CN112852529A - Formula of wire drawing oil - Google Patents
Formula of wire drawing oil Download PDFInfo
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- CN112852529A CN112852529A CN202110098576.6A CN202110098576A CN112852529A CN 112852529 A CN112852529 A CN 112852529A CN 202110098576 A CN202110098576 A CN 202110098576A CN 112852529 A CN112852529 A CN 112852529A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/05—Metals; Alloys
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/10—Compounds containing silicon
- C10M2201/105—Silica
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
- C10M2207/401—Fatty vegetable or animal oils used as base material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/064—Di- and triaryl amines
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
- C10M2229/04—Siloxanes with specific structure
- C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
Abstract
The invention discloses a formula of drawing oil, relating to the field of drawing oil, comprising 40-55 parts by mass of vegetable cottonseed oil; 20-30 parts of yellow mineral oil; 13-29 parts by mass of coconut oil; 2-5 parts of polyethylene glycol; 6-9 parts of an antioxidant; 4-7 parts of a bactericide; 2-6 parts of modified organic silicon defoaming agent; 4-8 parts of benzotriazole. The base oil used in the invention is environment-friendly oil, so that the environment is less damaged, the second three oil products have good mixed lubrication effect and less damage to human bodies, the used antioxidant can avoid the conditions of blackening, discoloration and the like caused by the combination of a large amount of oxygen and copper in the production process, the surface quality of copper is improved, the bactericide can inhibit bacterial growth and play a role in protecting other metals of copper, and the modified organic silicon defoamer can effectively eliminate foam, so that the wire drawing oil achieves good cleaning performance, bright outgoing lines, mold protection and the like.
Description
Technical Field
The invention relates to the field of drawing oil, in particular to a formula of drawing oil.
Background
The wire drawing oil is prepared by blending high-performance vulcanized lard oil and vulcanized fatty acid ester serving as main agents, is used for drawing wires of copper, aluminum, stainless steel and the like, has excellent extreme pressure abrasion resistance, cannot cause galling and strain of workpieces, improves the smoothness, and effectively prolongs the service life of a die.
Sulfuric acid or caustic soda is added into the existing wire drawing oil, so that corrosion of copper and generation of compounds are caused to a certain extent, and bacteria generated in the wire drawing oil can cause scaling and blackening of copper after contacting with the copper in production, and the like, so that the surface quality of the copper is influenced.
Disclosure of Invention
The invention aims to: the formula of the wire drawing oil is provided in order to solve the problems that sulfuric acid or caustic soda is added into the formula of the existing wire drawing oil, so that copper corrosion and compound generation are caused to a certain extent, bacteria generated in the wire drawing oil can cause scaling and blackening of copper after contacting with the copper in production, and the like, and the surface quality of the copper is affected.
In order to achieve the purpose, the invention provides the following technical scheme: the formula of the drawing oil comprises 40-55 parts by mass of vegetable cottonseed oil; 20-30 parts of yellow mineral oil; 13-29 parts by mass of coconut oil; 2-5 parts of polyethylene glycol; 6-9 parts of an antioxidant; 4-7 parts of a bactericide; 2-6 parts of modified organic silicon defoaming agent; 4-8 parts of benzotriazole.
Preferably, the antioxidant is a mixture of a p-phenylenediamine antioxidant and a phenylpropazole antioxidant, wherein the ratio of the p-phenylenediamine antioxidant to the phenylpropazole antioxidant is 1: 1.5.
preferably, the bactericide is nano-silver antibacterial powder.
Preferably, the modified silicone defoaming agent is a mixture of dimethyl silicone oil and SiO2 aerosol, and the preparation process comprises the following steps:
s1: carrying out hydrophobic treatment on SiO2 aerosol, mixing a silane coupling agent containing hydrophobic groups with silicon alkoxide, and preparing SiO2 by sol, gel, aging and drying;
s2: then mixing the SiO2 aerosol subjected to hydrophobic treatment into the simethicone, and heating and stirring;
s3: controlling the temperature at 70-90 ℃ and the stirring speed at 70-80 r/min;
s4: stirring for 4-5 hours.
Preferably, the preparation process comprises the following steps:
the method comprises the following steps: heating vegetable cottonseed oil, yellow mineral oil and coconut oil to above 40 deg.C, mixing, stirring under sealed condition for a while, stopping heating, naturally cooling, and stirring at room temperature for a while;
step two: heating the mixed oil to 90 ℃, adding the antioxidant, the bactericide and the modified organic silicon defoamer into the mixed oil, continuously stirring, stirring for a period of time, standing for 30-45min, then continuously adding the polyethylene glycol and the benzotriazole into the mixed oil, and continuously stirring;
step three: heating and stirring, heating to 110 ℃ within 2 hours, stopping heating, waiting to cool to room temperature, and stopping stirring;
step four: cooling and canning to obtain the finished product.
Preferably, the first step: heating vegetable cottonseed oil, yellow mineral oil and coconut oil to above 40 deg.C, mixing, stirring under sealed condition for a period of time, stopping heating, naturally cooling, stirring at room temperature for a period of time, controlling the sealed stirring time at 40-50min, controlling the stirring speed at 80-85 r/min, and stirring at room temperature for 10-15 min.
Preferably, the step four: after cooling, canning the finished product to obtain a finished product, wherein the finished product wiredrawing oil is stored in a sealed manner at room temperature for one year, the storage period is shortened in the continuous high-temperature and low-temperature weather, the storage temperature is not lower than 15 ℃ in winter, and the finished product wiredrawing oil is stored in a shade place in summer without being exposed to sunlight; before use in winter, the product is stored for a plurality of days in the environment of 15-35 ℃ and is recovered, and can be conditionally moved to a warm oil chamber to be recovered, so that enough fluidity is ensured, and barrel pouring and liquid preparation are convenient; it should be noted that fire protection and the warehouse should be kept well ventilated.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the invention, through the arrangement of the vegetable cottonseed oil, the yellow mineral oil, the coconut oil, the polyethylene glycol, the antioxidant, the bactericide, the modified organic silicon defoamer and the benzotriazole, firstly, the used base oil is an environment-friendly oil product, so that the environment is slightly damaged, secondly, the three oil products have good mixed lubrication effect and are slightly damaged to a human body, the used antioxidant can avoid blackening, discoloration and other conditions caused by the large combination of copper and oxygen in the production process, the surface quality of copper is improved, the bactericide is characterized in that the wiredrawing oil and some natural other components form the environment in which the bacteria exist, the bacteria can erode the wiredrawing oil, so that the wiredrawing oil is changed into an acidic component, the pH value is reduced, and special odor is accompanied, the surface quality of the copper is influenced, the lubricity of the emulsion is reduced, so that the bactericide can inhibit the breeding of bacteria, and the purpose of protecting other metals of, the modified organic silicon defoaming agent is used for directly influencing the lubrication, wear resistance, cooling, rust prevention, cleaning and the like of the wire drawing oil, and the foam can be effectively eliminated by using the modified organic silicon defoaming agent, so that the wire drawing oil achieves good cleaning performance, bright outgoing lines, mold protection and the like.
Drawings
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", etc., indicate orientations and positional relationships shown, are merely for convenience in describing the present invention and simplifying the description, and do not indicate or imply that the device or element referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first," "second," and "third" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance. In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "connected," and "disposed" are to be construed broadly, e.g., as meaning either a fixed connection, a removable connection, or an integral connection; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art. The following describes an embodiment of the present invention based on its overall structure.
Example 1
The formula of the drawing oil comprises 46 parts by mass of vegetable cotton seed oil; 20 parts of yellow mineral oil; 13 parts by mass of coconut oil; 2 parts of polyethylene glycol; 9 parts of antioxidant; 4 parts of a bactericide; 2 parts of modified organic silicon defoaming agent; 4 parts of benzotriazole.
The preparation process comprises the following steps:
the method comprises the following steps: heating vegetable cottonseed oil, yellow mineral oil and coconut oil to above 40 deg.C, mixing, stirring under sealed condition for a while, stopping heating, naturally cooling, and stirring at room temperature for a while;
step two: heating the mixed oil to 90 ℃, adding the antioxidant, the bactericide and the modified organic silicon defoamer into the mixed oil, continuously stirring, stirring for a period of time, standing for 30-45min, then continuously adding the polyethylene glycol and the benzotriazole into the mixed oil, and continuously stirring;
step three: heating and stirring, heating to 110 ℃ within 2 hours, stopping heating, waiting to cool to room temperature, and stopping stirring;
step four: cooling and canning to obtain the finished product.
In the embodiment, more antioxidants are adopted, and the antioxidants are the mixture of p-phenylenediamine antioxidants and phenylpropazole antioxidants, so that the contact of air with copper and other metals can be effectively prevented, the oxidation condition is relieved, and the condition that the copper and other metals are discolored and blackened is reduced.
Example 2
The formula of the drawing oil comprises 46 parts by mass of vegetable cotton seed oil; 20 parts of yellow mineral oil; 13 parts by mass of coconut oil; 2 parts of polyethylene glycol; 6 parts of an antioxidant; 7 parts of a bactericide; 2 parts of modified organic silicon defoaming agent; 4 parts of benzotriazole.
The preparation process comprises the following steps:
the method comprises the following steps: heating vegetable cottonseed oil, yellow mineral oil and coconut oil to above 40 deg.C, mixing, stirring under sealed condition for a while, stopping heating, naturally cooling, and stirring at room temperature for a while;
step two: heating the mixed oil to 90 ℃, adding the antioxidant, the bactericide and the modified organic silicon defoamer into the mixed oil, continuously stirring, stirring for a period of time, standing for 30-45min, then continuously adding the polyethylene glycol and the benzotriazole into the mixed oil, and continuously stirring;
step three: heating and stirring, heating to 110 ℃ within 2 hours, stopping heating, waiting to cool to room temperature, and stopping stirring;
step four: cooling and canning to obtain the finished product.
In the embodiment, more bactericides are adopted, and the bactericides are nano silver antibacterial powder, so that the condition that the wiredrawing oil breeds bacteria can be effectively inhibited, the PH value of copper and other metals is prevented from being damaged by the bacteria, and the condition that the surfaces of the copper and other metals are damaged is avoided.
Example 3
The formula of the drawing oil comprises 46 parts by mass of vegetable cotton seed oil; 20 parts of yellow mineral oil; 13 parts by mass of coconut oil; 2 parts of polyethylene glycol; 6 parts of an antioxidant; 4 parts of a bactericide; 5 parts of modified organic silicon defoaming agent; 4 parts of benzotriazole.
The preparation process comprises the following steps:
the method comprises the following steps: heating vegetable cottonseed oil, yellow mineral oil and coconut oil to above 40 deg.C, mixing, stirring under sealed condition for a while, stopping heating, naturally cooling, and stirring at room temperature for a while;
step two: heating the mixed oil to 90 ℃, adding the antioxidant, the bactericide and the modified organic silicon defoamer into the mixed oil, continuously stirring, stirring for a period of time, standing for 30-45min, then continuously adding the polyethylene glycol and the benzotriazole into the mixed oil, and continuously stirring;
step three: heating and stirring, heating to 110 ℃ within 2 hours, stopping heating, waiting to cool to room temperature, and stopping stirring;
step four: cooling and canning to obtain the finished product.
In the embodiment, more modified organic silicon defoaming agents are adopted, the modified organic silicon defoaming agents are a mixture of SiO2 aerosol subjected to hydrophobic treatment and dimethyl silicone oil, and the modified organic silicon defoaming agents can effectively eliminate foams, so that the wire drawing oil achieves good cleaning performance, the outgoing line is bright, a die is protected, and the like.
Example 4
The formula of the drawing oil comprises 46 parts by mass of vegetable cotton seed oil; 20 parts of yellow mineral oil; 16 parts of coconut oil; 2 parts of polyethylene glycol; 6 parts of an antioxidant; 4 parts of a bactericide; 2 parts of modified organic silicon defoaming agent; 4 parts of benzotriazole.
The preparation process comprises the following steps:
the method comprises the following steps: heating vegetable cottonseed oil, yellow mineral oil and coconut oil to above 40 deg.C, mixing, stirring under sealed condition for a while, stopping heating, naturally cooling, and stirring at room temperature for a while;
step two: heating the mixed oil to 90 ℃, adding the antioxidant, the bactericide and the modified organic silicon defoamer into the mixed oil, continuously stirring, stirring for a period of time, standing for 30-45min, then continuously adding the polyethylene glycol and the benzotriazole into the mixed oil, and continuously stirring;
step three: heating and stirring, heating to 110 ℃ within 2 hours, stopping heating, waiting to cool to room temperature, and stopping stirring;
step four: cooling and canning to obtain the finished product.
In the embodiment, more plant cottonseed oil and coconut oil are adopted, the proportion of the yellow mineral oil is less, the lubricating effect is good, and the used oil product is more environment-friendly.
The characteristics of example 1, example 2, example 3 and example 4 are shown in the following table
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (7)
1. The formula of the drawing oil is characterized by comprising 40-55 parts by mass of vegetable cottonseed oil; 20-30 parts of yellow mineral oil; 13-29 parts by mass of coconut oil; 2-5 parts of polyethylene glycol; 6-9 parts of an antioxidant; 4-7 parts of a bactericide; 2-6 parts of modified organic silicon defoaming agent; 4-8 parts of benzotriazole.
2. The drawing oil formulation according to claim 1, wherein: the antioxidant is a mixture of a p-phenylenediamine antioxidant and a phenylpropazole antioxidant, wherein the ratio of the p-phenylenediamine antioxidant to the phenylpropazole antioxidant is 1: 1.5.
3. the drawing oil formulation according to claim 1, wherein: the bactericide is nano silver antibacterial powder.
4. The drawing oil formulation according to claim 1, wherein: the modified organic silicon defoaming agent is a mixture of dimethyl silicone oil and SiO2 aerosol, and the preparation process comprises the following steps:
s1: carrying out hydrophobic treatment on SiO2 aerosol, mixing a silane coupling agent containing hydrophobic groups with silicon alkoxide, and preparing SiO2 by sol, gel, aging and drying;
s2: then mixing the SiO2 aerosol subjected to hydrophobic treatment into the simethicone, and heating and stirring;
s3: controlling the temperature at 70-90 ℃ and the stirring speed at 70-80 r/min;
s4: stirring for 4-5 hours.
5. The drawing oil formulation according to claim 1, wherein: the preparation process comprises the following steps:
the method comprises the following steps: heating vegetable cottonseed oil, yellow mineral oil and coconut oil to above 40 deg.C, mixing, stirring under sealed condition for a while, stopping heating, naturally cooling, and stirring at room temperature for a while;
step two: heating the mixed oil to 90 ℃, adding the antioxidant, the bactericide and the modified organic silicon defoamer into the mixed oil, continuously stirring, stirring for a period of time, standing for 30-45min, then continuously adding the polyethylene glycol and the benzotriazole into the mixed oil, and continuously stirring;
step three: heating and stirring, heating to 110 ℃ within 2 hours, stopping heating, waiting to cool to room temperature, and stopping stirring;
step four: cooling and canning to obtain the finished product.
6. The drawing oil formulation according to claim 5, wherein: the first step is as follows: heating vegetable cottonseed oil, yellow mineral oil and coconut oil to above 40 deg.C, mixing, stirring under sealed condition for a period of time, stopping heating, naturally cooling, stirring at room temperature for a period of time, controlling the sealed stirring time at 40-50min, controlling the stirring speed at 80-85 r/min, and stirring at room temperature for 10-15 min.
7. The drawing oil formulation according to claim 5, wherein: the fourth step is that: after cooling, canning the finished product to obtain a finished product, wherein the finished product wiredrawing oil is stored in a sealed manner at room temperature for one year, the storage period is shortened in the continuous high-temperature and low-temperature weather, the storage temperature is not lower than 15 ℃ in winter, and the finished product wiredrawing oil is stored in a shade place in summer without being exposed to sunlight; before use in winter, the product is stored for a plurality of days in the environment of 15-35 ℃ and is recovered, and can be conditionally moved to a warm oil chamber to be recovered, so that enough fluidity is ensured, and barrel pouring and liquid preparation are convenient; it should be noted that fire protection and the warehouse should be kept well ventilated.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110098576.6A CN112852529A (en) | 2021-01-25 | 2021-01-25 | Formula of wire drawing oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110098576.6A CN112852529A (en) | 2021-01-25 | 2021-01-25 | Formula of wire drawing oil |
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| CN112852529A true CN112852529A (en) | 2021-05-28 |
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Application publication date: 20210528 |