CN112755944A - Super-capacitor carbon filtering and washing device and using method thereof - Google Patents
Super-capacitor carbon filtering and washing device and using method thereof Download PDFInfo
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- CN112755944A CN112755944A CN202011569993.6A CN202011569993A CN112755944A CN 112755944 A CN112755944 A CN 112755944A CN 202011569993 A CN202011569993 A CN 202011569993A CN 112755944 A CN112755944 A CN 112755944A
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- reaction kettle
- super
- inlet pipe
- water inlet
- filter pressing
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- 239000003990 capacitor Substances 0.000 title claims abstract description 28
- 238000005406 washing Methods 0.000 title claims abstract description 27
- 238000009298 carbon filtering Methods 0.000 title claims abstract description 10
- 238000000034 method Methods 0.000 title claims description 8
- 238000006243 chemical reaction Methods 0.000 claims abstract description 51
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 17
- 238000010438 heat treatment Methods 0.000 claims abstract description 13
- 239000007788 liquid Substances 0.000 claims abstract description 13
- 239000002002 slurry Substances 0.000 claims description 12
- 238000011085 pressure filtration Methods 0.000 claims description 6
- 230000008602 contraction Effects 0.000 claims description 3
- 238000001514 detection method Methods 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 239000012065 filter cake Substances 0.000 claims description 3
- 238000005086 pumping Methods 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims 6
- 230000000694 effects Effects 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/01—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/96—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor in which the filtering elements are moved between filtering operations; Particular measures for removing or replacing the filtering elements; Transport systems for filters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D35/00—Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
- B01D35/02—Filters adapted for location in special places, e.g. pipe-lines, pumps, stop-cocks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
- B01J4/002—Nozzle-type elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C18/00—Disintegrating by knives or other cutting or tearing members which chop material into fragments
- B02C18/06—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
- B02C18/08—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives within vertical containers
- B02C18/10—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives within vertical containers with drive arranged above container
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C18/00—Disintegrating by knives or other cutting or tearing members which chop material into fragments
- B02C18/06—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
- B02C18/16—Details
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2201/00—Details relating to filtering apparatus
- B01D2201/20—Pressure-related systems for filters
- B01D2201/202—Systems for applying pressure to filters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00177—Controlling or regulating processes controlling the pH
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Carbon And Carbon Compounds (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention discloses a super-capacitor carbon filtering and washing device which comprises a reaction kettle, wherein a feed inlet is formed in the reaction kettle, the reaction kettle is of a double-layer structure, a heating device is arranged in the reaction kettle, a water inlet pipe is arranged in the reaction kettle, a nozzle is arranged on the water inlet pipe, one end of the water inlet pipe is connected with a liquid storage tank through a connector, the liquid storage tank is communicated with the connector through a hose, a pump is arranged on the hose, a filter disc is arranged in the reaction kettle, a filter pressing device capable of moving up and down is arranged in the reaction kettle, a telescopic cylinder is arranged at the upper end of the reaction kettle, and a fixing. The structure is simple, and the use is convenient; the integrated structure has small occupied area, and the totally-enclosed structure reduces the pollution to the outside; heating treatment is carried out to accelerate the reaction effect; the filter pressing and the smashing are repeated in a circulating mode, the capacitor carbon is washed and filtered back and forth, the washing is more thorough, the washing effect is good, and the working efficiency is high.
Description
Technical Field
The invention relates to the technical field of super-capacitor carbon, in particular to a super-capacitor carbon filtering and washing device and a using method thereof.
Background
The super-capacitor activated carbon is a novel high-adsorption activated carbon, is mainly used for super capacitors (also called double-electric-layer capacitors and electrochemical capacitors), and has the characteristics of super large specific surface area, good electrochemical performance, high capacity and the like. The super capacitor is a passive device which is produced in batch in recent years, is arranged between a battery and a common capacitor, has the characteristics of high-current quick charge and discharge of the capacitor and energy storage of the battery, has long service life, and releases current by utilizing electrons between moving conductors (without depending on chemical reaction) during discharge, thereby providing power for equipment. The super capacitor has extremely long service life and rapid charge-discharge characteristics, and is also applied to wide fields of electric vehicles, hybrid vehicles, electric tools, electric toys, railway systems, electric power systems and the like.
The existing washing process adopts a gravity settling method to separate washing liquid and active carbon, and has the disadvantages of long washing time, low working efficiency and poor economic benefit.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides a super-capacitor carbon filtering and washing device and a using method thereof.
In order to achieve the purpose of the invention, the invention adopts the technical scheme that:
a super-capacitor carbon filtering and washing device comprises a reaction kettle, wherein a feed inlet is formed in the reaction kettle, the reaction kettle is of a double-layer structure, a heating device is arranged in the reaction kettle, a water inlet pipe is arranged in the reaction kettle, a nozzle is arranged on the water inlet pipe, one end of the water inlet pipe is connected with a liquid storage tank through a connector, the liquid storage tank is communicated with the connector through a hose, a pump is arranged on the hose, a filter disc is arranged in the reaction kettle, a filter pressing device which can move up and down is arranged in the reaction kettle, a telescopic cylinder is arranged at the upper end of the reaction kettle, a fixing frame is arranged on the telescopic cylinder, a crushing motor is arranged on the fixing frame, a rotating shaft is arranged at the front end of the crushing motor and connected with the filter pressing device, a blade is arranged on the filter pressing device, one end of the discharge pipe is connected with a centrifugal pump, and one end of the centrifugal pump is communicated with the reaction kettle through a pipeline.
Furthermore, the power source of the telescopic cylinder adopts hydraulic or pneumatic.
Further, the water inlet pipe is of an annular structure.
Furthermore, a three-way valve is arranged on the discharge pipe.
Further, a temperature sensor and a PH value detection device are arranged in the reaction kettle.
Further, the filter pressing device is a plate and frame filter press.
Further, the filter disc is detachably connected with the reaction kettle.
A use method of a super-capacitor carbon filtering and washing device comprises the following steps:
step (2), introducing the super-capacitor carbon into a reaction kettle from a feed inlet, controlling a pump to introduce water in a liquid storage tank into the reaction kettle, and adding water into the super-capacitor carbon and heating to 90 +/-10 ℃;
controlling contraction by a telescopic cylinder to enable a fixing frame to move downwards so as to drive a rotating shaft to move downwards, enabling a filter pressing device to work, and pressing for 1-2 hours under the saturation pressure of 0.8 MPa;
step, starting a grinding motor to drive a filter pressing device to rotate, adding water and stirring to be in a slurry state from the filter cake obtained in the step,
and step (3) discharging the slurry obtained in the step (b) from a discharge port, pumping the slurry by a centrifugal pump, putting the slurry into a reaction kettle, continuously adding water, heating, and repeatedly performing pressure filtration by a pressure filtration device until the pH value is qualified after washing.
The invention has the beneficial effects that: the structure is simple, and the use is convenient; the integrated structure has small occupied area, and the totally-enclosed structure reduces the pollution to the outside; heating treatment is carried out to accelerate the reaction effect; the filter pressing and the smashing are repeated in a circulating mode, the capacitor carbon is washed and filtered back and forth, the washing is more thorough, the washing effect is good, and the working efficiency is high.
Drawings
FIG. 1 is a schematic structural view of the present invention;
reference symbol comparison table:
1. the device comprises a reaction kettle, 2, a feed inlet, 3, a heating device, 4, a water inlet pipe, 5, a liquid storage tank, 6, a pump, 7, a filter disc, 8, a filter pressing device, 9, a telescopic cylinder, 10, a fixing frame, 11, a crushing motor, 12, a rotating shaft, 13, a blade, 14, a discharge pipe, 15, a centrifugal pump, 16 and a three-way valve.
Detailed Description
The following further describes embodiments of the present invention with reference to the accompanying drawings. In which like parts are designated by like reference numerals. It should be noted that the terms "front," "back," "left," "right," "upper" and "lower" used in the following description refer to directions in the drawings, and the terms "inner" and "outer" refer to directions toward and away from, respectively, the geometric center of a particular component.
In order to make the content of the present invention more clearly understood, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention.
As shown in fig. 1, a super capacitor carbon filtering and washing device comprises a reaction kettle 1, wherein a feed inlet 2 is arranged on the reaction kettle 1, the reaction kettle 1 is of a double-layer structure, a heating device 3 is arranged in the reaction kettle 1, a water inlet pipe 4 is arranged in the reaction kettle 1, a nozzle is arranged on the water inlet pipe 4, one end of the water inlet pipe 4 is connected with a liquid storage tank 5 through an interface, the liquid storage tank 5 is communicated with the interface through a hose, a pump 6 is arranged on the hose, a filter disc 7 is arranged in the reaction kettle 1, a filter pressing device 8 which can move up and down is arranged in the reaction kettle 1, a telescopic cylinder 9 is arranged at the upper end of the reaction kettle 1, a fixing frame 10 is arranged on the telescopic cylinder 9, a crushing motor 11 is arranged on the fixing frame 10, a rotating shaft 12 is arranged at the front end of the crushing motor 11, the, the bottom of reation kettle 1 is equipped with the discharge opening, the one end of discharge opening is connected with discharge tube 14, the one end of discharge tube 14 is connected with centrifugal pump 15, the one end of centrifugal pump 15 passes through the pipeline and communicates with reation kettle 1.
The power source of the telescopic cylinder 9 adopts hydraulic or pneumatic.
The water inlet pipe 4 is of an annular structure.
A three-way valve 16 is arranged on the discharge pipe 14.
A temperature sensor and a PH value detection device are arranged in the reaction kettle 1.
The filter pressing device 8 is a plate and frame filter press.
The filter disc 7 is detachably connected with the reaction kettle 1.
A use method of a super-capacitor carbon filtering and washing device comprises the following steps:
step 1, adding super-capacitor carbon into a reaction kettle 1 from a feed inlet 2, controlling a pump 6 to introduce water in a liquid storage tank 5 into the reaction kettle 1, and adding water into the super-capacitor carbon and heating to 90 +/-10 ℃;
step 3, starting the filter cake obtained in the step 2 by a grinding motor 11, driving a filter pressing device 8 to rotate, adding water and stirring to be in a slurry state,
and 4, discharging the slurry obtained in the step 3 from a discharge port, pumping the slurry by a centrifugal pump 15, putting the slurry into the reaction kettle 1, continuously adding water for heating, and repeatedly performing pressure filtration by a pressure filtration device 8 until the pH value is qualified after washing.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the present invention, and any modifications, equivalents and improvements made within the spirit and principle of the present invention should be included in the scope of the present invention.
Claims (8)
1. The utility model provides a super capacitor carbon filters washing unit, includes reation kettle (1), its characterized in that: the improved automatic feeding device is characterized in that a feeding hole (2) is formed in the reaction kettle (1), the reaction kettle (1) is of a double-layer structure, a heating device (3) is arranged in the reaction kettle (1), a water inlet pipe (4) is arranged in the reaction kettle (1), a nozzle is arranged on the water inlet pipe (4), one end of the water inlet pipe (4) is connected with a liquid storage tank (5) through an interface, the liquid storage tank (5) is communicated with the interface through a hose, a pump (6) is arranged on the hose, a filter disc (7) is arranged in the reaction kettle (1), a filter pressing device (8) capable of moving up and down is arranged in the reaction kettle (1), a telescopic cylinder (9) is arranged at the upper end of the reaction kettle (1), a fixing frame (10) is arranged on the telescopic cylinder (9), a crushing motor (11) is arranged on the fixing, rotation axis (12) are connected with filter pressing device (8), be equipped with blade (13) on filter pressing device (8), the bottom of reation kettle (1) is equipped with the discharge opening, the one end of discharge opening is connected with discharge tube (14), the one end of discharge tube (14) is connected with centrifugal pump (15), the one end of centrifugal pump (15) is passed through the pipeline and is linked together with reation kettle (1).
2. The supercapacitor carbon filtration washing device according to claim 1, wherein: the power source of the telescopic cylinder (9) adopts hydraulic or pneumatic.
3. The supercapacitor carbon filtration washing device according to claim 1, wherein: the water inlet pipe (4) is of an annular structure.
4. The supercapacitor carbon filtration washing device according to claim 1, wherein: a three-way valve (16) is arranged on the discharge pipe (14).
5. The supercapacitor carbon filtration washing device according to claim 1, wherein: and a temperature sensor and a PH value detection device are arranged in the reaction kettle (1).
6. The supercapacitor carbon filtration washing device according to claim 1, wherein: the filter pressing device (8) is a plate-and-frame filter press.
7. The supercapacitor carbon filtration washing device according to claim 1, wherein: the filter disc (7) is detachably connected with the reaction kettle (1).
8. A use method of a super-capacitor carbon filtering and washing device is characterized by comprising the following steps:
step 1, introducing super-capacitor carbon into a reaction kettle (1) from a feed inlet (2), controlling a pump (6) to introduce water in a liquid storage tank (5) into the reaction kettle (1), and adding water into the super-capacitor carbon and heating to 90 +/-10 ℃;
step 2, controlling contraction by a telescopic cylinder (9) to enable a fixing frame (10) to move downwards so as to drive a rotating shaft (12) to move downwards, enabling a filter pressing device (8) to work, and pressing for 1-2 hours under the saturation pressure of 0.8 MPa;
step 3, starting a grinding motor (11) from the filter cake obtained in the step 2, driving a filter pressing device (8) to rotate, adding water and stirring to be in a slurry state,
and 4, discharging the slurry obtained in the step 3 from a discharge port, pumping the slurry by a centrifugal pump (15), putting the slurry into the reaction kettle (1), continuously adding water, heating, and repeatedly performing pressure filtration by a pressure filtration device (8) until the pH value is qualified after washing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011569993.6A CN112755944A (en) | 2020-12-26 | 2020-12-26 | Super-capacitor carbon filtering and washing device and using method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011569993.6A CN112755944A (en) | 2020-12-26 | 2020-12-26 | Super-capacitor carbon filtering and washing device and using method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112755944A true CN112755944A (en) | 2021-05-07 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011569993.6A Pending CN112755944A (en) | 2020-12-26 | 2020-12-26 | Super-capacitor carbon filtering and washing device and using method thereof |
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| Country | Link |
|---|---|
| CN (1) | CN112755944A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0529845A1 (en) * | 1991-08-27 | 1993-03-03 | Ekokem Oy Ab | Device and method for purification of liquids and for cleansing of the filtering material used in the device |
| CN202898035U (en) * | 2012-10-24 | 2013-04-24 | 无锡东恒新能源材料有限公司 | Carbon nano tube purification system for filter-pressing pulp by using plate-and-frame filter press |
| CN109850897A (en) * | 2018-12-21 | 2019-06-07 | 滑县大潮林物产有限责任公司 | A kind of super capacitor carbon production rinse-system |
| CN211688287U (en) * | 2019-08-12 | 2020-10-16 | 青海启迪清源新材料有限公司 | Lithium hydroxide monohydrate crystallization separation purification device |
-
2020
- 2020-12-26 CN CN202011569993.6A patent/CN112755944A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0529845A1 (en) * | 1991-08-27 | 1993-03-03 | Ekokem Oy Ab | Device and method for purification of liquids and for cleansing of the filtering material used in the device |
| CN202898035U (en) * | 2012-10-24 | 2013-04-24 | 无锡东恒新能源材料有限公司 | Carbon nano tube purification system for filter-pressing pulp by using plate-and-frame filter press |
| CN109850897A (en) * | 2018-12-21 | 2019-06-07 | 滑县大潮林物产有限责任公司 | A kind of super capacitor carbon production rinse-system |
| CN211688287U (en) * | 2019-08-12 | 2020-10-16 | 青海启迪清源新材料有限公司 | Lithium hydroxide monohydrate crystallization separation purification device |
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Application publication date: 20210507 |
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