CN112885593A - Heat treatment method for high-precision current sensor magnetic core - Google Patents

Heat treatment method for high-precision current sensor magnetic core Download PDF

Info

Publication number
CN112885593A
CN112885593A CN202110124954.3A CN202110124954A CN112885593A CN 112885593 A CN112885593 A CN 112885593A CN 202110124954 A CN202110124954 A CN 202110124954A CN 112885593 A CN112885593 A CN 112885593A
Authority
CN
China
Prior art keywords
magnetic core
minutes
magnetic field
heat treatment
magnetic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202110124954.3A
Other languages
Chinese (zh)
Inventor
黄剑威
曹前进
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Foshan Zhongyan Amorphous Technology Co ltd
Original Assignee
Foshan Zhongyan Amorphous Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Foshan Zhongyan Amorphous Technology Co ltd filed Critical Foshan Zhongyan Amorphous Technology Co ltd
Priority to CN202110124954.3A priority Critical patent/CN112885593A/en
Publication of CN112885593A publication Critical patent/CN112885593A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F41/00Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
    • H01F41/02Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets
    • H01F41/0206Manufacturing of magnetic cores by mechanical means
    • H01F41/0213Manufacturing of magnetic circuits made from strip(s) or ribbon(s)
    • H01F41/022Manufacturing of magnetic circuits made from strip(s) or ribbon(s) by winding the strips or ribbons around a coil
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R19/00Arrangements for measuring currents or voltages or for indicating presence or sign thereof
    • G01R19/0092Arrangements for measuring currents or voltages or for indicating presence or sign thereof measuring current only

Landscapes

  • Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Heat Treatment Of Articles (AREA)

Abstract

The invention discloses a heat treatment method for a magnetic core of a high-precision current sensor, which comprises the following steps: winding a nanocrystalline alloy strip into a magnetic core with a magnetic path length larger than 8 cm; placing the magnetic core in a vacuum environment, carrying out heat treatment at the temperature of 150-700 ℃ for 10-1200 minutes, and cooling the magnetic core subjected to heat treatment at normal temperature for 10-60 minutes; and step three, applying a transverse magnetic field to the magnetic core, wherein the duration time of the transverse magnetic field is 10-150 minutes, the magnetic field intensity of the transverse magnetic field is 50-1500 Gs, simultaneously preserving the heat at 150-500 ℃ for 10-120 minutes, and cooling the magnetic core after heat preservation for 10-60 minutes at normal temperature. The invention has the beneficial effects that: the initial permeability mu i of the nano gold alloy magnetic core is improved to be more than 180000, which is improved by 60 percent compared with the initial permeability of the existing nano crystal alloy product with the same magnetic field length of more than 8cm, thereby effectively improving the measurement precision level of the current sensor.

Description

Heat treatment method for high-precision current sensor magnetic core
Technical Field
The invention relates to the technical field of magnetic core heat treatment, in particular to a high-precision current sensor magnetic core heat treatment method.
Background
The power battery system is a core part of a new energy vehicle, wherein the SOC (state of charge) calculation of a battery pack is one of key technologies, and not only influences the accuracy of the endurance mileage, but also relates to the safety and the service life of the whole battery pack; the battery pack is prevented from being affected by overcharge and overdischarge, so that accurate determination of the SOC is very important, and the measurement accuracy of the current sensor is a direct factor for accurately determining the SOC.
At present, the initial magnetic permeability of the nano gold alloy magnetic core of the traditional current sensor on the market is insufficient, so that the measurement accuracy of the current sensor cannot meet the requirement well.
Disclosure of Invention
In order to solve the problems, the invention provides a heat treatment method for a high-precision current sensor magnetic core, which mainly solves the problem of insufficient initial permeability of a nano gold alloy magnetic core.
In order to solve the technical problems, the technical scheme of the invention is as follows:
a heat treatment method for a high-precision current sensor magnetic core comprises the following steps:
winding a nanocrystalline alloy strip into a magnetic core with a magnetic path length larger than 8 cm;
secondly, placing the magnetic core in a furnace, vacuumizing, carrying out heat treatment at 150-700 ℃ for 10-1200 minutes, and cooling the magnetic core subjected to heat treatment at normal temperature for 10-60 minutes;
and step three, applying a transverse magnetic field to the magnetic core, wherein the duration time of the transverse magnetic field is 10-150 minutes, the magnetic field intensity of the transverse magnetic field is 50-1500 Gs, simultaneously preserving the heat at 150-500 ℃ for 10-120 minutes, and cooling the magnetic core after heat preservation for 10-60 minutes at normal temperature.
The invention has the beneficial effects that: the initial permeability mu i of the nano gold alloy magnetic core is improved to be more than 180000, which is improved by 60 percent compared with the initial permeability of the existing nano crystal alloy product with the same magnetic field length of more than 8cm, thereby effectively improving the measurement precision level of the current sensor.
Drawings
FIG. 1 is a schematic illustration of the static hysteresis loop and the basic magnetization curve of a heat treated magnetic core;
fig. 2 is a schematic diagram of the basic magnetization curve and permeability curve of a heat-treated magnetic core.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention clearer and clearer, the following detailed description of the present invention is provided with reference to the accompanying drawings and detailed description. It is to be understood that the specific embodiments described herein are merely illustrative of the invention and are not limiting of the invention. It should be further noted that, for the convenience of description, only some but not all of the relevant aspects of the present invention are shown in the drawings.
The embodiment provides a heat treatment method for a high-precision current sensor magnetic core, which comprises the following steps:
winding a nanocrystalline alloy strip into a magnetic core with a magnetic path length larger than 8 cm;
secondly, placing the magnetic core in a furnace, vacuumizing, carrying out heat treatment at 150-700 ℃ for 10-1200 minutes, and cooling the magnetic core subjected to heat treatment at normal temperature for 10-60 minutes;
and step three, applying a transverse magnetic field to the magnetic core, wherein the duration time of the transverse magnetic field is 10-150 minutes, the magnetic field intensity of the transverse magnetic field is 50-1500 Gs, simultaneously preserving the heat at 150-500 ℃ for 10-120 minutes, and cooling the magnetic core after heat preservation for 10-60 minutes at normal temperature.
As shown in fig. 1 and 2, the initial permeability μ i of the nano-gold alloy magnetic core after the heat treatment is raised to 180000(180k) or more.
The initial permeability mu i of the nano gold alloy magnetic core after the heat treatment is improved to be more than 180000(180K), which is improved by 60 percent compared with the initial permeability of the conventional nano crystal alloy product with the same magnetic field length of more than 8cm, thereby effectively improving the measurement precision level of the current sensor.
The specific implementation principle is as follows:
the implementation principle and the process background of the invention refer to the specific magnetization process of a magnetic substance, and a transverse magnetic field corresponding to a corresponding product is provided in the production to enable the material to be magnetized in a reversible segment in three stages (reversible segment → part of reversible segment → completion of irreversible segment) from a zero magnetization state to a saturated magnetization curve, so that the magnetic domain structure and magnetic anisotropy are changed, and the magnetic permeability is further improved;
example one
Winding a nanocrystalline alloy strip into a magnetic core with a magnetic path length of 8 cm;
secondly, placing the magnetic core in a furnace, vacuumizing, carrying out heat treatment at 150 ℃ for 10 minutes, and cooling the magnetic core subjected to heat treatment for 10 minutes at normal temperature;
and step three, applying a transverse magnetic field to the magnetic core, wherein the duration time of the transverse magnetic field is 10 minutes, the magnetic field intensity of the transverse magnetic field is 50Gs, simultaneously preserving the heat at 150 ℃ for 10 minutes, and cooling the magnetic core after heat preservation for 10 minutes at normal temperature.
Example two
Winding a nanocrystalline alloy strip into a magnetic core with a magnetic path length of 8 cm;
secondly, placing the magnetic core in a furnace, vacuumizing, performing heat treatment at 700 ℃ for 1200 minutes, and cooling the magnetic core subjected to heat treatment for 60 minutes at normal temperature;
and step three, applying a transverse magnetic field to the magnetic core, wherein the duration time of the transverse magnetic field is 150 minutes, the magnetic field intensity of the transverse magnetic field is 1500Gs, simultaneously preserving the heat at 500 ℃ for 120 minutes, and cooling the magnetic core after heat preservation for 60 minutes at normal temperature.
Description of the test:
1. test results under different processes
Figure BDA0002923666990000041
Remarking: the materials, equipment and production batches used in the above tests are all quantitative, and the only variable is the annealing process.
The average value of initial permeability μ i obtained in the process of example one was 194K, and the average value of initial permeability μ i obtained in the process of example two was 164K.
Comparative process 1: only adopting the first step and the second step of the implementation process; the third process step is not implemented, and the average value of the obtained initial magnetic permeability mu i is 94K;
comparative process 2: adopting the first step and the second step of the implementation process; performing transverse magnetic field annealing at a temperature outside the range of 150-500 ℃ in the third step without changing other parameters, wherein the average value of the obtained initial permeability mu i is 114K;
comparative process 3: adopting the first step and the second step of the implementation process; performing transverse magnetic field annealing by adopting the magnetic field intensity outside the range of 50-1500 Gs in the process magnetic field intensity in the third step, wherein other parameters in the third step are unchanged, and the average value of the obtained initial magnetic permeability mu i is 112K;
comparative process 4: adopting the first step and the second step of the implementation process; and (3) carrying out transverse magnetic field annealing by adopting the process in the third step, wherein the transverse magnetic field duration is outside the interval of 10-15 minutes, other parameters in the third step are unchanged, and the average value of the obtained initial permeability mu i is 125K.
2. Example results of different test batches under one Process
Figure BDA0002923666990000042
Remarking: the process used in the tests is quantitative, and the same grade of material is adopted, and different test batches are tested
The above embodiments are only for illustrating the technical concept and features of the present invention, and the purpose thereof is to enable those skilled in the art to understand the contents of the present invention and implement the present invention accordingly, and not to limit the protection scope of the present invention accordingly. All equivalent changes or modifications made in accordance with the spirit of the present disclosure are intended to be covered by the scope of the present disclosure.

Claims (1)

1. A heat treatment method for a high-precision current sensor magnetic core is characterized by comprising the following steps:
winding a nanocrystalline alloy strip into a magnetic core with a magnetic path length larger than 8 cm;
secondly, placing the magnetic core in a furnace, vacuumizing, carrying out heat treatment at 150-700 ℃ for 10-1200 minutes, and cooling the magnetic core subjected to heat treatment in the furnace for 10-60 minutes;
and step three, applying a transverse magnetic field to the magnetic core, wherein the duration time of the transverse magnetic field is 10-150 minutes, the magnetic field intensity of the transverse magnetic field is 50-1500 Gs, simultaneously preserving the heat at 150-500 ℃ for 10-120 minutes, and cooling the magnetic core after heat preservation for 10-60 minutes at normal temperature.
CN202110124954.3A 2021-01-29 2021-01-29 Heat treatment method for high-precision current sensor magnetic core Pending CN112885593A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110124954.3A CN112885593A (en) 2021-01-29 2021-01-29 Heat treatment method for high-precision current sensor magnetic core

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110124954.3A CN112885593A (en) 2021-01-29 2021-01-29 Heat treatment method for high-precision current sensor magnetic core

Publications (1)

Publication Number Publication Date
CN112885593A true CN112885593A (en) 2021-06-01

Family

ID=76053569

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110124954.3A Pending CN112885593A (en) 2021-01-29 2021-01-29 Heat treatment method for high-precision current sensor magnetic core

Country Status (1)

Country Link
CN (1) CN112885593A (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105702408A (en) * 2016-03-15 2016-06-22 徐亚红 Preparation method of nanocrystalline soft magnetic material
CN109706290A (en) * 2019-01-14 2019-05-03 杭州曼德新材料有限公司 A kind of nanocrystalline magnet core magnetic field heat treatment process protected suitable for the leakage of A type
CN111354560A (en) * 2020-03-20 2020-06-30 杭州曼德新材料有限公司 Heat treatment method of common-mode inductance nanocrystalline magnetic core

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105702408A (en) * 2016-03-15 2016-06-22 徐亚红 Preparation method of nanocrystalline soft magnetic material
CN109706290A (en) * 2019-01-14 2019-05-03 杭州曼德新材料有限公司 A kind of nanocrystalline magnet core magnetic field heat treatment process protected suitable for the leakage of A type
CN111354560A (en) * 2020-03-20 2020-06-30 杭州曼德新材料有限公司 Heat treatment method of common-mode inductance nanocrystalline magnetic core

Similar Documents

Publication Publication Date Title
Mydosh et al. Electrical resistivity of Au Fe alloys in the spin-glass, mictomagnetic, and ferromagnetic regimes
CN107728072A (en) A kind of method for quick predicting of cycle life of lithium ion battery
Bucher et al. Magnetic susceptibility and specific heat of nearly ferromagnetic NiRh alloys
Lam et al. Self‐diffusion in silver at low temperatures
Paine et al. Effect of shape anisotropy on the coercive force of elongated single-magnetic-domain iron particles
Pyle et al. The Influence of Cyclic Plastic Strain on the Transient Dissolution Behavior of 18/8 Stainless Steel in 3.7 M H 2 SO 4
Goldman et al. Magnetostriction and order-disorder
CN105518441A (en) Method for locating a wafer in the ingot of same
CN101187065B (en) Method of identifying crystal defect region in monocrystalline silicon using metal contamination and heat treatment
CN113608132A (en) Method and system for determining residual capacity of lithium ion battery and storage medium
CN112885593A (en) Heat treatment method for high-precision current sensor magnetic core
CN108872867B (en) Battery self-discharge test method
Jones et al. Diffusion of indium into cadmium sulphide
CN116297229A (en) Method for detecting aging degree of crosslinked polyethylene insulating material based on yellow degree evolution
CN106383946A (en) Accelerated degradation model parameter estimation method
Witowski et al. Influence of the exchange interaction on far-infrared spin-flip resonances in zero-gap Hg 1− x Mn x Se
CN108089109B (en) Method for testing minority carrier lifetime in semiconductor silicon material
Kobayashi et al. Hysteresis scaling behavior in a remanent magnetization state
Dunifer et al. Electron Spin Resonance in Ferromagnetic Sc3+ x In Alloys
Mukaibo et al. Heat treatment for the stabilization of hydrogen and vacancies in electrodeposited Ni-Fe alloy films
CN109935530B (en) Experimental method for evaluating reliability of ferroelectric thin film in ferroelectric device
Bondaruk et al. Ion Track Etching Revisited: Influence of Aging on Parameters of Irradiated Polymers as Required for Advanced Devices
SU920860A1 (en) Method of obtaining predetermined value of magnet coercive force
CN115700395A (en) Method for improving efficiency of high-temperature irreversible flux loss test of neodymium iron boron
CN118011257A (en) Battery polarization distribution nondestructive testing method and battery rapid classification method

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20210601