CN112807750A - Gas-liquid separation device for chemical industry - Google Patents

Gas-liquid separation device for chemical industry Download PDF

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Publication number
CN112807750A
CN112807750A CN202110107828.7A CN202110107828A CN112807750A CN 112807750 A CN112807750 A CN 112807750A CN 202110107828 A CN202110107828 A CN 202110107828A CN 112807750 A CN112807750 A CN 112807750A
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liquid
wall
gas
shell
fixedly connected
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刘美金
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D19/00Degasification of liquids
    • B01D19/0042Degasification of liquids modifying the liquid flow
    • B01D19/0052Degasification of liquids modifying the liquid flow in rotating vessels, vessels containing movable parts or in which centrifugal movement is caused
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D19/00Degasification of liquids
    • B01D19/0005Degasification of liquids with one or more auxiliary substances
    • B01D19/001Degasification of liquids with one or more auxiliary substances by bubbling steam through the liquid

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention relates to the technical field of chemical gas-liquid separation, and discloses a chemical gas-liquid separation device which comprises a motor, a cooling liquid circulator, an air pump and a shell, wherein the shell is divided into an upper layer and a lower layer, a heating mechanism is arranged at the lower end of the shell, a top shell is fixedly connected at the upper end of the shell, a downdraft wall is fixedly connected at the upper side in the shell, an air delivery port is arranged in the middle of the downdraft wall, a lubricating liquid wall is fixedly connected at the upper end of the lubricating liquid wall, the side edge of the upper end of the lubricating liquid wall is fixedly connected with the inner wall of the top shell, a spiral wall is arranged in the shell, a liquid inlet is arranged at the starting end of the upper side of the spiral wall, the tail end of the lower side of the spiral wall extends. The chemical gas-liquid separation device is simple in structure, capable of effectively separating gas and liquid in chemical liquid and guaranteeing the purity of the chemical gas, low in use cost control, fast and convenient to use and has a value in the technical field of chemical gas-liquid separation.

Description

Gas-liquid separation device for chemical industry
Technical Field
The invention relates to the technical field of chemical gas-liquid separation, in particular to a chemical gas-liquid separation device.
Background
Chemical engineering is a short term for "chemical process", "chemical industry", "chemical engineering", etc., and all techniques of changing the composition, structure or synthesizing new substances by using chemical methods belong to chemical production techniques, i.e., chemical processes, and the obtained products are called chemicals or chemical products. Chemical engineering is a science for researching the general rule of the production process of chemical products. The relationship between human beings and chemical industry is very close, and some chemical products play epoch-making important roles in the development history of human beings, and the production and the application of the chemical products even represent a certain history stage of human civilization.
The Chinese patent publication No. CN211676691U discloses a gas-liquid separation device for chemical production, which comprises a tank body and an input pipe, wherein a gas phase output pipe is arranged in the center of the top of the tank body, a water outlet pipe is arranged in the center of the bottom of the tank body, the input pipe is a bent pipe, the front end of the input pipe extends into the tank body from the lower part of the side surface of the tank body, the front end of the input pipe is connected with a diffusion cover, and the middle part of the input pipe penetrates through the water outlet pipe; when the device is used for gas-liquid separation treatment, mixed gas and liquid enter through the input pipe and are output to the tank body through the bottom of the diffusion cover, the gas-liquid separation is realized through gravity settling in the tank body, and the liquid falling downwards can be subjected to heat exchange with the input pipe when being discharged through the water outlet pipe, so that the mixed gas and liquid in the input pipe are cooled, and the efficiency of the gas and liquid separation in the tank body is improved.
This patent gas-liquid separation is thorough inadequately, can't guarantee the liquid purity of chemical industry liquid, also can't guarantee the gaseous purity of chemical industry, and the gas diffusion in the chemical industry liquid is slower simultaneously, relatively influences operating time.
Disclosure of Invention
The invention aims to provide a gas-liquid separation device for chemical engineering, which aims to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a gas-liquid separation device for chemical industry comprises a motor, a cooling liquid circulator, an air pump and a shell, wherein the shell is divided into an upper layer and a lower layer, the lower end of the shell is provided with a heating mechanism, the upper end of the shell is fixedly connected with a top shell, the upper side inside the shell is fixedly connected with a gas-guiding wall, the middle part of the gas-guiding wall is provided with an air conveying port, the upper end of the air conveying port is fixedly connected with a synovial wall, the upper end side of the synovial wall is fixedly connected with the inner wall of the top shell, the inside of the shell is provided with a spiral wall, the starting end of the upper side of the spiral wall is provided with an inlet, the lower end of the spiral wall extends to the bottom of the shell, the middle part of the lower end of the shell is rotatably connected with a stirring frame, the lower end of the stirring frame is fixedly connected with a first bevel gear, a liquid outlet is arranged at the lower side of the shell.
As a further scheme of the invention: the heating mechanism comprises a heat insulation wall, the upper end inner ring and the lower end inner ring of the heat insulation wall are fixedly connected with the upper layer and the lower layer of the shell respectively, a heat conduction wall is arranged between the upper layer and the lower layer of the shell, a cavity is arranged between the heat conduction wall and the heat insulation wall, the upper side of the heat insulation wall is provided with a hot steam inlet, and the lower side of the heat insulation wall is provided with a.
As a still further scheme of the invention: the heat conducting wall is made of aluminum plate.
As a still further scheme of the invention: the spiral wall is discontinuously provided with a plurality of inclined plates.
As a still further scheme of the invention: the motor downside fixed connection bedplate, bedplate upper end left and right sides fixed connection support, support upside fixed connection thermal-insulated wall.
As a still further scheme of the invention: condensation mechanism includes the coolant liquid circulator, the coolant liquid circulator sets up two sets of transfer lines and imbeds respectively in the top shell is inside extends to the condensing box, and the condensing box left and right sides is provided with branch liquid frame, controls the side divide one side pipe connection transfer line that the liquid frame kept away from each other, control the side divide a plurality of spiral transfer lines of pipe connection between the liquid frame.
As a still further scheme of the invention: the spiral infusion tube and the condensing box are made of glass.
As a still further scheme of the invention: a plurality of water condensation rods are arranged on the lower side of the condensing box.
Compared with the prior art, the invention has the beneficial effects that:
the invention discloses a gas-liquid separation device for chemical industry, which is provided with a heating mechanism, hot steam is input through a hot steam input port, heat is diffused into chemical liquid through a heat conducting wall, the gas dissolving amount in the chemical liquid is effectively reduced, a stirring frame is arranged, a first bevel gear is driven to rotate through a motor to control the stirring frame to rotate, the gas dispersing speed is increased, a spiral wall is arranged, the flow stroke of the chemical liquid can be increased when the chemical liquid is input, the gas diffusion buffering time and the gas amount are increased, a condensing mechanism is arranged, cooling liquid can be conveyed into a condensing box through a cooling liquid circulator, the conveying stroke of the cooling liquid is increased through a spiral conveying pipe, the condensing box is enabled to cool gas flowing upwards, the dissolved moisture in the gas can be condensed onto a water condensing rod, and the purity of the gas is increased. The chemical gas-liquid separation device is simple in structure, capable of effectively separating gas and liquid in chemical liquid and guaranteeing the purity of the chemical gas, low in use cost control, fast and convenient to use and has a value in the technical field of chemical gas-liquid separation.
Drawings
Fig. 1 is a schematic structural view of a chemical gas-liquid separation device.
Fig. 2 is a schematic sectional structure view of a housing and a top shell of the gas-liquid separation device for chemical industry.
Fig. 3 is a schematic structural view of the inside of a condenser box in the chemical gas-liquid separation device.
In the figure: 1-bracket, 2-water outlet, 3-heat insulation wall, 4-heat conduction wall, 5-hot steam inlet, 6-shell, 7-air-guiding wall, 8-water condensation rod, 9-cooling liquid circulator, 10-condensing box, 11-air outlet, 12-air pump, 13-spiral liquid conveying pipe, 14-synovial wall, 15-top shell, 16-liquid inlet, 17-spiral wall, 18-liquid outlet, 19-stirring frame, 20-first bevel gear, 21-second bevel gear, 22-motor and 23-seat plate.
Detailed Description
In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "middle", "left", "right", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, are only for convenience in describing the invention and simplifying the description, and do not indicate or imply that the referred device or element must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention.
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
Referring to fig. 1-2, a gas-liquid separating device for chemical industry comprises a motor 22, a coolant circulator 9, an air extractor 12 and a casing 6, wherein the casing 6 is divided into an upper layer and a lower layer, a heating mechanism is arranged at the lower end of the casing 6, the heating mechanism comprises a heat insulating wall 3, the inner rings at the upper end and the lower end of the heat insulating wall 3 are respectively and fixedly connected with the upper layer and the lower layer of the casing 6, a heat conducting wall 4 is arranged between the upper layer and the lower layer of the casing 6, a cavity is arranged between the heat conducting wall 4 and the heat insulating wall 3, the heat conducting wall 4 is made of an aluminum plate, a hot steam inlet is arranged at the upper side of the heat insulating wall 3, a water outlet 2 is arranged at the lower side of the heat insulating wall 3, a heating mechanism is arranged, hot steam is input through the hot steam inlet, the heat is diffused into chemical industry liquid by the heat conducting wall 4, the middle part of the gas conveying wall 7 is provided with a gas conveying port, the upper end of the gas conveying port is fixedly connected with a liquid sliding wall 14, the side of the upper end of the liquid sliding wall 14 is fixedly connected with the inner wall of a top shell 15, a spiral wall 17 is arranged inside the shell 6, the starting end of the upper side of the spiral wall 17 is provided with a liquid inlet 16, the tail end of the lower side of the spiral wall 17 extends to the bottom of the shell 6, the spiral wall 17 is arranged, the flow stroke of chemical liquid can be increased and the buffer time and the gas amount of gas diffusion can be increased when the chemical liquid is input, the middle part of the lower end of the shell 6 is rotatably connected with a stirring frame 19, the lower end of the stirring frame 19 is fixedly connected with a first bevel gear 20, the first bevel gear 20 is meshed with a second bevel gear 21, the center of the second bevel gear 21 is fixedly connected with the output end of, the lower side of the motor 22 is fixedly connected with a seat plate 23, the left side and the right side of the upper end of the seat plate 23 are fixedly connected with a bracket 1, the upper side of the bracket 1 is fixedly connected with a heat insulation wall 3, and the bracket 1 has the supporting function.
Referring to fig. 1-3, a condensing mechanism is arranged on the upper side inside the top shell 15, the condensing mechanism includes a coolant circulator 9, the coolant circulator 9 is provided with two sets of liquid conveying pipes which are respectively embedded into the top shell 15 and extend into the condensing box 10, liquid separating frames are arranged on the left and right sides of the condensing box 10, one side of each liquid separating frame, which is far away from the other side, is connected with the liquid conveying pipe, a plurality of spiral liquid conveying pipes 13 are connected between the liquid separating frames on the left and right sides through pipelines, the spiral liquid conveying pipes 13 and the condensing box 10 are made of glass materials and are beneficial to cold transfer, a plurality of water condensing rods 8 are arranged on the lower side of the condensing box 10 to accelerate the formation of water drops, the condensing mechanism is arranged to convey coolant into the condensing box 10 through the coolant circulator 9, the conveying stroke of the coolant is increased through the spiral liquid conveying pipes 13, so that the condensing box 10 cools the gas flowing upwards, and can condense the dissolved, increase gaseous purity, top shell 15 upper end sets up gas outlet 11, and 11 upsides in gas outlet set up air extractor 12, can extract the chemical industry gas of separation, 6 downside of casing is provided with liquid outlet 18, can discharge the chemical industry liquid after the separation.
Example 2
Referring to fig. 1, the present embodiment is different from the above embodiment 1 in that a plurality of inclined plates are intermittently disposed on the spiral wall 17 to increase the flow resistance of the chemical liquid and increase the gas diffusion efficiency by using the impact.
The working principle of the invention is as follows: when the device is used for chemical gas-liquid separation, firstly, chemical liquid is conveyed into a shell 6 through a liquid inlet 16 and can slide to the bottom of the shell 6 from the starting end of a spiral wall 17, after the chemical liquid is input, a motor 22 is turned on, the motor 22 can drive a stirring frame 19 to rotate, then hot steam is input through a hot steam inlet 5, the hot steam carries out heat transmission on the chemical liquid through a heat conducting wall 4, so that the chemical liquid is heated, gas in the chemical liquid can be rapidly diffused under the conditions of stirring and heating, a gas transmission port is rapidly concentrated through the gas conducting wall 7, then a cooling liquid circulator 9 is turned on, cooling liquid is conveyed in a spiral liquid conveying pipe 13 and can cool the wall of a condensation box 10, the chemical gas can condense on a water condensation rod 8 when contacting the wall of the condensation box 10, and can automatically drop on the liquid sliding wall 14 when water drops are large, then the gas slides into the shell 6, the air pump is started to discharge dry gas, and then the chemical liquid is discharged through the liquid outlet 18, so that the gas-liquid separation process of the chemical liquid is completed. The chemical gas-liquid separation device is simple in structure, capable of effectively separating gas and liquid in chemical liquid and guaranteeing the purity of the chemical gas, low in use cost control, fast and convenient to use and has a value in the technical field of chemical gas-liquid separation.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein, and any reference signs in the claims are not intended to be construed as limiting the claim concerned.
Although the preferred embodiments of the present patent have been described in detail, the present patent is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present patent within the knowledge of those skilled in the art.

Claims (8)

1. A gas-liquid separation device for chemical industry comprises a motor (22), a cooling liquid circulator (9), an air extractor (12) and a shell (6), and is characterized in that the shell (6) is divided into an upper layer and a lower layer, the lower end of the shell (6) is provided with a heating mechanism, the upper end of the shell (6) is fixedly connected with a top shell (15), the upper side inside the shell (6) is fixedly connected with a cis-gas wall (7), the middle part of the cis-gas wall (7) is provided with an air delivery port, the upper end of the air delivery port is fixedly connected with a lubricating liquid wall (14), the upper end side of the lubricating liquid wall (14) is fixedly connected with the inner wall of the top shell (15), a spiral wall (17) is arranged inside the shell (6), the upper side initial end of the spiral wall (17) is provided with a liquid inlet (16), the lower side end of the spiral wall (17) extends to the bottom of the shell (6), the middle part of the lower end, first bevel gear (20) meshing connection second bevel gear (21), the output of the center fixed connection motor (22) of second bevel gear (21), the inside upside of top shell (15) sets up condensation mechanism, and top shell (15) upper end sets up gas outlet (11), and gas outlet (11) upside sets up air extractor (12), casing (6) downside is provided with liquid outlet (18).
2. The chemical gas-liquid separation device according to claim 1, wherein the heating mechanism comprises a heat insulation wall (3), the inner rings of the upper and lower ends of the heat insulation wall (3) are respectively and fixedly connected with the upper and lower layers of the housing (6), a heat conduction wall (4) is arranged between the upper and lower layers of the housing (6), a cavity is arranged between the heat conduction wall (4) and the heat insulation wall (3), a hot steam inlet is arranged on the upper side of the heat insulation wall (3), and a water outlet (2) is arranged on the lower side of the heat insulation wall (3).
3. The gas-liquid separation device for chemical industry according to claim 2, wherein the heat conducting wall (4) is made of aluminum plate.
4. The chemical gas-liquid separator according to claim 1, wherein the spiral wall (17) is provided with a plurality of inclined plates intermittently.
5. The chemical gas-liquid separation device according to claim 1 or 2, wherein a seat plate (23) is fixedly connected to the lower side of the motor (22), the left side and the right side of the upper end of the seat plate (23) are fixedly connected with the bracket (1), and the upper side of the bracket (1) is fixedly connected with the heat insulation wall (3).
6. The chemical gas-liquid separation device according to claim 1, wherein the condensing mechanism comprises a cooling liquid circulator (9), the cooling liquid circulator (9) is provided with two groups of liquid conveying pipes which are respectively embedded into the top shell (15) and extend into the condensing box (10), liquid separating frames are arranged on the left side and the right side of the condensing box (10), one side of the left liquid separating frame and the right liquid separating frame, which are far away from each other, are connected with the liquid conveying pipes through pipelines, and a plurality of spiral liquid conveying pipes (13) are connected between the left liquid separating frame and the right liquid separating frame through pipelines.
7. The chemical gas-liquid separation device according to claim 6, wherein the spiral liquid conveying pipe (13) and the condensation tank (10) are made of glass.
8. The chemical gas-liquid separation device according to claim 6, wherein a plurality of water condensation rods (8) are provided under the condensation tank (10).
CN202110107828.7A 2021-01-27 2021-01-27 Gas-liquid separation device for chemical industry Pending CN112807750A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110107828.7A CN112807750A (en) 2021-01-27 2021-01-27 Gas-liquid separation device for chemical industry

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Application Number Priority Date Filing Date Title
CN202110107828.7A CN112807750A (en) 2021-01-27 2021-01-27 Gas-liquid separation device for chemical industry

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH682982A5 (en) * 1990-06-11 1993-12-31 Asea Brown Boveri Apparatus for heating and degassing of water.
CN206715380U (en) * 2016-10-13 2017-12-08 广州市臻善生物科技有限公司 A kind of high efficiency air liquid separation device for bio-pharmaceuticals
CN208389451U (en) * 2018-04-10 2019-01-18 珠海金鸡化工有限公司 For producing the gas-liquid separator of carboxylic styrene butadiene latex
CN109260769A (en) * 2018-12-04 2019-01-25 攀枝花荣鑫油漆有限责任公司 A kind of paint defoaming device
CN208711124U (en) * 2018-06-13 2019-04-09 河源诚展科技有限公司 A kind of constant temperature and pressure defoaming device
CN210138489U (en) * 2019-06-12 2020-03-13 江西晟高科技有限公司 Slurry degassing device
CN210786296U (en) * 2019-08-29 2020-06-19 扬州市众鑫化工有限公司 Novel gas-liquid separator

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH682982A5 (en) * 1990-06-11 1993-12-31 Asea Brown Boveri Apparatus for heating and degassing of water.
CN206715380U (en) * 2016-10-13 2017-12-08 广州市臻善生物科技有限公司 A kind of high efficiency air liquid separation device for bio-pharmaceuticals
CN208389451U (en) * 2018-04-10 2019-01-18 珠海金鸡化工有限公司 For producing the gas-liquid separator of carboxylic styrene butadiene latex
CN208711124U (en) * 2018-06-13 2019-04-09 河源诚展科技有限公司 A kind of constant temperature and pressure defoaming device
CN109260769A (en) * 2018-12-04 2019-01-25 攀枝花荣鑫油漆有限责任公司 A kind of paint defoaming device
CN210138489U (en) * 2019-06-12 2020-03-13 江西晟高科技有限公司 Slurry degassing device
CN210786296U (en) * 2019-08-29 2020-06-19 扬州市众鑫化工有限公司 Novel gas-liquid separator

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
杨青主编: "《化工单元操作》", 31 January 2017, 西南交通大学出版社 *

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