CN112964656A - Automatic spectrum analyzer control system - Google Patents

Automatic spectrum analyzer control system Download PDF

Info

Publication number
CN112964656A
CN112964656A CN202110164242.4A CN202110164242A CN112964656A CN 112964656 A CN112964656 A CN 112964656A CN 202110164242 A CN202110164242 A CN 202110164242A CN 112964656 A CN112964656 A CN 112964656A
Authority
CN
China
Prior art keywords
spectrum analyzer
circuit
heating
signal
gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN202110164242.4A
Other languages
Chinese (zh)
Inventor
沈云峰
沈永水
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Langxi Jiebo Electric Appliance Technology Co ltd
Original Assignee
Langxi Jiebo Electric Appliance Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Langxi Jiebo Electric Appliance Technology Co ltd filed Critical Langxi Jiebo Electric Appliance Technology Co ltd
Priority to CN202110164242.4A priority Critical patent/CN112964656A/en
Publication of CN112964656A publication Critical patent/CN112964656A/en
Withdrawn legal-status Critical Current

Links

Images

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

The invention discloses an automatic spectrum analyzer control system, which relates to the technical field of spectrum analyzer control and solves the technical problem that the fault rate of a spectrum analyzer is increased because the circuit monitoring of the spectrum analyzer cannot be carried out in the prior art, the circuit data of the spectrum analyzer is analyzed by a circuit detection unit to obtain the circuit data of the spectrum analyzer, the detection coefficient JCi of a circuit of the spectrum analyzer is obtained by a formula, if the detection coefficient JCi is less than the threshold value of the circuit detection coefficient, a circuit abnormal signal is generated and sent to an analysis control platform, and after the analysis control platform receives the circuit abnormal signal, a circuit maintenance signal is sent to a mobile phone terminal of an operator; carry out the circuit monitoring to spectral analysis appearance, effectively reduce spectral analysis appearance's fault rate, improved work efficiency, will in time restore the unusual circuit simultaneously, effectively prolonged spectral analysis appearance's life.

Description

Automatic spectrum analyzer control system
Technical Field
The invention relates to the technical field of control of spectrum analyzers, in particular to an automatic spectrum analyzer control system.
Background
A spectrum analyzer is an instrument for measuring the radiation spectrum of a luminophore, namely the index parameters of the luminophore itself. Spectrum analyzers can be divided into two broad categories: classical spectrometers and new types of spectrometers. The classical spectral instrument is an instrument based on the spatial dispersion principle, and the novel spectral instrument is an instrument based on the modulation principle. The analysis principle of the spectrum analyzer is as follows: and absorbing the characteristic spectrum of the element to be detected radiated by the light source by the ground state atoms of the element to be detected in the steam of the sample, and obtaining the content of the element to be detected in the sample according to the weakened degree of the emission spectrum.
A metal or alloy sample is placed in a crucible in a pulse heating furnace to be heated, so that gas in the sample is released. The carrier gas is sent into a chromatographic column for separation under the carrier gas flow and then passes through a heat conduction pool detector. When the substance to be measured flows through the heat conduction pool detector, the bridge arm resistance value of the heat conduction pool is changed due to the difference of the heat conductivity coefficients of different substances, and an electric signal is generated. The signal is sent to a microcomputer and processed by a chromatographic workstation to obtain the distillation peak. The qualitative determination is carried out according to the sequence of the distillation peaks, and the quantitative determination is carried out according to the peak height or the peak area of the distillation peaks.
However, in the prior art, the circuit monitoring of the optical spectrum analyzer cannot be performed, and the failure rate of the optical spectrum analyzer is increased.
Disclosure of Invention
The invention aims to provide an automatic spectrum analyzer control system, which analyzes circuit data of a spectrum analyzer through a circuit detection unit so as to detect the spectrum analyzer, obtains a voltage floating value in a circuit of the spectrum analyzer, a maximum potential difference in the circuit of the spectrum analyzer and an average current value in the circuit of the spectrum analyzer, obtains a detection coefficient JCi of the circuit of the spectrum analyzer through a formula, judges that a corresponding circuit is normal if the detection coefficient JCi of the circuit of the spectrum analyzer is not less than a circuit detection coefficient threshold value, generates a normal circuit signal and sends the normal circuit signal to a mobile phone terminal of a manager; if the detection coefficient JCi of the circuit of the spectrum analyzer is smaller than the circuit detection coefficient threshold value, judging that the corresponding circuit is abnormal, generating a circuit abnormal signal and sending the circuit abnormal signal to an analysis control platform, and after receiving the circuit abnormal signal, the analysis control platform generates a circuit maintenance signal and sends the circuit maintenance signal to a mobile phone terminal of an operator; carry out the circuit monitoring to spectral analysis appearance, effectively reduce spectral analysis appearance's fault rate, improved work efficiency, will in time restore the unusual circuit simultaneously, effectively prolonged spectral analysis appearance's life.
The purpose of the invention can be realized by the following technical scheme:
an automatic spectrum analyzer control system comprises a circuit detection unit, an instrument detection unit, a gas detection unit, a heating monitoring unit, an analysis control platform, a registration unit and a database;
the circuit detection unit is used for analyzing the circuit data of the spectrum analyzer so as to detect the spectrum analyzer, the circuit data of the spectrum analyzer comprises voltage data, potential data and current data, the voltage data is a voltage floating value in a circuit of the spectrum analyzer, the potential data is a maximum potential difference in the circuit of the spectrum analyzer, the current data is an average current value in the circuit of the spectrum analyzer, the circuit of the spectrum analyzer is marked as i, i is 1, 2, … …, n and n is a positive integer, and the specific analysis and detection process is as follows:
step one, acquiring a voltage floating value in a circuit of a spectrum analyzer, and marking the voltage floating value in the circuit of the spectrum analyzer as FDi;
acquiring the maximum potential difference in the circuit of the spectrum analyzer, and marking the maximum potential difference in the circuit of the spectrum analyzer as DWi;
acquiring an average current value in a circuit of the spectrum analyzer, and marking the average current value in the circuit of the spectrum analyzer as DLi;
step four, passing through a formula
Figure BDA0002937022100000031
Obtaining detection coefficients JCi of a spectrum analyzer circuit, wherein a1, a2 and a3 are all proportionality coefficients, and a1 is more than a2 is more than a3 is more than 0;
step five, comparing the detection coefficient JCi of the spectrum analyzer circuit with a circuit detection coefficient threshold value:
if the detection coefficient JCi of the circuit of the spectrum analyzer is not less than the circuit detection coefficient threshold, judging that the corresponding circuit is normal, generating a normal circuit signal and sending the normal circuit signal to a mobile phone terminal of a manager;
and if the detection coefficient JCi of the circuit of the spectrum analyzer is less than the circuit detection coefficient threshold value, judging that the corresponding circuit is abnormal, generating a circuit abnormal signal and sending the circuit abnormal signal to the analysis control platform, and after receiving the circuit abnormal signal, the analysis control platform generates a circuit maintenance signal and sends the circuit maintenance signal to the mobile phone terminal of an operator.
Further, the instrument detection unit is used for analyzing instrument data of the spectrum analyzer, so as to detect the spectrum analyzer, the instrument data of the spectrum analyzer is the temperature of a chromatographic column in the spectrum analyzer, the flow rate of flushing gas and the internal pressure value, the spectrum analyzer is marked as o, o is 1, 2, … …, m and m are positive integers, and the specific analysis and detection process is as follows:
step S1: acquiring the temperature of a chromatographic column in the spectrum analyzer, and marking the temperature of the chromatographic column in the spectrum analyzer as Wi;
step S2: acquiring the flow of the flushing gas in the spectrum analyzer, and marking the flow of the flushing gas in the spectrum analyzer as Li;
step S3: acquiring a pressure value inside the spectrum analyzer, and marking the pressure value inside the spectrum analyzer as Yi;
step S4: by the formula Xi ═ e (Wi × b1+ Li × b2+ Yi × b3)b1+b2+b3Obtaining an instrument detection coefficient Xi of the spectrum analyzer, wherein b1, b2 and b3 are all proportionality coefficients, b1 is greater than b2 is greater than b3 is greater than 0, and e is a natural constant;
step S5: comparing the instrument detection coefficient Xi of the spectrum analyzer with an instrument detection coefficient threshold value:
if the instrument detection coefficient Xi of the spectrum analyzer is larger than or equal to the instrument detection coefficient threshold value, judging that the detection of the spectrum analyzer instrument is normal, generating an instrument normal signal and sending the instrument normal signal to a mobile phone terminal of a manager;
and if the instrument detection coefficient Xi of the spectrum analyzer is less than the instrument detection coefficient threshold value, judging that the detection of the spectrum analyzer is abnormal, generating an instrument abnormal signal and sending the instrument abnormal signal to the analysis control platform, and after receiving the instrument abnormal signal, the analysis control platform generates an instrument maintenance signal and sends the instrument maintenance signal to a mobile phone terminal of an operator.
Further, the gas detection unit is used for analyzing gas data of the spectrum analyzer so as to detect the operation of the spectrum analyzer, the gas data of the spectrum analyzer comprises content ratios of hydrogen, nitrogen and carbon dioxide generated when the sample is melted, consumption of oxygen in the sample melting process and generation of carbon monoxide in the sample melting process, and the specific analysis and detection process comprises the following steps:
step SS 1: acquiring the content ratios of hydrogen, nitrogen and carbon dioxide generated by the spectrum analyzer during sample melting, and marking the content ratios of hydrogen, nitrogen and carbon dioxide generated by the spectrum analyzer during sample melting as BZ;
step SS 2: acquiring the consumption of oxygen in the sample melting process of the spectrum analyzer, and marking the consumption of oxygen in the sample melting process of the spectrum analyzer as XH;
step SS 3: acquiring the generation amount of carbon monoxide in the sample melting process of the spectrum analyzer, and marking the generation amount of the carbon monoxide in the sample melting process of the spectrum analyzer as SC;
step SS 4: by the formula
Figure BDA0002937022100000041
Acquiring a gas detection coefficient QT of the spectrum analyzer, wherein v1, v2 and v3 are all proportionality coefficients, and v1 is more than v2 is more than v3 is more than 0;
step SS 5: comparing a gas detection coefficient QT of the spectrum analyzer with a gas detection coefficient threshold value:
if the gas detection coefficient QT of the spectrum analyzer is larger than or equal to the gas detection coefficient threshold value, determining that the gas detection is normal in the operation process of the spectrum analyzer, generating a gas normal signal and sending the gas normal signal to a mobile phone terminal of a manager;
if the gas detection coefficient QT of the spectrum analyzer is less than the gas detection coefficient threshold value, determining that gas detection is abnormal in the operation process of the spectrum analyzer, generating a gas abnormal signal and sending the gas abnormal signal to an analysis control platform, and after receiving the gas abnormal signal, the analysis control platform generates a gas control signal and sends the gas control signal to a mobile phone terminal of an operator.
Further, the heating monitoring unit is used for heating information of the spectrum analyzer in the operation process, so that the operation of the spectrum analyzer is monitored, the heating information of the spectrum analyzer comprises the rising speed of the temperature in the heating process of the spectrum analyzer, the maximum heating temperature value of the spectrum analyzer and the continuous heating duration in the heating process of the spectrum analyzer, and the specific analysis monitoring process is as follows:
step L1: acquiring the temperature rising speed of the optical spectrum analyzer in the heating process, and marking the temperature rising speed of the optical spectrum analyzer in the heating process as SDi;
step L2: acquiring the highest heating temperature value of the spectrum analyzer, and marking the highest heating temperature value of the spectrum analyzer as WDi;
step L3: acquiring the continuous heating time in the heating process of the spectrum analyzer, and marking the continuous heating time in the heating process of the spectrum analyzer as SCi;
step L4: by the formula
Figure BDA0002937022100000051
Obtaining a heating monitoring coefficient JRi of the spectrum analyzer, wherein g1, g2 and g3 are proportional coefficients, and g1 is more than g2 is more than g3 is more than 0;
step L5: comparing the heating monitoring coefficient JRi of the spectrum analyzer to a heating monitoring coefficient threshold:
if the heating monitoring coefficient JRi of the spectrum analyzer is larger than or equal to the heating monitoring coefficient threshold value, determining that the heating of the spectrum analyzer is normal, generating a normal heating signal and sending the normal heating signal to a mobile phone terminal of a manager;
if the heating monitoring coefficient JRi of the spectrum analyzer is smaller than the heating monitoring coefficient threshold value, judging that the heating of the spectrum analyzer is abnormal, generating a heating abnormal signal and sending the heating abnormal signal to the analysis control platform, and after receiving the heating abnormal signal, the analysis control platform generates a heating adjusting signal and sends the heating adjusting signal to a mobile phone terminal of an operator.
Further, the registration login unit is used for submitting operator information and manager information for registration through mobile phone terminals by operators and managers, and sending the operator information and the manager information which are successfully registered to the database for storage, wherein the operator information comprises names, ages, time of entry and mobile phone numbers of real name authentication of the operators, and the manager information comprises names, ages, time of entry and mobile phone numbers of real name authentication of the managers.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the method, circuit data of a spectrum analyzer are analyzed through a circuit detection unit, so that the spectrum analyzer is detected, a voltage floating value in a circuit of the spectrum analyzer, a maximum potential difference in the circuit of the spectrum analyzer and an average current value in the circuit of the spectrum analyzer are obtained, a detection coefficient JCi of the circuit of the spectrum analyzer is obtained through a formula, if the detection coefficient JCi of the circuit of the spectrum analyzer is larger than or equal to a circuit detection coefficient threshold value, the corresponding circuit is judged to be normal, a normal circuit signal is generated, and the normal circuit signal is sent to a mobile phone terminal of a manager; if the detection coefficient JCi of the circuit of the spectrum analyzer is smaller than the circuit detection coefficient threshold value, judging that the corresponding circuit is abnormal, generating a circuit abnormal signal and sending the circuit abnormal signal to an analysis control platform, and after receiving the circuit abnormal signal, the analysis control platform generates a circuit maintenance signal and sends the circuit maintenance signal to a mobile phone terminal of an operator; the circuit monitoring is carried out on the spectrum analyzer, the fault rate of the spectrum analyzer is effectively reduced, the working efficiency is improved, meanwhile, the abnormal circuit is repaired in time, and the service life of the spectrum analyzer is effectively prolonged;
2. in the invention, the gas detection unit is used for analyzing the gas data of the spectrum analyzer, so that the operation of the spectrum analyzer is detected, the gas data of the spectrum analyzer is obtained, the gas detection coefficient QT of the spectrum analyzer is obtained through a formula, and the gas detection coefficient QT of the spectrum analyzer is compared with a gas detection coefficient threshold value: if the gas detection coefficient QT of the spectrum analyzer is larger than or equal to the gas detection coefficient threshold value, determining that the gas detection is normal in the operation process of the spectrum analyzer, generating a gas normal signal and sending the gas normal signal to a mobile phone terminal of a manager; if the gas detection coefficient QT of the spectrum analyzer is less than the gas detection coefficient threshold value, determining that gas detection is abnormal in the operation process of the spectrum analyzer, generating a gas abnormal signal and sending the gas abnormal signal to an analysis control platform, and after receiving the gas abnormal signal, the analysis control platform generates a gas control signal and sends the gas control signal to a mobile phone terminal of an operator; gas in the working process of the spectrum analyzer is monitored, the analysis efficiency is improved, meanwhile, the reaction problem can be timely monitored in the operation process, the cost is reduced, and the working efficiency is improved.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the drawings without creative efforts.
Fig. 1 is a schematic block diagram of the present invention.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
As shown in fig. 1, an automatic spectrum analyzer control system includes a circuit detection unit, an instrument detection unit, a gas detection unit, a heating monitoring unit, an analysis control platform, a registration unit and a database;
the registration login unit is used for submitting operator information and manager information to register through a mobile phone terminal by an operator and a manager, and sending the successfully registered operator information and manager information to the database for storage, wherein the operator information comprises the name, the age, the time of entry and the mobile phone number of real name authentication of the person, and the manager information comprises the name, the age, the time of entry and the mobile phone number of real name authentication of the person;
the circuit detection unit is used for analyzing the circuit data of the spectrum analyzer so as to detect the spectrum analyzer, the circuit data of the spectrum analyzer comprises voltage data, potential data and current data, the voltage data is a voltage floating value in a circuit of the spectrum analyzer, the potential data is a maximum potential difference in the circuit of the spectrum analyzer, the current data is an average current value in the circuit of the spectrum analyzer, the circuit of the spectrum analyzer is marked as i, i is 1, 2, … …, n and n is a positive integer, and the specific analysis and detection process is as follows:
step one, acquiring a voltage floating value in a circuit of a spectrum analyzer, and marking the voltage floating value in the circuit of the spectrum analyzer as FDi;
acquiring the maximum potential difference in the circuit of the spectrum analyzer, and marking the maximum potential difference in the circuit of the spectrum analyzer as DWi;
acquiring an average current value in a circuit of the spectrum analyzer, and marking the average current value in the circuit of the spectrum analyzer as DLi;
step four, passing through a formula
Figure BDA0002937022100000081
Obtaining detection coefficients JCi of a spectrum analyzer circuit, wherein a1, a2 and a3 are all proportionality coefficients, and a1 is more than a2 is more than a3 is more than 0;
step five, comparing the detection coefficient JCi of the spectrum analyzer circuit with a circuit detection coefficient threshold value:
if the detection coefficient JCi of the circuit of the spectrum analyzer is not less than the circuit detection coefficient threshold, judging that the corresponding circuit is normal, generating a normal circuit signal and sending the normal circuit signal to a mobile phone terminal of a manager;
if the detection coefficient JCi of the circuit of the spectrum analyzer is smaller than the circuit detection coefficient threshold value, judging that the corresponding circuit is abnormal, generating a circuit abnormal signal and sending the circuit abnormal signal to an analysis control platform, and after receiving the circuit abnormal signal, the analysis control platform generates a circuit maintenance signal and sends the circuit maintenance signal to a mobile phone terminal of an operator;
the instrument detection unit is used for analyzing instrument data of the spectrum analyzer so as to detect the spectrum analyzer, the instrument data of the spectrum analyzer is the temperature of a chromatographic column in the spectrum analyzer, the flow of flushing gas and the internal pressure value, the spectrum analyzer is marked as o, o is 1, 2, … …, m and m are positive integers, and the specific analysis and detection process is as follows:
step S1: acquiring the temperature of a chromatographic column in the spectrum analyzer, and marking the temperature of the chromatographic column in the spectrum analyzer as Wi;
step S2: acquiring the flow of the flushing gas in the spectrum analyzer, and marking the flow of the flushing gas in the spectrum analyzer as Li;
step S3: acquiring a pressure value inside the spectrum analyzer, and marking the pressure value inside the spectrum analyzer as Yi;
step S4: by the formula Xi ═ e (Wi × b1+ Li × b2+ Yi × b3)b1+b2+b3Obtaining an instrument detection coefficient Xi of the spectrum analyzer, wherein b1, b2 and b3 are all proportionality coefficients, b1 is greater than b2 is greater than b3 is greater than 0, and e is a natural constant;
step S5: comparing the instrument detection coefficient Xi of the spectrum analyzer with an instrument detection coefficient threshold value:
if the instrument detection coefficient Xi of the spectrum analyzer is larger than or equal to the instrument detection coefficient threshold value, judging that the detection of the spectrum analyzer instrument is normal, generating an instrument normal signal and sending the instrument normal signal to a mobile phone terminal of a manager;
if the instrument detection coefficient Xi of the spectrum analyzer is smaller than the instrument detection coefficient threshold value, judging that the instrument detection of the spectrum analyzer is abnormal, generating an instrument abnormal signal and sending the instrument abnormal signal to an analysis control platform, and after receiving the instrument abnormal signal, the analysis control platform generates an instrument maintenance signal and sends the instrument maintenance signal to a mobile phone terminal of an operator;
the gas detection unit is used for analyzing the gas data of the spectrum analyzer, so as to detect the operation of the spectrum analyzer, the gas data of the spectrum analyzer comprises the content ratio of hydrogen, nitrogen and carbon dioxide generated when a sample is melted, the consumption of oxygen in the sample melting process and the generation of carbon monoxide in the sample melting process, and the specific analysis and detection process comprises the following steps:
step SS 1: acquiring the content ratios of hydrogen, nitrogen and carbon dioxide generated by the spectrum analyzer during sample melting, and marking the content ratios of hydrogen, nitrogen and carbon dioxide generated by the spectrum analyzer during sample melting as BZ;
step SS 2: acquiring the consumption of oxygen in the sample melting process of the spectrum analyzer, and marking the consumption of oxygen in the sample melting process of the spectrum analyzer as XH;
step SS 3: acquiring the generation amount of carbon monoxide in the sample melting process of the spectrum analyzer, and marking the generation amount of the carbon monoxide in the sample melting process of the spectrum analyzer as SC;
step SS 4: by the formula
Figure BDA0002937022100000101
Acquiring a gas detection coefficient QT of the spectrum analyzer, wherein v1, v2 and v3 are all proportionality coefficients, and v1 is more than v2 is more than v3 is more than 0;
step SS 5: comparing a gas detection coefficient QT of the spectrum analyzer with a gas detection coefficient threshold value:
if the gas detection coefficient QT of the spectrum analyzer is larger than or equal to the gas detection coefficient threshold value, determining that the gas detection is normal in the operation process of the spectrum analyzer, generating a gas normal signal and sending the gas normal signal to a mobile phone terminal of a manager;
if the gas detection coefficient QT of the spectrum analyzer is less than the gas detection coefficient threshold value, determining that gas detection is abnormal in the operation process of the spectrum analyzer, generating a gas abnormal signal and sending the gas abnormal signal to an analysis control platform, and after receiving the gas abnormal signal, the analysis control platform generates a gas control signal and sends the gas control signal to a mobile phone terminal of an operator;
the heating monitoring unit is used for the heating information of spectral analysis appearance at the operation in-process to monitor spectral analysis appearance's operation, the duration of heating in spectral analysis appearance's the heating information includes the rising speed of spectral analysis appearance heating in-process temperature, spectral analysis appearance's the highest heating temperature value and the heating process of spectral analysis appearance, and specific analysis monitoring process is as follows:
step L1: acquiring the temperature rising speed of the optical spectrum analyzer in the heating process, and marking the temperature rising speed of the optical spectrum analyzer in the heating process as SDi;
step L2: acquiring the highest heating temperature value of the spectrum analyzer, and marking the highest heating temperature value of the spectrum analyzer as WDi;
step L3: acquiring the continuous heating time in the heating process of the spectrum analyzer, and marking the continuous heating time in the heating process of the spectrum analyzer as SCi;
step L4: by the formula
Figure BDA0002937022100000111
Obtaining a heating monitoring coefficient JRi of the spectrum analyzer, wherein g1, g2 and g3 are proportional coefficients, and g1 is more than g2 is more than g3 is more than 0;
step L5: comparing the heating monitoring coefficient JRi of the spectrum analyzer to a heating monitoring coefficient threshold:
if the heating monitoring coefficient JRi of the spectrum analyzer is larger than or equal to the heating monitoring coefficient threshold value, determining that the heating of the spectrum analyzer is normal, generating a normal heating signal and sending the normal heating signal to a mobile phone terminal of a manager;
if the heating monitoring coefficient JRi of the spectrum analyzer is smaller than the heating monitoring coefficient threshold value, judging that the heating of the spectrum analyzer is abnormal, generating a heating abnormal signal and sending the heating abnormal signal to the analysis control platform, and after receiving the heating abnormal signal, the analysis control platform generates a heating adjusting signal and sends the heating adjusting signal to a mobile phone terminal of an operator.
The working principle of the invention is as follows:
when the automatic spectrum analyzer control system works, circuit data of a spectrum analyzer are analyzed through a circuit detection unit, so that the spectrum analyzer is detected, a voltage floating value in a circuit of the spectrum analyzer, a maximum potential difference in the circuit of the spectrum analyzer and an average current value in the circuit of the spectrum analyzer are obtained, a detection coefficient JCi of the circuit of the spectrum analyzer is obtained through a formula, if the detection coefficient JCi of the circuit of the spectrum analyzer is not less than a circuit detection coefficient threshold value, the corresponding circuit is judged to be normal, a normal circuit signal is generated, and the normal circuit signal is sent to a mobile phone terminal of a manager; if the detection coefficient JCi of the circuit of the spectrum analyzer is smaller than the circuit detection coefficient threshold value, judging that the corresponding circuit is abnormal, generating a circuit abnormal signal and sending the circuit abnormal signal to an analysis control platform, and after receiving the circuit abnormal signal, the analysis control platform generates a circuit maintenance signal and sends the circuit maintenance signal to a mobile phone terminal of an operator;
analyzing the gas data of the spectrum analyzer through a gas detection unit, detecting the operation of the spectrum analyzer, obtaining the gas data of the spectrum analyzer, obtaining a gas detection coefficient QT of the spectrum analyzer through a formula, if the gas detection coefficient QT of the spectrum analyzer is larger than or equal to a gas detection coefficient threshold value, judging that the gas detection of the spectrum analyzer in the operation process is normal, generating a gas normal signal and sending the gas normal signal to a mobile phone terminal of a manager; if the gas detection coefficient QT of the spectrum analyzer is less than the gas detection coefficient threshold value, determining that gas detection is abnormal in the operation process of the spectrum analyzer, generating a gas abnormal signal and sending the gas abnormal signal to an analysis control platform, and after receiving the gas abnormal signal, the analysis control platform generates a gas control signal and sends the gas control signal to a mobile phone terminal of an operator; gas in the working process of the spectrum analyzer is monitored, the analysis efficiency is improved, meanwhile, the reaction problem can be timely monitored in the operation process, the cost is reduced, and the working efficiency is improved.
The above formulas are all calculated by taking the numerical value of the dimension, the formula is a formula which obtains the latest real situation by acquiring a large amount of data and performing software simulation, and the preset parameters in the formula are set by the technical personnel in the field according to the actual situation.
The foregoing is merely exemplary and illustrative of the present invention and various modifications, additions and substitutions may be made by those skilled in the art to the specific embodiments described without departing from the scope of the invention as defined in the following claims.

Claims (5)

1. An automatic spectrum analyzer control system is characterized by comprising a circuit detection unit, an instrument detection unit, a gas detection unit, a heating monitoring unit, an analysis control platform, a registration unit and a database;
the circuit detection unit is used for analyzing the circuit data of the spectrum analyzer so as to detect the spectrum analyzer, the circuit data of the spectrum analyzer comprises voltage data, potential data and current data, the voltage data is a voltage floating value in a circuit of the spectrum analyzer, the potential data is a maximum potential difference in the circuit of the spectrum analyzer, the current data is an average current value in the circuit of the spectrum analyzer, the circuit of the spectrum analyzer is marked as i, i is 1, 2, … …, n and n is a positive integer, and the specific analysis and detection process is as follows:
step one, acquiring a voltage floating value in a circuit of a spectrum analyzer, and marking the voltage floating value in the circuit of the spectrum analyzer as FDi;
acquiring the maximum potential difference in the circuit of the spectrum analyzer, and marking the maximum potential difference in the circuit of the spectrum analyzer as DWi;
acquiring an average current value in a circuit of the spectrum analyzer, and marking the average current value in the circuit of the spectrum analyzer as DLi;
step four, passing through a formula
Figure FDA0002937022090000011
Obtaining detection coefficients JCi of a spectrum analyzer circuit, wherein a1, a2 and a3 are all proportionality coefficients, and a1 is more than a2 is more than a3 is more than 0;
step five, comparing the detection coefficient JCi of the spectrum analyzer circuit with a circuit detection coefficient threshold value:
if the detection coefficient JCi of the circuit of the spectrum analyzer is not less than the circuit detection coefficient threshold, judging that the corresponding circuit is normal, generating a normal circuit signal and sending the normal circuit signal to a mobile phone terminal of a manager;
and if the detection coefficient JCi of the circuit of the spectrum analyzer is less than the circuit detection coefficient threshold value, judging that the corresponding circuit is abnormal, generating a circuit abnormal signal and sending the circuit abnormal signal to the analysis control platform, and after receiving the circuit abnormal signal, the analysis control platform generates a circuit maintenance signal and sends the circuit maintenance signal to the mobile phone terminal of an operator.
2. The automatic spectrum analyzer control system of claim 1, wherein the instrument detection unit is configured to analyze instrument data of a spectrum analyzer, so as to detect the spectrum analyzer, the instrument data of the spectrum analyzer is temperature of a chromatographic column in the spectrum analyzer, flow rate of a purge gas and internal pressure value, the spectrum analyzer is labeled as o, o is 1, 2, … …, m, m is a positive integer, and specific analysis and detection processes are as follows:
step S1: acquiring the temperature of a chromatographic column in the spectrum analyzer, and marking the temperature of the chromatographic column in the spectrum analyzer as Wi;
step S2: acquiring the flow of the flushing gas in the spectrum analyzer, and marking the flow of the flushing gas in the spectrum analyzer as Li;
step S3: acquiring a pressure value inside the spectrum analyzer, and marking the pressure value inside the spectrum analyzer as Yi;
step S4: by the formula Xi ═ e (Wi × b1+ Li × b2+ Yi × b3)b1+b2+b3Obtaining an instrument detection coefficient Xi of the spectrum analyzer, wherein b1, b2 and b3 are all proportionality coefficients, b1 is greater than b2 is greater than b3 is greater than 0, and e is a natural constant;
step S5: comparing the instrument detection coefficient Xi of the spectrum analyzer with an instrument detection coefficient threshold value:
if the instrument detection coefficient Xi of the spectrum analyzer is larger than or equal to the instrument detection coefficient threshold value, judging that the detection of the spectrum analyzer instrument is normal, generating an instrument normal signal and sending the instrument normal signal to a mobile phone terminal of a manager;
and if the instrument detection coefficient Xi of the spectrum analyzer is less than the instrument detection coefficient threshold value, judging that the detection of the spectrum analyzer is abnormal, generating an instrument abnormal signal and sending the instrument abnormal signal to the analysis control platform, and after receiving the instrument abnormal signal, the analysis control platform generates an instrument maintenance signal and sends the instrument maintenance signal to a mobile phone terminal of an operator.
3. The automatic spectrum analyzer control system of claim 1, wherein the gas detection unit is configured to analyze gas data of the spectrum analyzer, so as to detect operation of the spectrum analyzer, the gas data of the spectrum analyzer includes content ratios of hydrogen, nitrogen and carbon dioxide generated when the sample is melted, consumption of oxygen during melting of the sample, and generation of carbon monoxide during melting of the sample, and the specific analysis and detection process includes:
step SS 1: acquiring the content ratios of hydrogen, nitrogen and carbon dioxide generated by the spectrum analyzer during sample melting, and marking the content ratios of hydrogen, nitrogen and carbon dioxide generated by the spectrum analyzer during sample melting as BZ;
step SS 2: acquiring the consumption of oxygen in the sample melting process of the spectrum analyzer, and marking the consumption of oxygen in the sample melting process of the spectrum analyzer as XH;
step SS 3: acquiring the generation amount of carbon monoxide in the sample melting process of the spectrum analyzer, and marking the generation amount of the carbon monoxide in the sample melting process of the spectrum analyzer as SC;
step SS 4: by the formula
Figure FDA0002937022090000031
Acquiring a gas detection coefficient QT of the spectrum analyzer, wherein v1, v2 and v3 are all proportionality coefficients, and v1 is more than v2 is more than v3 is more than 0;
step SS 5: comparing a gas detection coefficient QT of the spectrum analyzer with a gas detection coefficient threshold value:
if the gas detection coefficient QT of the spectrum analyzer is larger than or equal to the gas detection coefficient threshold value, determining that the gas detection is normal in the operation process of the spectrum analyzer, generating a gas normal signal and sending the gas normal signal to a mobile phone terminal of a manager;
if the gas detection coefficient QT of the spectrum analyzer is less than the gas detection coefficient threshold value, determining that gas detection is abnormal in the operation process of the spectrum analyzer, generating a gas abnormal signal and sending the gas abnormal signal to an analysis control platform, and after receiving the gas abnormal signal, the analysis control platform generates a gas control signal and sends the gas control signal to a mobile phone terminal of an operator.
4. The automatic spectrum analyzer control system of claim 1, wherein the heating monitoring unit is configured to monitor the operation of the spectrum analyzer by using heating information of the spectrum analyzer during operation, the heating information of the spectrum analyzer includes a temperature rise rate during the heating process of the spectrum analyzer, a maximum heating temperature value of the spectrum analyzer, and a continuous heating duration during the heating process of the spectrum analyzer, and the specific analysis monitoring process is as follows:
step L1: acquiring the temperature rising speed of the optical spectrum analyzer in the heating process, and marking the temperature rising speed of the optical spectrum analyzer in the heating process as SDi;
step L2: acquiring the highest heating temperature value of the spectrum analyzer, and marking the highest heating temperature value of the spectrum analyzer as WDi;
step L3: acquiring the continuous heating time in the heating process of the spectrum analyzer, and marking the continuous heating time in the heating process of the spectrum analyzer as SCi;
step L4: by the formula
Figure FDA0002937022090000041
Obtaining a heating monitoring coefficient JRi of the spectrum analyzer, wherein g1, g2 and g3 are proportional coefficients, and g1 is more than g2 is more than g3 is more than 0;
step L5: comparing the heating monitoring coefficient JRi of the spectrum analyzer to a heating monitoring coefficient threshold:
if the heating monitoring coefficient JRi of the spectrum analyzer is larger than or equal to the heating monitoring coefficient threshold value, determining that the heating of the spectrum analyzer is normal, generating a normal heating signal and sending the normal heating signal to a mobile phone terminal of a manager;
if the heating monitoring coefficient JRi of the spectrum analyzer is smaller than the heating monitoring coefficient threshold value, judging that the heating of the spectrum analyzer is abnormal, generating a heating abnormal signal and sending the heating abnormal signal to the analysis control platform, and after receiving the heating abnormal signal, the analysis control platform generates a heating adjusting signal and sends the heating adjusting signal to a mobile phone terminal of an operator.
5. The automatic spectrum analyzer control system of claim 1, wherein the registration login unit is configured to allow an operator and a manager to submit operator information and manager information via a mobile phone terminal for registration, and send the operator information and the manager information that are successfully registered to the database for storage, wherein the operator information includes a name, an age, an attendance time of the operator and a mobile phone number for personal real name authentication, and the manager information includes a name, an age, an attendance time of the manager and a mobile phone number for personal real name authentication.
CN202110164242.4A 2021-02-05 2021-02-05 Automatic spectrum analyzer control system Withdrawn CN112964656A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110164242.4A CN112964656A (en) 2021-02-05 2021-02-05 Automatic spectrum analyzer control system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110164242.4A CN112964656A (en) 2021-02-05 2021-02-05 Automatic spectrum analyzer control system

Publications (1)

Publication Number Publication Date
CN112964656A true CN112964656A (en) 2021-06-15

Family

ID=76274806

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110164242.4A Withdrawn CN112964656A (en) 2021-02-05 2021-02-05 Automatic spectrum analyzer control system

Country Status (1)

Country Link
CN (1) CN112964656A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117852779A (en) * 2024-03-08 2024-04-09 广东立胜综合能源服务有限公司 Industrial park carbon emission calculation method and system

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117852779A (en) * 2024-03-08 2024-04-09 广东立胜综合能源服务有限公司 Industrial park carbon emission calculation method and system

Similar Documents

Publication Publication Date Title
CN114184229A (en) Switch cabinet operation environment monitoring system
CN116320832B (en) Monitoring equipment fault monitoring method and device
CN113783272B (en) Safety control method based on super capacitor monitoring management system
CN1289038A (en) Intelligent analysts system and method for electric equipment filled with fluid
CN112526070B (en) LEL and VOC combination formula waste gas analysis system
CN112964656A (en) Automatic spectrum analyzer control system
JPH0762667B2 (en) Solution quantitative analysis device, quantitative analysis method, and water quality control system for nuclear reactor
CN107515595A (en) A kind of coal acetylene production information intelligent billboard with data analysis function
Dobney et al. Laser ablation inductively coupled plasma mass spectrometry as a tool for studying heterogeneity within polymers
Dion et al. Prediction of low-voltage tetrafluoromethane emissions based on the operating conditions of an aluminium electrolysis cell
US7991039B2 (en) Electric arc furnace monitoring system and method
EP0281037B1 (en) Method of measuring oxygen in silicon
Mills Use of emission spectroscopy for welding arc analysis
CN116865672A (en) Photovoltaic module abnormality recognition method and device and computer readable storage medium
CN112307597B (en) Performance evaluation method of electric flocculation water treatment device
CN115758066A (en) Method for counting carbon emission in whole life cycle of transformer
CN113091808A (en) Chemical industry industrial control instrument with comprehensive information management system and system thereof
JPH10113776A (en) Recognizing method of dust generating state
CN117788021B (en) Method and system for rapidly screening quality of coal carbon emission data of furnace charging of emission control enterprise
Zylka et al. Rapid dissolved gas analysis by means of electrochemical gas sensors
CN104731955A (en) Methods and systems for diagnostic standard establishment and intelligent diagnosis of wind generation set oil monitoring
CN113640225B (en) Sulfuric acid concentration monitoring system applied to manganese sulfate production
CN101039044A (en) Electrical distribution monitoring system and monitoring method
JPS61201147A (en) Sample heating furnace in gas extraction type sample analyzing instrument
CN117937686A (en) Intelligent battery management method and system

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WW01 Invention patent application withdrawn after publication

Application publication date: 20210615

WW01 Invention patent application withdrawn after publication