CN112939458A - Antibacterial ceramic glaze for wall and floor tiles and application method of glaze - Google Patents
Antibacterial ceramic glaze for wall and floor tiles and application method of glaze Download PDFInfo
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- CN112939458A CN112939458A CN202010375201.5A CN202010375201A CN112939458A CN 112939458 A CN112939458 A CN 112939458A CN 202010375201 A CN202010375201 A CN 202010375201A CN 112939458 A CN112939458 A CN 112939458A
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- glaze
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- floor tiles
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B11/00—Apparatus or processes for treating or working the shaped or preshaped articles
- B28B11/04—Apparatus or processes for treating or working the shaped or preshaped articles for coating or applying engobing layers
- B28B11/044—Apparatus or processes for treating or working the shaped or preshaped articles for coating or applying engobing layers with glaze or engobe or enamel or varnish
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B11/00—Apparatus or processes for treating or working the shaped or preshaped articles
- B28B11/04—Apparatus or processes for treating or working the shaped or preshaped articles for coating or applying engobing layers
- B28B11/045—Apparatus or processes for treating or working the shaped or preshaped articles for coating or applying engobing layers by dipping
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B11/00—Apparatus or processes for treating or working the shaped or preshaped articles
- B28B11/04—Apparatus or processes for treating or working the shaped or preshaped articles for coating or applying engobing layers
- B28B11/049—Recycling of the coating material
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Structural Engineering (AREA)
- Ceramic Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Finishing Walls (AREA)
Abstract
The invention relates to the technical field of wall and floor tiles and discloses an antibacterial ceramic glaze for wall and floor tiles, which comprises, by mass, 40-50 parts of titanium dioxide, 0.5-0.8 part of zinc nitrate, 0.5-0.8 part of cerium nitrate, 3-5 parts of glacial acetic acid, 8-12 parts of distilled water, 30-40 parts of absolute ethyl alcohol, 0.2-0.3 part of surfactant and 600-1200 parts of granite. According to the antibacterial ceramic glaze for the wall and floor tiles and the using method of the glaze, titanium dioxide is modified and doped with related metal elements, so that the antibacterial property is achieved in a visible light area of the glaze, meanwhile, the components are scientifically and reasonably proportioned, the glaze is smooth, uniform in color and luster, good in dispersibility, acid and alkali resistant and wider in application range, the glaze is uniformly attached to the outside of a blank by an automatic process, the labor intensity is reduced while the working efficiency is improved, and the antibacterial ceramic glaze for the wall and floor tiles can enable the glaze of a product to have a self-cleaning function, achieve lasting and effective antifouling performance and have wide application prospects.
Description
Technical Field
The invention relates to the technical field of wall and floor tiles, in particular to an antibacterial ceramic glaze for wall and floor tiles and a using method of the glaze.
Background
The ceramic tile with the water absorption rate of more than 10 percent is generally called as an inner wall tile in the market, is widely used for wall decoration of buildings such as residential houses, hotels, restaurants, public places and the like, is a main product for indoor decoration, is called as a ceramic tile with the water absorption rate of less than 0.5 percent, namely a vitrified tile, is mostly used for floor paving and is subjected to surface polishing treatment, so the polished tile is also called as a polished tile, is widely used for ground decoration of various buildings and is also a main product for indoor decoration, one part of the ceramic tile with the water absorption rate of between 0.5 and 10 percent is used for outer wall decoration, and the other part of the ceramic tile is mainly used for decoration of indoor ground, is mostly used in toilets and is matched with the inner wall tile for use.
The inorganic antibacterial materials are widely used in the prior art, and are divided into metal ion type inorganic antibacterial materials and photocatalytic type inorganic antibacterial materials, the metal ion type inorganic antibacterial materials generally use Ag ions as antibacterial carriers, the cost of the Ag ions is high, and the Ag ions are easy to change color, so the application of the Ag ions is greatly limited.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides an antibacterial ceramic glaze for wall and floor tiles and a using method of the glaze, which have the advantages of improving the antibacterial capability of the wall and floor tiles and multi-station automatic glazing, and solves the problems that the cost of Ag ions is high and the color of the Ag ions is easy to change because the Ag ions are generally used as antibacterial carriers in metal ion type inorganic antibacterial materials, so the application of the Ag ions is greatly limited, titanium dioxide is directly added in the prior art, the mixture has no corresponding physical change and is equivalent to pure titanium dioxide, however, the research finds that the pure titanium dioxide has no antibacterial property under visible light.
(II) technical scheme
In order to achieve the purposes of improving the antibacterial capability of the wall and floor tiles and multi-station automatic glazing, the invention provides the following technical scheme: the processing equipment comprises (1), (2), (3), (4), (5), (6), (7), (8), (9), (10), (11) and (12), wherein the inside of (1) is fixedly connected with (2), the left end of the top of (1) is fixedly connected with (3), the inside of (3) is movably connected with (4), the right end of the bottom of (4) and the opposite side of the right end of the top of (1) are respectively movably connected with the two ends of (5), the top of (4) is fixedly installed with (6), the middle part of the top of (4) is movably connected with (7), the outsides of the driving shafts of (7) and (6) are fixedly connected with (8), the outside of (8) is connected with (9), the outside of the top of (7) is fixedly installed with (10), and the one end of (7) is fixedly connected with (11) far away from (11), the left side of the (1) is fixedly connected with a (12).
Preferably, (1) including mesa and supporting leg, four supporting legs equidistance distribute in the bottom of mesa, the material mouth has been seted up at the middle part on mesa top.
Preferably, the number of (3) is two, and two (3) front and back symmetric distributions are at the left end at (1) top, and spacing hole has all been seted up to the inside of two (3), and the inside swing joint in spacing hole has the bearing.
Preferably, the left ends of the front surface and the back surface of the bearing (4) are fixedly connected with limiting rods, the limiting rods are fixedly connected with the bearing inside the bearing (3), and the left end of the top of the bearing (4) is provided with a rectangular through hole.
Preferably, the right end of the top of the mounting seat (1) and the right end of the bottom of the mounting seat (4) are both fixedly provided with two mounting seats which are movably connected with the mounting seats (5).
Preferably, a plurality of circular through holes are formed in the middle of the top end of the bearing (4) at equal intervals, the inside of each circular through hole is movably connected with a bearing, the bearings are fixedly connected with the bearing (7), and the circular through holes are distributed linearly at equal intervals.
Preferably, the (11) is rubber, and the number of the (10) is two.
The invention provides an antibacterial ceramic glaze for wall and floor tiles and a use method of the glaze, and the method comprises the following steps:
1) processing the antibacterial agent comprising titanium dioxide, zinc nitrate, cerium nitrate, glacial acetic acid, distilled water, absolute ethyl alcohol and a surfactant into glaze according to the mass fraction of 40-50 parts of titanium dioxide, 0.5-0.8 part of zinc nitrate, 0.5-0.8 part of cerium nitrate, 3-5 parts of glacial acetic acid, 8-12 parts of distilled water, 30-40 parts of absolute ethyl alcohol, 0.2-0.3 part of surfactant and 600-1200 parts of granite, and pouring the processed glaze into the interior of the step (12) in advance;
2) placing the blank to be processed outside the plurality of blanks (7) in sequence, starting the (10) to push the blanks (11) and (11) outwards to contact with the outer side of the blank to be processed and fixing the blank to be processed;
3) starting (5) to push outwards (4), rotating anticlockwise to enable the blank to be processed outside (7) to be immersed in the glaze pre-stored in the inner part (12), starting (6) to enable the blank to be processed outside (9) to drive the blank (7) to rotate, and enabling the blank to be processed outside (7) to rotate in the glaze to enable the glaze to be completely attached to the surface of the blank to be processed;
4) closing the step (6) and starting the step (5) to retract, enabling the glaze on the surface of the blank body to fall into the step (2), and taking down the blank body from the step (7) after the glaze is dried, thereby completing glazing of the blank body to be processed.
(III) advantageous effects
Compared with the prior art, the invention provides an antibacterial ceramic glaze for wall and floor tiles and a using method of the glaze, and the antibacterial ceramic glaze has the following beneficial effects:
1. the antibacterial ceramic glaze for wall and floor tiles and the use method of the glaze have the advantages that Ti02 is a very good photocatalytic antibacterial material, the photocatalytic activity is high, the stability is good, the glaze is harmless to human bodies, the cost is low and the like, zinc ions have a certain antibacterial effect, the cost is low, the color is stable, the toxicity is low, Ce is one of rare earth elements, the rare earth ions are used for the antibacterial material in the field of medicine for a long time due to safety and broad-spectrum antibacterial property, pure titanium dioxide has no antibacterial property under visible light, therefore, the photoresponse range of the pure titanium dioxide is expanded to the visible light region by doping metal ions so as to improve the quantum efficiency, and the titanium dioxide doped with zinc and cerium has the photocatalytic property in the visible light region. The glaze surface is smooth, the color is uniform, the dispersibility is good, the acid and alkali resistance is realized, and the application range is wider.
2. According to the antibacterial ceramic glaze for the wall and floor tiles and the using method of the glaze, granite is used as a granite waste material, lead is not contained, the granite waste material can replace feldspar and quartz raw materials to prepare ceramic glaze, the glaze which does not contain lead or is subjected to lead removal treatment is selected to have higher economic value, and meanwhile, resources are regenerated, titanium dioxide is obtained by performing impurity removal and innocent treatment on titanium waste residues, a large amount of titanium-containing waste residues are generated in a titanium production process, and a large amount of titanium dioxide and other metal salts are contained in the titanium waste residues and are directly used for producing the glaze after impurity removal and innocent treatment, so that comprehensive utilization of titanium industrial waste residues can be realized, the production cost is reduced, and the pollution to the environment is reduced.
Drawings
Fig. 1 is a front view of the novel structure of the present invention. In the figure: the device comprises a supporting platform 1, a recovery box 2, a supporting seat 3, a movable plate 4, a first electric push rod 5, a driving motor 6, a stand column 7, a driving wheel 8, a conveying belt 9, a second electric push rod 10, a fixing clamping arm 11 and a storage material 12.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows: an antibacterial ceramic glaze for wall and floor tiles and a using method of the glaze comprise the following steps:
1) processing the antibacterial agent comprising titanium dioxide, zinc nitrate, cerous nitrate, glacial acetic acid, distilled water, absolute ethyl alcohol and a surfactant into glaze according to the mass fraction of 40 parts of titanium dioxide, 0.5 part of zinc nitrate, 0.5 part of cerous nitrate, 3 parts of glacial acetic acid, 8 parts of distilled water, 30 parts of absolute ethyl alcohol, 0.2 part of surfactant and 600 parts of granite, and pouring the processed glaze into the interior of the step (12) in advance;
2) placing the blank to be processed outside the plurality of blanks (7) in sequence, starting the (10) to push the blanks (11) and (11) outwards to contact with the outer side of the blank to be processed and fixing the blank to be processed;
3) starting (5) to push outwards (4), rotating anticlockwise to enable the blank to be processed outside (7) to be immersed in the glaze pre-stored in the inner part (12), starting (6) to enable the blank to be processed outside (9) to drive the blank (7) to rotate, and enabling the blank to be processed outside (7) to rotate in the glaze to enable the glaze to be completely attached to the surface of the blank to be processed;
4) closing the step (6) and starting the step (5) to retract, enabling the glaze on the surface of the blank body to fall into the step (2), and taking down the blank body from the step (7) after the glaze is dried, thereby completing glazing of the blank body to be processed.
Example two: an antibacterial ceramic glaze for wall and floor tiles and a using method of the glaze comprise the following steps:
1) processing the antibacterial agent comprising titanium dioxide, zinc nitrate, cerous nitrate, glacial acetic acid, distilled water, absolute ethyl alcohol and a surfactant into glaze according to the mass fraction of 45 parts of titanium dioxide, 0.6 part of zinc nitrate, 0.6 part of cerous nitrate, 3 parts of glacial acetic acid, 10 parts of distilled water, 35 parts of absolute ethyl alcohol, 0.2 part of surfactant and 800 parts of granite, and pouring the processed glaze into the interior of the step (12) in advance;
2) placing the blank to be processed outside the plurality of blanks (7) in sequence, starting the (10) to push the blanks (11) and (11) outwards to contact with the outer side of the blank to be processed and fixing the blank to be processed;
3) starting (5) to push outwards (4), rotating anticlockwise to enable the blank to be processed outside (7) to be immersed in the glaze pre-stored in the inner part (12), starting (6) to enable the blank to be processed outside (9) to drive the blank (7) to rotate, and enabling the blank to be processed outside (7) to rotate in the glaze to enable the glaze to be completely attached to the surface of the blank to be processed;
4) closing the step (6) and starting the step (5) to retract, enabling the glaze on the surface of the blank body to fall into the step (2), and taking down the blank body from the step (7) after the glaze is dried, thereby completing glazing of the blank body to be processed.
Example three: an antibacterial ceramic glaze for wall and floor tiles and a using method of the glaze comprise the following steps:
1) the antibacterial agent comprises titanium dioxide, zinc nitrate, cerium nitrate, glacial acetic acid, distilled water, absolute ethyl alcohol and a surfactant, wherein the glaze is prepared by processing 50 parts of titanium dioxide, 0.8 part of zinc nitrate, 0.8 part of cerium nitrate, 5 parts of glacial acetic acid, 12 parts of distilled water, 40 parts of absolute ethyl alcohol, 0.3 part of surfactant and 1200 parts of granite according to the mass fraction, and the processed glaze is poured into the interior of the step (12) in advance;
2) placing the blank to be processed outside the plurality of blanks (7) in sequence, starting the (10) to push the blanks (11) and (11) outwards to contact with the outer side of the blank to be processed and fixing the blank to be processed;
3) starting (5) to push outwards (4), rotating anticlockwise to enable the blank to be processed outside (7) to be immersed in the glaze pre-stored in the inner part (12), starting (6) to enable the blank to be processed outside (9) to drive the blank (7) to rotate, and enabling the blank to be processed outside (7) to rotate in the glaze to enable the glaze to be completely attached to the surface of the blank to be processed;
4) closing the step (6) and starting the step (5) to retract, enabling the glaze on the surface of the blank body to fall into the step (2), and taking down the blank body from the step (7) after the glaze is dried, thereby completing glazing of the blank body to be processed.
The invention has the beneficial effects that: ti02 is a very good photocatalytic antibacterial material, has the advantages of high photocatalytic activity, good stability, no harm to human body, low cost and the like, zinc ions have a certain antibacterial effect, low cost, stable color and low toxicity, Ce is one of rare earth elements, the rare earth ions are used as antibacterial materials in the field of medicine for a long time due to safety and broad-spectrum antibacterial property, and pure titanium dioxide has no antibacterial property under visible light, so the photoresponse range of the pure titanium dioxide is expanded to a visible light region by doping metal ions to improve the quantum efficiency of the pure titanium dioxide, and the titanium dioxide doped with zinc and cerium has photocatalytic performance in the visible light region. Acid and alkali resistance, wider application range, the granite waste is used as the granite waste and does not contain lead, the granite waste can replace feldspar and quartz raw materials to prepare ceramic glaze, the glaze which does not contain lead or is subjected to lead removal treatment is higher in economic value, and simultaneously, resources are regenerated, the titanium dioxide is obtained by performing impurity removal and innocent treatment on titanium waste, in the titanium production process, a large amount of titanium-containing waste residue is generated, and a large amount of titanium dioxide and other metal salts are contained in the titanium waste residue and are directly used for producing the glaze after impurity removal and innocent treatment, so that the comprehensive utilization of titanium industrial waste residue can be realized, the production cost is reduced, the environmental pollution is reduced, the problem that the metal ion type inorganic antibacterial material generally uses Ag ions as antibacterial carriers, the cost of the Ag ions is high, the color of the Ag ions is easy to change is solved, the application of the Ag ions is greatly limited, the titanium dioxide is directly added in the prior art, there was no corresponding physical change in the mixture, corresponding to "pure" titanium dioxide, which, however, was found to be a problem of no antibacterial properties under visible light.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. The antibacterial ceramic glaze for the wall and floor tiles is characterized by comprising the following raw materials in parts by weight: the antibacterial agent comprises, by mass, 40-50 parts of titanium dioxide, 0.5-0.8 part of zinc nitrate, 0.5-0.8 part of cerium nitrate, 3-5 parts of glacial acetic acid, 8-12 parts of distilled water, 30-40 parts of absolute ethyl alcohol, 0.2-0.3 part of a surfactant and 600-1200 parts of granite.
2. An application method of antibacterial ceramic glaze for wall and floor tiles is characterized by comprising the following steps:
1) preparing a plurality of blank bodies to be processed, preparing a processing device, comprising (1), (2), (3), (4), (5), (6), (7), (8), (9), (10), (11) and (12), wherein the inside of (1) is fixedly connected with (2), the left end of the top of (1) is fixedly connected with (3), the inside of (3) is movably connected with (4), the right end of the bottom of (4) and the opposite side of the right end of the top of (1) are respectively movably connected with the two ends of (5), the top of (4) is fixedly installed with (6), the middle of the top of (4) is movably connected with (7), the outside of the driving shaft of (7) and (6) is fixedly connected with (8), the outside of (8) is connected with (9), the outside of the top of (7) is fixedly installed with (10), one end of the (11) far away from the (7) is fixedly connected with the (11), and the left side of the (1) is fixedly connected with the (12);
2) pouring the processed glaze into the interior of the blank body (12) in advance, then placing the blank body to be processed outside the blank bodies (7) in sequence, starting the blank body (10) to push outwards (11), contacting the blank body to be processed with the outer side of the blank body to be processed, fixing the blank body to be processed, starting the blank body (5) to push outwards (4), rotating anticlockwise to enable the blank body to be processed outside the blank body (7) to be immersed into the glaze material pre-stored in the interior of the blank body (12), starting the blank body (6) to enable the blank body (9) to drive the blank body (7) to rotate, enabling the blank body to be processed outside the blank body (7) to rotate in the glaze material, enabling the glaze material to be completely attached to the surface of the blank body to be processed, then closing the blank body (6) and starting the blank body (5) to retract, enabling the glaze material on the surface of the blank body to fall into the blank body (2), and taking down the blank body from the blank.
3. The use method of the antibacterial ceramic glaze for the wall and floor tiles is characterized by comprising the following steps: the material feeding device is characterized in that the material feeding device (1) comprises a table top and four supporting legs, wherein the four supporting legs are distributed at the bottom of the table top at equal intervals, and a material feeding port is formed in the middle of the top end of the table top.
4. The use method of the antibacterial ceramic glaze for the wall and floor tiles is characterized by comprising the following steps: the quantity of (3) is two, and two (3) front and back symmetric distributions are in the left end at (1) top, and spacing hole has all been seted up to the inside of two (3), and the inside swing joint in spacing hole has the bearing.
5. The use method of the antibacterial ceramic glaze for the wall and floor tiles is characterized by comprising the following steps: the equal fixedly connected with gag lever post of the left end at (4) front and the back, gag lever post and (3) inside bearing fixed connection, (4) the left end at top has seted up the rectangle through-hole.
6. The use method of the antibacterial ceramic glaze for the wall and floor tiles is characterized by comprising the following steps: the right-hand member of (1) top and the right-hand member of (4) bottom all fixed mounting have two mount pads, mount pad and (5) swing joint.
7. The use method of the antibacterial ceramic glaze for the wall and floor tiles is characterized by comprising the following steps: a plurality of circular through holes are formed in the middle of the top end of the bearing (4) at equal intervals, bearings are movably connected inside the circular through holes, the bearings are fixedly connected with the bearing (7), and the circular through holes are distributed linearly at equal intervals.
8. The use method of the antibacterial ceramic glaze for the wall and floor tiles is characterized by comprising the following steps: the (11) is rubber, and the number of the (10) is two.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010375201.5A CN112939458A (en) | 2020-05-07 | 2020-05-07 | Antibacterial ceramic glaze for wall and floor tiles and application method of glaze |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010375201.5A CN112939458A (en) | 2020-05-07 | 2020-05-07 | Antibacterial ceramic glaze for wall and floor tiles and application method of glaze |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113733302A (en) * | 2021-09-27 | 2021-12-03 | 阜阳市鑫源建材有限公司 | Preparation method of high-permeability clean water permeable brick |
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| US3868902A (en) * | 1972-07-29 | 1975-03-04 | Service Eng Ltd | Multi-station printing machine for ceramic ware |
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| CN113733302A (en) * | 2021-09-27 | 2021-12-03 | 阜阳市鑫源建材有限公司 | Preparation method of high-permeability clean water permeable brick |
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Application publication date: 20210611 |