CN113118194A

CN113118194A - Oxidation treatment device for biopharmaceutical residues

Info

Publication number: CN113118194A
Application number: CN202110538980.0A
Authority: CN
Inventors: 隋艳晖
Original assignee: Weihai Vocational College
Current assignee: Weihai Vocational College
Priority date: 2018-12-29
Filing date: 2018-12-29
Publication date: 2021-07-16
Anticipated expiration: 2038-12-29
Also published as: CN113118194B; CN109590315A; CN109590315B

Abstract

The invention discloses an oxidation treatment device for biopharmaceutical residues, which comprises a bottom plate, wherein the top of the bottom plate is fixedly connected with a treatment box and a mixing box in sequence from left to right, the top of the right side of the treatment box is fixedly connected with a protection box, the inside of the protection box is fixedly connected with a U-shaped pipe, one end of the U-shaped pipe penetrates through the bottom of the protection box and extends to the lower part of the protection box, and a first support plate and a second support plate are fixedly connected between the opposite sides of the treatment box and the mixing box in sequence from top to bottom. This an oxidation treatment device for bio-pharmaceuticals residue utilizes the cooperation of water pump and outlet pipe, can arrange solution in the U type pipe at a high speed, and when solution passed through pipe connection spare, it can break up solution earlier to utilize the mixing arm, then the guide vane that usable slope set up makes solution be the heliciform and flows for the mixture of residue and reactant is favorable to the quick oxidative decomposition of residue.

Description

Oxidation treatment device for biopharmaceutical residues

Technical Field

The invention relates to the technical field of oxidation devices, in particular to an oxidation treatment device for biopharmaceutical residues.

Background

The oxidation treatment is a chemical treatment method of wastewater, which converts pollutants in the wastewater into harmless or nontoxic forms by utilizing chemical oxidation reaction. The action of electron loss is called oxidation reaction, and conversely, the action of electron gain is called reduction. The oxidation reaction in the narrow sense means that a substance combines with oxygen; reduction refers to the loss of oxygen from a material. The oxidation number increases during oxidation and decreases during reduction. Oxidation and reduction refer to reactants (molecules, ions or atoms), and oxidation is also referred to as oxidation. When the organic matter reacts, the action of introducing oxygen into the organic matter or removing hydrogen is called oxidation; the introduction of hydrogen or the loss of oxygen is called reduction. The oxidation of a substance slowly reacting with oxygen to slowly generate heat without emitting light is called slow oxidation, such as metal corrosion, biological respiration and the like. The intense light-emitting and heat-emitting oxidation is called combustion. Typically, oxidation of a substance with oxygen is exothermic and individual substances may absorb heat, such as nitrogen and oxygen. In electrochemistry, the anode is oxidized, and the cathode is reduced. The oxidation reaction is mainly classified into air (oxygen) oxidation and chemical agent oxidation according to the difference between an oxidizing agent and an oxidation process. The chemical reagent oxidation has the advantages of good selectivity, simple process, convenience, flexibility and the like, and in the field of pharmaceutical chemicals, the chemical reagent oxidation method is used for multiple purposes due to the small tonnage of products.

The method is characterized in that the biological pharmacy residues need to be subjected to oxidation treatment, so that the modified properties of the biological pharmacy residues can be safely discharged, the existing biological pharmacy residues are usually subjected to simple stirring by directly adding an oxidizing agent during treatment, the residues cannot be fully mixed with the oxidizing agent, so that part of the residues are difficult to completely oxidize, excessive oxidizing agent needs to be added, the cost is wasted, and more time needs to be consumed.

Disclosure of Invention

Aiming at the defects of the prior art, the invention provides an oxidation treatment device for biopharmaceutical residues, which solves the problems that the residues cannot be fully mixed with an oxidizing agent due to simple stirring by directly adding the oxidizing agent, excessive oxidizing agent needs to be added, the cost is wasted, and more time is consumed.

In order to achieve the purpose, the invention is realized by the following technical scheme: an oxidation treatment device for biological pharmacy residues comprises a bottom plate, wherein the top of the bottom plate is fixedly connected with a treatment box and a mixing box from left to right in sequence, the top of the right side of the treatment box is fixedly connected with a protection box, the inside of the protection box is fixedly connected with a U-shaped pipe, one end of the U-shaped pipe penetrates through the bottom of the protection box and extends to the lower part of the protection box, a first supporting plate and a second supporting plate are fixedly connected between the opposite sides of the treatment box and the mixing box from top to bottom in sequence, the top of the first supporting plate is fixedly connected with a water pump, the water outlet of the water pump is communicated with a water outlet pipe, the top end of the water outlet pipe is communicated with one end of the U-shaped pipe positioned at the bottom of the protection box, the water inlet of the water pump is communicated with a water inlet pipe, the one end that the water pump was kept away from to the inlet tube runs through the left wall of mixing box and extends to the bottom of mixing box inner chamber.

The first motor of top fixedly connected with of second backup pad, the right-hand member of first motor output shaft passes through the first (mixing) shaft of shaft coupling fixedly connected with, the right-hand member of first (mixing) shaft runs through the left wall of mixing box and extends to the inside of mixing box, and the right-hand member of first (mixing) shaft rotates with the right side of mixing box inner wall to be connected, the right side intercommunication at mixing box top has a feeding section of thick bamboo, the top of bottom plate just is located the back fixedly connected with dust removal case of handling the case, bracing piece fixedly connected with dust extraction case is passed through at the top of dust removal case.

The top fixedly connected with gear box of processing case, the top fixedly connected with motor case of gear box, and the inside fixedly connected with second motor of motor case, the bottom of second motor output shaft runs through motor case and gear box in proper order and extends to the inside of gear box, the inside intermediate rotation of gear box is connected with first gear, and the top of first gear and the bottom fixed connection of second motor output shaft, one side meshing of first gear has the second gear, the tooth's socket has been seted up to the internal surface of gear box, and one side and the tooth's socket intermeshing of second gear, the equal fixedly connected with second (mixing) shaft in bottom of first gear and second gear.

The utility model discloses a protection box, including U type pipe, pipe connector, inlet pipe, protection box, mixing box inner chamber, U type pipe is provided with a plurality ofly, communicate through the pipe connector between the U type pipe, the internal surface fixedly connected with guide plate of pipe connector, the internal surface of pipe connector just is located one side fixedly connected with hybrid pole of guide plate, the one end intercommunication that the pipe connector was kept away from to the U type pipe has the inlet pipe, the one end that the U type pipe was kept away from to the inlet pipe runs through the guard box in proper order and handles the case and extend to the bottom of handling the incasement chamber, the left side fixedly connected with oxygenator at mixing box top.

The surface of first (mixing) shaft just is located the inside fixedly connected with puddler of mixing box, the fixed surface of second (mixing) shaft is connected with the stirring leaf, the surface cover of second (mixing) shaft is equipped with the rotor plate, and the surface of rotor plate is connected with the interior surface rotation who handles the roof portion.

The middle of a feeding section of thick bamboo top communicates there is the water injection pipe, the top of a feeding section of thick bamboo and the left and right sides that is located the water injection pipe all communicate there is the feeder hopper, the inside fixedly connected with mixing bucket of a feeding section of thick bamboo, the top fixedly connected with control box of guard box, the front of control box from left to right fixedly connected with display screen and starting switch in proper order, the left and right sides of guard box inner wall just is located fixedly connected with ultraviolet tube between the U type pipe.

The inside of dust extraction case is through mount fixedly connected with third motor, the top fixedly connected with of third motor output shaft rotates the cover, and rotates the fixed surface of cover and be connected with the blade, the top intercommunication of dust extraction case has the air inlet fill, the top intercommunication of air inlet fill has the exhaust tube, the one end that the air inlet was fought and the top intercommunication of handling the case are kept away from to the exhaust tube, the bottom intercommunication of dust extraction case has the air outlet fill, the bottom intercommunication of air outlet fill has the outlet duct, the bottom of outlet duct runs through the top of dust removal case and extends to the bottom of dust removal incasement chamber.

Preferably, a liquid inlet pipe penetrates through the upper portion of the back face of the dust removal box, a drain pipe is communicated with the lower portion of the back face of the dust removal box, a manual control valve is fixedly connected to the surface of the drain pipe, and an exhaust hole is formed in the top of the dust removal box.

Preferably, the surface of inlet pipe just is located the inside cover that handles the case and is equipped with first spacing ring, and one side of first spacing ring and the right side fixed connection who handles the incasement wall, the surface of inlet pipe just is located the inside cover that the mixing box is equipped with the second spacing ring, and one side of second spacing ring and the left side fixed connection of mixing box inner wall.

Preferably, handle the first glass observation window of left side fixedly connected with of case, the left side fixedly connected with second glass observation window of dust removal case, the left side intercommunication of handling the case has the blow off pipe, the left end threaded connection of blow off pipe has sealed lid.

Preferably, a groove is formed in the front side of the top of the treatment box, a magnetic ring is fixedly connected to the bottom of the inner surface of the groove, a metal block is movably connected to the inside of the groove, a sampling rod is fixedly connected to the bottom of the metal block, the bottom end of the sampling rod sequentially penetrates through the magnetic ring and the top of the treatment box and extends to the inside of the treatment box, a sampling groove is formed in the surface of the sampling rod and located inside the treatment box, a pull ring is fixedly connected to the top of the metal block, and a sealing gasket is fixedly connected to the bottom of the metal block and located outside the sampling rod.

Preferably, four corners of the bottom plate are fixedly connected with pad feet, the bottom of the pad feet is fixedly connected with a damping pad, the number of the second gears is two, and the two second gears are symmetrically distributed around the circle center of the first gear.

On the other hand, the invention also provides an oxidation treatment method for the biopharmaceutical residue, which comprises the steps of adding a medicament into a dust removal box 14 through a liquid inlet pipe 44, respectively adding the residue and an oxidant into a feeding cylinder 13 from two feed hoppers 31, simultaneously connecting a water injection pipe 30 with the water pipe, discharging water into the feeding cylinder 13, mixing the water with the residue and the oxidant, starting a first motor 11, driving a first stirring shaft 12 to rotate by the first motor 11, mixing the water with the residue and the oxidant by using a stirring rod 27, then starting an oxygenator 25 and a water pump 8, pumping the solution by using the water pump 8 through a water inlet pipe 10, discharging the solution into a U-shaped pipe 5 at a high speed by using a water outlet pipe 9, simultaneously discharging oxygen into the water inlet pipe 9 through an air outlet pipe 26 by the oxygenator 25 to be mixed with the solution, then when the solution passes through a pipeline connecting piece 21, firstly scattering the solution by using a mixing rod 23, then enabling the solution to flow, promote the thorough mixing of the residue and the reactant, start the ultraviolet lamp 36 at the same time, kill the drug germ in the solution, preheat easily at the same time, then the solution is discharged into the treatment box 2 through the feed pipe 24, start the second motor 63, the second motor 63 drives the first gear 18 to rotate, drive the second stirring shaft 20 to rotate through the second gear 19 that is meshed with each other, make the second stirring shaft 20 drive the stirring blade 28 to rotate, and the second stirring shaft 20 of both sides rotates around the second stirring shaft 20 in the center, promote the reaction rate, start the third motor 37, the third motor 37 drives the blade 39 to rotate through the rotating sleeve 38, utilize the exhaust pipe 41 to pump the waste gas generated in the reaction, utilize the outlet pipe 43 to discharge into the dust removal box 14, the medicament decomposes the harmful waste gas, then the air is discharged through the exhaust hole 47, finally close the device, open the sealing cover 53 to discharge the waste liquid in the treatment box 2, the manual valve 46 is then opened to drain the waste liquid from the dust box 14.

Advantageous effects

The invention provides an oxidation treatment device for biopharmaceutical residues. The method has the following beneficial effects:

(1) the oxidation treatment device for the bio-pharmaceutical residues is characterized in that a U-shaped pipe is fixedly connected inside a protection box, one end of the U-shaped pipe penetrates through the bottom of the protection box and extends to the lower part of the protection box, a first supporting plate and a second supporting plate are fixedly connected between one opposite side of the treatment box and a mixing box from top to bottom in sequence, a water pump is fixedly connected to the top of the first supporting plate, a water outlet of the water pump is communicated with a water outlet pipe, the top end of the water outlet pipe is communicated with one end, located at the bottom of the protection box, of the U-shaped pipe, the U-shaped pipe is communicated with the mixing box through a pipeline connecting piece, a guide piece is fixedly connected to the inner surface of the pipeline connecting piece, a mixing rod is fixedly connected to the inner surface of the pipeline connecting piece and one side, located on the guide piece, the mixing rod is matched with, then the solution can flow spirally by utilizing the guide sheet which is arranged obliquely, so that the mixing of the residue and the reactant is accelerated, and the rapid oxidative decomposition of the residue is facilitated.

(2) This an oxidation treatment device for bio-pharmaceuticals residue, it has the water injection pipe to communicate through the centre at a feeding section of thick bamboo top, the top of a feeding section of thick bamboo and the left and right sides that is located the water injection pipe all communicate there is the feeder hopper, the inside fixedly connected with of a feeding section of thick bamboo mixes the fill, set up two feeder hoppers, residue and reactant can be added simultaneously, and be convenient for add in proportion, the medicament has been practiced thrift, and it can make the residue dissolve partly to be provided with the water injection pipe, and the water pump extraction of being convenient for, and utilize the mixing to fight and can make water, the preliminary mixing of medicament and residue, be favorable to improving the progress.

(3) This an oxidation treatment device for bio-pharmaceuticals residue, through the first motor of top fixedly connected with in the second backup pad, the right-hand member of first motor output shaft passes through the first (mixing) shaft of shaft coupling fixedly connected with, the inside fixedly connected with puddler on the surface of first (mixing) shaft and the position in mixing box utilizes first motor and first (mixing) shaft, the cooperation of puddler, can fully mix water, medicament and residue, and can break up the residue of caking, avoid blocking the water pump, can improve work efficiency simultaneously.

(4) This an oxidation treatment device for bio-pharmaceuticals residue, it is connected with first gear to rotate through the centre inside the gear box, and the top of first gear and the bottom fixed connection of second motor output shaft, one side meshing of first gear has the second gear, the tooth's socket has been seted up to the internal surface of gear box, and one side and the tooth's socket intermeshing of second gear, the equal fixedly connected with second (mixing) shaft in bottom of first gear and second gear, the fixed surface of second (mixing) shaft is connected with the stirring leaf, utilize the second motor, the cooperation of first gear and second gear, can make three second (mixing) shafts drive the stirring leaf and rotate simultaneously, utilize the structural feature of stirring leaf, can make solution roll from top to bottom, and the second (mixing) shaft of both sides can rotate around middle second (mixing) shaft, working range has been increased, stirring efficiency and quality have been improved.

(5) This an oxidation treatment device for bio-pharmaceuticals residue, there is the air inlet fill through the top intercommunication at the suction dust case, the top intercommunication that the air inlet was fought has the exhaust tube, the one end that the air inlet was fought is kept away from to the exhaust tube and the top intercommunication of handling the case, the bottom intercommunication of suction dust case has the play wind fill, the bottom intercommunication that goes out the wind fill has the outlet duct, the bottom of outlet duct runs through the top of dust removal case and extends to the bottom of dust removal incasement chamber, utilize suction dust case and air inlet fill, the cooperation of exhaust tube, can take the harmful gas who produces when handling the incasement reaction out, and through the play wind fill, the outlet duct is discharged and is carried out the reaction and decomposition in the dust removal incasement, influence the environment in avoiding harmful gas.

(6) The oxidation treatment device for the bio-pharmaceutical residues is characterized in that a groove is formed in the front side of the top of a treatment box, a magnetic ring is fixedly connected to the bottom of the inner surface of the groove, a metal block is movably connected inside the groove, a sampling rod is fixedly connected to the bottom of the metal block, the bottom end of the sampling rod sequentially penetrates through the magnetic ring and the top of the treatment box and extends to the inside of the treatment box, a sampling groove is formed in the surface of the sampling rod and located inside the treatment box, a pull ring is fixedly connected to the top of the metal block, a sealing gasket is fixedly connected to the bottom of the metal block and located outside the sampling rod, and the sampling rod is matched with the sampling, can extract a small amount of samples at any time during work to detect whether the oxidation is completed or not, is convenient to use, and the sealing gasket can block the gap by utilizing the mutual attraction of the magnetic ring and the metal block, thereby avoiding gas leakage for a long time.

(7) This an oxidation treatment device for bio-pharmaceuticals residue through the first glass observation window of left side fixedly connected with who handles the case, and the left side fixedly connected with second glass observation window of dust removal case sets up first glass observation window and second glass observation window, can observe the behavior of handling case and dust removal incasement at any time to adjust convenient to use at any time.

Drawings

FIG. 1 is a schematic structural view of the present invention;

FIG. 2 is a side view of the internal structure of the dust box of the present invention;

FIG. 3 is a schematic view of the external structure of the dust removing box and the treating box of the present invention;

FIG. 4 is a schematic view of the internal structure of the feed cylinder of the present invention;

FIG. 5 is a schematic structural view of a U-shaped tube according to the present invention;

FIG. 6 is a schematic view showing the internal structure of the pipe coupling of the present invention;

fig. 7 is a partial enlarged view of the invention at a in fig. 2.

In the figure: 1 bottom plate, 2 processing box, 3 mixing box, 4 protection box, 5U-shaped pipe, 6 first support plate, 7 second support plate, 8 water pump, 9 water outlet pipe, 10 water inlet pipe, 11 first motor, 12 first stirring shaft, 13 feeding cylinder, 14 dust removing box, 15 dust extracting box, 16 gear box, 17 motor box, 18 first gear, 19 second gear, 20 second stirring shaft, 21 pipeline connector, 22 guide plate, 23 mixing rod, 24 feeding pipe, 25 oxygen charging machine, 26 air outlet pipe, 27 stirring rod, 28 stirring blade, 29 rotating plate, 30 water injection pipe, 31 feeding hopper, 32 mixing hopper, 33 control box, 34 display screen, 35 starting switch, 36 ultraviolet lamp tube, 37 third motor, 38 rotating sleeve, 39 blade, 40 air inlet hopper, 41 air outlet pipe, 42 air outlet hopper, 43 air outlet pipe, 44 liquid inlet pipe, 45 water outlet pipe, 46 manual control valve, 47 exhaust hole, 48 first limit ring, 49 second limit ring, 50 first glass observation windows, 51 second glass observation windows, 52 sewage pipes, 53 sealing covers, 54 grooves, 55 magnetic rings, 56 metal blocks, 57 sampling rods, 58 sampling grooves, 59 pull rings, 60 sealing gaskets, 61 foot pads, 62 shock-absorbing pads and 63 second motors.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to figures 1-7 of the drawings,

example 1

An oxidation treatment device for biological pharmacy residues comprises a bottom plate, wherein the top of the bottom plate is fixedly connected with a treatment box and a mixing box from left to right in sequence, the top of the right side of the treatment box is fixedly connected with a protection box, the inside of the protection box is fixedly connected with a U-shaped pipe, one end of the U-shaped pipe penetrates through the bottom of the protection box and extends to the lower part of the protection box, a first supporting plate and a second supporting plate are fixedly connected between the opposite sides of the treatment box and the mixing box from top to bottom in sequence, the top of the first supporting plate is fixedly connected with a water pump, the water outlet of the water pump is communicated with a water outlet pipe, the top end of the water outlet pipe is communicated with one end of the U-shaped pipe positioned at the bottom of the protection box, the water inlet of the water pump is communicated with a water inlet pipe, the one end that the water pump was kept away from to the inlet tube runs through the left wall of mixing box and extends to the bottom of mixing box inner chamber.

Preferably, the surface of first (mixing) shaft just is located the inside fixedly connected with puddler of mixing box, the fixed surface of second (mixing) shaft is connected with the stirring leaf, the surface cover of second (mixing) shaft is equipped with the rotor plate, and the surface of rotor plate is connected with the interior surface rotation who handles the roof portion.

An oxidation treatment method for bio-pharmaceutical residues comprises adding a medicament into a dust removal box 14 through a liquid inlet pipe 44, adding residues and an oxidant into a feeding cylinder 13 from two feeding hoppers 31 respectively, connecting a water injection pipe 30 with a water pipe, discharging water into the feeding cylinder 13, mixing the residues and the oxidant, starting a first motor 11, driving a first stirring shaft 12 to rotate by the first motor 11, mixing the water with the residues and the oxidant by using a stirring rod 27, starting an oxygenator 25 and a water pump 8, pumping the solution by using the water pump 8 through a water inlet pipe 10, discharging the solution into a U-shaped pipe 5 at a high speed by using a water outlet pipe 9, mixing oxygen with the solution by using the oxygenator 25 through a water outlet pipe 26 and a water discharge pipe 9, scattering the solution when the solution passes through a pipe connector 21, leading the mixing rod 23 to break up the solution, leading the solution to spirally flow by using a guide sheet 22 which is obliquely arranged, and promoting the sufficient mixing of the residues and the reactants, simultaneously starting the ultraviolet lamp tube 36 to kill drug germs in the solution and simultaneously preheat the solution, then discharging the solution into the treatment box 2 through the feeding pipe 24, starting the second motor 63, driving the first gear 18 to rotate by the second motor 63, driving the second stirring shaft 20 to rotate by the second gear 19 which is meshed with each other, driving the stirring blade 28 to rotate by the second stirring shaft 20, driving the second stirring shafts 20 at two sides to rotate around the second stirring shaft 20 at the center, promoting the reaction rate, starting the third motor 37, driving the blade 39 to rotate by the third motor 37 through the rotating sleeve 38, pumping in waste gas generated in the reaction by the air pumping pipe 41, discharging the waste gas into the dust removal box 14 by the air outlet pipe 43, decomposing harmful waste gas by a medicament, then discharging air through the air outlet hole 47, finally closing the device, opening the sealing cover 53 to discharge waste liquid in the treatment box 2, then opening the manual control valve 46, the waste liquid in the dust removal tank 14 is discharged.

Example 2

Preferably, the middle of a feeding section of thick bamboo top communicates there is the water injection pipe, the top of a feeding section of thick bamboo and the left and right sides that is located the water injection pipe all communicate there is the feeder hopper, the inside fixedly connected with mixing hopper of a feeding section of thick bamboo, the top fixedly connected with control box of guard box, fixedly connected with display screen and starting switch in proper order from left to right in the front of control box, the left and right sides of guard box inner wall just is located fixedly connected with ultraviolet tube between the U type pipe.

Example 3

Preferably, the inside of dust extraction case is through mount fixedly connected with third motor, the top fixedly connected with of third motor output shaft rotates the cover, and rotates the fixed surface of cover and be connected with the blade, the top intercommunication of dust extraction case has the air inlet fill, the top intercommunication of air inlet fill has the exhaust tube, the one end that the air inlet was fought and the top intercommunication of handling the case are kept away from to the exhaust tube, the bottom intercommunication of dust extraction case has the air outlet fill, the bottom intercommunication of air outlet fill has the outlet duct, the bottom of outlet duct runs through the top of dust removal case and extends to the bottom of dust removal incasement chamber.

Example 4

Example 5

Example 6

Example 7

Example 8

Example 9

The invention provides a technical scheme that: an oxidation treatment device for bio-pharmaceutical residues comprises a base plate 1, wherein four corners of the bottom of the base plate 1 are fixedly connected with pad feet 61, the bottom of the pad feet 61 is fixedly connected with a shock absorption pad 62, two second gears 19 are arranged, the two second gears 19 are symmetrically distributed about the circle center of a first gear 18, the top of the base plate 1 is fixedly connected with a treatment box 2 and a mixing box 3 from left to right in sequence, the left side of the treatment box 2 is fixedly connected with a first glass observation window 50, the left side of a dust removal box 14 is fixedly connected with a second glass observation window 51, the first glass observation window 50 and the second glass observation window 51 are arranged, the working conditions in the treatment box 2 and the dust removal box 14 can be observed at any time so as to be adjusted at any time, the use is convenient, the left side of the treatment box 2 is communicated with a sewage discharge pipe 52, the left end of the sewage discharge pipe 52 is in threaded connection with a sealing cover 53, a, the bottom of the inner surface of the groove 54 is fixedly connected with a magnetic ring 55, the inside of the groove 54 is movably connected with a metal block 56, the bottom of the metal block 56 is fixedly connected with a sampling rod 57, the bottom end of the sampling rod 57 sequentially penetrates through the magnetic ring 55 and the top of the processing box 2 and extends to the inside of the processing box 2, a sampling groove 58 is formed in the surface of the sampling rod 57 and is positioned in the processing box 2, the top of the metal block 56 is fixedly connected with a pull ring 59, the bottom of the metal block 56 and the outside of the sampling rod 57 are fixedly connected with a sealing gasket 60, by matching the sampling rod 57 and the sampling groove 58, a small amount of samples can be extracted at any time in work for detection, whether the samples are completely oxidized or not can be checked, the use is convenient, and by utilizing the mutual attraction of the magnetic ring 55 and the metal block 56, the sealing gasket 60 can block gaps, the, inside fixedly connected with U type pipe 5 of guard box 4, the one end of U type pipe 5 runs through the bottom of guard box 4 and extends to the below of guard box 4, from the top down in proper order first backup pad 6 of fixedly connected with and second backup pad 7 between the one side that handles case 2 and mixing box 3 are relative, the top fixedly connected with water pump 8 of first backup pad 6, water pump 8's delivery port intercommunication has outlet pipe 9, the top of outlet pipe 9 and the one end intercommunication that U type pipe 5 is located the guard box 4 bottom, water pump 8's water inlet intercommunication has inlet tube 10, the one end that water pump 8 was kept away from to inlet tube 10 runs through the left wall of mixing box 3 and extends to the bottom of 3 inner chambers of mixing box.

The top of the second supporting plate 7 is fixedly connected with a first motor 11, the right end of the output shaft of the first motor 11 is fixedly connected with a first stirring shaft 12 through a coupler, the surface of the first stirring shaft 12 and the inner part of the mixing box 3 are fixedly connected with a stirring rod 27, the first motor 11 is matched with the first stirring shaft 12 and the stirring rod 27, water, medicament and residues can be fully mixed, and the caked residues can be scattered, so that the water pump 8 is prevented from being blocked, the working efficiency can be improved, the surface of the second stirring shaft 20 is fixedly connected with stirring blades 28, the second motor 63 and the first gear 18 are matched with the second gear 19, three second stirring shafts 20 can drive the stirring blades 28 to simultaneously rotate, the solution can roll up and down by utilizing the structural characteristics of the stirring blades 28, and the second stirring shafts 20 at two sides can rotate around the second stirring shaft 20 in the middle, so that the working range is enlarged, the stirring efficiency and the quality are improved, the surface sleeve of the second stirring shaft 20 is provided with the rotating plate 29, the surface of the rotating plate 29 is rotatably connected with the inner surface of the top of the treatment box 2, the right end of the first stirring shaft 12 penetrates through the left wall of the mixing box 3 and extends to the inside of the mixing box 3, the right end of the first stirring shaft 12 is rotatably connected with the right side of the inner wall of the mixing box 3, the right side of the top of the mixing box 3 is communicated with the feeding cylinder 13, the middle of the top of the feeding cylinder 13 is communicated with the water injection pipe 30, the top of the feeding cylinder 13 is communicated with the feed hoppers 31 on the left side and the right side of the water injection pipe 30, the mixing hoppers 32 are fixedly connected inside the feeding cylinder 13, the two feed hoppers 31 are arranged, residues and reactants can be added simultaneously, the adding according to the proportion is convenient, the chemicals are saved, the water injection pipe 30 is arranged to dissolve part of the residues, The preliminary mixing of medicament and residue is favorable for improving the progress of subsequent work, the top of the protection box 4 is fixedly connected with a control box 33, the front of the control box 33 is fixedly connected with a display screen 34 and a starting switch 35 from left to right in sequence, the left and right sides of the inner wall of the protection box 4 are fixedly connected with ultraviolet lamp tubes 36 between U-shaped tubes 5, the ultraviolet lamp tubes 36 have a heating effect and a certain sterilization effect and kill drug germs in the residue, the top of the bottom plate 1 and the back of the processing box 2 are fixedly connected with a dust removal box 14, a liquid inlet tube 44 penetrates through the upper part of the back of the dust removal box 14, the lower part of the back of the dust removal box 14 is communicated with a drain tube 45, the surface of the drain tube 45 is fixedly connected with a manual control valve 46, the top of the dust removal box 14 is provided with an exhaust hole 47, the top of the dust removal box 14 is fixedly connected with a dust extraction, the top end of the output shaft of the third motor 37 is fixedly connected with a rotating sleeve 38, the surface of the rotating sleeve 38 is fixedly connected with blades 39, the top of the dust pumping box 15 is communicated with an air inlet hopper 40, the top of the air inlet hopper 40 is communicated with an air exhaust pipe 41, one end of the air exhaust pipe 41, which is far away from the air inlet hopper 40, is communicated with the top of the processing box 2, the bottom of the dust pumping box 15 is communicated with an air outlet hopper 42, the bottom of the air outlet hopper 42 is communicated with an air outlet pipe 43, the bottom end of the air outlet pipe 43 penetrates through the top of the dust removing box 14 and extends to the bottom of the inner cavity of the dust removing box 14, and by utilizing the matching of the dust pumping box 15, the air inlet hopper 40 and the air exhaust pipe 41, harmful gas generated during reaction in the processing box 2 can be exhausted, and is exhausted into the dust removing box 14 through.

Handle the top fixedly connected with gear box 16 of case 2, the top fixedly connected with motor case 17 of gear box 16, and the inside fixedly connected with second motor 63 of motor case 17, the bottom of second motor 63 output shaft runs through motor case 17 and gear box 16 in proper order and extends to the inside of gear box 16, the inside intermediate rotation of gear box 16 is connected with first gear 18, and the top of first gear 18 and the bottom fixed connection of second motor 63 output shaft, one side meshing of first gear 18 has second gear 19, the tooth's socket has been seted up to the internal surface of gear box 16, and one side and the tooth's socket intermeshing of second gear 19, the equal fixedly connected with second (mixing) shaft 20 in bottom of first gear 18 and second gear 19.

The U-shaped pipes 5 are provided with a plurality of U-shaped pipes 5 which are communicated with each other through a pipe connecting piece 21, the inner surface of the pipe connecting piece 21 is fixedly connected with a guide plate 22, the inner surface of the pipe connecting piece 21 and one side of the guide plate 22 are fixedly connected with a mixing rod 23, the solution can be discharged into the U-shaped pipes 5 at high speed by utilizing the matching of a water pump 8 and a water outlet pipe 9, when the solution passes through the pipe connecting piece 21, the solution can be firstly scattered by utilizing the mixing rod 23, then the solution can flow spirally by utilizing the guide plate 22 which is arranged obliquely, the mixing of the residue and the reactant is accelerated, the rapid oxidative decomposition of the residue is facilitated, one end of the U-shaped pipe 5, which is far away from the pipe connecting piece 21, is communicated with a feed pipe 24, a first limit ring 48 is sleeved on the surface of the feed pipe 24 and positioned inside the treatment box 2, one side of the first limit ring 48 is fixedly connected with, and one side of second spacing ring 49 and the left side fixed connection of mixing box 3 inner wall, the one end that U type pipe 5 was kept away from to inlet pipe 24 runs through guard box 4 in proper order and handles case 2 and extend to the bottom of handling the case 2 inner chamber, the left side fixed connection at mixing box 3 top has oxygenator 25, oxygenator 25's gas outlet intercommunication has outlet duct 26, and the left end of outlet duct 26 communicates with the surface of outlet pipe 9.

Example 11

When the device works, a medicament is added into the dust removal box 14 through the liquid inlet pipe 44, residues and an oxidant are respectively added into the feeding cylinder 13 from the two feeding hoppers 31, the water injection pipe 30 is connected with the water pipe, water is discharged into the feeding cylinder 13 and is mixed with the residues and the oxidant, the first motor 11 is started, the first motor 11 drives the first stirring shaft 12 to rotate, water is mixed with the residues and the oxidant through the stirring rod 27, then the oxygenating machine 25 and the water pump 8 are started, the water pump 8 pumps the solution through the water inlet pipe 10 and discharges the solution into the U-shaped pipe 5 at a high speed through the water outlet pipe 9, meanwhile, the oxygenating machine 25 discharges oxygen into the water inlet and outlet pipe 9 through the air outlet pipe 26 to be mixed with the solution, then when the solution passes through the pipeline connecting piece 21, the mixing rod 23 firstly breaks up the solution, then the guide piece 22 which is obliquely arranged enables the solution to flow spirally, full mixing of the residues and the, the drug and germs in the solution are killed, simultaneously the solution is easy to be preheated, then the solution is discharged into the treatment box 2 through the feed pipe 24, the second motor 63 is started, the second motor 63 drives the first gear 18 to rotate, the second stirring shaft 20 is driven to rotate through the second gear 19 which is meshed with each other, so that the second stirring shaft 20 drives the stirring blades 28 to rotate, and the second stirring shaft 20 at the two sides rotates around the second stirring shaft 20 at the center, the reaction rate is promoted, the third motor 37 is started, the third motor 37 drives the blades 39 to rotate through the rotating sleeve 38, the exhaust gas generated in the reaction is pumped in by the exhaust pipe 41 and is exhausted into the dust removing box 14 by the exhaust pipe 43, the harmful exhaust gas is decomposed by the medicament, the air is then exhausted through the exhaust port 47 and finally the device is closed, the sealing lid 53 is opened to exhaust the waste liquid in the treatment tank 2, and then the manual valve 46 is opened to exhaust the waste liquid in the dust removal tank 14.

Claims

1. An oxidation treatment device for biopharmaceutical residues, comprising a base plate (1), characterized in that: the top of the bottom plate (1) is fixedly connected with a processing box (2) and a mixing box (3) from left to right in sequence, the top on the right side of the processing box (2) is fixedly connected with a protection box (4), the inside of the protection box (4) is fixedly connected with a U-shaped pipe (5), one end of the U-shaped pipe (5) penetrates through the bottom of the protection box (4) and extends to the lower part of the protection box (4), a first supporting plate (6) and a second supporting plate (7) are fixedly connected between the opposite sides of the processing box (2) and the mixing box (3) from top to bottom in sequence, the top of the first supporting plate (6) is fixedly connected with a water pump (8), a water outlet of the water pump (8) is communicated with a water outlet pipe (9), the top end of the water pump (9) is communicated with one end, located at the bottom of the protection box (4), of the U-shaped pipe (5), the, one end of the water inlet pipe (10), which is far away from the water pump (8), penetrates through the left wall of the mixing box (3) and extends to the bottom of the inner cavity of the mixing box (3);

the top of the second supporting plate (7) is fixedly connected with a first motor (11), the right end of an output shaft of the first motor (11) is fixedly connected with a first stirring shaft (12) through a coupler, the right end of the first stirring shaft (12) penetrates through the left wall of the mixing box (3) and extends into the mixing box (3), the right end of the first stirring shaft (12) is rotatably connected with the right side of the inner wall of the mixing box (3), the right side of the top of the mixing box (3) is communicated with a feeding barrel (13), the top of the bottom plate (1) is fixedly connected with a dust removal box (14) on the back of the treatment box (2), and the top of the dust removal box (14) is fixedly connected with a dust extraction box (15) through a supporting rod;

the top of the processing box (2) is fixedly connected with a gear box (16), the top of the gear box (16) is fixedly connected with a motor box (17), a second motor (63) is fixedly connected inside the motor box (17), the bottom end of an output shaft of the second motor (63) sequentially penetrates through the motor box (17) and the gear box (16) and extends to the inside of the gear box (16), a first gear (18) is rotatably connected in the middle of the interior of the gear box (16), and the top of the first gear (18) is fixedly connected with the bottom end of the output shaft of the second motor (63), a second gear (19) is meshed with one side of the first gear (18), a tooth groove is formed in the inner surface of the gear box (16), one side of the second gear (19) is meshed with the tooth grooves, and the bottoms of the first gear (18) and the second gear (19) are fixedly connected with a second stirring shaft (20);

the device comprises a plurality of U-shaped pipes (5), wherein the U-shaped pipes (5) are communicated with each other through a pipe connecting piece (21), a guide sheet (22) is fixedly connected to the inner surface of the pipe connecting piece (21), a mixing rod (23) is fixedly connected to one side, located on the guide sheet (22), of the inner surface of the pipe connecting piece (21), one end, far away from the pipe connecting piece (21), of each U-shaped pipe (5) is communicated with a feeding pipe (24), one end, far away from the U-shaped pipes (5), of each feeding pipe (24) sequentially penetrates through a protection box (4) and a treatment box (2) and extends to the bottom of an inner cavity of the treatment box (2), an oxygenator (25) is fixedly connected to the left side of the top of the mixing box (3), an air outlet of the oxygenator (25) is communicated with an air outlet pipe (26), and the left end of the;

the surface of the first stirring shaft (12) and the inner part of the mixing box (3) are fixedly connected with a stirring rod (27), the surface of the second stirring shaft (20) is fixedly connected with a stirring blade (28), the surface of the second stirring shaft (20) is sleeved with a rotating plate (29), and the surface of the rotating plate (29) is rotatably connected with the inner surface of the top of the treatment box (2);

the middle of the top of the feeding barrel (13) is communicated with a water injection pipe (30), the top of the feeding barrel (13) and the left and right sides of the water injection pipe (30) are communicated with feed hoppers (31), the interior of the feeding barrel (13) is fixedly connected with a mixing hopper (32), the top of the protection box (4) is fixedly connected with a control box (33), the front of the control box (33) is fixedly connected with a display screen (34) and a starting switch (35) from left to right, and the left and right sides of the inner wall of the protection box (4) and the positions between the U-shaped pipes (5) are fixedly connected with ultraviolet lamp tubes (36);

the inside of dust extraction case (15) is through mount fixedly connected with third motor (37), the top fixedly connected with of third motor (37) output shaft rotates cover (38), and rotates fixed surface who overlaps (38) and be connected with blade (39), the top intercommunication of dust extraction case (15) has air inlet hopper (40), the top intercommunication of air inlet hopper (40) has exhaust tube (41), the one end that air inlet hopper (40) were kept away from in exhaust tube (41) and the top intercommunication of handling case (2), the bottom intercommunication of dust extraction case (15) has air outlet hopper (42), the bottom intercommunication of air outlet hopper (42) has outlet duct (43), the bottom of outlet duct (43) runs through the top of dust extraction case (14) and extends to the bottom of dust extraction case (14) inner chamber.

2. An oxidation treatment unit for biopharmaceutical residues as claimed in claim 1, wherein: the top at dust removal case (14) back is run through and is had feed liquor pipe (44), the below intercommunication at dust removal case (14) back has drain pipe (45), the fixed surface of drain pipe (45) is connected with manual valve (46), exhaust hole (47) have been seted up at the top of dust removal case (14).

3. An oxidation treatment unit for biopharmaceutical residues as claimed in claim 1, wherein: the surface of inlet pipe (24) just is located the inside cover of handling case (2) and is equipped with first spacing ring (48), and one side of first spacing ring (48) and the right side fixed connection who handles case (2) inner wall, the surface of inlet tube (10) just is located the inside cover of mixing box (3) and is equipped with second spacing ring (49), and the left side fixed connection of one side of second spacing ring (49) and mixing box (3) inner wall.

4. An oxidation treatment unit for biopharmaceutical residues as claimed in claim 1, wherein: handle first glass observation window (50) of left side fixedly connected with of case (2), left side fixedly connected with second glass observation window (51) of dust removal case (14), the left side intercommunication of handling case (2) has blow off pipe (52), the left end threaded connection of blow off pipe (52) has sealed lid (53).

5. An oxidation treatment unit for biopharmaceutical residues as claimed in claim 1, wherein: the utility model discloses a processing box (2) is characterized in that the front side at top is opened and is equipped with recess (54), the bottom fixedly connected with magnetic ring (55) of recess (54) internal surface, the inside swing joint of recess (54) has metal block (56), the bottom fixedly connected with sampling rod (57) of metal block (56), the bottom of sampling rod (57) runs through magnetic ring (55) in proper order and handles the top of case (2) and extend to the inside of handling case (2), sampling groove (58) have been seted up to the surface of sampling rod (57) and the inside that is located handling case (2), the top fixedly connected with pull ring (59) of metal block (56), the outside fixedly connected with seal gasket (60) of bottom and the sample rod (57) that are located of metal block (56).

6. An oxidation treatment unit for biopharmaceutical residues as claimed in claim 1, wherein: the four corners of bottom plate (1) bottom all fixedly connected with pad foot (61), the bottom fixedly connected with shock pad (62) of pad foot (61), second gear (19) are provided with two, and two second gear (19) are around the centre of a circle symmetric distribution of first gear (18).