CN112743081A - Manufacturing method of cross for acetabular file and cross for acetabular file - Google Patents

Manufacturing method of cross for acetabular file and cross for acetabular file Download PDF

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CN112743081A
CN112743081A CN202011471971.6A CN202011471971A CN112743081A CN 112743081 A CN112743081 A CN 112743081A CN 202011471971 A CN202011471971 A CN 202011471971A CN 112743081 A CN112743081 A CN 112743081A
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cross
acetabular
manufacturing
file
degreasing
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CN112743081B (en
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许琳琳
陈灏
胡庆洋
邓强
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Guangzhou Tianying Precision Tool Co ltd
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Guangzhou Tianying Precision Tool Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F5/00Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B17/00Surgical instruments, devices or methods, e.g. tourniquets
    • A61B17/16Bone cutting, breaking or removal means other than saws, e.g. Osteoclasts; Drills or chisels for bones; Trepans
    • A61B17/1659Surgical rasps, files, planes, or scrapers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/10Sintering only
    • B22F3/1017Multiple heating or additional steps
    • B22F3/1021Removal of binder or filler
    • B22F3/1025Removal of binder or filler not by heating only
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/22Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces for producing castings from a slip
    • B22F3/225Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces for producing castings from a slip by injection molding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/24After-treatment of workpieces or articles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B17/00Surgical instruments, devices or methods, e.g. tourniquets
    • A61B2017/00526Methods of manufacturing
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B17/00Surgical instruments, devices or methods, e.g. tourniquets
    • A61B17/16Bone cutting, breaking or removal means other than saws, e.g. Osteoclasts; Drills or chisels for bones; Trepans
    • A61B2017/1602Mills
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/24After-treatment of workpieces or articles
    • B22F2003/247Removing material: carving, cleaning, grinding, hobbing, honing, lapping, polishing, milling, shaving, skiving, turning the surface

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Surgery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dentistry (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Orthopedic Medicine & Surgery (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Biomedical Technology (AREA)
  • Heart & Thoracic Surgery (AREA)
  • Medical Informatics (AREA)
  • Molecular Biology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Prostheses (AREA)

Abstract

The invention provides a method for manufacturing a cross for an acetabular bone file, which is characterized by comprising the following steps of: (1) molding the raw materials by using a mold to obtain a cross; (2) and (4) degreasing the cross, and then sintering to obtain the finished product of the cross for the acetabular file. The method for manufacturing the cross for the acetabular file adopts the die integrated molding sintering process to manufacture the cross for the acetabular file, and the obtained cross has high strength and precision.

Description

Manufacturing method of cross for acetabular file and cross for acetabular file
Technical Field
The invention particularly relates to a manufacturing method of a cross for an acetabular bone file, and further relates to the cross for the acetabular bone file manufactured by the method.
Background
The hip joint replacement surgery aims at the surgery of hip joint injury, adopts artificial joints to replace damaged or diseased joint surfaces so as to achieve the purposes of relieving joint pain, correcting deformity, recovering and improving the motion function of the joints. In hip surgery, an acetabular file is one of the indispensable tools, and the acetabular file is used for processing an acetabular fossa and removing necrotic tissue so as to install an artificial acetabulum. The acetabular file mainly comprises a hemispherical knife shell. The bottom of the hemispherical cutter shell of the acetabular file is connected with a cross, and the cross is used for connecting the hemispherical cutter shell with a connecting rod. The existing cross for the acetabular file is manufactured in a machining or welding mode, and the manufactured cross is easy to deform, has the problems of flatness, accuracy and poor strength, and therefore influences the overall use effect of the acetabular file.
Disclosure of Invention
The invention aims to provide a manufacturing method of a cross for an acetabular file, which solves the technical problems of poor strength and accuracy of the existing cross for the acetabular file.
The first purpose of the invention is realized by the following technical scheme:
a manufacturing method of a cross for an acetabular file comprises the following steps:
(1) molding the raw materials by using a mold to obtain a cross;
(2) and (4) degreasing the cross, and then sintering to obtain the finished product of the cross for the acetabular file.
The raw materials in the invention are 304 stainless steel materials.
In the invention, the molding pressure is 100-120MPa, the temperature of the injected melt is 180-200 ℃, and the material temperature of the mold material is 108-135 ℃.
Further, the molding pressure is 110MPa, the temperature of the injected melt is 190 ℃, and the material temperature of the mold material is 120 ℃.
The invention can be improved by adopting acid treatment or high-temperature degreasing. When degreasing is performed after sintering, organic substances in the molded body are decomposed and reduced to generate carbon, hydrocarbons, carbon monoxide, zinc vapor, and the like in the absence of oxygen during sintering, and these substances are harmful to products, heating elements, and furnace materials, and particularly fatal failures occur when the molded body touches heating elements of molybdenum and tungsten, and therefore degreasing is performed before sintering.
Further, the acid treatment degreasing temperature is 100-.
Further, the acid treatment adopts flowing acid treatment, and the acid inlet flow is 2-3m3The acid feeding time is 280-350 min.
Preferably, the acid is nitric acid with a concentration of 98% or more. Concentrated nitric acid is adopted for degreasing, and passivation protection is achieved on the surface of the raw material while degreasing is achieved.
Further, the high-temperature degreasing temperature is 500-.
Furthermore, the degreasing rate is controlled to be more than or equal to 95 percent. The degreasing is to remove additives such as stearic acid, zinc stearate, lithium stearate, paraffin wax, resin and the like during powder press forming, when the additives enter a high-temperature furnace during sintering, the additives are decomposed and reduced to generate carbon, hydrocarbon, carbon monoxide and the like due to the absence of oxygen, and the gas gasified at high temperature causes defects such as cracking of parts, so that the additives need to be removed before sintering, the higher the degreasing rate is, the better the degreasing rate is, and the degreasing rate is not lower than 95% after a large amount of practices.
In the invention, the sintering temperature is 1050-.
The invention can be further improved by further comprising a shaping treatment after sintering, wherein the shaping treatment is to treat the part in a surface cold extrusion mode. The dimensional accuracy of the part is improved through the shaping treatment.
Further, the pressure maintaining pressure in the shaping process is 60-90MPa, and the pressure maintaining time is 20-35 min.
The invention can also be improved as follows, the shaping treatment also comprises a magnetic polishing (magnetic polishing) step, the rotating speed of the magnetic polishing is 400-600r/min, the magnetic polishing time is 4-6min, and the magnetic polishing frequency is 45-60 Hz.
Further, the magnetic polishing medium is a 1 x 8mm steel needle.
The second purpose of the invention is realized by the following technical scheme:
a cross for an acetabular file is manufactured by the manufacturing method.
Further, the top of the cross frame is arranged in a horizontal plane. The cross frame is used for being connected the in-process with the connecting rod, and upper and lower face and side all contact with the connecting rod, and cross top horizontal plane sets up, can improve the plane degree of acetabular bone file, and is connected more firmly with the connecting rod simultaneously.
Furthermore, the joints of the end surfaces of the four legs of the cross and the top plane are arranged in a reverse right angle mode.
Furthermore, the joint of two adjacent legs at the center of the cross is set by a concave arc fillet, a chamfer angle or a convex arc fillet.
Compared with the prior art, the invention has the following beneficial effects:
(1) the method for manufacturing the cross for the acetabular file adopts the die integrated molding sintering process to manufacture the cross for the acetabular file, and the obtained cross has high strength and precision.
(2) In the method, the acetabulum file cross is treated by adopting the degreasing treatment before sintering and the shaping treatment after sintering, and the obtained acetabulum file cross has high flatness and precision. And the flatness and the precision of the cross are further improved by adopting magnetic polishing treatment.
Drawings
FIG. 1 is an overall configuration view of a cross for an acetabular file prepared in example 1 of the present invention;
FIG. 2 is a front view of a cross for an acetabular file prepared in example 1 of the present invention;
FIG. 3 is a rear view of a cross for an acetabular file prepared in example 1 of the present invention;
FIG. 4 is a left side view of a cross for an acetabular file prepared in example 1 of the present invention;
FIG. 5 is an overall configuration view of a cross for an acetabular file prepared in example 2 of the present invention;
FIG. 6 is a front view of a cross for an acetabular file prepared in example 2 of the present invention;
FIG. 7 is a rear view of a cross for acetabular files prepared in example 2 of the present invention;
FIG. 8 is a left side view of a cross for an acetabular file prepared in example 2 of the present invention;
FIG. 9 is an overall configuration view of a cross for an acetabular file prepared in example 3 of the present invention;
FIG. 10 is a front view of a cross for acetabular files prepared in example 3 of the present invention;
FIG. 11 is a rear view of a cross for acetabular files prepared in example 3 of the present invention;
FIG. 12 is a left side view of a cross for acetabular files prepared in example 3 of the present invention.
Detailed Description
The present invention is further described below in conjunction with specific examples to better understand and implement the technical solutions of the present invention for those skilled in the art.
Example 1
A manufacturing method of a cross for an acetabular file comprises the following steps:
(1) molding the raw material 304 stainless steel by using a mold, wherein the molding pressure is 120MPa, the temperature of a melt injected by a nozzle is 195 ℃, and the temperature of a mold material is 125 ℃, so as to obtain the cross shown in the figure 1-4, wherein the top of the cross is arranged in a horizontal plane, the connecting parts of the end surfaces of four legs and the plane of the top are arranged in a right-angled manner, and the connecting parts of two adjacent legs in the center of the cross are arranged in a concave arc-shaped and rounded manner;
(2) the cross is treated by using 98 percent nitric acid as flowing acid for degreasing treatment, and the acid inlet flow is 2.5m3H, acid feeding time is 300min, degreasing temperature is 120 ℃, and degreasing rate is 99.3%; then sintering is carried out, the sintering temperature is 1350 ℃, and the heat preservation time is 200 min; shaping after sintering, wherein the pressure maintaining pressure in the shaping process is 80MPa, and the pressure maintaining time is 30 min; and performing magnetic polishing after the reshaping treatment, wherein a medium adopted by the magnetic polishing is a 1 x 8mm steel needle (the diameter is 1mm, the length is 8mm), the rotating speed of the magnetic polishing is 450r/min, the magnetic polishing time is 6min, and the magnetic polishing frequency is 50Hz, so that the finished product of the cross for the acetabular file is obtained.
Example 2
A manufacturing method of a cross for an acetabular file comprises the following steps:
(1) molding the raw material 304 stainless steel by using a mold, wherein the molding pressure is 110MPa, the temperature of a melt injected by a nozzle is 190 ℃, and the temperature of a mold material is 115 ℃ to obtain the cross shown in the figure 5-8, wherein the top of the cross is arranged in a horizontal plane, the connecting parts of the end surfaces of four legs and the plane of the top are arranged in a right-angled manner, and the connecting parts of two adjacent legs in the center of the cross are arranged in a straight chamfer manner;
(2) the cross is treated by using 98 percent nitric acid as flowing acid for degreasing treatment, and the acid inlet flow is 3m3H, acid feeding time is 280min, degreasing temperature is 135 ℃, and degreasing rate is 99.5%; then sintering is carried out, the sintering temperature is 1250 ℃, and the heat preservation time is 200 min; shaping after sintering, wherein the pressure maintaining pressure in the shaping process is 80MPa, and the pressure maintaining time is 30 min; and performing magnetic polishing after the reshaping treatment, wherein a medium adopted by the magnetic polishing is a 1 x 8mm steel needle, the rotating speed of the magnetic polishing is 600r/min, the magnetic polishing time is 4min, and the magnetic polishing frequency is 60Hz, so that the finished product of the cross for the acetabular file is obtained.
Example 3
A manufacturing method of a cross for an acetabular file comprises the following steps:
(1) molding the raw material 304 stainless steel by using a mold, wherein the molding pressure is 105MPa, the temperature of a melt injected by a nozzle is 200 ℃, and the temperature of a mold material is 135 ℃, so as to obtain the cross shown in figures 9-12, wherein the top of the cross is arranged in a horizontal plane, the connecting parts of the end surfaces of four legs and the plane of the top are arranged in a reversed right angle mode, and the connecting parts of two adjacent legs in the center of the cross are arranged in a convex arc reversed angle mode;
(2) the cross is treated by using 98 percent nitric acid as flowing acid for degreasing treatment, and the acid inlet flow is 2m3H, acid feeding time is 350min, degreasing temperature is 145 ℃, and degreasing rate is 99.7%; then sintering is carried out, the sintering temperature is 1150 ℃, and the heat preservation time is 200 min; shaping after sintering, wherein the pressure maintaining pressure in the shaping process is 80MPa, and the pressure maintaining time is 30 min; and performing magnetic polishing after the reshaping treatment, wherein a medium adopted by the magnetic polishing is a 1 x 8mm steel needle, the rotating speed of the magnetic polishing is 400r/min, the magnetic polishing time is 6min, and the magnetic polishing frequency is 55Hz, so that the finished product of the cross for the acetabular file is obtained.
Example 4
The difference between the embodiment and the embodiment 1 is that high temperature degreasing is adopted, the degreasing temperature is 550 ℃, the heat preservation time is 50min, and the degreasing rate is 99.5%.
Performance testing
The flatness of the top surface of the cross for the acetabular file prepared in example 1, the symmetry degree of a single rod body to the rod axis and the perpendicularity of the two rod body axes are detected, and specific data are shown in the following table 1.
TABLE 1 Cross accuracy and flatness conditions for acetabular files
Figure BDA0002834291000000061
Figure BDA0002834291000000071
The above embodiments illustrate various embodiments of the present invention in detail, but the embodiments of the present invention are not limited thereto, and those skilled in the art can achieve the objectives of the present invention based on the disclosure of the present invention, and any modifications and variations based on the concept of the present invention fall within the scope of the present invention, which is defined by the claims.

Claims (10)

1. A manufacturing method of a cross for an acetabular file is characterized by comprising the following steps:
(1) molding the raw materials by using a mold to obtain a cross;
(2) and (4) degreasing the cross, and then sintering to obtain the finished product of the cross for the acetabular file.
2. The method for manufacturing a cross for an acetabular file as claimed in claim 1, wherein the molding pressure is 100-120MPa, the temperature of the injected melt is 180-200 ℃, and the temperature of the molding material is 108-135 ℃.
3. The method of manufacturing a cross for acetabular files according to claim 2, wherein the degreasing is performed by acid treatment or high temperature degreasing.
4. The method for manufacturing a cross for an acetabular file as claimed in claim 3, wherein the degreasing temperature of the acid treatment is 100-150 ℃, the acid treatment is carried out by using nitric acid with a concentration of 98% or more as the flowing acid, and the flow rate of the flowing acid is 2-3m3The acid feeding time is 280-350 min.
5. The method for manufacturing the cross for the acetabular file as claimed in claim 4, wherein the sintering temperature is 1050-.
6. The method of claim 4, wherein the step of sintering further comprises a reshaping step, wherein the reshaping step is performed by cold surface pressing the component.
7. The method of manufacturing a cross for acetabular files according to claim 6, wherein the pressure holding pressure during the shaping process is 60 to 90MPa and the pressure holding time is 20 to 35 min.
8. The method for manufacturing a cross for an acetabular file according to claim 1, wherein the method further comprises a magnetic polishing step after the plastic processing, wherein the magnetic polishing rotation speed is 400-.
9. A cross for acetabular files, produced by the method of any one of claims 1 to 8.
10. The cross for acetabular files of claim 9, wherein the top of the cross is disposed in a horizontal plane; the joint of two adjacent legs at the center of the cross is set by a concave arc fillet, a chamfer angle or a convex arc fillet.
CN202011471971.6A 2020-12-14 2020-12-14 Manufacturing method of cross for acetabular file and cross for acetabular file Active CN112743081B (en)

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104550973A (en) * 2013-10-11 2015-04-29 浙江一火科技有限公司 Method for preparing artificial acetabulum cup
CN104688297A (en) * 2015-03-26 2015-06-10 常州玛斯特精密工具有限公司 Acetabular bone file
CN105290392A (en) * 2015-12-08 2016-02-03 重庆文理学院 304L stainless steel metal powder injection molding method
CN107812933A (en) * 2017-09-21 2018-03-20 东莞华晶粉末冶金有限公司 304 powder of stainless steel are injection moulded feeding and preparation method and product
CN109848420A (en) * 2019-04-02 2019-06-07 湖南英捷高科技有限责任公司 A kind of 440C stainless steel metal powder injection forming method and its product
CN110202153A (en) * 2019-06-20 2019-09-06 上海富驰高科技股份有限公司 A kind of MIM preparation for processing of special-shaped product
CN111647826A (en) * 2020-06-15 2020-09-11 江苏精研科技股份有限公司 Method for preparing antibacterial stainless steel by adopting powder injection molding process

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104550973A (en) * 2013-10-11 2015-04-29 浙江一火科技有限公司 Method for preparing artificial acetabulum cup
CN104688297A (en) * 2015-03-26 2015-06-10 常州玛斯特精密工具有限公司 Acetabular bone file
CN105290392A (en) * 2015-12-08 2016-02-03 重庆文理学院 304L stainless steel metal powder injection molding method
CN107812933A (en) * 2017-09-21 2018-03-20 东莞华晶粉末冶金有限公司 304 powder of stainless steel are injection moulded feeding and preparation method and product
CN109848420A (en) * 2019-04-02 2019-06-07 湖南英捷高科技有限责任公司 A kind of 440C stainless steel metal powder injection forming method and its product
CN110202153A (en) * 2019-06-20 2019-09-06 上海富驰高科技股份有限公司 A kind of MIM preparation for processing of special-shaped product
CN111647826A (en) * 2020-06-15 2020-09-11 江苏精研科技股份有限公司 Method for preparing antibacterial stainless steel by adopting powder injection molding process

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Denomination of invention: A manufacturing method for a cross for acetabular files and a cross for acetabular files

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