CN112827443A - Microemulsion stirring intelligence reation kettle for heating - Google Patents
Microemulsion stirring intelligence reation kettle for heating Download PDFInfo
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- CN112827443A CN112827443A CN201911171916.2A CN201911171916A CN112827443A CN 112827443 A CN112827443 A CN 112827443A CN 201911171916 A CN201911171916 A CN 201911171916A CN 112827443 A CN112827443 A CN 112827443A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00132—Controlling the temperature using electric heating or cooling elements
- B01J2219/00135—Electric resistance heaters
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Abstract
The invention discloses a microemulsion stirring intelligent heating reaction kettle, which comprises a kettle body, a frame body and a heating and stirring device, wherein the frame body is fixed outside the kettle body, and the kettle body is provided with a feeding port and a discharging port; the heating and stirring device comprises a power motor and a transformer, wherein the power motor is connected with a motor rod, the motor rod is provided with a crankshaft stirring part, a connecting part is arranged between the crankshaft stirring part and the motor rod, and the crankshaft stirring part comprises a main journal and an eccentric part; the connecting part is fixedly connected with an electric heating element, the electric heating element comprises an upper heating ring, a lower heating ring and four vertical heating rods, the four vertical heating rods are uniformly arranged, an upper connecting rod is arranged in the upper heating ring, and the upper heating ring is fixedly connected with the connecting part through the upper connecting rod; the invention provides a reaction kettle which can realize stirring and heating of microemulsion without additional heating equipment, and saves the cost of additional heating equipment.
Description
Technical Field
The invention relates to the technical field of reaction kettles, in particular to a reaction kettle for intelligent heating of microemulsion stirring.
Background
The microemulsion method is a common method for synthesizing nano particles, and is characterized in that under the action of an amphiphilic molecular surfactant, two immiscible continuous media are fused to form emulsion microbubbles, each microbubble is used as an independent nano reactor, and the nano particles with controllable sizes are obtained through nucleation, coalescence, agglomeration and growth. Two mutually insoluble continuous media as reactants, wherein the micelle particles contained in the two continuous media collide with each other during the reaction, and exchange substances to initiate chemical reaction. Because the particle size of the water core in the microbubble is fixed, the water cores with different particle sizes can not exchange materials, and most of the energy absorbed by the water cores comes from the collision among the particles, the effective collision energy is obtained by controlling the effective collision times of the particles, and the method is an effective way for realizing the control of the morphology and the size of the nano particles.
Stirring is a common experimental means in a microemulsion method, the process of injecting energy into the microemulsion by stirring is favorable for breaking agglomeration among micelle particles, the prior view is that the process of injecting energy into a system by stirring is favorable for generating nano particles with smaller size, which is mainly because the specific surface of small particles is larger and is easy to absorb the energy in the system, and the process of obtaining the nano particles with smaller particle size by improving the stirring speed is one of the common theories of the prior art, however, in the process of injecting energy by stirring, except for the generation of kinetic energy transfer, the other non-negligible energy, namely the exchange among heat energy, also exists, due to the limitation of a stirring mode, the heat energy exchange only occurs in a local area in the system, and in the process of injecting energy in a heat energy form, the particles are more prone to aggregation and growth to form large particles, and due to the uneven heat distribution, resulting in non-uniform particle size.
Stirring is the important means that is used for the homogeneous mixing different compositions, along with the continuous progress of science and technology, has appeared on the market various power mixer, drives stirring vane through the motor and stirs, stirs more evenly, and the stirring of engineering concrete is big, and little is the stirring of drink. The conventional stirring mode mostly adopts coaxial stirring, namely continuous stirring is carried out by taking the position of a stirring device or an extension line as an axis, and one view is that the stirring mode is favorable for forming a reaction system with uniform concentration in the emulsion and forming particles with uniform appearance. However, the stirring method still cannot control the dispersion of the reaction heat, and in addition, the energy injected by stirring is too high to form nanowires or nanorods with stable and remarkable shapes instead of removing nanoparticles.
The microemulsion method is mostly carried out in a reaction kettle, in the prior art, the function of the reaction kettle is single, if the microemulsion needs to be stirred and heated, stirring and heating equipment needs to be additionally arranged, the equipment arrangement cost is high, and the operation is troublesome.
Disclosure of Invention
The invention aims to solve the technical problem that the defects in the prior art are overcome, and provides a reaction kettle for intelligent heating of microemulsion stirring, which can realize heating of microemulsion while stirring is realized, no additional heating equipment is needed, the cost of additional heating equipment is saved, a crankshaft stirring part with an eccentric part is used as a main body of the reaction kettle, the characteristic that the crankshaft stirring part is not concentric is utilized, the existing axial stirring mode is changed, the phenomenon that the concentration distribution of the microemulsion is uneven due to local overheating, the formation and the growth of nano particles are influenced, and the structure is simple. The invention has the advantages of reasonable design, convenient use and operation, uniform stirring, complete functions, high working stability and reliability, strong practicability and convenient popularization and use.
In order to solve the technical problems, the invention adopts the technical scheme that: the utility model provides a microemulsion stirring intelligence reation kettle for heating which characterized in that: the device comprises a kettle body, a frame body and a heating and stirring device, wherein the frame body is fixed outside the kettle body, and a feeding port and a discharging port are formed in the kettle body;
the heating and stirring device comprises a power motor and a transformer, wherein the power motor and the transformer are both fixedly connected with a frame body, the power motor is connected with a motor rod, one end of the motor rod, which is far away from the power motor, is provided with a crankshaft stirring part, the crankshaft stirring part extends into the kettle body, a connecting part for connecting the crankshaft stirring part and the motor rod is arranged between the crankshaft stirring part and the motor rod, the connecting part is fixedly connected with the crankshaft stirring part and the motor rod, the crankshaft stirring part comprises a main journal and an eccentric part, and the main journal is fixedly connected with the eccentric part;
the connecting part is fixedly connected with an electric heating element, the electric heating element comprises an upper heating ring and a lower heating ring which are arranged at intervals up and down, and four vertical heating rods which are vertically connected between the upper heating ring and the lower heating ring, the four vertical heating rods are uniformly arranged, an upper connecting rod is arranged in the upper heating ring, and the upper heating ring is fixedly connected with the connecting part through the upper connecting rod;
the inner wall of the kettle body is fixedly connected with a thermocouple for detecting the temperature in the kettle body, the outer wall of the kettle body is fixedly connected with a heating and stirring controller, the heating and stirring controller comprises a single chip microcomputer, a voltage conversion circuit module for supplying power to each power utilization module in the heating and stirring controller, a crystal oscillator circuit module, a reset circuit module and a data storage circuit module, the crystal oscillator circuit module, the reset circuit module and the data storage circuit module are connected with the single chip microcomputer, the voltage conversion circuit module is connected with the output end of a transformer through a power switch, the input end of the single chip microcomputer is also connected with a motor start-stop button for inputting a power motor start-stop control signal, a heating control button for inputting a heating control signal and a signal conditioning circuit module for conditioning a signal output by the thermocouple, the output end of the thermocouple is connected with the input end of the signal conditioning, the output end of the single chip microcomputer is connected with a heating control relay for controlling the heating of the electric heating element and a power motor control relay for controlling the starting and stopping of a power motor, the electric heating element is connected with the output end of the transformer through the heating control relay, and the power motor is connected with the output end of the transformer through the power motor control relay;
the main journals comprise a first main journal and a second main journal, and the eccentric parts are multiple; the first main journal and the second main journal are not connected, the axial lead of the first main journal and the axial lead of the second main journal are collinear, one end of the first main journal is connected with the connecting part, the other end of the first main journal is connected with the eccentric part, and the second main journal is arranged between two adjacent eccentric parts;
the first main journal is provided with threads, and the connecting part is internally provided with a threaded hole matched with the threads.
Foretell microemulsion stirring intelligence reation kettle for heating which characterized in that: the eccentric portion includes left eccentric portion and right eccentric portion, left eccentric portion and right eccentric portion set up in turn.
Foretell microemulsion stirring intelligence reation kettle for heating which characterized in that: the eccentric part and the main journal are integrally formed.
Foretell microemulsion stirring intelligence reation kettle for heating which characterized in that: the number of the left eccentric parts is not equal to that of the right eccentric parts.
Foretell microemulsion stirring intelligence reation kettle for heating which characterized in that: the power motor is a stepping motor.
Foretell microemulsion stirring intelligence reation kettle for heating which characterized in that: the upper heating ring is positioned above the eccentric part, and the lower heating ring is positioned below the eccentric part.
Foretell microemulsion stirring intelligence reation kettle for heating which characterized in that: two lower connecting rods are arranged in the lower heating ring, and the two lower connecting rods are arranged in a crossed mode.
Compared with the prior art, the invention has the following advantages:
1. the reaction kettle provided by the invention can realize stirring and heating of microemulsion at the same time, does not need additional heating equipment, saves the cost of additional heating equipment, and has the advantages of simple structure, reasonable design, convenience in realization and low cost.
2. The invention takes the crankshaft stirring part with the eccentric part as the main body of the reaction kettle, changes the existing axial stirring mode by utilizing the characteristic of the eccentric part of the crankshaft stirring part, and can effectively avoid the influence of the uneven concentration distribution of the microemulsion on the formation and the growth of the nano particles caused by local overheating.
3. The crankshaft stirring part comprises a main journal and an eccentric part, is directly contacted with different parts of the microemulsion, and can disperse heat generated by stirring to other parts of the system in time, so that the microemulsion cannot influence the controllable synthesis of the nano material due to uneven concentration distribution caused by local heat accumulation.
4. The invention has high working stability and reliability, does not need frequent maintenance and repair, and saves manpower and material resources consumed by maintenance and repair.
The technical solution of the present invention is further described in detail by the accompanying drawings and embodiments.
Drawings
FIG. 1 is a schematic structural diagram of the present invention.
Fig. 2 is a schematic view of a connection relationship between the first main journal and the connecting portion.
FIG. 3 is a schematic block diagram of the electric circuit of the intelligent heating reactor for stirring microemulsion according to the present invention.
Description of reference numerals:
1-a power motor; 2-motor shaft; 3-a connecting part;
4-1 — left eccentric portion; 4-2-right eccentric portion; 4-3 — a first main journal;
4-4 — a second main journal; 5, a frame body; 6-upper heating ring;
7-lower connecting rod; 8, a transformer; 9-lower heating ring;
10-vertical heating rod; 11-an upper connecting rod; 12-a thermocouple;
13-a heating and stirring controller; 14-a liquid filling port; 16-a liquid outlet pipe;
17-a kettle body; 18-a single chip microcomputer; 19-a voltage conversion circuit module;
20-crystal oscillator circuit module; 21-a reset circuit module; 22-a data storage circuit module;
23-power switch; 24-motor start-stop button; 25-heating control button;
26-a signal conditioning circuit module; 27-a heating control relay; 28, controlling a relay by a power motor;
30-electric heating element.
Detailed Description
As shown in fig. 1, fig. 2 and fig. 3, the intelligent heating reactor for stirring microemulsion in this embodiment is characterized in that: the device comprises a kettle body 17, a frame body 5 and a heating and stirring device, wherein the frame body 5 is fixed outside the kettle body 17, and the kettle body 17 is provided with a feed inlet 14 and a discharge outlet 16;
the heating and stirring device comprises a power motor 1 and a transformer 8, wherein the power motor 1 and the transformer 8 are both fixedly connected with a frame body 17, the power motor 1 is connected with a motor rod 2, one end, far away from the power motor 1, of the motor rod 2 is provided with a crankshaft stirring part, the crankshaft stirring part extends into the kettle body 17, a connecting part 3 for connecting the crankshaft stirring part and the motor rod 2 is arranged between the crankshaft stirring part and the motor rod 2, the connecting part 3 is fixedly connected with the crankshaft stirring part and the motor rod 2, the crankshaft stirring part comprises a main journal and an eccentric part, and the main journal is fixedly connected with the eccentric part;
the connecting part 3 is fixedly connected with an electric heating element, the electric heating element comprises an upper heating ring 6 and a lower heating ring 9 which are arranged at intervals up and down, and four vertical heating rods 10 which are vertically connected between the upper heating ring 6 and the lower heating ring 9, the four vertical heating rods 10 are uniformly arranged, an upper connecting rod 11 is arranged in the upper heating ring 6, and the upper heating ring 6 is fixedly connected with the connecting part 3 through the upper connecting rod 11;
the inner wall of the kettle body 17 is fixedly connected with a thermocouple 12 for detecting the temperature inside the kettle body 17, the outer wall of the kettle body 17 is fixedly connected with a heating and stirring controller 13, the heating and stirring controller 13 comprises a single chip microcomputer 18, a voltage conversion circuit module 19 for supplying power to each power module in the heating and stirring controller 13, a crystal oscillator circuit module 20, a reset circuit module 21 and a data storage circuit module 22 which are connected with the single chip microcomputer 18, the voltage conversion circuit module 19 is connected with the output end of the transformer 8 through a power switch 23, the input end of the single chip microcomputer 18 is further connected with a motor start-stop button 24 for inputting a start-stop control signal of the power motor 1, a heating control button 25 for inputting a heating control signal and a signal conditioning circuit module 26 for conditioning the signal output by the thermocouple 12, the output end of the thermocouple 12 is connected with the input end of the signal conditioning circuit module 26, the output end of the single chip microcomputer 18 is connected with a heating control relay 27 for controlling the heating of the electric heating element 30 and a power motor control relay 28 for controlling the starting and stopping of the power motor 1, the electric heating element 30 is connected with the output end of the transformer 8 through the heating control relay 27, and the power motor 1 is connected with the output end of the transformer 8 through the power motor control relay 28. The invention provides a reaction kettle capable of heating microemulsion while stirring, which does not need to be additionally provided with heating equipment, saves the cost of additionally provided heating equipment, has simple structure, reasonable design, convenient realization, low cost, convenient installation and convenient use and operation, takes a crankshaft stirring part with an eccentric part as the main body of the reaction kettle, changes the existing axial stirring mode by utilizing the characteristic of the eccentric part of the crankshaft stirring part, and can effectively avoid the phenomenon that the concentration of the microemulsion is unevenly distributed due to local overheating to influence the formation and the growth of nano particles.
As shown in fig. 1, the intelligent heating reactor for stirring microemulsion in this embodiment is characterized in that: the main journals comprise a first main journal 4-3 and a second main journal 4-4, and the eccentric parts are multiple; the first main journal 4-3 and the second main journal 4-4 are not connected, the axial lead of the first main journal 4-3 and the axial lead of the second main journal 4-4 are collinear, one end of the first main journal 4-3 is connected with the connecting portion 3, the other end of the first main journal 4-3 is connected with the eccentric portion, and the second main journal 4-4 is arranged between two adjacent eccentric portions. The main journal of the crankshaft stirring part and the eccentric part rotate to directly contact with different parts of the microemulsion, and heat generated by stirring can be timely dispersed to other parts of the system, so that the microemulsion cannot cause uneven concentration distribution due to local heat accumulation to influence the controllable synthesis of the nano material.
As shown in fig. 2, the intelligent heating reactor for stirring microemulsion in this embodiment is characterized in that: the first main journal 4-3 is provided with threads, and the connecting part 3 is internally provided with a threaded hole matched with the threads. The crankshaft stirring part is connected with the connecting part through threads, so that the crankshaft stirring part is convenient to disassemble and assemble.
As shown in fig. 1, the intelligent heating reactor for stirring microemulsion in this embodiment is characterized in that: the eccentric part comprises a left eccentric part 4-1 and a right eccentric part 4-2, and the left eccentric part 4-1 and the right eccentric part 4-2 are alternately arranged. The contact area between the micro-emulsion and the reaction kettle is increased by the left eccentric part and the right eccentric part which are alternately arranged, and meanwhile, the eccentric rotation of the reaction kettle is more favorably realized.
As shown in fig. 1, the intelligent heating reactor for stirring microemulsion in this embodiment is characterized in that: the eccentric part and the main journal 4-3 are integrally formed. The eccentric part and the main journal are integrally formed, so that impurities are not introduced into the microemulsion to influence the synthesis of the nano material due to the contact of the connecting joint part and the microemulsion.
As shown in fig. 1, the intelligent heating reactor for stirring microemulsion in this embodiment is characterized in that: the number of the left eccentric parts 4-1 is not equal to the number of the right eccentric parts 4-2. The quantity of the left eccentric parts is unequal to that of the right eccentric parts, which is beneficial to realizing the stability of the reaction kettle and improving the stirring efficiency.
As shown in fig. 1, the intelligent heating reactor for stirring microemulsion in this embodiment is characterized in that: the power motor 1 is a stepping motor.
As shown in fig. 1, the intelligent heating reactor for stirring microemulsion in this embodiment is characterized in that: the upper heating ring 6 is located above the eccentric portion, and the lower heating ring 9 is located below the eccentric portion.
As shown in fig. 1, the intelligent heating reactor for stirring microemulsion in this embodiment is characterized in that: two lower connecting rods 7 are arranged in the lower heating ring 9, and the two lower connecting rods 7 are arranged in a crossed mode.
The installation and use method of the intelligent heating reaction kettle for stirring microemulsion comprises the following steps: placing a crankshaft stirring part between an upper heating ring 6 and a lower heating ring 9, screwing one end of a first main journal 4-3 with threads into a threaded hole of a connecting part 3 to finish assembly, adding microemulsion reaction liquid into an assembled reaction kettle, turning on a power supply, driving a motor rod 2 to rotate by a power motor 1, driving the crankshaft stirring part to rotate by the motor rod 2, and simultaneously rotating the main journal of the crankshaft stirring part, a left eccentric part 4-1 and a right eccentric part 4-2 to realize eccentric stirring of microemulsion; the upper heating ring 6, the lower heating ring 9 and the four vertical heating rods 10 start to heat, so that the microemulsion is heated.
The reaction kettle can realize the eccentric stirring of the microemulsion and simultaneously realize the heating of the microemulsion, does not need to be additionally provided with heating equipment, and saves the cost of additionally provided heating equipment. The main body of reation kettle is regarded as to the bent axle stirring portion that has the eccentric part, utilizes the characteristics of bent axle stirring portion decentraction, changes the mode of current axle center stirring, can effectively avoid the microemulsion to cause the concentration uneven distribution because of local overheat, influences the formation and the growing up of nano-particle.
The invention has high working stability and reliability, does not need frequent maintenance and repair, and saves manpower and material resources consumed by maintenance and repair.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention, and all simple modifications, changes and equivalent structural changes made to the above embodiment according to the technical spirit of the present invention still fall within the protection scope of the technical solution of the present invention.
Claims (7)
1. The utility model provides a microemulsion stirring intelligence reation kettle for heating which characterized in that: the device comprises a kettle body (17), a frame body (5) and a heating and stirring device, wherein the frame body (5) is fixed outside the kettle body (17), and the kettle body (17) is provided with a feed inlet (14) and a discharge outlet (16);
the heating and stirring device comprises a power motor (1) and a transformer (8), wherein the power motor (1) and the transformer (8) are fixedly connected with a frame body (17), a motor rod (2) is connected to the power motor (1), a crankshaft stirring part is arranged at one end, away from the power motor (1), of the motor rod (2), the crankshaft stirring part extends into the kettle body (17), a connecting part (3) used for connecting the crankshaft stirring part and the motor rod (2) is arranged between the crankshaft stirring part and the motor rod (2), the connecting part (3) is fixedly connected with the crankshaft stirring part and the motor rod (2), the crankshaft stirring part comprises a main journal and an eccentric part, and the main journal and the eccentric part are fixedly connected;
the connecting part (3) is fixedly connected with an electric heating element, the electric heating element comprises an upper heating ring (6) and a lower heating ring (9) which are arranged at intervals up and down, and four vertical heating rods (10) which are vertically connected between the upper heating ring (6) and the lower heating ring (9), the four vertical heating rods (10) are uniformly arranged, an upper connecting rod (11) is arranged in the upper heating ring (6), and the upper heating ring (6) is fixedly connected with the connecting part (3) through the upper connecting rod (11);
fixedly connected with is used for carrying out thermocouple (12) that detect kettle body (17) internal temperature on the inner wall of kettle body (17), fixedly connected with heating stirring controller (13) on the outer wall of kettle body (17), heating stirring controller (13) include singlechip (18) and do voltage conversion circuit module (19) that each power consumption module supplied power among heating stirring controller (13), and with crystal oscillator circuit module (20), reset circuit module (21) and data storage circuit module (22) that singlechip (18) met, voltage conversion circuit module (19) meet with the output of transformer (8) through switch (23), the input of singlechip (18) still meets motor start-stop button (24) that are used for inputting power motor (1) start-stop control signal, is used for inputting heating control signal's heating control button (25) and is used for carrying out the signal of opsonizing to thermocouple (12) output and opening signal The output end of the thermocouple (12) is connected with the input end of the signal conditioning circuit module (26), the output end of the single chip microcomputer (18) is connected with a heating control relay (27) for controlling the heating of the electric heating element (30) and a power motor control relay (28) for controlling the starting and stopping of the power motor (1), the electric heating element (30) is connected with the output end of the transformer (8) through the heating control relay (27), and the power motor (1) is connected with the output end of the transformer (8) through the power motor control relay (28);
the main journal comprises a first main journal (4-3) and a second main journal (4-4), and the eccentric part is multiple; the first main journal (4-3) and the second main journal (4-4) are not connected, the axial lead of the first main journal (4-3) is collinear with the axial lead of the second main journal (4-4), one end of the first main journal (4-3) is connected with the connecting part (3), the other end of the first main journal (4-3) is connected with the eccentric part, and the second main journal (4-4) is arranged between two adjacent eccentric parts;
the first main journal (4-3) is provided with threads, and the connecting part (3) is internally provided with a threaded hole matched with the threads.
2. The microemulsion stirring intelligent heating reaction kettle according to claim 1, which is characterized in that: the eccentric part comprises a left eccentric part (4-1) and a right eccentric part (4-2), and the left eccentric part (4-1) and the right eccentric part (4-2) are alternately arranged.
3. The microemulsion stirring intelligent heating reaction kettle according to claim 1, which is characterized in that: the eccentric part and the main journal (4-3) are integrally formed.
4. The microemulsion stirring intelligent heating reaction kettle according to claim 1, which is characterized in that: the number of the left eccentric parts (4-1) is not equal to the number of the right eccentric parts (4-2).
5. The microemulsion stirring intelligent heating reaction kettle according to claim 1, which is characterized in that: the power motor (1) is a stepping motor.
6. The microemulsion stirring intelligent heating reaction kettle according to claim 1, which is characterized in that: the upper heating ring (6) is positioned above the eccentric part, and the lower heating ring (9) is positioned below the eccentric part.
7. The microemulsion stirring intelligent heating reaction kettle according to claim 1, which is characterized in that: two lower connecting rods (7) are arranged in the lower heating ring (9), and the two lower connecting rods (7) are arranged in a crossed mode.
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CN113617317A (en) * | 2021-07-19 | 2021-11-09 | 上海欧河机械设备有限公司 | PLC thermostatic control agitating unit |
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CN113617317A (en) * | 2021-07-19 | 2021-11-09 | 上海欧河机械设备有限公司 | PLC thermostatic control agitating unit |
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Application publication date: 20210525 |