CN112760181A - Production method of black rice yellow wine - Google Patents

Production method of black rice yellow wine Download PDF

Info

Publication number
CN112760181A
CN112760181A CN202110192218.1A CN202110192218A CN112760181A CN 112760181 A CN112760181 A CN 112760181A CN 202110192218 A CN202110192218 A CN 202110192218A CN 112760181 A CN112760181 A CN 112760181A
Authority
CN
China
Prior art keywords
rice
black rice
yellow wine
fermentation
soaking
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202110192218.1A
Other languages
Chinese (zh)
Inventor
杨柳
周悦
姚升飞
徐尚英
李井雷
孙汉巨
何述栋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hefei University of Technology
Original Assignee
Hefei University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hefei University of Technology filed Critical Hefei University of Technology
Priority to CN202110192218.1A priority Critical patent/CN112760181A/en
Publication of CN112760181A publication Critical patent/CN112760181A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/02Preparation of other alcoholic beverages by fermentation
    • C12G3/021Preparation of other alcoholic beverages by fermentation of botanical family Poaceae, e.g. wheat, millet, sorghum, barley, rye, or corn
    • C12G3/022Preparation of other alcoholic beverages by fermentation of botanical family Poaceae, e.g. wheat, millet, sorghum, barley, rye, or corn of botanical genus Oryza, e.g. rice

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The invention discloses a production method of black rice yellow wine, which takes black rice as a fermentation raw material, wherein the black rice contains a large amount of anthocyanin, but the rice husk layer is thick and is not beneficial to the dissolution of the anthocyanin. According to the invention, the rice soaking water of the black rice is applied to fermentation, so that the discharge of waste water is reduced, the environment is protected, the loss of anthocyanin is reduced, the utilization rate of the anthocyanin is improved, the chromaticity of wine is increased, caramel is not required to be added, and the cost is reduced; the invention adds the cellulase into the rice mash to carry out fermentation production of the yellow wine, the cellulase is added to be beneficial to the destruction of the aleurone layer of the black rice, the dissolution and enzymolysis of starch and protein in the black rice are promoted, the conversion rate of raw materials and the wine yield are improved, the increase of the dissolution rate of the protein is beneficial to improving the content of amino acid nitrogen in the product, and the flavor of the yellow wine is improved.

Description

Production method of black rice yellow wine
Technical Field
The invention belongs to the technical field of fermentation, relates to a yellow wine fermentation process technology, in particular to a fermentation technology of health care and health maintenance type yellow wine prepared by pre-gelatinizing and performing enzymolysis on black rice and performing co-treatment fermentation, and particularly relates to a method for producing black rice yellow wine by using the black rice.
Background
The yellow wine is prepared by taking grains such as rice, glutinous rice or millet as raw materials and fermenting, wherein the yellow wine is light yellow, and caramel pigment is added to adjust the color tone of the yellow wine. The consistent food safety resulting from the illicit addition of caramel color was questioned by consumers (Liushaw, Raney. caramel color safety [ J ] quality and standardization 2015, 10: 38).
The black rice is brown rice without husk, and is rich in protein, minerals and vitamins. The rice husk layer of the black rice contains a large amount of black rice anthocyanidin which has the physiological functions of resisting oxidation, reducing blood fat, inhibiting cancer, resisting bacteria, resisting inflammation, resisting allergy and the like (Rijie Qiang, Zhu Biyan, Chen Ming Qing. Special rice nutrition analysis [ J ]. academic newspaper of south China Master university: Nature science edition, 2005,1: 95-98; Chenling Hua, Chen Zu, Zuoming, efficacy of black rice anthocyanin [ J ]. modern food, 2017,10: 08-11).
Although the black rice is rich in nutrition, the black rice is difficult to be gelatinized and is difficult to be steamed compared with the japonica rice and the glutinous rice due to the compactness and the integrity of the structure of the outer skin layer of the black rice. When the method is applied to fermented foods, the black rice is pretreated mainly by methods such as airflow puffing, grinding, high-temperature fluidization and the like. For example, Wuhuifang takes black rice as a raw material, the black rice is processed by adopting a low-temperature high-pressure puffing method, and then saccharifying enzyme and yeast are added to produce yellow wine by a liquid fermentation method (Wuhuifang, black rice yellow wine new process research [ J ] brewing science and technology, 2007(6):98-100), the wine yield is high, but the liquid fermentation wine has the defect of low taste; chenshiping et al extract black rice melanin with 20-30% ethanol, then blend the rice wine liquor and add color fixative to produce black rice yellow wine (Chengshiping, Zhoushui, Wuhuiwei, et al. research on black rice yellow wine technology and product stability [ J ] brewing science and technology, 2006 (75-77), this method is relatively complex in operation and relatively high in production cost.
Disclosure of Invention
The invention aims to provide a production method of black rice yellow wine.
The purpose of the invention can be realized by the following technical scheme:
a production method of black rice yellow wine comprises the following steps:
the first step is as follows: soaking rice;
the second step is that: pre-pasting;
the third step: steaming rice to obtain black rice;
the fourth step: mixing the black rice, distiller's yeast and cellulase, fermenting for a period of time, adding activated dry yeast and the rice soaking water obtained by rice soaking in the first step, fermenting, and filtering after fermentation to obtain the black rice yellow wine.
As a further scheme of the invention, the specific steps of soaking rice in the first step are as follows: selecting clean black rice without mildew and rot, placing the black rice in a rice soaking tank, and mixing the black rice and the black rice according to the proportion of 1:2, adding tap water for soaking, and soaking for 48 hours at 20-40 ℃ to finish rice soaking.
As a further scheme of the invention, the step of pre-gelatinization in the second step is that steam is introduced into the rice-water mixture obtained after the rice soaking in the first step, the temperature is controlled at 50-70 ℃, and the heat preservation time is 30-90min to complete the pre-gelatinization.
In a further embodiment of the present invention, the cellulase is added before the fermentation of black rice is started.
In a further embodiment of the present invention, the rice-soaking water is added to the black rice after being sterilized.
As a further scheme of the invention, the black rice, the distiller's yeast and the cellulase are mixed and put into a tank, and then are fermented for 12-24 hours, and then the active dry yeast and the rice soaking water obtained in the first step of rice soaking are added into the tank.
As a further embodiment of the present invention, the activation conditions of the active dry yeast are: preparing a glucose solution with the mass fraction of 2.5%, weighing a certain amount of active dry yeast, and activating in the prepared glucose solution with the temperature of 28 ℃ for 30 min.
As a further scheme of the invention, the addition amount of the cellulase is 40-50U/g of black rice; the ratio of material to water is 1:1.5-1:3.0 during fermentation; the addition amount of the distiller's yeast is 0.2-0.5% of the dry weight of the black rice, and the addition amount of the active dry yeast is 0.2-0.5% of the dry weight of the black rice.
As a further aspect of the present invention, the fermentation conditions in the fourth step are as follows: fermenting at 18-32 deg.C for more than 25 days; wherein the fermentation period is 0-5 days, the stirring is carried out once every 4-5 hours, the temperature is controlled at 26-32 ℃, the fermentation period is 6-25 days, and the temperature is controlled at 18-25 ℃.
As a further scheme of the invention, the alcohol content of the black rice yellow wine produced by the method is 15-17%, the content of amino acid nitrogen is 0.21-0.30g/L, the chroma is 0.80-0.99 measured by the wavelength A420nm, and the content of anthocyanin is 0.05-0.08 mg/ml.
The invention has the beneficial effects that:
1. the yellow wine is prepared from black rice as a fermentation raw material, wherein the protein content of the black rice is 6.7% higher than that of common rice, and the black rice contains a large amount of various amino acids, trace elements such as manganese, zinc, iron and the like, vitamins and the like which are necessary for human bodies, and importantly, the black rice contains a large amount of anthocyanin, so that the quality of the yellow wine is improved to a great extent, and the nutritional value and the efficacy of the yellow wine are improved.
2. The black rice contains a large amount of anthocyanin, but the rice husk layer of the black rice is thick, so that the anthocyanin is not favorably dissolved out.
3. According to the invention, the rice soaking water of the black rice is applied to fermentation, so that the discharge of waste water is reduced, the environment is protected, the loss of anthocyanin is reduced, the utilization rate of the anthocyanin is improved, the chromaticity of wine is increased, caramel is not required to be added, and the cost is reduced.
4. The invention adds the cellulase into the rice mash to carry out fermentation production of the yellow wine, the cellulase is added to be beneficial to the destruction of the aleurone layer of the black rice, the dissolution and enzymolysis of starch and protein in the black rice are promoted, the conversion rate of raw materials and the wine yield are improved, the increase of the dissolution rate of the protein is beneficial to improving the content of amino acid nitrogen in the product, and the flavor of the yellow wine is improved.
Drawings
The invention is described in further detail below with reference to the figures and specific embodiments.
FIG. 1 is a flow diagram of a production method of black rice yellow wine according to the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
A production method of black rice yellow wine is shown in figure 1, and the black rice is pre-gelatinized and enzymolyzed to produce the yellow wine by fermentation, and the production method specifically comprises the following steps:
soaking 0.5 ton of fructus Zizaniae Caduciflorae in tap water at 35-40 deg.C for 48 hr, introducing 0.1MPa steam until the temperature of the rice soaking water is 70 deg.C, pre-gelatinizing for about 60min, draining water, and steaming with high pressure rice steaming machine. After steaming, adding cellulase when the rice is cooled to 50-60 ℃, adding 50U/g of black rice, continuously cooling to 30 ℃, adding a small amount of water and 3.0kg of distiller's yeast, and starting fermentation.
Fermenting black rice for 12h, adding boiled and cooled rice soaking water 2 tons and active dry yeast (yellow wine) 4Kg into the rice, mixing well, and continuing fermenting.
The fermentation is carried out for 0-5 days, which belongs to the pre-fermentation stage, and the stirring is carried out once every 4-5 hours, and the temperature is controlled at 26-32 ℃; fermenting for 6-25 days, and controlling the temperature at 18-25 deg.C. After the fermentation is finished, filtering the fermented mash by a plate-and-frame filter press to obtain the yellow wine liquid, wherein the alcohol content of the wine liquid is 15.9% (Vol/Vol), the amino acid nitrogen content in the wine liquid is 0.525g/L, the chroma (A420nm) is 0.98, the anthocyanin content is 0.08mg/ml, and the wine liquid is decocted, filtered, bottled and sterilized to obtain a finished product.
Example 2
Adding tap water into 0.4 ton of black rice, soaking at 35-40 deg.C for 48 hr, introducing 0.1MPa steam until the temperature of rice soaking water is 60 deg.C, soaking for 60min, draining water, and steaming with high pressure rice steamer. After the rice steaming is finished, when the rice is cooled to 40-50 ℃, 6Kg of 45U/g cellulase and distiller's yeast are added, the fermentation is started, after the fermentation is carried out for about 24 hours, 2 tons of sterile water (tap water and rice soaking water) and 4Kg of active dry yeast are added into the rice, and the fermentation is continued after the uniform mixing.
The fermentation is carried out for 0-5 days, which belongs to the pre-fermentation stage, and the stirring is carried out once every 4-5 hours, and the temperature is controlled at 26-32 ℃; fermenting for 6-25 days, and controlling the temperature at 18-25 deg.C. After the fermentation is finished, filtering the fermented mash by a plate-and-frame filter press to obtain the yellow wine liquid, wherein the alcohol content of the wine liquid is 15.6% (Vol/Vol), the content of amino acid nitrogen in the wine liquid is 0.472g/L, and the chroma (A420nm) is 0.96. The wine liquid is processed by wine decocting, filtering, bottling and sterilizing to obtain the finished product.
Example 3
0.4 ton of black rice is soaked in tap water at 20-25 deg.C for about 72 hr, and then dewatered, and then steamed in a high pressure rice steamer. Adding cellulase at 40-50 deg.C into cooked rice, adding 50U/g fructus Zizaniae Caduciflorae, adding distiller's yeast 6Kg, starting fermentation, adding sterile water (tap water and rice soaking water) 2 tons and active dry yeast 6Kg into cooked rice, mixing, and fermenting.
The fermentation is carried out for 0-5 days, which belongs to the pre-fermentation stage, and the stirring is carried out once every 4-5 hours, and the temperature is controlled at 26-32 ℃; fermenting for 6-25 days, and controlling the temperature at 18-25 deg.C. After the fermentation is finished, filtering the fermented mash by a plate-and-frame filter press to obtain the yellow wine liquid, wherein the alcohol content of the wine liquid is 15.3% (Vol/Vol), the content of amino acid nitrogen in the wine liquid is 0.467g/L, and the chroma (A420nm) is 0.91. The wine liquid is processed by wine decocting, filtering, bottling and sterilizing to obtain the finished product.
Example 4
0.3 ton black rice is soaked in 0.5 ton tap water at 20-25 deg.C for about 48 hr, after water is drained off, 0.1MPa steam is introduced until the temperature of rice soaking water is 60 deg.C, the ventilation is stopped, soaking is carried out for 60min, and rice is steamed by a high-pressure rice steaming machine. After the rice steaming is finished, when the rice is cooled to the normal temperature, 7.5Kg of distiller's yeast is added, the fermentation is started, after the fermentation is carried out for about 24 hours, 1.8 tons of sterile water (tap water and rice soaking water) and 7.5Kg of active dry yeast are added into the rice, and the mixture is uniformly mixed and then is continuously fermented.
The fermentation is carried out for 0-5 days, which belongs to the pre-fermentation stage, and the stirring is carried out once every 4-5 hours, and the temperature is controlled at 26-32 ℃; fermenting for 6-25 days, and controlling the temperature at 18-25 deg.C. After the fermentation is finished, filtering the fermented mash by a plate-and-frame filter press to obtain the yellow wine liquid, wherein the alcohol content of the wine liquid is 15.2% (Vol/Vol), the amino acid nitrogen content in the wine liquid is 0.415g/L, the chroma (A420nm) is 0.88, the anthocyanin content is 0.05mg/ml, and the wine liquid is subjected to wine decocting, filtering, bottling and sterilizing to obtain a finished product.
Compared with the prior art, the invention has the beneficial effects that:
1) aiming at the defects of functional components in the traditional yellow wine, the black rice with higher nutritive value is used as the fermentation raw material, and the black rice contains a large amount of anthocyanin, so that the nutritive value and the efficacy of the yellow wine are greatly improved
2) Compared with the method of directly adding black rice to perform yellow wine fermentation, the method adopts black rice pre-gelatinization and enzymolysis treatment to perform fermentation, thereby not only improving the quality of the product, but also reducing the production cost.
3) The black rice has poor water absorption and long cooking time due to the compact aleurone layer, and the pre-gelatinization treatment can accelerate water distribution, accelerate cooking, shorten the cooking time and reduce the cost.
4) The black rice contains more active substances such as anthocyanin and the like, but the aleurone layer contains a large amount of cellulose, so that the substances are difficult to dissolve out and the enzymolysis is difficult, the cellulase is added into the rice containing the black rice, the integrity of the black rice can be reduced, the compact aleurone layer structure of the black rice is damaged, the dissolution rate of the substances is improved, the water release is increased, the liquor content is improved, the alcohol production is accelerated, the content of substances such as amino acid state and the like in the yellow rice wine is increased, and the content of nutritional ingredients of the yellow rice wine is improved.
The foregoing is merely exemplary and illustrative of the present invention and various modifications, additions and substitutions may be made by those skilled in the art to the specific embodiments described without departing from the scope of the invention as defined in the following claims.

Claims (10)

1. The production method of the black rice yellow wine is characterized by comprising the following steps:
the first step is as follows: soaking rice;
the second step is that: pre-pasting;
the third step: steaming rice to obtain black rice;
the fourth step: mixing the black rice, the yellow wine starter and the cellulase, putting into a tank for fermentation for a period of time, adding activated dry yeast and the rice soaking water obtained by rice soaking in the first step for fermentation, and filtering after the fermentation is finished to obtain the black rice yellow wine.
2. The production method of the black rice yellow wine according to claim 1, wherein the specific steps of soaking rice in the first step are as follows: selecting clean black rice without mildew and rot, placing the black rice in a rice soaking tank, and mixing the black rice and the black rice according to the proportion of 1:2, adding tap water for soaking at the temperature of 20-40 ℃ for 48-72h, and then completing rice soaking.
3. The production method of black rice yellow wine according to claim 2, wherein the specific step of the pre-gelatinization in the second step is that steam is introduced into the rice-water mixture obtained after the rice soaking in the first step, the temperature is controlled at 50-70 ℃, and the heat preservation time is 30-90min to complete the pre-gelatinization.
4. The method for producing black rice yellow wine according to claim 1, wherein the cellulase is added before the fermentation of black rice is started.
5. The method for producing black rice yellow wine according to claim 1, wherein the rice-soaking water is added to black rice after being sterilized.
6. The method for producing black rice yellow wine according to claim 1, wherein the fourth step is that the black rice is cooled to about 40-60 ℃, the cellulase is added, the yellow koji is added after the cooling to about 30 ℃, the fermentation is started, the black rice is mixed with the distiller's yeast and the cellulase and put into a tank, then the fermentation is carried out for 12-24h, and then the active dry yeast and the rice soaking water obtained by rice soaking in the first step are added.
7. The production method of black rice yellow wine according to claim 1, wherein the activation conditions of the active dry yeast are as follows: preparing a glucose solution with the mass fraction of 2.5%, weighing a certain amount of active dry yeast, and activating in the prepared glucose solution with the temperature of 28 ℃ for 30 min.
8. The production method of black rice yellow wine according to claim 1, wherein the addition amount of cellulase is 40-50U/g of black rice; the ratio of material to water during fermentation is 1:2.5-1: 3.0; the addition amount of the yellow wine yeast is 0.2-0.5% of the dry weight of the black rice, and the addition amount of the active dry yeast is 0.2-0.5% of the dry weight of the black rice.
9. The production method of black rice yellow wine according to claim 1, wherein the fermentation conditions in the fourth step are as follows: fermenting at 18-32 deg.C for more than 25 days; wherein the fermentation period is 0-5 days, the stirring is carried out once every 4-5 hours, the temperature is controlled at 26-32 ℃, the fermentation period is 6-25 days, and the temperature is controlled at 18-25 ℃.
10. The method for producing black rice yellow wine according to any one of claims 1 to 7, wherein the alcohol content of the black rice yellow wine produced by the method is 15 to 17%, the content of amino acid nitrogen is 0.21 to 0.30g/L, the chroma measured by the wavelength A420nm is 0.80 to 0.99, and the content of anthocyanin is 0.05 to 0.08 mg/ml.
CN202110192218.1A 2021-02-19 2021-02-19 Production method of black rice yellow wine Pending CN112760181A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110192218.1A CN112760181A (en) 2021-02-19 2021-02-19 Production method of black rice yellow wine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110192218.1A CN112760181A (en) 2021-02-19 2021-02-19 Production method of black rice yellow wine

Publications (1)

Publication Number Publication Date
CN112760181A true CN112760181A (en) 2021-05-07

Family

ID=75705553

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110192218.1A Pending CN112760181A (en) 2021-02-19 2021-02-19 Production method of black rice yellow wine

Country Status (1)

Country Link
CN (1) CN112760181A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113136287A (en) * 2021-05-14 2021-07-20 襄阳市竹林翠峰茶业有限责任公司 White spirit brewed by mixing green tea seeds and grains and brewing method thereof
CN113583783A (en) * 2021-09-03 2021-11-02 华中农业大学 Brewing method of high-anthocyanin-content and flavor-enhanced fully-fermented black rice wine
CN114617221A (en) * 2022-03-14 2022-06-14 江南大学 Preparation method of fresh wet black rice flour

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103387900A (en) * 2013-07-09 2013-11-13 陕西朱鹮黑米酒业有限公司 A black rice wine production method for improving an anthocyanin content
CN106343291A (en) * 2016-08-29 2017-01-25 广东省农业科学院蚕业与农产品加工研究所 Method for preparing black rice enzymatic hydrolysate and black rice polyphenol compound beverage
CN106754082A (en) * 2017-02-15 2017-05-31 刘煜华 A kind of production method of black rice thick wine
CN108175032A (en) * 2016-12-08 2018-06-19 陕西理工大学 A kind of black rice enzymolysis liquid is prepared and black rice pigments extracting method
CN108913429A (en) * 2018-07-19 2018-11-30 安徽海神黄酒集团有限公司 A kind of production method of black rice cooking wine

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103387900A (en) * 2013-07-09 2013-11-13 陕西朱鹮黑米酒业有限公司 A black rice wine production method for improving an anthocyanin content
CN106343291A (en) * 2016-08-29 2017-01-25 广东省农业科学院蚕业与农产品加工研究所 Method for preparing black rice enzymatic hydrolysate and black rice polyphenol compound beverage
CN108175032A (en) * 2016-12-08 2018-06-19 陕西理工大学 A kind of black rice enzymolysis liquid is prepared and black rice pigments extracting method
CN106754082A (en) * 2017-02-15 2017-05-31 刘煜华 A kind of production method of black rice thick wine
CN108913429A (en) * 2018-07-19 2018-11-30 安徽海神黄酒集团有限公司 A kind of production method of black rice cooking wine

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
谢邦祥等, 金盾出版社 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113136287A (en) * 2021-05-14 2021-07-20 襄阳市竹林翠峰茶业有限责任公司 White spirit brewed by mixing green tea seeds and grains and brewing method thereof
CN113136287B (en) * 2021-05-14 2022-08-16 襄阳市竹林翠峰茶业有限责任公司 White spirit brewed by mixing green tea seeds and grains and brewing method thereof
CN113583783A (en) * 2021-09-03 2021-11-02 华中农业大学 Brewing method of high-anthocyanin-content and flavor-enhanced fully-fermented black rice wine
CN113583783B (en) * 2021-09-03 2023-08-11 华中农业大学 Brewing method of full-fermentation black rice wine with high anthocyanin content and enhanced flavor
CN114617221A (en) * 2022-03-14 2022-06-14 江南大学 Preparation method of fresh wet black rice flour
CN114617221B (en) * 2022-03-14 2024-03-01 江南大学 Preparation method of fresh wet black rice flour

Similar Documents

Publication Publication Date Title
CN112760181A (en) Production method of black rice yellow wine
CN106261361A (en) A kind of ferment Fructus Rosae Normalis health-preserving beverage and preparation technology thereof
CN109837163A (en) A kind of brewing method of highland barley Ai Er beer
CN106047566A (en) Glutinous rice wine and production technology thereof
CN102102058A (en) Production process for mulberry glutinous rice wine
CN104232464A (en) Vinegar brewing method and vinegar
CN106367269B (en) Preparation method of castanea henryi red koji wine
CN108913429A (en) A kind of production method of black rice cooking wine
CN105886176A (en) Brewing method for mulberry beer
CN105062856A (en) Brewing method of healthcare black persimmon vinegar
CN112029603A (en) Fructus cannabis beer and preparation method thereof
CN103773669A (en) Preparation method for cactus-black rice nutritional vinegar
CN103074191A (en) Low-ethyl carbamate Hakka mother wine and production method thereof
CN106689951A (en) Fermented amino acid beverage and preparation method thereof
CN104962418B (en) Chaenomeles speciosa and glutinous rice wine and production technology thereof
CN101967432A (en) Method for preparing beer with high polyphenol content
CN106635612A (en) Rice wine beverage injected with nitrogen and carbon dioxide and preparation method of rice wine beverage
KR100815198B1 (en) The manufacturing method of raw wine containing turnip
CN104928112A (en) Fruit wine
CN108517264A (en) A kind of fruit wine of nutrition and health care and preparation method thereof
CN107779333A (en) The preparation method of mountain lichee health liquor
CN105861266B (en) Strawberry and mulberry compound rice vinegar and preparation method thereof
CN108728306A (en) A kind of preparation method of Yellow wine of buckwheat
CN108308476A (en) A kind of mulberry health care fruit vinegar beverage and preparation method thereof
CN105950335A (en) Quinoa rice wine and dioscorea opposita thunb juice and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20210507