CN113025199A - Tire blackening curing agent and preparation method thereof - Google Patents
Tire blackening curing agent and preparation method thereof Download PDFInfo
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- CN113025199A CN113025199A CN202110142774.8A CN202110142774A CN113025199A CN 113025199 A CN113025199 A CN 113025199A CN 202110142774 A CN202110142774 A CN 202110142774A CN 113025199 A CN113025199 A CN 113025199A
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- tire
- blackening
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
Abstract
The invention discloses a tire blackening curing agent and a preparation method thereof, and relates to the technical field of tire blackening curing agents, wherein the tire blackening curing agent is prepared from the following raw material components in percentage by weight: 5-12% of zwitterionic surfactant, 8-12% of siloxane, 3-5% of alkylbenzene sulfonate, 10-15% of citric acid, 3-6% of pH regulator, 1-3% of antistatic agent, 0.008-0.012% of complexing agent, 0.008-0.012% of essence and the balance of deionized water. The tire blackening curing agent provided by the invention is simple to use, can be used for decontamination, brightening, blackening, preventing tire aging and cracking and preventing dust from being adsorbed again only by being sprayed on a tire and lightly wiped, and has the effect of curing tire rubber, wherein the tire blackening effect is more durable than that of the traditional tire oil and can reach 15 days.
Description
Technical Field
The invention relates to the technical field of tire blackening curing agents, in particular to a tire blackening curing agent and a preparation method thereof.
Background
With the rapid increase of the usage of automobiles, the maintenance of automobiles by owners is not limited to the maintenance of machines, and the maintenance of tires is increasingly emphasized. The existing product for maintaining the tire is tire oil, has short blackening and brightening effects after use, is only about 3 days, is easy to block air holes of the tire, can reduce the shock absorption of the tire, and makes the tire hard.
At present, no blackening curing agent which has the effects of removing dirt, brightening, blackening, preventing tire aging and cracking, preventing dust from being adsorbed again and curing tire rubber is available in the market and is specially used for tires.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides a tire blackening curing agent and a preparation method thereof.
The tire blackening curing agent is prepared from the following raw materials in percentage by weight: 5-12% of zwitterionic surfactant, 8-12% of siloxane, 3-5% of alkylbenzene sulfonate, 10-15% of citric acid, 3-6% of pH regulator, 1-3% of antistatic agent, 0.008-0.012% of complexing agent, 0.008-0.012% of essence and the balance of deionized water.
Preferably, the zwitterionic surfactant is a mixture of lecithin, glycine betaine, sodium lauroyl glutamate and sodium cocoyl glycinate, and the weight part ratio of the lecithin to the glycine betaine, the sodium lauroyl glutamate and the sodium cocoyl glycinate is 1:0.4:5: 3.
Preferably, the siloxane is a mixture of dimethyl siloxane and hexamethyldisiloxane, and the weight part ratio of the dimethyl siloxane to the hexamethyldisiloxane is 2: 1.
Preferably, the alkylbenzene sulfonate is a mixture of sodium alkylbenzene sulfonate and sodium dodecylbenzene sulfonate, and the weight part ratio of the sodium alkylbenzene sulfonate to the sodium dodecylbenzene sulfonate is 1: 1.
Preferably, the antistatic agent is a mixture of fatty alcohol-polyoxyethylene ether, sodium alkyl sulfonate and ethoxy lauryl tyramine, and the weight part ratio of the fatty alcohol-polyoxyethylene ether, the sodium alkyl sulfonate and the ethoxy lauryl tyramine is 3:1: 1.
Preferably, the complexing agent is a mixture of tartaric acid, gluconic acid, sodium trimetaphosphate and EDTA, and the weight part ratio of the tartaric acid, the gluconic acid, the sodium trimetaphosphate and the EDTA is 0.3:0.5:1: 2.
The preparation method of the tire blackening curing agent comprises the following steps:
s1, adding a zwitterionic surfactant, siloxane, alkylbenzene sulfonate, citric acid, an antistatic agent, a complexing agent and essence into deionized water, heating and stirring to obtain a mixed solution A;
and S2, adding a PH regulator into the mixed solution A, and regulating the PH value to 7 to obtain the tire blackening curing agent.
Preferably, in step S1, the temperature is raised to 40-50 ℃.
Preferably, in step S1, the stirring is performed at 50-60 rpm for 15-20 minutes.
The invention has the following functions of the raw material components:
zwitterionic surfactant: and the alkyl benzene sulfonate is synergistic to clean the dirt of the tire.
Siloxane: and brightening the light.
Alkyl benzene sulfonate: deep penetration detergent activator.
Citric acid: cleaning and enhancing tinting strength
pH regulators: adjusting pH
Antistatic agent: preventing the dirt from being adsorbed again.
Complexing agent: preventing the generation of precipitate, softening the water quality, ensuring the product not to deteriorate and having the functions of dispersing and suspending without staining the surfaces of towels and car paints.
Essence to increase taste comfort.
The invention has the beneficial effects that:
(1) the tire blackening curing agent provided by the invention is simple to use, can be used for decontamination, brightening, blackening, preventing tire aging and cracking and preventing dust from being adsorbed again only by being sprayed on a tire and lightly wiped, and has the effect of curing tire rubber, wherein the tire blackening effect is more durable than that of the traditional tire oil and can reach 15 days.
(2) The preparation method of the tire blackening curing agent provided by the invention is simple to operate, the raw materials are easy to obtain, the technology is stable, and the prepared tire cleaning agent has excellent performance and extremely high commercial value.
Detailed Description
Hereinafter, embodiments of the present invention will be described in detail. The following examples are only for illustrating the technical solutions of the present invention more clearly, and therefore are only examples, and the protection scope of the present invention is not limited thereby.
It is to be noted that, unless otherwise specified, technical or scientific terms used herein shall have the ordinary meaning as understood by those skilled in the art to which the invention pertains.
Example 1
The tire blackening curing agent is prepared from the following raw material components in percentage by weight:
7% of zwitterionic surfactant, 8% of siloxane, 3% of alkylbenzene sulfonate, 10% of citric acid, 3% of pH regulator, 1% of antistatic agent, 0.008% of complexing agent, 0.008% of essence and the balance of deionized water.
The zwitterionic surfactant is a mixture of lecithin, betaine, sodium lauroyl glutamate and sodium cocoyl glycinate, and the weight part ratio of the lecithin to the betaine to the sodium lauroyl glutamate is 1:0.4:5: 3.
The siloxane is a mixture of dimethyl siloxane and hexamethyldisiloxane, and the weight part ratio of the dimethyl siloxane to the hexamethyldisiloxane is 2: 1.
The alkylbenzene sulfonate is a mixture of sodium alkylbenzene sulfonate and sodium dodecyl benzene sulfonate, and the weight part ratio of the sodium alkylbenzene sulfonate to the sodium dodecyl benzene sulfonate is 1: 1.
The antistatic agent is a mixture of fatty alcohol-polyoxyethylene ether, sodium alkylsulfonate and ethoxy lauryl tyramine, and the weight part ratio of the fatty alcohol-polyoxyethylene ether to the sodium alkylsulfonate to the ethoxy lauryl tyramine is 3:1: 1.
The complexing agent is a mixture of tartaric acid, gluconic acid, sodium trimetaphosphate and EDTA, and the weight part ratio of the tartaric acid, the gluconic acid, the sodium trimetaphosphate and the EDTA is 0.3:0.5:1: 2.
The preparation method of the tire blackening curing agent comprises the following steps:
s1, adding a zwitterionic surfactant, siloxane, alkylbenzene sulfonate, citric acid, an antistatic agent, a complexing agent and essence into deionized water, heating and stirring to obtain a mixed solution A;
and S2, adding a PH regulator into the mixed solution A, and regulating the PH value to 7 to obtain the tire blackening curing agent.
In step S1, the temperature is raised to 50 ℃.
In step S1, the stirring is performed at 60 rpm for 20 minutes.
Example 2
The tire blackening curing agent is prepared from the following raw material components in percentage by weight:
8.5% of zwitterionic surfactant, 10% of siloxane, 4% of alkylbenzene sulfonate, 12.5% of citric acid, 4.5% of pH regulator, 2% of antistatic agent, 0.01% of complexing agent, 0.01% of essence and the balance of deionized water.
The zwitterionic surfactant is a mixture of lecithin, betaine, sodium lauroyl glutamate and sodium cocoyl glycinate, and the weight part ratio of the lecithin to the betaine to the sodium lauroyl glutamate is 1:0.4:5: 3.
The siloxane is a mixture of dimethyl siloxane and hexamethyldisiloxane, and the weight part ratio of the dimethyl siloxane to the hexamethyldisiloxane is 2: 1.
The alkylbenzene sulfonate is a mixture of sodium alkylbenzene sulfonate and sodium dodecyl benzene sulfonate, and the weight part ratio of the sodium alkylbenzene sulfonate to the sodium dodecyl benzene sulfonate is 1: 1.
The antistatic agent is a mixture of fatty alcohol-polyoxyethylene ether, sodium alkylsulfonate and ethoxy lauryl tyramine, and the weight part ratio of the fatty alcohol-polyoxyethylene ether to the sodium alkylsulfonate to the ethoxy lauryl tyramine is 3:1: 1.
The complexing agent is a mixture of tartaric acid, gluconic acid, sodium trimetaphosphate and EDTA, and the weight part ratio of the tartaric acid, the gluconic acid, the sodium trimetaphosphate and the EDTA is 0.3:0.5:1: 2.
The preparation method of the tire blackening curing agent comprises the following steps:
s1, adding a zwitterionic surfactant, siloxane, alkylbenzene sulfonate, citric acid, an antistatic agent, a complexing agent and essence into deionized water, heating and stirring to obtain a mixed solution A;
and S2, adding a PH regulator into the mixed solution A, and regulating the PH value to 7 to obtain the tire blackening curing agent.
In step S1, the temperature is raised to 50 ℃.
In step S1, the stirring is performed at 60 rpm for 20 minutes.
Example 3
The tire blackening curing agent is prepared from the following raw material components in percentage by weight:
10% of zwitterionic surfactant, 12% of siloxane, 5% of alkylbenzene sulfonate, 15% of citric acid, 6% of pH regulator, 3% of antistatic agent, 0.012% of complexing agent, 0.012% of essence and the balance of deionized water.
The zwitterionic surfactant is a mixture of lecithin, betaine, sodium lauroyl glutamate and sodium cocoyl glycinate, and the weight part ratio of the lecithin to the betaine to the sodium lauroyl glutamate is 1:0.4:5: 3.
The siloxane is a mixture of dimethyl siloxane and hexamethyldisiloxane, and the weight part ratio of the dimethyl siloxane to the hexamethyldisiloxane is 2: 1.
The alkylbenzene sulfonate is a mixture of sodium alkylbenzene sulfonate and sodium dodecyl benzene sulfonate, and the weight part ratio of the sodium alkylbenzene sulfonate to the sodium dodecyl benzene sulfonate is 1: 1.
The antistatic agent is a mixture of fatty alcohol-polyoxyethylene ether, sodium alkylsulfonate and ethoxy lauryl tyramine, and the weight part ratio of the fatty alcohol-polyoxyethylene ether to the sodium alkylsulfonate to the ethoxy lauryl tyramine is 3:1: 1.
The complexing agent is a mixture of tartaric acid, gluconic acid, sodium trimetaphosphate and EDTA, and the weight part ratio of the tartaric acid, the gluconic acid, the sodium trimetaphosphate and the EDTA is 0.3:0.5:1: 2.
The preparation method of the tire blackening curing agent comprises the following steps:
s1, adding a zwitterionic surfactant, siloxane, alkylbenzene sulfonate, citric acid, an antistatic agent, a complexing agent and essence into deionized water, heating and stirring to obtain a mixed solution A;
and S2, adding a PH regulator into the mixed solution A, and regulating the PH value to 7 to obtain the tire blackening curing agent.
In step S1, the temperature is raised to 50 ℃.
In step S1, the stirring is performed at 60 rpm for 20 minutes.
Test examples
1. Appearance index of tire blackening curing agent obtained in examples 1 to 3
TABLE 1
| Example 1 | Example 2 | Example 3 | |
| Appearance of the product | Liquid, method for producing the same and use thereof | Liquid, method for producing the same and use thereof | Liquid, method for producing the same and use thereof |
| Color | Black color transparent | Black color transparent | Black colorIs transparent |
| Smell(s) | Slightly fragrant | Slightly fragrant | Slightly fragrant |
| Impurities | Is free of | Is free of | Is free of |
2. Effect of the tire blackening curing Agents obtained in examples 1 to 3 on the Properties of rubber
The test method comprises the following steps: GB/T23436-2009
TABLE 2
3. Test of Effect of tire blackening curing Agents obtained in examples 1 to 3 on appearance of rubber
The test method comprises the following steps: the tire blackening curing agent prepared in examples 1 to 3 was applied to the surface of a chloroprene rubber test piece
TABLE 3
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; such modifications and substitutions do not depart from the spirit and scope of the present invention, and they should be construed as being included in the following claims and description.
Claims (9)
1. The tire blackening curing agent is characterized in that: the tire blackening curing agent is prepared from the following raw materials in percentage by weight: 5-12% of zwitterionic surfactant, 8-12% of siloxane, 3-5% of alkylbenzene sulfonate, 10-15% of citric acid, 3-6% of pH regulator, 1-3% of antistatic agent, 0.008-0.012% of complexing agent, 0.008-0.012% of essence and the balance of deionized water.
2. A tire blackening curing agent according to claim 1, wherein: the zwitterionic surfactant is a mixture of lecithin, betaine, sodium lauroyl glutamate and sodium cocoyl glycinate, and the weight part ratio of the lecithin to the betaine to the sodium lauroyl glutamate is 1:0.4:5: 3.
3. A tire blackening curing agent according to claim 1, wherein: the siloxane is a mixture of dimethyl siloxane and hexamethyldisiloxane, and the weight part ratio of the dimethyl siloxane to the hexamethyldisiloxane is 2: 1.
4. A tire blackening curing agent according to claim 1, wherein: the alkylbenzene sulfonate is a mixture of sodium alkylbenzene sulfonate and sodium dodecyl benzene sulfonate, and the weight part ratio of the sodium alkylbenzene sulfonate to the sodium dodecyl benzene sulfonate is 1: 1.
5. A tire blackening curing agent according to claim 1, wherein: the antistatic agent is a mixture of fatty alcohol-polyoxyethylene ether, sodium alkylsulfonate and ethoxy lauryl tyramine, and the weight part ratio of the fatty alcohol-polyoxyethylene ether to the sodium alkylsulfonate to the ethoxy lauryl tyramine is 3:1: 1.
6. A tire blackening curing agent according to claim 1, wherein: the complexing agent is a mixture of tartaric acid, gluconic acid, sodium trimetaphosphate and EDTA, and the weight part ratio of the tartaric acid, the gluconic acid, the sodium trimetaphosphate and the EDTA is 0.3:0.5:1: 2.
7. A process for producing a tire blackening curing agent as claimed in any one of claims 1 to 6, wherein: the preparation method comprises the following steps:
s1, adding a zwitterionic surfactant, siloxane, alkylbenzene sulfonate, citric acid, an antistatic agent, a complexing agent and essence into deionized water, heating and stirring to obtain a mixed solution A;
and S2, adding a PH regulator into the mixed solution A, and regulating the PH value to 7 to obtain the tire blackening curing agent.
8. A method for producing a tire blackening curing agent according to claim 7, wherein: in step S1, the temperature is raised to 40-50 ℃.
9. A method for producing a tire blackening curing agent according to claim 7, wherein: in step S1, the stirring is carried out for 15-20 minutes at 50-60 r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110142774.8A CN113025199A (en) | 2021-02-02 | 2021-02-02 | Tire blackening curing agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110142774.8A CN113025199A (en) | 2021-02-02 | 2021-02-02 | Tire blackening curing agent and preparation method thereof |
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| CN113025199A true CN113025199A (en) | 2021-06-25 |
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| CN202110142774.8A Pending CN113025199A (en) | 2021-02-02 | 2021-02-02 | Tire blackening curing agent and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101514313A (en) * | 2008-12-31 | 2009-08-26 | 北京绿伞化学股份有限公司 | Vehicle tyre maintenance agent and preparation method thereof |
| CN107118879A (en) * | 2017-06-03 | 2017-09-01 | 明光速耐德实心轮胎有限公司 | A kind of automobile tire cleaning sealing compound and preparation method |
| CN206483658U (en) * | 2017-02-10 | 2017-09-12 | 成都众友合力汽车服务有限公司 | A kind of automobile tire automatic glue sprayer |
| CN107474978A (en) * | 2012-10-15 | 2017-12-15 | 艺康美国股份有限公司 | Leather and/or vinylite cleaning agent and wetting agent and its manufacture method |
-
2021
- 2021-02-02 CN CN202110142774.8A patent/CN113025199A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101514313A (en) * | 2008-12-31 | 2009-08-26 | 北京绿伞化学股份有限公司 | Vehicle tyre maintenance agent and preparation method thereof |
| CN107474978A (en) * | 2012-10-15 | 2017-12-15 | 艺康美国股份有限公司 | Leather and/or vinylite cleaning agent and wetting agent and its manufacture method |
| CN206483658U (en) * | 2017-02-10 | 2017-09-12 | 成都众友合力汽车服务有限公司 | A kind of automobile tire automatic glue sprayer |
| CN107118879A (en) * | 2017-06-03 | 2017-09-01 | 明光速耐德实心轮胎有限公司 | A kind of automobile tire cleaning sealing compound and preparation method |
Non-Patent Citations (1)
| Title |
|---|
| 赵敏: "一种车用轮胎养护剂及其制备方法", 《轮胎工业》 * |
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