, scanning interval t and powder layer spreading thickness h;
(2) the obtained different metal components are subjected to tensile property test to obtain the yield strength sigma thereofyAnd an elongation δ;
(3) by using process and performance data, with vth/P value as abscissa and sigma respectivelyyAnd δ is the ordinate plotting σy-vth/P and δ -vth/P relationship maps; and the parameter k is obtained through linear fitting1,k2,b1And b2Wherein k is1And k2As the slope of the fitted curve, b1And b2Is the intercept of the fitted curve;
(4) further predicting the maximum value sigma of the tensile property of the metal member through the curve fitted in the step (3)yAnd δ; or the process parameters P, v,t, h and parameter value k1,k2,b1And b2Directly into the following equation:
σy=k1(vth/P)+b1
δ=k2(vth/P)+b2
and calculating to obtain a predicted value of the tensile property.
2. The method of claim 1, wherein the powdered metal is 316 stainless steel, and the composition comprises, by mass, 16.0-18.0% of Cr, 10.0-14.0% of Ni, 2.0-3.0% of Mo, 2.00% of Mn, 1.00% of Si, and the balance Fe.
3. The method for predicting the tensile property of a laser selective melting formed metal component according to claim 1, wherein the protective gas in the 3D printing process is high-purity argon gas; pre-laying a layer of stainless steel powder before printing, wherein the particle size of the powder is controlled to be 25-53 mu m; preheating the substrate to 80 ℃; the scraper is a steel scraper.
4. The method as claimed in claim 1, wherein the laser power is 200-300W, the scanning speed is 800-1000mm/s, the scanning distance is 0.1mm, and the thickness of the powder layer is 0.02-0.04 mm.
5. The method of claim 1, wherein the step (2) of performing the tensile property test on the series of metal members under the same experimental conditions.
6. The method for predicting the tensile property of a laser selective melting formed metal member according to claim 1, wherein the step (3) is performed by fitting the data with professional data processing software, and the constraint correlation degree is not lower than 0.95.
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CN117110346A (en) * | 2023-10-23 | 2023-11-24 | 中国空气动力研究与发展中心设备设计与测试技术研究所 | Analysis method for microstructure of laser selective melting plate |
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CN117110346A (en) * | 2023-10-23 | 2023-11-24 | 中国空气动力研究与发展中心设备设计与测试技术研究所 | Analysis method for microstructure of laser selective melting plate |
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