CN112960970B - Prefabrication forming method of alumina fiber module - Google Patents

Prefabrication forming method of alumina fiber module Download PDF

Info

Publication number
CN112960970B
CN112960970B CN202110162241.6A CN202110162241A CN112960970B CN 112960970 B CN112960970 B CN 112960970B CN 202110162241 A CN202110162241 A CN 202110162241A CN 112960970 B CN112960970 B CN 112960970B
Authority
CN
China
Prior art keywords
fiber
fibers
alumina
alumina gel
gel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202110162241.6A
Other languages
Chinese (zh)
Other versions
CN112960970A (en
Inventor
高明
华玉喜
张�杰
范宗忠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shandong Dongheng National Fiber New Material Co ltd
Original Assignee
Shandong Dongheng National Fiber New Material Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shandong Dongheng National Fiber New Material Co ltd filed Critical Shandong Dongheng National Fiber New Material Co ltd
Priority to CN202110162241.6A priority Critical patent/CN112960970B/en
Publication of CN112960970A publication Critical patent/CN112960970A/en
Application granted granted Critical
Publication of CN112960970B publication Critical patent/CN112960970B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/10Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62227Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
    • C04B35/62231Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on oxide ceramics
    • C04B35/62236Fibres based on aluminium oxide
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/602Making the green bodies or pre-forms by moulding
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567Treatment time
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74Physical characteristics
    • C04B2235/77Density
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/95Products characterised by their size, e.g. microceramics
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/50Glass production, e.g. reusing waste heat during processing or shaping
    • Y02P40/57Improving the yield, e-g- reduction of reject rates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Nonwoven Fabrics (AREA)

Abstract

The invention discloses a prefabrication and forming method of an alumina fiber module, which comprises the following steps: firstly, carding alumina gel fibers; then, filling the alumina gel fiber into a mold; then, molding the alumina gel fiber; then, sintering the alumina gel fiber; finally, the alumina gel fiber is packed, and the fiber is molded in a gel fiber stage, because the alumina fiber has very good flexibility, processability and compressibility in the gel fiber stage, the method selects to carry out pretreatment molding on the alumina fiber in the gel fiber stage, and the density of the alumina fiber reaches a desired value through a molding device.

Description

Prefabrication forming method of alumina fiber module
Technical Field
The invention belongs to the field of inorganic materials, and relates to a preforming method of an alumina fiber module.
Background
The alumina fiber is divided into two categories, short fiber loose cotton and continuous fiber, according to the length of the alumina fiber. The short fiber obtained in the production process is similar to cotton in daily life, and is usually disorderly gathered together, and the bulk density of the fiber is lower than 5Kg/m 3 If these low density fibers are directly packed, the packing density and transportation efficiency will be low, and the secondary treatment of the finished fibers will cause irreversible damage to the fibers, which will cause dust damage to the environment and affect the fiber length and later use properties. Therefore, how to overcome the difficulty by a production enterprise is an urgent problem to be solved, which can not cause secondary damage to the fiber, but also can improve the stacking density of the fiber, reduce the cost and improve the transportation efficiency.
Disclosure of Invention
The invention designs and develops a method for prefabricating and forming an alumina fiber module, wherein the density of the prefabricated module reaches a certain density, and then the prefabricated module is sintered at a proper high temperature to prepare the alumina fiber module.
The prefabrication and forming method of the alumina fiber module comprises the following steps:
s1, carded alumina gel fibers, theThe length of the alumina gel fiber is L, L is more than or equal to 20cm and less than or equal to 200cm, and the bulk density of the alumina gel fiber is not more than 5Kg/m 3
S2, filling alumina gel fibers into a mold;
s3, molding the alumina gel fiber;
s4, sintering the alumina gel fiber;
and S5, packaging the alumina gel fibers.
According to some embodiments of the present invention, the step S1 is to comb the alumina gel short fibers by hand, and the worker wears a silicone glove with smooth surface and no static electricity to tear and finish the fibers.
According to some embodiments of the present invention, the step S1 is mechanical carding of alumina gel short fibers, and the alumina gel short fibers are carded by a roller carding and elastic card clothing structure.
According to some specific embodiments of the present invention, the step S1 includes:
s11, chopping, namely chopping the alumina gel short fibers to segmented fibers with the length of L by using a guillotine type chopping machine, wherein L is more than or equal to 5mm and less than or equal to 100 mm;
s12, opening, namely opening the segmented fibers in the step S11 by adopting an elastic card clothing structure type opener;
according to some embodiments of the present invention, in the step S12, the elastic card clothing structure type opener uses a rubber-based elastic card clothing, the elastic card clothing has a circular card and a diameter of 1mm, the elastic card is formed into carbon structural steel, and the surface of the elastic card clothing is galvanized.
According to some embodiments of the present invention, in step S3, the alumina gel fiber is molded by using a compression preforming device, the pressure of the molding process is not greater than 1MPa, the compression time is not less than 10min, and the bulk density of the molded alumina gel fiber is not less than 20Kg/m 3
According to some embodiments of the present invention, in step S3, the mold of the compression preforming device is an insulating material piece made of PP organic material.
According to some embodiments of the invention, in the step S4, the sintering temperature of the alumina gel short fiber is T: t is more than or equal to 1000 ℃ and less than or equal to 1400 ℃.
The method has the advantages that the key point of the method for prefabricating and forming the alumina fiber module is that short fibers are formed and molded in the gel fiber stage, and the alumina fibers have very good flexibility, processability and compressibility in the gel fiber stage, so that the method selects to pretreat and form the alumina fibers in the gel fiber stage, the density of the alumina fibers reaches an expected value through a molding device, and research and comparison are carried out on the alumina fibers in two crystal forms of a gamma phase and a mullite phase.
Drawings
FIG. 1 is a flow chart of a method of preforming an alumina fiber module according to an embodiment of the invention;
FIG. 2 is a schematic representation of the gel fibers prior to preforming;
FIG. 3 is a schematic representation of the stacking state before gel fiber pre-forming;
FIG. 4 is a schematic representation of the gel fibers after they have been pre-formed;
FIG. 5 is a schematic representation of the stacking state after gel fiber pre-forming.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring now to fig. 1 to 5, a method for preforming an alumina fiber module according to an embodiment of the present invention includes the steps of:
s1, carding the alumina gel fibers, wherein the length of the alumina gel fibers is L, L is more than or equal to 20cm and less than or equal to 200cm, and the bulk density of the alumina gel fibers is not more than 5Kg/m 3
S2, filling alumina gel fibers into a mold;
s3, molding the alumina gel fiber;
s4, sintering the alumina gel fiber;
and S5, packaging the alumina gel fibers.
The length of the raw material alumina gel fiber is very long, generally more than 20cm, the length can reach more than 200cm, the average length is about 50cm, and complex and disordered winding can be generated among the gel fibers in the spinning or blowing process, so that the reasonable and controllable carding of the gel fibers is a key step for increasing the density of the gel fibers.
According to some embodiments of the present invention, the step S1 is to comb the alumina gel short fibers by hand, and the worker wears a silicone glove with smooth surface and no static electricity to tear and finish the fibers. The carding and forming of the alumina fiber adopt two modes of manual carding or mechanical carding. The manual carding is that a person tears and finishes the fibers by selecting to take silica gel gloves with smooth surfaces to achieve the purpose of uniform dispersion of the fibers in a mould, wherein the gloves are silica gel gloves with smooth surfaces and no static electricity.
The manual carding method has the advantages that people wear silica gel gloves, static electricity is not easy to generate, the flexibility and the softness of hands do not damage fibers, meanwhile, people can better control carding effect through real-time observation and judgment, and gel fibers are changed into a relatively uniformly dispersed state from a disordered state. In addition, because the fiber is in a large number of locks, the fiber is difficult to tear by hand, the length of the fiber is not changed in the tearing and dispersing process (the fiber length is still more than 20cm, and the average length is 50cm), so that the fiber is still kept in the original length state, the uniformity of the fiber in a three-dimensional space is limited, and the density of the compression molding process is influenced.
According to some embodiments of the present invention, the step S1 is mechanical carding of alumina gel short fibers, and the alumina gel short fibers are carded by a structure mainly composed of a roller and an elastic card clothing through an opener. Aiming at the characteristic that the alumina gel fiber is not easy to comb, the roller carding and elastic card clothing structure is selected and carded at a low speed, so that the aim of carding and dispersing the gel fiber uniformly is fulfilled. Since the method is only for preforming to increase the packing density, the carding standard is not as high as that of the non-woven textile type, as long as the requirement of increasing the density without damaging the fibers is met.
Although the gel fiber has better flexibility and processability compared with the alumina fiber, the gel fiber has a large difference compared with organic fibers such as terylene, acrylic fiber, chinlon, polypropylene fiber and the like, so that the gel fiber is greatly damaged by directly using equipment for carding and forming the organic fibers (a cylinder comprising a stainless steel roller, a stainless steel card clothing and other hard card clothing), and the fibers are torn and crushed.
According to some specific embodiments of the present invention, the step S1 includes:
s11, chopping, namely chopping the alumina gel short fiber into segmented fiber with the length of L by using a guillotine-type chopping machine, wherein L is more than or equal to 5mm and less than or equal to 100 mm;
s12, opening, namely opening the segmented fibers in the step S11 by adopting an elastic card clothing structure type opener;
the mechanical opening method comprises the following two steps:
the first step is chopping, the chopper is of a guillotine type, the structure has less damage to the fibers compared with a high-speed rotary chopper, and the fibers are chopped to 5-100mm in the process so as to be prepared for opening. Because the fibers are too long (average length 50cm) and the gel fibers are weak, if opened directly, the high stiffness and strength of the opener (less gentle than a human hand) easily breaks the fibers.
The second step is opening, the opening equipment adopts an opener with a special elastic card clothing structure, and the opener consists of a feeding roller and an elastic opening cylinder (card clothing). The opening process is that fibers collected in the production process are conveyed to the opening part through a roller, and then the fibers are torn by a needle type structure on the opening cylinder, so that the gel fibers achieve the purpose of better dispersion forming compared with manual opening and carding.
The specifications of the elastic card clothing are as follows: the rubber-based elastic card clothing is adopted, round needles with the diameter of 1mm are adopted, and the material is carbon structural steel (surface galvanized) or stainless steel.
According to some embodiments of the present invention, in the step S12, the elastic card clothing structure type opener uses rubber-based elastic card clothing, an elastic needle of the rubber-based elastic card clothing is a circular needle, a diameter of the elastic needle is 1mm, the elastic needle is formed of carbon structural steel, and a surface of the elastic needle is galvanized.
According to some embodiments of the present invention, in step S3, the alumina gel fiber is molded by using a compression preforming device, the pressure of the molding process is not greater than 1MPa, and the bulk density of the molded alumina gel fiber is not less than 20Kg/m 3
The opening carding process is to achieve a better dispersion effect of the fibers in three-dimensional space, and the compression molding process is to increase the bulk density of the gel fibers to 20Kg/m from a density of less than 5Kg/m3 3 Therefore, the fiber density after sintering is improved, and simultaneously, the fiber achieves the purposes of preforming and modularization through the process.
According to some embodiments of the present invention, in step S3, the mold of the compression preforming device is an insulating material piece made of PP organic material.
The process adopts self-designed compression preforming equipment, the power is hydraulic pressure or air pressure, the die is made of PP and other organic insulating materials (the static electricity is not easy to generate in the using process, and the problem of electrostatic adsorption does not exist with the fiber), and the shape is longThe square structure (the corresponding size, the length is 500- 3
According to some embodiments of the invention, in the step S4, the alumina gel staple fiber has a sintering temperature T: t is more than or equal to 1000 ℃ and less than or equal to 1400 ℃. The sintering process is a process for converting gel fiber into alumina fiber, the temperature in the process is 1000-1400 ℃, firstly, moisture in the gel fiber is volatilized by using high temperature, secondly, organic matters and other inorganic chemical components which can be oxidized and volatilized are burnt, and finally, aluminum, silicon and other needed components are converted into needed crystal phases (gamma phase, mullite phase or alpha phase), in the process, the preformed gel fiber becomes alumina fiber products, and simultaneously, the fiber module generates about 1/2 volume shrinkage in volume due to the volatilization of moisture in the gel fiber and the reconstruction of chemical elements in the fiber, and simultaneously, the density is further increased.
According to the prefabrication forming method of the alumina fiber module, the key point is that short fibers are subjected to carding forming and die pressing in a gel fiber stage, and because the alumina fibers have very good flexibility, processability and compressibility in the gel fiber stage, the alumina fibers are subjected to pretreatment forming in the gel fiber stage, firstly, the fibers are subjected to better cross gap filling through carding, and secondly, the density of the alumina fibers reaches a desired value through die pressing equipment.
The invention mainly researches and compares alumina fibers in two crystal forms of a gamma phase and a mullite phase, and because the influence of the gamma phase and the mullite phase fibers on the volume can be ignored, the module prepared by the method has no difference in volume, and only because the fibers have better flexibility under the condition of the gamma phase, the obtained module also has better operability.
The method for preforming an alumina fiber module according to an embodiment of the present invention will be described with reference to specific embodiments.
Example 1
2.5Kg of gel fiber with a density of 4.6Kg/m is taken 3 Opening and carding the fibers by manual carding, and filling into a PP mold with the size of 750 × 550 × 300mm 3 Uniformly dispersing the fiber in a die, molding the fiber in the die by using a pneumatic press (pressure value is between 0 and 1MPa), keeping the pressure at 0.2MPa for 5min, and making the preformed gel fiber module have the size of 795 multiplied by 650 multiplied by 200mm 3 Density of 25Kg/m 3 Sintering at 1050 deg.C for 30min to obtain final product fiber module with mass of 1.25Kg and size of 450 × 300 × 120mm 3 Density of 77Kg/m 3 The crystal phase is a dell phase.
Example 2
2.5Kg of gel fiber with a density of 4.6Kg/m is taken 3 Opening and carding the fibers by manual carding, and filling into a PP mold with the size of 750 × 550 × 300mm 3 Uniformly dispersing the fiber in a die, and molding the fiber in the die by using a pneumatic press (the pressure value is between 0 and 1MPa), wherein the pressure is 0.4MPa, the retention time is 10min, and the size of a preformed gel fiber module is 780 multiplied by 620 multiplied by 190mm 3 Density of 27Kg/m 3 Sintering at 1050 deg.C for 30min to obtain fiber module with mass of 1.25Kg and size of 430 × 280 × 115mm 3 The density is 90Kg/m 3 The crystal phase is a dell phase.
Example 3
Taking 2.5Kg of gel fiber, chopping the fiber by a guillotine type chopping machine (the chopping frequency is 60times/min), the chopped fiber length is 50-80mm, then opening and carding the fiber by a mechanical carding mode, and loading the fiber into a PP mold with the size of 750X 550X 300mm 3 Uniformly dispersing the fiber in a mold, molding the fiber in the mold by a pneumatic press (pressure value of 0-1MPa) under 0.4MPa for 10min, wherein the size of the preformed gel fiber module is 765 × 610 × 185mm 3 Density of 29Kg/m 3 At 1050 ℃ CSintering for 30min to obtain fiber module with mass of 1.25Kg and size of 410 × 275 × 110mm 3 Density of 101Kg/m 3 The crystal phase is a dellite phase.
Example 4
Taking 2.5Kg of gel fiber, chopping the fiber by a guillotine type chopping machine (the chopping frequency is 60times/min), the chopped fiber length is between 70 and 100mm, then opening and carding the fiber by a mechanical carding mode, and loading the fiber into a PP mold with the size of 750 multiplied by 550 multiplied by 300mm 3 Uniformly dispersing the fiber in a die, and molding the fiber in the die by using a pneumatic press (the pressure value is between 0 and 1MPa), wherein the pressure is 0.4MPa, the holding time is 10min, and the size of a preformed gel fiber module is 775 multiplied by 615 multiplied by 195mm 3 The density is 27Kg/m 3 Sintering at 1050 deg.C for 30min to obtain fiber module with mass of 1.25Kg and size of 418 × 280 × 110mm 3 The density is 97Kg/m 3 The crystal phase is a dell phase.
Example 5
Sintering at 1300 deg.C for 30min to obtain fiber module with mass of 1.25Kg and size of 410X 270X 110mm as in example 3 3 The density is 103Kg/m 3 The crystal phase is mullite phase.
Example 6
2.5Kg of gel fiber with a density of 4.6Kg/m is taken 3 The fiber is directly opened and carded by a mechanical carding mode, the length of the fiber is between 1 and 5mm, and the fiber cannot be molded by compression after being too broken and filled into a mold.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.

Claims (3)

1. The prefabrication and forming method of the alumina fiber module is characterized by comprising the following steps:
s1, carding the alumina gel fibers, wherein the length of the alumina gel fibers is L, L is more than or equal to 20cm and less than or equal to 200cm, and the bulk density of the alumina gel fibers is not more than 5kg/m 3 (ii) a Short-cutting treatment, namely, short-cutting the alumina gel short fibers into segmented fibers with the length of l by using a guillotine type short-cutting machine, wherein l is more than or equal to 5mm and less than or equal to 100 mm; opening, namely opening the segmented fibers by using an elastic card clothing structure type opener; the opener with the elastic card clothing structure adopts rubber-based elastic card clothing, an elastic needle of the rubber-based elastic card clothing is a round needle, the diameter of the elastic needle is 1mm, the elastic needle is formed into carbon structural steel, and the surface of the elastic needle is galvanized;
s2, filling alumina gel fibers into a mold;
s3, molding the alumina gel fiber;
s4, sintering the alumina gel fiber;
s5, packaging the alumina gel fibers;
in the step S3, the alumina gel fiber is molded by a compression preforming device, the molding time is not less than 10min, and the bulk density of the molded alumina gel fiber is not less than 20kg/m 3 (ii) a The mould of the compression preforming equipment is an insulating material piece made of a PP (polypropylene) organic material;
in the step S4, the sintering temperature of the alumina gel short fiber is T: t is more than or equal to 1000 ℃ and less than or equal to 1400 ℃;
the power of the compression preforming equipment is hydraulic pressure or air pressure, the pressure range is 0.2-1MPa, the shape of the mould is a cuboid structure, the length is 500-1000mm, the width is 300-600mm, and the height is 100-300 mm.
2. The method for preforming an alumina fiber module according to claim 1, wherein: and step S1, manually carding the alumina gel short fibers, and tearing and finishing the fibers by workers wearing silica gel gloves with smooth surfaces and no static electricity.
3. The method for preforming an alumina fiber module according to claim 1, wherein: and step S1, mechanically carding alumina gel short fibers, and carding the alumina gel short fibers by adopting a roller carding and elastic card clothing structure.
CN202110162241.6A 2021-04-23 2021-04-23 Prefabrication forming method of alumina fiber module Active CN112960970B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110162241.6A CN112960970B (en) 2021-04-23 2021-04-23 Prefabrication forming method of alumina fiber module

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110162241.6A CN112960970B (en) 2021-04-23 2021-04-23 Prefabrication forming method of alumina fiber module

Publications (2)

Publication Number Publication Date
CN112960970A CN112960970A (en) 2021-06-15
CN112960970B true CN112960970B (en) 2022-09-20

Family

ID=76274547

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110162241.6A Active CN112960970B (en) 2021-04-23 2021-04-23 Prefabrication forming method of alumina fiber module

Country Status (1)

Country Link
CN (1) CN112960970B (en)

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2959683B2 (en) * 1991-04-30 1999-10-06 三井鉱山株式会社 Method for producing high-purity alumina fiber molded body
JP6608692B2 (en) * 2015-12-16 2019-11-20 イビデン株式会社 Manufacturing method of holding sealing material
CN106087437B (en) * 2016-06-15 2018-04-06 无锡市明江保温材料有限公司 The preparation method of mineral wool panels peculiar to vessel
CN109208171B (en) * 2018-10-17 2022-04-01 江苏腾利特种纤维科技有限公司 Preparation method of polycrystalline alumina fiber needle-punched liner

Also Published As

Publication number Publication date
CN112960970A (en) 2021-06-15

Similar Documents

Publication Publication Date Title
CN105401334B (en) A kind of preparation method of needle punched non-woven fabrics
CN103074739B (en) Production method for polypropylene spun-bonded needle-punched geotextile
CN105525435B (en) A kind of layered structure filler and preparation method thereof
CN101691045B (en) Plate and manufacture method thereof
CN101906700A (en) Filling cotton and preparation method thereof
EP2834402B1 (en) Method of converting a glass fibre fabric material and products obtained by the method
CN112960970B (en) Prefabrication forming method of alumina fiber module
GB8724970D0 (en) Composite material
CN108277577A (en) It is a kind of to utilize waste and old textile fabric manufacture heat insulating elastic non-woven material and preparation method thereof
CN1907185A (en) Method for preparing red hemp environmental protection needling non-woven carpet for automobile
ES8702544A1 (en) Method and apparatus for making fibre mats as starting materials for moulded articles.
CN111648035A (en) ES fiber core material product and preparation method thereof
PL362933A1 (en) Method and device for producing a composite yarn
ES8605722A1 (en) Method and apparatus for making fibre sheets for use as preforms for pressed articles.
CN103225171B (en) Manufacturing method of tailorable silk floss
CN102206884A (en) Method for developing and applying regenerated aramid fiber
CN101929079A (en) Method for manufacturing medicinal ventilated adhesive tape base material
CN100432309C (en) Method of producing blending yarn of natural silk and spun silk by jet spinning
AU2018238310A1 (en) Transformation process of carbon fibers, carbonised from synthetic fibers and vegetable fibers into non-woven fabric
CN203345229U (en) Packing device of cotton carding and dust filtering machine
CN104665527A (en) Manufacturing technology for fiber blanket
CN202895403U (en) Production device for coconut fiber plate
CN101580981B (en) Draft making method by stretch breaking and silk spinning
CN217973601U (en) Composite fabric production equipment
CN111519339A (en) Mattress material and manufacturing method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
TA01 Transfer of patent application right
TA01 Transfer of patent application right

Effective date of registration: 20220907

Address after: Room 204, East Office Building, 50 meters south of the intersection of Fuqian Street and Chizhou Road, Development Zone, Dongying City, Shandong Province, 257000

Applicant after: Shandong Dongheng national fiber new material Co.,Ltd.

Address before: 1818 Xinyuan Avenue, Tianqiao District, Jinan City, Shandong Province

Applicant before: SHANDONG DONGHANG COLLOIDAL MATERIAL CO.,LTD.

PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: A Prefabrication Method for Alumina Fiber Module

Effective date of registration: 20231228

Granted publication date: 20220920

Pledgee: Weihai commercial bank Limited by Share Ltd. Dongying branch

Pledgor: Shandong Dongheng national fiber new material Co.,Ltd.

Registration number: Y2023980074970