CN112853762A - Novel fluffy soft polyester fabric finishing agent and production process thereof - Google Patents
Novel fluffy soft polyester fabric finishing agent and production process thereof Download PDFInfo
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- CN112853762A CN112853762A CN202110191203.3A CN202110191203A CN112853762A CN 112853762 A CN112853762 A CN 112853762A CN 202110191203 A CN202110191203 A CN 202110191203A CN 112853762 A CN112853762 A CN 112853762A
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- silicone oil
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- fluffy
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/65—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing epoxy groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a novel fluffy soft polyester fabric finishing agent and a production process thereof. Comprises a component A which comprises fluffy silicone oil with the weight portion of 35-50; 30-40 parts of polybasic copolymerized silicone oil; and amino silicone oil, its weight portion is 20-25; a component B which is a surfactant; a component C which is glacial acetic acid; and water. The invention can well solve the problem that the softness, the smoothness and the thickness of the polyester fabric can not coexist, so that the polyester fabric is thick, has smoothness and thickness and has certain elasticity.
Description
Technical Field
The invention relates to the technical field of textile processing, in particular to a novel fluffy soft type polyester fabric finishing agent and a production process thereof.
Background
The prior polyester fabric generally has good softness, but has poor smoothness and thickness. The conventional organic silicon products can treat polyester fabrics to be very soft, but have poor fluffiness and thickness, and if the polyester polyether products are used for treating the fabrics, the smoothness can not be achieved.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides a novel fluffy soft type polyester fabric finishing agent and a production process thereof.
In order to solve the technical problems, the invention is solved by the following technical scheme:
a novel fluffy soft type polyester fabric finishing agent comprises
The component A comprises fluffy silicone oil, and the weight part of the fluffy silicone oil is 35-50 parts; 30-40 parts of polybasic copolymerized silicone oil; and amino silicone oil, its weight portion is 20-25;
a component B which is a surfactant;
a component C which is glacial acetic acid; and water.
In the above technical scheme, preferably, the multipolymer silicone oil is terpolymer modified organic silicone oil.
In the above technical scheme, preferably, the ternary polymerization modified silicone oil includes polyether amine, amino-terminated polyoxypropylene ether and amino-terminated polyoxyethylene ether, and the molecular structure contains ether bonds.
In the above technical solution, preferably, the structural formula of the polyether amine is as follows:
the molecular formula is as follows: c3H10N2O
Molecular weight: 90.1243
CAS NO：9046-10-0。
In the above technical solution, preferably, the structural formula of the multipolymer silicone oil is as follows:
molecular weight: 4K-20K.
In the technical scheme, preferably, the glacial acetic acid is high-concentration glacial acetic acid, the concentration of the glacial acetic acid is 99%, and the weight part of the glacial acetic acid is 2% -4% of the total weight of the component A.
In the above technical scheme, preferably, the weight part of the surfactant is 10% -30% of the weight part of the amino silicone oil.
The production process of the novel fluffy soft polyester fabric finishing agent comprises the following steps:
a. preparing a component A: mixing fluffy silicone oil, multi-component copolymerized silicone oil and amino silicone oil in an emulsifying pot according to the metering requirement, and stirring to prepare a component A;
b. adding a surfactant into the component A according to the metering requirement in the stirring process;
c. adding glacial acetic acid according to the metering requirement in the stirring process;
d. and slowly adding water for emulsification in the stirring process until the emulsion is completely uniform and transparent in appearance, so as to prepare the novel fluffy soft type polyester fabric finishing agent.
In the above technical solution, preferably, the temperature of the emulsifying pot is 30-50 ℃, and the stirring speed of the emulsifying pot is 110-.
In the above technical scheme, preferably, the emulsifying time is 30-50 minutes.
The invention has the beneficial effects that:
the invention can well solve the problem that the softness, the smoothness and the thickness of the polyester fabric can not coexist, so that the polyester fabric is thick, has smoothness and thickness and has certain elasticity.
Detailed Description
The invention is described in further detail below by means of specific embodiments:
example 1:
a novel fluffy soft type polyester fabric finishing agent comprises
The component A comprises fluffy silicone oil, and the weight part of the fluffy silicone oil is 35 parts; 40 parts of multipolymer silicone oil, namely 40 parts of terpolymer modified organic silicone oil; 25 parts of amino silicone oil;
and the component B is a surfactant, and the weight part of the surfactant is 10% of that of the amino silicone oil.
The component C is glacial acetic acid which is high-concentration glacial acetic acid, the concentration of the glacial acetic acid is 99%, and the weight part of the glacial acetic acid is 2% of the total weight of the component A; and water.
The production process of the novel fluffy soft polyester fabric finishing agent comprises the following steps:
a. preparing a component A: mixing fluffy silicone oil, multi-component copolymerized silicone oil and amino silicone oil in an emulsifying pot according to the metering requirement, and stirring to prepare a component A;
b. adding a surfactant into the component A according to the metering requirement in the stirring process;
c. adding glacial acetic acid according to the metering requirement in the stirring process;
d. and slowly adding water for emulsification in the stirring process until the emulsion is completely uniform and transparent in appearance, so as to prepare the novel fluffy soft type polyester fabric finishing agent.
In the preparation process, the temperature of the emulsifying pot is 30 ℃, the stirring speed is 110 r/min, and the emulsifying time is 30 min.
The silicone oil with a special structure can increase the thickness of the product, does not affect the softness and smoothness of the original product, mainly enhances the thickness and generates chemical reaction when the fabric is shaped at high temperature, so that the fabric becomes smooth and elastic.
The silicone oil with the special structure adopts multi-component copolymerized silicone oil, and is the ternary copolymerized modified silicone oil which is successfully developed through an organic silicon modification technology on the basis of the most advanced ternary copolymerized amino silicone oil at present. The novel modified organic silicon fabric has a brand-new modified organic silicon chemical structure and can give full, fluffy and thickened handfeel to the fabric by matching with double modified functional groups. The silicone oil mainly adopts special polyether ammonia containing various functional groups, amino-terminated polyoxypropylene ether, amino-terminated polyoxyethylene ether and the like, and the molecular structure contains ether bonds.
The structure of such polyether amines is as follows:
structural formula (xvi):
the molecular formula is as follows: c3H10N2O
Molecular weight: 90.1243
CAS NO：9046-10-0
Structure the structure of such multipolymer silicone oil is as follows:
molecular weight: 4K to 20K.
Example 2:
a novel fluffy soft type polyester fabric finishing agent comprises
The component A comprises 50 parts of fluffy silicone oil; 30 parts of multipolymer silicone oil which is ternary polymerization modified organic silicone oil; and 20 parts of amino silicone oil;
and the component B is a surfactant, and the weight part of the surfactant is 30% of that of the amino silicone oil.
The component C is glacial acetic acid which is high-concentration glacial acetic acid, the concentration of the glacial acetic acid is 99%, and the weight part of the glacial acetic acid is 4% of the total weight of the component A; and water.
The production process of the novel fluffy soft polyester fabric finishing agent comprises the following steps:
a. preparing a component A: mixing fluffy silicone oil, multi-component copolymerized silicone oil and amino silicone oil in an emulsifying pot according to the metering requirement, and stirring to prepare a component A;
b. adding a surfactant into the component A according to the metering requirement in the stirring process;
c. adding glacial acetic acid according to the metering requirement in the stirring process;
d. and slowly adding water for emulsification in the stirring process until the emulsion is completely uniform and transparent in appearance, so as to prepare the novel fluffy soft type polyester fabric finishing agent.
In the preparation process, the temperature of the emulsifying pot is 50 ℃, the stirring speed is 130 r/min, and the emulsifying time is 50 min.
The silicone oil with a special structure can increase the thickness of the product, does not affect the softness and smoothness of the original product, mainly enhances the thickness and generates chemical reaction when the fabric is shaped at high temperature, so that the fabric becomes smooth and elastic.
The silicone oil with the special structure adopts multi-component copolymerized silicone oil, and is the ternary copolymerized modified silicone oil which is successfully developed through an organic silicon modification technology on the basis of the most advanced ternary copolymerized amino silicone oil at present. The novel modified organic silicon fabric has a brand-new modified organic silicon chemical structure and can give full, fluffy and thickened handfeel to the fabric by matching with double modified functional groups. The silicone oil mainly adopts special polyether ammonia containing various functional groups, amino-terminated polyoxypropylene ether, amino-terminated polyoxyethylene ether and the like, and the molecular structure contains ether bonds.
The structure of such polyether amines is as follows:
structural formula (xvi):
the molecular formula is as follows: c3H10N2O
Molecular weight: 90.1243
CAS NO：9046-10-0
Structure the structure of such multipolymer silicone oil is as follows:
molecular weight: 4K to 20K.
Example 3:
a novel fluffy soft type polyester fabric finishing agent comprises
The component A comprises 40 parts of fluffy silicone oil; the multielement copolymerized silicone oil is ternary copolymerized modified organic silicone oil, and the weight part of the multielement copolymerized silicone oil is 37 parts; and 23 parts of amino silicone oil;
and the component B is a surfactant, and the weight part of the surfactant is 20% of that of the amino silicone oil.
The component C is glacial acetic acid which is high-concentration glacial acetic acid, the concentration of the glacial acetic acid is 99%, and the weight part of the glacial acetic acid is 3% of the total weight of the component A; and water.
The production process of the novel fluffy soft polyester fabric finishing agent comprises the following steps:
a. preparing a component A: mixing fluffy silicone oil, multi-component copolymerized silicone oil and amino silicone oil in an emulsifying pot according to the metering requirement, and stirring to prepare a component A;
b. adding a surfactant into the component A according to the metering requirement in the stirring process;
c. adding glacial acetic acid according to the metering requirement in the stirring process;
d. and slowly adding water for emulsification in the stirring process until the emulsion is completely uniform and transparent in appearance, so as to prepare the novel fluffy soft type polyester fabric finishing agent.
In the preparation process, the temperature of the emulsifying pot is 40 ℃, the stirring speed is 120 r/min, and the emulsifying time is 40 min.
The silicone oil with a special structure can increase the thickness of the product, does not affect the softness and smoothness of the original product, mainly enhances the thickness and generates chemical reaction when the fabric is shaped at high temperature, so that the fabric becomes smooth and elastic.
The silicone oil with the special structure adopts multi-component copolymerized silicone oil, and is the ternary copolymerized modified silicone oil which is successfully developed through an organic silicon modification technology on the basis of the most advanced ternary copolymerized amino silicone oil at present. The novel modified organic silicon fabric has a brand-new modified organic silicon chemical structure and can give full, fluffy and thickened handfeel to the fabric by matching with double modified functional groups. The silicone oil mainly adopts special polyether ammonia containing various functional groups, amino-terminated polyoxypropylene ether, amino-terminated polyoxyethylene ether and the like, and the molecular structure contains ether bonds.
The structure of such polyether amines is as follows:
structural formula (xvi):
the molecular formula is as follows: c3H10N2O
Molecular weight: 90.1243
CAS NO：9046-10-0
Structure the structure of such multipolymer silicone oil is as follows:
molecular weight: 4K to 20K.
The above examples are only intended to illustrate the technical solution of the present invention, but not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and such modifications or substitutions do not depart from the spirit and scope of the corresponding technical solutions of the embodiments of the present invention.
Claims (10)
1. Novel fluffy soft type polyester fabric finishing agent is characterized in that: comprises that
The component A comprises fluffy silicone oil, and the weight part of the fluffy silicone oil is 35-50 parts; 30-40 parts of polybasic copolymerized silicone oil; and amino silicone oil, its weight portion is 20-25;
a component B which is a surfactant;
a component C which is glacial acetic acid; and
and (3) water.
2. The novel fluffy and soft type polyester fabric finishing agent of claim 1, characterized in that: the multielement copolymerized silicone oil is ternary copolymerized modified organic silicone oil.
3. The novel fluffy and soft type polyester fabric finishing agent of claim 2, characterized in that: the ternary polymerization modified organic silicone oil comprises polyether ammonia, amino-terminated polyoxypropylene ether and amino-terminated polyoxyethylene ether, and the molecular structure of the ternary polymerization modified organic silicone oil contains ether bonds.
4. The novel fluffy and soft type polyester fabric finishing agent of claim 3, characterized in that: the structural formula of the polyether ammonia is as follows:
the molecular formula is as follows: c3H10N2O
Molecular weight: 90.1243
CAS NO：9046-10-0。
5. Novel fluffy soft type polyester fabric finishing agent according to any of claims 1-4, characterized in that: the structural formula of the multipolymer silicone oil is as follows:
molecular weight: 4K-20K.
6. The novel fluffy and soft type polyester fabric finishing agent of claim 1, characterized in that: the glacial acetic acid is high-concentration glacial acetic acid, the concentration of the glacial acetic acid is 99%, and the weight part of the glacial acetic acid is 2% -4% of the total weight of the component A.
7. The novel fluffy and soft type polyester fabric finishing agent of claim 1, characterized in that: the weight part of the surfactant is 10-30% of the weight part of the amino silicone oil.
8. The production process of the novel fluffy soft polyester fabric finishing agent is characterized by comprising the following steps:
a. preparing a component A: mixing fluffy silicone oil, multi-component copolymerized silicone oil and amino silicone oil in an emulsifying pot according to the metering requirement, and stirring to prepare a component A;
b. adding a surfactant into the component A according to the metering requirement in the stirring process;
c. adding glacial acetic acid according to the metering requirement in the stirring process;
d. and slowly adding water for emulsification in the stirring process until the emulsion is completely uniform and transparent in appearance, so as to prepare the novel fluffy soft type polyester fabric finishing agent.
9. The production process of the novel fluffy soft type polyester fabric finishing agent according to claim 7, characterized in that: the temperature of the emulsifying pot is 30-50 ℃, and the stirring speed of the emulsifying pot is 110-130 r/min.
10. The production process of the novel fluffy soft type polyester fabric finishing agent according to claim 7, characterized in that: the emulsifying time is 30-50 minutes.
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| CN202110191203.3A CN112853762A (en) | 2021-02-20 | 2021-02-20 | Novel fluffy soft polyester fabric finishing agent and production process thereof |
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| CN202110191203.3A CN112853762A (en) | 2021-02-20 | 2021-02-20 | Novel fluffy soft polyester fabric finishing agent and production process thereof |
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Citations (9)
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|---|---|---|---|---|
| CN102644200A (en) * | 2012-05-04 | 2012-08-22 | 浙江润禾有机硅新材料有限公司 | Super-soft finishing agent of silicone oil |
| CN104086779A (en) * | 2014-07-02 | 2014-10-08 | 佛山市传化富联精细化工有限公司 | Super-soft/smooth block silicon oil and preparation method thereof |
| CN104650363A (en) * | 2015-02-05 | 2015-05-27 | 南通斯恩特纺织科技有限公司 | Preparation method of hyperbranched ternary polymerization organic silicon |
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| CN112482031A (en) * | 2020-11-27 | 2021-03-12 | 苏州联胜化学有限公司 | Fluffy elastic silicone oil for terylene and preparation method thereof |
-
2021
- 2021-02-20 CN CN202110191203.3A patent/CN112853762A/en active Pending
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Application publication date: 20210528 |