CN112980524A - Micro-emulsified diesel oil product oil and production process thereof - Google Patents

Micro-emulsified diesel oil product oil and production process thereof Download PDF

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Publication number
CN112980524A
CN112980524A CN202110276711.1A CN202110276711A CN112980524A CN 112980524 A CN112980524 A CN 112980524A CN 202110276711 A CN202110276711 A CN 202110276711A CN 112980524 A CN112980524 A CN 112980524A
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Prior art keywords
diesel oil
micro
emulsified diesel
emulsified
oil
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CN202110276711.1A
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Inventor
廖美玲
邵化民
楼永青
董启愚
郑国胜
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Zhejiang Shunhang Energy Co ltd
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Zhejiang Shunhang Energy Co ltd
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00Liquid carbonaceous fuels
    • C10L1/32Liquid carbonaceous fuels consisting of coal-oil suspensions or aqueous emulsions or oil emulsions
    • C10L1/328Oil emulsions containing water or any other hydrophilic phase
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2250/00Structural features of fuel components or fuel compositions, either in solid, liquid or gaseous state
    • C10L2250/08Emulsion details

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Liquid Carbonaceous Fuels (AREA)

Abstract

The invention discloses a micro-emulsified diesel oil product oil, which comprises the following components in percentage by concentration: a process for producing a micro-emulsified diesel finished oil comprises the following steps of S1, S2, S3 and S4. According to the invention, the diesel oil preparation formula is optimized, the diesel oil preparation efficiency is improved through the arranged micro-emulsified diesel oil emulsification aid, the reaction time is reduced, and the optimized preparation method is adopted, so that sampling detection is respectively carried out from different positions in the preparation process and after preparation, the quality of the finished product oil is ensured, and the product quality problem is prevented.

Description

Micro-emulsified diesel oil product oil and production process thereof
Technical Field
The invention relates to the technical field of micro-emulsified diesel oil, in particular to micro-emulsified diesel oil product oil and a production process thereof.
Background
The diesel oil is a light petroleum product, is a mixture of complex hydrocarbons (with carbon atoms of about 10-22), is a diesel fuel, and is mainly prepared from diesel oil fractions produced in the processes of crude oil distillation, catalytic cracking, thermal cracking, hydrocracking, petroleum coking and the like; the diesel oil can also be prepared by processing shale oil and liquefying coal, is divided into two categories of light diesel oil (the boiling point range is about 180-370 ℃) and heavy diesel oil (the boiling point range is about 350-410 ℃), is widely applied to large vehicles, railway locomotives and ships, and the most important purpose of the diesel oil is to be used for diesel engines of vehicles and ships. Compared with gasoline, diesel fuel has high energy density and low fuel consumption, but exhaust gas contains many harmful components (NO, particulate matter, etc.).
The traditional diesel oil generates more waste gas in the using process, and the fuel oil performance needs to be further improved, so that a micro-emulsified diesel oil finished product oil and a production flow thereof are provided.
Disclosure of Invention
Therefore, the invention aims to provide a micro-emulsified diesel oil product oil and a production process thereof, wherein the micro-emulsified diesel oil production efficiency is improved and the reaction time is reduced by optimizing the diesel oil production formula and the arranged micro-emulsified diesel oil emulsification auxiliary agent, and the optimized preparation method is used for respectively carrying out sampling detection from different positions in the preparation process and after the preparation process, so that the quality of the product oil is ensured and the product quality problem is prevented.
To solve the above technical problem, according to an aspect of the present invention, the present invention provides the following technical solutions:
a micro-emulsified diesel oil product oil comprises the following components in percentage by concentration:
75 to 85 percent of diesel oil
15 to 20 percent of water
1-3% of a micro-emulsified diesel oil emulsifying auxiliary agent.
A micro-emulsified diesel oil product production process as claimed in claim 1, which comprises the following steps,
s1: firstly, preparing raw materials required by emulsified diesel oil production, injecting the prepared diesel oil, water and a micro-emulsified diesel oil emulsification aid into corresponding storage tanks for storage, and strictly controlling the storage temperature of the raw materials within a safety range by a producer;
s2: before preparing the micro-emulsified diesel, a raw material sample extractor is used for respectively extracting samples at the upper part, the middle part and the lower part of a raw material, the quality detection is respectively carried out on the samples at different positions, whether the raw material is changed or not is judged, the optimal manufacturing state of the raw material is ensured, and the service performance of the micro-emulsified diesel after production is ensured;
s3: injecting all the detected raw materials in the optimal state into a stirring tank, setting the operation time of the stirring tank, and fully mixing diesel oil, water and the micro-emulsified diesel oil emulsification additive to prepare the micro-emulsified diesel oil;
s4, detecting the prepared finished micro-emulsified diesel oil, judging the use performance of the finished micro-emulsified diesel oil, filling and delivering the finished micro-emulsified diesel oil out of a warehouse if the performance meets the requirement, and adding raw materials again to carry out optimized production if the performance does not meet the requirement, so as to ensure the quality of the finished oil.
As a preferable scheme of the production process of the micro-emulsified diesel oil product, in the step S1, the storage temperature is controlled to be 20-35 ℃.
As a preferable scheme of the production process of the micro-emulsified diesel oil product, the stirring time in the step S3 is 4-7 h.
As a preferable scheme of the production process of the micro-emulsified diesel oil product, the forward rotation time and the reverse rotation time of the stirring tank in the step S3 are equal.
As a preferable scheme of the production process of the micro-emulsified diesel oil product, when finished diesel oil is detected in the step S4, the raw material extraction mode is the same as that in the step S2.
Compared with the prior art, the invention has the beneficial effects that: the method comprises the steps of optimizing a diesel oil preparation formula, improving the diesel oil preparation efficiency through the arranged micro-emulsified diesel oil emulsification aid, reducing the reaction time, performing sampling detection from different positions respectively in the preparation process and after preparation through an optimized preparation method, ensuring the quality of the finished oil, and preventing the product quality problem, when the method is used specifically, firstly preparing raw materials required by emulsified diesel oil production, injecting the prepared diesel oil, water and the micro-emulsified diesel oil emulsification aid into corresponding storage tanks for storage, strictly controlling the storage temperature of the raw materials within a safe range by a producer, before the micro-emulsified diesel oil is prepared, respectively extracting samples at the upper part, the middle part and the lower part of the raw materials by using a raw material sample extractor, performing quality detection on the samples at different positions respectively, judging whether the raw materials are changed, and ensuring the raw materials to be in the optimal preparation state, the method comprises the steps of ensuring the service performance of the micro-emulsified diesel after production, completely injecting detected raw materials in the optimal state into a stirring tank, setting the operation time of the stirring tank, fully mixing diesel, water and a micro-emulsified diesel emulsification aid to prepare the micro-emulsified diesel, detecting the prepared micro-emulsified diesel finished oil, judging the service performance of the micro-emulsified diesel finished oil, filling and storing the micro-emulsified diesel finished oil if the performance meets the requirement, and adding the raw materials again to optimize and manufacture if the performance does not meet the requirement, so as to ensure the quality of the finished oil.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the present invention will be described in detail below with reference to the accompanying drawings and detailed embodiments, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings without inventive exercise. Wherein:
FIG. 1 is a flow chart of a micro-emulsified diesel oil product oil and a production process thereof.
Detailed Description
In order to make the aforementioned objects, features and advantages of the present invention comprehensible, embodiments accompanied with figures are described in detail below.
In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present invention, but the present invention may be practiced in other ways than those specifically described herein, and it will be apparent to those of ordinary skill in the art that the present invention may be practiced without departing from the spirit and scope of the present invention, and therefore the present invention is not limited to the specific embodiments disclosed below.
Next, the present invention will be described in detail with reference to the drawings, and in the detailed description of the embodiments of the present invention, the cross-sectional views illustrating the structure of the device are not enlarged partially according to the general scale for convenience of illustration, and the drawings are only examples, which should not limit the scope of the present invention. In addition, the three-dimensional dimensions of length, width and depth should be included in the actual fabrication.
In order to make the objects, technical solutions and advantages of the present invention more apparent, embodiments of the present invention will be described in detail with reference to the accompanying drawings.
The invention provides a micro-emulsified diesel oil product oil and a production process thereof, wherein the micro-emulsified diesel oil production efficiency is improved and the reaction time is reduced by optimizing a diesel oil production formula and setting a micro-emulsified diesel oil emulsification auxiliary agent, and the optimized preparation method is used for respectively carrying out sampling detection from different positions in the preparation process and after preparation, so that the quality of the product oil is ensured and the product quality problem is prevented.
Example 1:
a micro-emulsified diesel oil product oil comprises the following components in percentage by concentration:
75 percent of diesel oil
15 percent of water
1% of micro-emulsified diesel oil emulsification auxiliary agent.
Example 2:
a micro-emulsified diesel oil product oil comprises the following components in percentage by concentration:
diesel oil 80%
17 percent of water
2 percent of micro-emulsified diesel oil emulsification additive.
Example 3:
a micro-emulsified diesel oil product oil comprises the following components in percentage by concentration:
85 percent of diesel oil
20 percent of water
3 percent of micro-emulsified diesel oil emulsification assistant.
Example 1
S1: firstly, preparing raw materials required by emulsified diesel oil production, injecting the prepared diesel oil, water and a micro-emulsified diesel oil emulsification aid into corresponding storage tanks for storage, and strictly controlling the storage temperature of the raw materials to be 20 ℃;
s2: before preparing the micro-emulsified diesel, a raw material sample extractor is used for respectively extracting samples at the upper part, the middle part and the lower part of a raw material, the quality detection is respectively carried out on the samples at different positions, whether the raw material is changed or not is judged, the optimal manufacturing state of the raw material is ensured, and the service performance of the micro-emulsified diesel after production is ensured;
s3: injecting all the detected raw materials in the optimal state into a stirring tank, setting the running time of the stirring tank to be controlled at 4h, and fully mixing diesel oil, water and the micro-emulsified diesel oil emulsification additive to prepare the micro-emulsified diesel oil;
s4, detecting the prepared finished micro-emulsified diesel oil, judging the use performance of the finished micro-emulsified diesel oil, filling and delivering the finished micro-emulsified diesel oil out of a warehouse if the performance meets the requirement, and adding raw materials again to carry out optimized production if the performance does not meet the requirement, so as to ensure the quality of the finished oil.
Example 2
S1: firstly, preparing raw materials required by emulsified diesel oil production, injecting the prepared diesel oil, water and a micro-emulsified diesel oil emulsification aid into corresponding storage tanks for storage, and strictly controlling the storage temperature of the raw materials to be 25 ℃;
s2: before preparing the micro-emulsified diesel, a raw material sample extractor is used for respectively extracting samples at the upper part, the middle part and the lower part of a raw material, the quality detection is respectively carried out on the samples at different positions, whether the raw material is changed or not is judged, the optimal manufacturing state of the raw material is ensured, and the service performance of the micro-emulsified diesel after production is ensured;
s3: injecting all the detected raw materials in the optimal state into a stirring tank, setting the running time of the stirring tank to be controlled at 5h, and fully mixing diesel oil, water and the micro-emulsified diesel oil emulsification additive to prepare the micro-emulsified diesel oil;
s4, detecting the prepared finished micro-emulsified diesel oil, judging the use performance of the finished micro-emulsified diesel oil, filling and delivering the finished micro-emulsified diesel oil out of a warehouse if the performance meets the requirement, and adding raw materials again to carry out optimized production if the performance does not meet the requirement, so as to ensure the quality of the finished oil.
Example 3
S1: firstly, preparing raw materials required by emulsified diesel oil production, injecting the prepared diesel oil, water and a micro-emulsified diesel oil emulsification aid into corresponding storage tanks for storage, and strictly controlling the storage temperature of the raw materials at 30 ℃ by a producer;
s2: before preparing the micro-emulsified diesel, a raw material sample extractor is used for respectively extracting samples at the upper part, the middle part and the lower part of a raw material, the quality detection is respectively carried out on the samples at different positions, whether the raw material is changed or not is judged, the optimal manufacturing state of the raw material is ensured, and the service performance of the micro-emulsified diesel after production is ensured;
s3: injecting all the detected raw materials in the optimal state into a stirring tank, setting the operation time of the stirring tank to be controlled at 7h, and fully mixing diesel oil, water and the micro-emulsified diesel oil emulsification aid to prepare the micro-emulsified diesel oil;
s4, detecting the prepared finished micro-emulsified diesel oil, judging the use performance of the finished micro-emulsified diesel oil, filling and delivering the finished micro-emulsified diesel oil out of a warehouse if the performance meets the requirement, and adding raw materials again to carry out optimized production if the performance does not meet the requirement, so as to ensure the quality of the finished oil.
Fig. 1 shows an overall flow diagram of a micro-emulsified diesel finished oil and a production flow implementation thereof, please refer to fig. 1, and the specific operation flow is as follows: firstly, preparing raw materials required by emulsified diesel oil production, injecting the prepared diesel oil, water and a micro-emulsified diesel oil emulsifying auxiliary agent into corresponding storage tanks for storage, strictly controlling the temperature for storing the raw materials to be between 20 and 30 ℃, before preparing the micro-emulsified diesel oil, respectively extracting samples at the upper part, the middle part and the lower part of the raw materials by using a raw material sample extractor, respectively carrying out quality detection on the samples at different positions, judging whether the raw materials are changed or not, ensuring the raw materials to be in the optimal manufacturing state, ensuring the usability after the micro-emulsified diesel oil is produced, injecting the detected raw materials in the optimal state into a stirring tank, setting the running time of the stirring tank to be controlled to be between 4 and 7 hours, fully mixing the diesel oil, the water and the micro-emulsified diesel oil emulsifying auxiliary agent to prepare the micro-emulsified diesel oil, and detecting the prepared finished oil of the micro-emulsified diesel oil, judging the use performance of the finished microemulsified diesel oil, filling and delivering the finished oil out of a warehouse if the performance meets the requirements, and adding raw materials again for optimized production if the performance does not meet the requirements to ensure the quality of the finished oil.
While the invention has been described above with reference to an embodiment, various modifications may be made and equivalents may be substituted for elements thereof without departing from the scope of the invention. In particular, the various features of the disclosed embodiments of the invention may be used in any combination, provided that no structural conflict exists, and the combinations are not exhaustively described in this specification merely for the sake of brevity and resource conservation. Therefore, it is intended that the invention not be limited to the particular embodiments disclosed, but that the invention will include all embodiments falling within the scope of the appended claims.

Claims (6)

1. A micro-emulsified diesel oil product is characterized by comprising the following components in percentage by concentration:
75 to 85 percent of diesel oil
15 to 20 percent of water
1-3% of a micro-emulsified diesel oil emulsifying auxiliary agent.
2. A process for producing a microemulsified diesel oil product as claimed in claim 1, which comprises the following steps,
s1: firstly, preparing raw materials required by emulsified diesel oil production, injecting the prepared diesel oil, water and a micro-emulsified diesel oil emulsification aid into corresponding storage tanks for storage, and strictly controlling the storage temperature of the raw materials within a safety range by a producer;
s2: before preparing the micro-emulsified diesel, a raw material sample extractor is used for respectively extracting samples at the upper part, the middle part and the lower part of a raw material, the quality detection is respectively carried out on the samples at different positions, whether the raw material is changed or not is judged, the optimal manufacturing state of the raw material is ensured, and the service performance of the micro-emulsified diesel after production is ensured;
s3: injecting all the detected raw materials in the optimal state into a stirring tank, setting the operation time of the stirring tank, and fully mixing diesel oil, water and the micro-emulsified diesel oil emulsification additive to prepare the micro-emulsified diesel oil;
s4, detecting the prepared finished micro-emulsified diesel oil, judging the use performance of the finished micro-emulsified diesel oil, filling and delivering the finished micro-emulsified diesel oil out of a warehouse if the performance meets the requirement, and adding raw materials again to carry out optimized production if the performance does not meet the requirement, so as to ensure the quality of the finished oil.
3. The process according to claim 2, wherein in the step S1, the storage temperature is controlled at 20-35 ℃.
4. The process according to claim 3, wherein the stirring time in step S3 is 4-7 h.
5. The process according to claim 4, wherein the forward rotation time and the reverse rotation time of the agitator tank in the step S3 are equal.
6. The process of claim 5, wherein the raw material extraction method in the step S4 is the same as the raw material extraction method in the step S2 when the finished diesel oil is tested.
CN202110276711.1A 2021-03-15 2021-03-15 Micro-emulsified diesel oil product oil and production process thereof Pending CN112980524A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116520784A (en) * 2023-05-10 2023-08-01 江苏辰威生物科技有限公司 Automatic production system for finished oil

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1054096A (en) * 1990-02-14 1991-08-28 冯宁生 Smoke elliminating and oil saving emulsifier
CN104232189A (en) * 2014-06-03 2014-12-24 长春工业大学 Preparation method of microemulsified diesel
CN105985818A (en) * 2015-01-28 2016-10-05 周国胜 Vehicle-use M15 alcohol-hydrocarbon composite fuel oil

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1054096A (en) * 1990-02-14 1991-08-28 冯宁生 Smoke elliminating and oil saving emulsifier
CN104232189A (en) * 2014-06-03 2014-12-24 长春工业大学 Preparation method of microemulsified diesel
CN105985818A (en) * 2015-01-28 2016-10-05 周国胜 Vehicle-use M15 alcohol-hydrocarbon composite fuel oil

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116520784A (en) * 2023-05-10 2023-08-01 江苏辰威生物科技有限公司 Automatic production system for finished oil
CN116520784B (en) * 2023-05-10 2024-05-10 江苏辰威生物科技有限公司 Automatic production system for finished oil

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