CN112876274A - Production process of carbon/carbon composite material crucible prefabricated part - Google Patents
Production process of carbon/carbon composite material crucible prefabricated part Download PDFInfo
- Publication number
- CN112876274A CN112876274A CN202110179347.7A CN202110179347A CN112876274A CN 112876274 A CN112876274 A CN 112876274A CN 202110179347 A CN202110179347 A CN 202110179347A CN 112876274 A CN112876274 A CN 112876274A
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 88
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 83
- 239000002131 composite material Substances 0.000 title claims abstract description 27
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 10
- 239000004744 fabric Substances 0.000 claims abstract description 70
- 229920000049 Carbon (fiber) Polymers 0.000 claims abstract description 66
- 239000004917 carbon fiber Substances 0.000 claims abstract description 66
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims abstract description 60
- 239000002121 nanofiber Substances 0.000 claims abstract description 32
- 238000000034 method Methods 0.000 claims abstract description 25
- 238000001035 drying Methods 0.000 claims abstract description 22
- 238000002791 soaking Methods 0.000 claims abstract description 21
- 238000009941 weaving Methods 0.000 claims abstract description 17
- 239000003822 epoxy resin Substances 0.000 claims abstract description 15
- 239000002105 nanoparticle Substances 0.000 claims abstract description 14
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 14
- 238000004804 winding Methods 0.000 claims abstract description 13
- 239000002904 solvent Substances 0.000 claims abstract description 10
- 238000002360 preparation method Methods 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 238000013329 compounding Methods 0.000 claims abstract description 7
- 238000005470 impregnation Methods 0.000 claims description 30
- 239000000243 solution Substances 0.000 claims description 20
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 230000008569 process Effects 0.000 claims description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 8
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims description 8
- 238000007598 dipping method Methods 0.000 claims description 6
- 239000005543 nano-size silicon particle Substances 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 5
- 235000012239 silicon dioxide Nutrition 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 239000002059 nanofabric Substances 0.000 claims description 2
- 238000000151 deposition Methods 0.000 abstract description 13
- 230000008021 deposition Effects 0.000 abstract description 12
- 239000000463 material Substances 0.000 abstract description 12
- 238000000280 densification Methods 0.000 abstract description 7
- 238000007740 vapor deposition Methods 0.000 abstract description 6
- 125000004432 carbon atom Chemical group C* 0.000 abstract description 5
- 239000003575 carbonaceous material Substances 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 description 14
- 230000000052 comparative effect Effects 0.000 description 11
- 239000011229 interlayer Substances 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 239000012159 carrier gas Substances 0.000 description 5
- 239000010949 copper Substances 0.000 description 4
- 239000010410 layer Substances 0.000 description 4
- 229910002804 graphite Inorganic materials 0.000 description 3
- 239000010439 graphite Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 229910021421 monocrystalline silicon Inorganic materials 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 239000002356 single layer Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 2
- 238000005229 chemical vapour deposition Methods 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 238000005137 deposition process Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 2
- 230000008595 infiltration Effects 0.000 description 2
- 238000001764 infiltration Methods 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000002035 prolonged effect Effects 0.000 description 2
- 239000002296 pyrolytic carbon Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 2
- KUBDPQJOLOUJRM-UHFFFAOYSA-N 2-(chloromethyl)oxirane;4-[2-(4-hydroxyphenyl)propan-2-yl]phenol Chemical compound ClCC1CO1.C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 KUBDPQJOLOUJRM-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000000861 blow drying Methods 0.000 description 1
- 238000003763 carbonization Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000001513 hot isostatic pressing Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 230000003137 locomotive effect Effects 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 238000007719 peel strength test Methods 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 229920002239 polyacrylonitrile Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 238000005019 vapor deposition process Methods 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/71—Ceramic products containing macroscopic reinforcing agents
- C04B35/78—Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
- C04B35/80—Fibres, filaments, whiskers, platelets, or the like
- C04B35/83—Carbon fibres in a carbon matrix
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/77—Density
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Composite Materials (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Woven Fabrics (AREA)
Abstract
Description
Claims (10)
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CN202110179347.7A CN112876274B (en) | 2021-02-07 | 2021-02-07 | Production process of carbon/carbon composite material crucible prefabricated part |
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CN202110179347.7A CN112876274B (en) | 2021-02-07 | 2021-02-07 | Production process of carbon/carbon composite material crucible prefabricated part |
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CN112876274B CN112876274B (en) | 2022-02-25 |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112759409A (en) * | 2021-02-07 | 2021-05-07 | 内蒙古中晶科技研究院有限公司 | Carbon/carbon composite material vapor deposition process |
CN113373505A (en) * | 2021-06-30 | 2021-09-10 | 内蒙古中晶科技研究院有限公司 | Single crystal furnace thermal field heat preservation cylinder and preparation method thereof |
CN113457280A (en) * | 2021-07-01 | 2021-10-01 | 杭州净自在环境科技有限公司 | Sugarcoated haws string type antibacterial and antiviral filter screen and manufacturing process thereof |
CN113896561A (en) * | 2021-11-18 | 2022-01-07 | 杭州幄肯新材料科技有限公司 | Liquid phase-vapor deposition carbon fiber/carbon composite thermal field material and preparation method thereof |
CN114920574A (en) * | 2022-06-07 | 2022-08-19 | 醴陵市东方电瓷电器有限公司 | Method for preparing large-size carbon-carbon crucible by three-dimensional weaving of carbon fibers |
WO2023124269A1 (en) * | 2021-12-30 | 2023-07-06 | 隆基绿能科技股份有限公司 | High-temperature-resistant carbon-carbon composite body and production method therefor, and carbon fiber prefab |
CN117265641A (en) * | 2023-11-20 | 2023-12-22 | 内蒙古鼎泰万邦新材料有限公司 | Braided crucible preform and manufacturing method |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2005262391A (en) * | 2004-03-18 | 2005-09-29 | Misuzu Kogyo:Kk | Composite material composed of nano carbon and carbonaceous second filler and its manufacturing method |
CN101157564A (en) * | 2007-09-13 | 2008-04-09 | 北京航空航天大学 | Method for reinforcing charcoal/charcoal component by charcoal nano-fibre |
CN101311334A (en) * | 2008-03-03 | 2008-11-26 | 湖南金博复合材料科技有限公司 | Single-crystal furnace guide shell and production process thereof |
CN101319353A (en) * | 2008-05-20 | 2008-12-10 | 湖南金博复合材料科技有限公司 | Carbon/carbon composite material crucible pot and preparing technique thereof |
CN102257221A (en) * | 2008-10-15 | 2011-11-23 | 默克尔复合技术公司 | Composite structural elements and method of making same |
CN103496997A (en) * | 2013-09-06 | 2014-01-08 | 航天材料及工艺研究所 | Preparation method for carbon/carbon composite material thermal-insulation hard felt |
CN103922780A (en) * | 2014-04-09 | 2014-07-16 | 中国科学院山西煤炭化学研究所 | Preparation method of nano clay reinforced carbon/carbon composite |
-
2021
- 2021-02-07 CN CN202110179347.7A patent/CN112876274B/en active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2005262391A (en) * | 2004-03-18 | 2005-09-29 | Misuzu Kogyo:Kk | Composite material composed of nano carbon and carbonaceous second filler and its manufacturing method |
CN101157564A (en) * | 2007-09-13 | 2008-04-09 | 北京航空航天大学 | Method for reinforcing charcoal/charcoal component by charcoal nano-fibre |
CN101311334A (en) * | 2008-03-03 | 2008-11-26 | 湖南金博复合材料科技有限公司 | Single-crystal furnace guide shell and production process thereof |
CN101319353A (en) * | 2008-05-20 | 2008-12-10 | 湖南金博复合材料科技有限公司 | Carbon/carbon composite material crucible pot and preparing technique thereof |
CN102257221A (en) * | 2008-10-15 | 2011-11-23 | 默克尔复合技术公司 | Composite structural elements and method of making same |
CN103496997A (en) * | 2013-09-06 | 2014-01-08 | 航天材料及工艺研究所 | Preparation method for carbon/carbon composite material thermal-insulation hard felt |
CN103922780A (en) * | 2014-04-09 | 2014-07-16 | 中国科学院山西煤炭化学研究所 | Preparation method of nano clay reinforced carbon/carbon composite |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112759409A (en) * | 2021-02-07 | 2021-05-07 | 内蒙古中晶科技研究院有限公司 | Carbon/carbon composite material vapor deposition process |
CN112759409B (en) * | 2021-02-07 | 2022-01-14 | 内蒙古中晶科技研究院有限公司 | Carbon/carbon composite material vapor deposition process |
CN113373505A (en) * | 2021-06-30 | 2021-09-10 | 内蒙古中晶科技研究院有限公司 | Single crystal furnace thermal field heat preservation cylinder and preparation method thereof |
CN113373505B (en) * | 2021-06-30 | 2022-09-13 | 内蒙古中晶科技研究院有限公司 | Single crystal furnace thermal field heat preservation cylinder and preparation method thereof |
CN113457280A (en) * | 2021-07-01 | 2021-10-01 | 杭州净自在环境科技有限公司 | Sugarcoated haws string type antibacterial and antiviral filter screen and manufacturing process thereof |
CN113896561A (en) * | 2021-11-18 | 2022-01-07 | 杭州幄肯新材料科技有限公司 | Liquid phase-vapor deposition carbon fiber/carbon composite thermal field material and preparation method thereof |
CN113896561B (en) * | 2021-11-18 | 2022-09-16 | 杭州幄肯新材料科技有限公司 | Liquid phase-vapor deposition carbon fiber/carbon composite thermal field material and preparation method thereof |
WO2023124269A1 (en) * | 2021-12-30 | 2023-07-06 | 隆基绿能科技股份有限公司 | High-temperature-resistant carbon-carbon composite body and production method therefor, and carbon fiber prefab |
CN114920574A (en) * | 2022-06-07 | 2022-08-19 | 醴陵市东方电瓷电器有限公司 | Method for preparing large-size carbon-carbon crucible by three-dimensional weaving of carbon fibers |
CN117265641A (en) * | 2023-11-20 | 2023-12-22 | 内蒙古鼎泰万邦新材料有限公司 | Braided crucible preform and manufacturing method |
CN117265641B (en) * | 2023-11-20 | 2024-01-30 | 内蒙古鼎泰万邦新材料有限公司 | Braided crucible preform and manufacturing method |
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Publication number | Publication date |
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CN112876274B (en) | 2022-02-25 |
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GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
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Denomination of invention: Production process of a carbon/carbon composite crucible preform Effective date of registration: 20230111 Granted publication date: 20220225 Pledgee: Hohhot Branch of Shanghai Pudong Development Bank Co.,Ltd. Pledgor: Inner Mongolia Zhongjing Technology Research Institute Co.,Ltd. Registration number: Y2023150000009 |
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Granted publication date: 20220225 Pledgee: Hohhot Branch of Shanghai Pudong Development Bank Co.,Ltd. Pledgor: Inner Mongolia Zhongjing Technology Research Institute Co.,Ltd. Registration number: Y2023150000009 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Production process of a carbon/carbon composite crucible preform Granted publication date: 20220225 Pledgee: Hohhot Branch of Shanghai Pudong Development Bank Co.,Ltd. Pledgor: Inner Mongolia Zhongjing Technology Research Institute Co.,Ltd. Registration number: Y2024150000045 |