CN112705144B - Unitized compound synthesis reaction kettle - Google Patents
Unitized compound synthesis reaction kettle Download PDFInfo
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- CN112705144B CN112705144B CN202011565543.XA CN202011565543A CN112705144B CN 112705144 B CN112705144 B CN 112705144B CN 202011565543 A CN202011565543 A CN 202011565543A CN 112705144 B CN112705144 B CN 112705144B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
- B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
Abstract
The invention is suitable for the field of chemical equipment, and particularly relates to a unitized compound synthesis reaction kettle, which comprises: the reaction kettle comprises a reaction kettle body, wherein a unitized feeding structure is arranged in the reaction kettle body; the unitized feeding structure is provided with spiral feeding pipes which are spirally distributed on the inner wall of the reaction kettle body; a plurality of discharging pipes are additionally arranged on the spiral feeding pipe and hinged through a hinge ball; the discharge pipe is provided with a main material guide cavity, and an outer layer material guide cavity is arranged on the outer side of the main material guide cavity; a plurality of discharge holes are communicated with the outer layer material guide cavity and are formed in the pipe wall of the discharge pipe in an inclined mode; the spiral feeding pipes are spirally distributed on the inner wall of the reaction kettle body and are superposed with vortexes formed by stirring, so that the compounds can be rapidly mixed and enter the reaction kettle; the raw materials that enter into outer guide intracavity portion simultaneously through being the discharge opening ejection of compact that the slope set up, because the counter force of the ejection of compact is the discharging pipe round articulated ball lateral rotation, realizes rotatory reinforced, further promotes the mixture.
Description
Technical Field
The invention relates to the field of chemical equipment, in particular to a unitized compound synthesis reaction kettle.
Background
The reaction kettle is a comprehensive reaction container, and the structural function and the configuration accessories of the reaction kettle are designed according to reaction conditions. The preset reaction steps can be completed with higher automation degree from the beginning of feeding, reaction and discharging, and the important parameters of temperature, pressure, mechanical control (stirring, blowing and the like), reactant/product concentration and the like in the reaction process are strictly regulated and controlled. The structure of the device is generally composed of a kettle body, a transmission device, a stirring device, a heating device, a cooling device and a sealing device. The corresponding supporting auxiliary assembly: fractionating column, condenser, water separator, collecting tank, filter, etc.
The reaction kettle is widely applied to pressure vessels for petroleum, chemical engineering, rubber, pesticides, dyes, medicines and foods, and is used for completing technological processes of vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation and the like, such as a reactor, a reaction kettle, a decomposition kettle, a polymerization kettle and the like.
The reaction kettle is a reaction device, and attention must be paid during operation, otherwise, the reaction kettle can be damaged due to a plurality of reasons, and the production is forced to stop. The operation of the reaction kettle needs to pay attention to many aspects, and the reaction kettle needs to be operated strictly according to the regulation; before operation, the existence of abnormal conditions should be carefully checked, and in normal operation, the upper cover and the wiring terminals on the contact plate should not be opened to avoid electric shock; strictly forbidding operation under pressure; in the process of testing the pressure by using the nitrogen, carefully observing the change of a pressure gauge to reach the pressure testing pressure, and immediately closing a nitrogen valve switch; the temperature rising speed is not suitable to be too fast, the pressurization is also carried out slowly, and particularly, the stirring speed is only allowed to rise slowly; finally, when the kettle body is heated to a higher temperature, the kettle body does not need to be contacted with the kettle body so as to avoid scalding; cooling should be carried out firstly after the experiment is finished; the temperature of the material is not required to be cooled quickly so as to prevent damage caused by excessive temperature difference pressure. And simultaneously, the power supply needs to be pulled out in time.
In the chemical reaction process, different raw materials are added into a reaction kettle and are mixed for chemical reaction; however, in the process of mixing different compounds, in order to accelerate the reaction process, the mixing needs to be accelerated, and most of the existing methods for accelerating the mixing are performed by stirring, but vortexes are easily formed in the stirring process, most of the compounds can be mixed into the vortexes, and the feeding is also a problem to be solved when the compounds are added for reaction, particularly how to rapidly mix the compounds into the vortexes to accelerate the reaction speed.
Disclosure of Invention
The invention aims to provide a unitized compound synthesis reaction kettle to solve the problems in the background technology. In order to achieve the purpose, the invention provides the following technical scheme:
a unitized compound synthesis reactor, comprising: the reaction kettle comprises a reaction kettle body, wherein a unitized feeding structure for feeding is arranged in the reaction kettle body; the stirring mechanism is detachably arranged in the unitized feeding structure and is used for stirring and mixing the compound;
the unitized feeding structure is provided with spiral feeding pipes which are spirally distributed on the inner wall of the reaction kettle body, each spiral feeding pipe consists of a plurality of sections of independent spiral pipes, and the plurality of sections of spiral pipes are independently fed by independent material injection pipes and are used for carrying out unitized chemical combination reaction; the spiral feeding pipe is additionally provided with a plurality of discharging pipes which are distributed in an array manner, the discharging pipes are hinged through a hinged ball and are communicated with the spiral feeding pipe through a liquid guide hole in the hinged ball, and the discharging pipes are used for feeding along with the direction adjustment of a vortex by using the hinged ball; the discharge pipe outside the main material guide cavity is provided with a plurality of outer layer material guide cavities distributed in an annular array; the outer layer material guide cavity is communicated with a plurality of discharge holes, and the discharge holes are formed in the pipe wall of the discharge pipe and are obliquely arranged.
The independently arranged material injection pipe supplies material to the spiral feeding pipe, and the spiral feeding pipe is spirally distributed on the inner wall of the reaction kettle body and is superposed with a vortex formed by stirring, so that the compound can be rapidly mixed and enter; the compound that gets into the spiral feeding pipe simultaneously enters into the inside outer guide chamber and the main guide chamber of discharging pipe through the drain hole of articulated ball inside, enters into the inside raw materials of outer guide chamber and through the discharge opening ejection of compact that is the slope setting, because the counter force of the ejection of compact is the discharging pipe round articulated ball lateral rotation, realizes rotatory reinforced, further promotes the mixture.
In the unitized compound synthesis reaction kettle of the invention: the discharge pipe is provided with a ball cavity matched with the hinged ball, the hinged ball is hinged in the ball cavity, and the ball cavity is communicated with a liquid guide hole formed in the hinged ball;
the outer layer material guide cavity and the main material guide cavity are communicated with the ball cavity;
the ball cavity is provided with an annular outer limiting block for sealing, the outer limiting block is arranged at a position close to the hinged ball and is smooth, and a wear-resistant material layer is laid on the outer limiting block.
Further scheme: the hinge ball is provided with an annular inner limiting block in the spherical cavity.
In the unitized compound synthesis reaction kettle of the invention: the hinge ball is communicated with the interior of a pipe body arranged on the spiral feeding pipe through a connecting pipe, and the connecting pipe is communicated with a liquid guide hole formed in the hinge ball.
In the unitized compound synthesis reaction kettle of the invention: the spiral feeding pipe is fixed on the fixed seat and is fixed at the bottom of the reaction kettle body through the fixed seat; the power device is arranged on the fixed seat in a matching way with the stirring mechanism and provides rotation power for the stirring mechanism; the power device is installed inside the fixing seat, and the inside power device that cooperates of fixing seat has seted up the installation cavity.
Further scheme: a precipitate auxiliary dissolving mechanism is arranged between the power device and the stirring mechanism and is arranged on the surface of the fixed seat; the fixing seat is provided with a cavity in a circular truncated cone shape on the surface close to the auxiliary dissolving mechanism for the sediment material, and the auxiliary dissolving mechanism for the sediment material is arranged inside the cavity.
Preferably: the auxiliary dissolving mechanism of the sediment material and the stirring mechanism are detachably arranged.
The auxiliary dissolving mechanism for the precipitation material is provided with a connecting disc structure, and a plurality of impellers distributed in an annular array are arranged on the periphery of the connecting disc structure; the connecting disc structure is provided with a connecting disc, the connecting disc is provided with a cross groove, and the stirring mechanism is detachably arranged on the auxiliary dissolving mechanism of the sediment material through the cross groove.
The power device provides rotating power for the auxiliary dissolving mechanism of the sediment and the stirring mechanism, and meanwhile, the auxiliary dissolving mechanism of the sediment utilizes the impeller to assist in stirring the sediment falling into the truncated cone-shaped concave cavity; the stirring mechanism stirs to form a vortex for stirring the mixed compound.
The stirring mechanism is provided with a rotating shaft, a plurality of stirring rods are arranged on the rotating shaft, and a cross convex edge is arranged on the rotating shaft in a matching manner with the cross groove.
In the unitized compound synthesis reaction kettle of the invention: the reaction kettle body consists of an outer shell and an inner shell arranged inside the outer shell; a gap cavity is formed between the outer shell and the inner shell, a plurality of connecting hoses communicated with the material injection pipes are inserted in the gap cavity in a penetrating mode, and the connecting hoses independently convey raw materials for the material injection pipes.
Further scheme: an end cover of the reaction kettle body is provided with a top cover, the other end of the reaction kettle body is provided with a base, a base plate is arranged on the base, a material discharging pipe is arranged on the base, and the material discharging pipe is communicated with the interior of the reaction kettle body.
Compared with the prior art, the unitized compound synthesis reaction kettle comprises: the reaction kettle comprises a reaction kettle body, wherein a unitized feeding structure for feeding is arranged in the reaction kettle body; the unitized feeding structure is provided with spiral feeding pipes which are spirally distributed on the inner wall of the reaction kettle body, each spiral feeding pipe consists of a plurality of sections of independent spiral pipes, and the plurality of sections of spiral pipes are independently fed by independent material injection pipes and are used for unitized chemical combination reaction; the spiral feeding pipe is additionally provided with a plurality of discharging pipes which are distributed in an array manner, the discharging pipes are hinged through a hinged ball and are communicated with the spiral feeding pipe through a liquid guide hole in the hinged ball, and the discharging pipes are used for feeding along with the direction adjustment of a vortex by using the hinged ball; the discharge pipe outside the main material guide cavity is provided with a plurality of outer layer material guide cavities distributed in a symmetrical annular array; a plurality of discharge holes are communicated with the outer layer material guide cavity and are formed in the pipe wall of the discharge pipe in an inclined mode; the independently arranged material injection pipe supplies material to the spiral feeding pipe, and the spiral feeding pipe is spirally distributed on the inner wall of the reaction kettle body and is superposed with a vortex formed by stirring, so that the compound can be rapidly mixed and enter; the compound that gets into the spiral feeding pipe simultaneously enters into the inside outer guide chamber and the main guide chamber of discharging pipe through the drain hole of articulated ball inside, enters into the inside raw materials of outer guide chamber and through the discharge opening ejection of compact that is the slope setting, because the counter force of the ejection of compact is the discharging pipe round articulated ball lateral rotation, realizes rotatory reinforced, further promotes the mixture.
Drawings
FIG. 1 is a schematic structural diagram of a unitized compound synthesis reactor of the present invention;
FIG. 2 is a schematic diagram of a transverse cross-sectional structure of the reaction kettle body in FIG. 1;
FIG. 3 is a schematic structural view of the unitized feed structure of FIG. 2;
FIG. 4 is an enlarged schematic view of the structure at A in FIG. 2;
FIG. 5 is a schematic illustration of the tapping pipe of FIG. 4;
FIG. 6 is a schematic drawing of a transverse sectional configuration of the tapping pipe from FIG. 4;
FIG. 7 is an enlarged view of the structure at B in FIG. 2;
fig. 8 is a schematic structural diagram of the land structure of fig. 7.
In the figure:
1-top cover, 2-reaction kettle body, 3-base, 4-base plate and 5-discharge pipe; 21-outer shell, 22-inner shell, 23-unitized feeding structure;
231-a fixed seat, 232-a power device, 233-a stirring mechanism, 234-a spiral feeding pipe, 235-an injection pipe and 236-a precipitate auxiliary dissolving mechanism;
2341-a pipe body, 2342-a connecting pipe, 2343-a hinged ball, 2344-a discharging pipe, 2345-a discharging hole, 2346-an outer layer material guide cavity, 2347-a main material guide cavity, 2348-an inner limiting block and 2349-an outer limiting block;
2361-connecting disc structure, 2362-impeller, 2363-mounting cavity, 2364-cross groove.
Detailed Description
The technical solution of the present invention will be described in further detail with reference to specific embodiments. In the description of the present invention, "a plurality" means two or more unless otherwise specified.
Aiming at adding different raw materials into a reaction kettle in the chemical reaction process, and carrying out a chemical reaction after mixing; however, in the process of mixing different compounds, the reaction process needs to be accelerated, and the mixing needs to be accelerated, while the existing accelerated mixing mode is mostly carried out by stirring, but vortex is easily formed in the stirring process, most of the compounds are mixed into the vortex, and feeding is also a problem to be solved when the compounds are added for reaction, particularly how to quickly mix the compounds into the vortex to accelerate the reaction speed. In order to achieve the purpose, the invention provides the following technical scheme:
in the embodiment of the present invention, as shown in fig. 1 to 6, a unitized compound synthesis reactor includes:
the reaction kettle comprises a reaction kettle body 2, wherein a unitized feeding structure 23 for feeding is arranged in the reaction kettle body 2;
the stirring mechanism 233 is detachably arranged inside the unitized feeding structure 23, and is used for stirring and mixing the compound;
the unitized feeding structure 23 is provided with a spiral feeding pipe 234 spirally distributed on the inner wall of the reaction kettle body 2, the spiral feeding pipe 234 is composed of a plurality of sections of independent spiral pipes, and the plurality of sections of spiral pipes are independently fed by independent material injection pipes 235 and are used for carrying out unitized chemical combination reaction; the spiral feeding pipe 234 is additionally provided with a plurality of discharging pipes 2344 distributed in an array manner, the discharging pipes 2344 are hinged through a hinged ball 2343 and are communicated with the spiral feeding pipe 234 through liquid guide holes in the hinged ball 2343, and the discharging pipes 2344 are used for feeding materials along with the adjustment of the direction of a vortex by means of the hinged ball 2343; the discharge pipe 2344 is provided with a main material guiding cavity 2347, and the discharge pipe 2344 outside the main material guiding cavity 2347 is provided with a plurality of outer layer material guiding cavities 2346 distributed in an annular array; the outer layer material guide cavity 2346 is communicated with a plurality of discharge holes 2345, the discharge holes 2345 are formed in the pipe wall of the discharge pipe 2344 and are arranged in an inclined mode (specifically, an included angle is formed between the discharge holes 2345 and the diameter direction of the circular cross section of the discharge pipe 2344).
In the embodiment of the invention, the spiral feeding pipe 234 is fed by the independently arranged feeding pipe 235, and the spiral feeding pipe 234 is spirally distributed on the inner wall of the reaction kettle body 2 and is overlapped with a vortex formed by stirring, so that the compound can be more favorably and rapidly mixed; the compound that gets into spiral feed pipe 234 simultaneously enters into the inside outer guide chamber 2346 and the main guide chamber 2347 of discharging pipe 2344 through the inside drain hole of articulated ball 2343 inside, enters into the inside raw materials of outer guide chamber 2346 and through the discharge hole 2345 ejection of compact that is the slope setting, because the counter force of the ejection of compact is discharging pipe 2344 round articulated ball 2343 horizontal rotation, realizes rotatory reinforced, further promotes the mixture.
In the embodiment of the invention, as shown in fig. 3-6, a ball cavity is formed in the discharging pipe 2344 in a manner of being matched with the hinge ball 2343, the hinge ball 2343 is hinged in the ball cavity, and the ball cavity is communicated with a liquid guide hole formed in the hinge ball 2343; the outer layer material guide cavity 2346 and the main material guide cavity 2347 are communicated with the ball cavity; be provided with on the ball die cavity and be annular and be used for sealed outer stopper 2349, outer stopper 2349 is smooth form in the setting of being close to articulated ball 2343 department, and has laid the wear-resisting material layer.
Specifically, the hinge ball 2343 is provided with annular inner limiting block 2348 in the spherical cavity for limiting the discharge pipe 2344 to rotate in a transition spherical hinge mode. Wherein, outer stopper 2349 and interior stopper 2348 all set up a plurality of smooth balls that can freely rotate on the face in opposite directions, utilize the pivoted smooth ball to provide mobility after outer stopper 2349 and interior stopper 2348 are close to reduce frictional force.
In the embodiment of the present invention, as shown in fig. 3 to 8, the spiral feeding pipe 234 is fixed on the fixing seat 231 and fixed at the bottom of the reaction kettle body 2 through the fixing seat 231; the power device 232 is arranged on the fixed seat 231 in cooperation with the stirring mechanism 233, and the power device 232 provides rotation power for the stirring mechanism 233; the power device 232 is installed inside the fixing base 231, and the fixing base 231 is provided with an installation cavity 2363 inside matching with the power device 232. Wherein, the power device 232 is a motor, and a protective cover is covered outside the motor.
A precipitation material auxiliary dissolving mechanism 236 is arranged between the power device 232 and the stirring mechanism 233, and the precipitation material auxiliary dissolving mechanism 236 is arranged on the surface of the fixed seat 231; the fixing seat 231 is provided with a cavity in a circular truncated cone shape (wherein, the cavity in the circular truncated cone shape is not limited except the circular truncated cone shape, but also the truncated pyramid shape or the circular truncated cone shape, and the specific structure is not limited as long as the requirement of collecting aggregates can be met, and the preferred cavity is in the circular truncated cone shape) on the surface close to the auxiliary dissolving mechanism 236 for the precipitation material, and the auxiliary dissolving mechanism 236 for the precipitation material is arranged inside the cavity.
The auxiliary dissolving mechanism 236 for the sediment material and the stirring mechanism 233 are detachably arranged; a connecting disc structure 2361 is arranged on the auxiliary sediment dissolving mechanism 236, and a plurality of impellers 2361 distributed in an annular array are arranged around the connecting disc structure 2361; the connecting disc structure 2361 is provided with a connecting disc, the connecting disc is provided with a cross groove 2364, and the stirring mechanism 233 is detachably mounted on the auxiliary sediment dissolving mechanism 236 through the cross groove 2364. The stirring mechanism 233 is provided with a rotating shaft, a plurality of stirring rods are arranged on the rotating shaft, and a cross convex edge is arranged on the rotating shaft in a matching manner with the cross groove 2364.
The power device 232 provides rotation power for the auxiliary sediment dissolving mechanism 236 and the stirring mechanism 233, and meanwhile, the auxiliary sediment dissolving mechanism 236 utilizes the impeller 2361 to assist in stirring sediment falling into the truncated cone-shaped cavity; the stirring mechanism 233 stirs to form a vortex for stirring the mixed compounds.
In the embodiment of the present invention, as shown in fig. 1 to 4, the reaction kettle body 2 is composed of an outer shell 21 and an inner shell 22 arranged inside the outer shell 21; a clearance cavity is formed between the outer shell 21 and the inner shell 22, a plurality of connecting hoses communicated with the material injection pipes 235 are inserted in the clearance cavity in a penetrating manner, and raw materials are independently conveyed to the material injection pipes 235; 2 an end cover of the reation kettle body is equipped with top cap 1, and the other end is provided with base 3, is provided with bed plate 4 on the base 3, and installs row material pipe 5 on the base 3, arranges inside material pipe 5 intercommunication reation kettle body 2.
Wherein, the plurality of connecting hoses are internally provided with switch valves and independently control the feeding; and, the inside check valve that is equipped with of notes material pipe 235 additional avoids the raw materials backward flow.
The invention discloses a unitized compound synthesis reaction kettle, which comprises: the reaction kettle comprises a reaction kettle body 2, wherein a unitized feeding structure 23 for feeding is arranged in the reaction kettle body 2; the unitized feeding structure 23 is provided with a spiral feeding pipe 234 spirally distributed on the inner wall of the reaction kettle body 2, the spiral feeding pipe 234 is composed of a plurality of sections of independent spiral pipes, and the plurality of sections of spiral pipes are independently fed by independent material injection pipes 235 and are used for unitized chemical combination reaction; the spiral feeding pipe 234 is additionally provided with a plurality of discharging pipes 2344 distributed in an array manner, the discharging pipes 2344 are hinged through a hinged ball 2343 and are communicated with the spiral feeding pipe 234 through liquid guide holes in the hinged ball 2343, and the discharging pipes 2344 are used for feeding materials along with the adjustment of the direction of a vortex by means of the hinged ball 2343; the discharge pipe 2344 is provided with a main material guiding cavity 2347, and the discharge pipe 2344 outside the main material guiding cavity 2347 is provided with a plurality of outer layer material guiding cavities 2346 distributed in a symmetrical annular array; a plurality of discharging holes 2345 are communicated with the outer layer material guiding cavity 2346, and the discharging holes 2345 are formed in the pipe wall of the discharging pipe 2344 and are obliquely arranged; the spiral feeding pipe 234 is fed through the independently arranged feeding pipe 235, and the spiral feeding pipe 234 is spirally distributed on the inner wall of the reaction kettle body 2 and is overlapped with a vortex formed by stirring, so that the compound can be rapidly mixed and enter; the compound that gets into spiral feed pipe 234 simultaneously enters into the inside outer guide chamber 2346 and the main guide chamber 2347 of discharging pipe 2344 through the inside drain hole of articulated ball 2343 inside, enters into the inside raw materials of outer guide chamber 2346 and through the discharge hole 2345 ejection of compact that is the slope setting, because the counter force of the ejection of compact is discharging pipe 2344 round articulated ball 2343 horizontal rotation, realizes rotatory reinforced, further promotes the mixture.
In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "connected," and "connected" are to be construed broadly, e.g., as meaning either a fixed connection, a removable connection, or an integral connection; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood by those of ordinary skill in the art through specific situations.
While the preferred embodiments of the present invention have been described in detail, the present invention is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present invention within the knowledge of those skilled in the art.
Claims (9)
1. A unitized compound synthesis reaction kettle, which is characterized in that,
the method comprises the following steps:
the reaction kettle comprises a reaction kettle body, wherein a unitized feeding structure for feeding is arranged in the reaction kettle body;
the stirring mechanism is detachably arranged in the unitized feeding structure and is used for stirring and mixing the compound;
the unitized feeding structure is provided with spiral feeding pipes which are spirally distributed on the inner wall of the reaction kettle body, each spiral feeding pipe consists of a plurality of sections of independent spiral pipes, and the plurality of sections of spiral pipes are independently fed by independent material injection pipes and are used for carrying out unitized chemical combination reaction;
the spiral feeding pipe is additionally provided with a plurality of discharging pipes which are distributed in an array manner, the discharging pipes are hinged through a hinged ball and are communicated with the spiral feeding pipe through a liquid guide hole in the hinged ball, and the discharging pipes are used for feeding along with the direction adjustment of a vortex by using the hinged ball;
the discharge pipe outside the main material guide cavity is provided with a plurality of outer layer material guide cavities distributed in an annular array;
the outer layer material guide cavity is communicated with a plurality of discharge holes, and the discharge holes are formed in the pipe wall of the discharge pipe and are obliquely arranged.
2. The unitized compound synthesis reaction kettle of claim 1,
the discharge pipe is provided with a ball cavity matched with the hinged ball, the hinged ball is hinged in the ball cavity, and the ball cavity is communicated with a liquid guide hole formed in the hinged ball;
the outer layer material guide cavity and the main material guide cavity are communicated with the ball cavity;
the ball cavity is provided with an annular outer limiting block for sealing, the outer limiting block is arranged at a position close to the hinged ball and is smooth, and a wear-resistant material layer is laid on the outer limiting block.
3. The unitized compound synthesis reaction kettle of claim 2, wherein the hinge ball is provided with an annular inner limiting block inside the spherical cavity.
4. The unitized compound synthesis reaction kettle of claim 1,
the hinge ball is communicated with the interior of a pipe body arranged on the spiral feeding pipe through a connecting pipe, and the connecting pipe is communicated with a liquid guide hole arranged in the hinge ball;
the spiral feeding pipe is fixed on the fixed seat and is fixed at the bottom of the reaction kettle body through the fixed seat;
the power device is arranged on the fixed seat in a matching way with the stirring mechanism and provides rotation power for the stirring mechanism;
the power device is installed inside the fixing seat, and the inside power device that cooperates of fixing seat has seted up the installation cavity.
5. The unitized compound synthesis reaction kettle of claim 4,
a precipitate auxiliary dissolving mechanism is arranged between the power device and the stirring mechanism and is arranged on the surface of the fixed seat;
the fixing seat is provided with a cavity in a circular truncated cone shape on the surface close to the auxiliary dissolving mechanism for the sediment material, and the auxiliary dissolving mechanism for the sediment material is arranged inside the cavity.
6. The unitized compound synthesis reaction kettle of claim 5, wherein said precipitate auxiliary dissolving mechanism and said stirring mechanism are detachably mounted.
7. The unitized compound synthesis reaction kettle of claim 6,
the auxiliary dissolving mechanism for the precipitation material is provided with a connecting disc structure, and a plurality of impellers distributed in an annular array are arranged on the periphery of the connecting disc structure;
the connecting disc structure is provided with a connecting disc, the connecting disc is provided with a cross groove, and the stirring mechanism is detachably arranged on the auxiliary dissolving mechanism of the sediment material through the cross groove.
8. A unitized compound synthesis reaction vessel according to any one of claims 1 to 7,
the reaction kettle body consists of an outer shell and an inner shell arranged inside the outer shell;
a gap cavity is formed between the outer shell and the inner shell, a plurality of connecting hoses communicated with the material injection pipes are inserted in the gap cavity in a penetrating mode, and the connecting hoses independently convey raw materials for the material injection pipes.
9. A modular compound synthesis reactor as claimed in claim 8, wherein the reactor body is provided with a top cover at one end and a base at the other end, the base is provided with a base plate, and the base is provided with a discharge pipe which is communicated with the inside of the reactor body.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202011565543.XA CN112705144B (en) | 2020-12-25 | 2020-12-25 | Unitized compound synthesis reaction kettle |
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| CN202011565543.XA CN112705144B (en) | 2020-12-25 | 2020-12-25 | Unitized compound synthesis reaction kettle |
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| CN112705144A CN112705144A (en) | 2021-04-27 |
| CN112705144B true CN112705144B (en) | 2022-04-19 |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109966939A (en) * | 2019-03-27 | 2019-07-05 | 浙江大学 | A kind of Venturi type microbubble generator and gas-liquid producer |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100673024B1 (en) * | 2006-01-16 | 2007-01-24 | 삼성전자주식회사 | Nozzle and apparatus for treating substrates with the nozzle |
| CN105749774B (en) * | 2014-12-20 | 2018-04-10 | 中国石油化工股份有限公司 | A kind of pipe-line mixer |
| CN205886880U (en) * | 2016-07-29 | 2017-01-18 | 湖南雅城新材料股份有限公司 | Reaction kettle feeding device |
| CN206276381U (en) * | 2016-11-29 | 2017-06-27 | 石家庄瑞凯化工有限公司 | A kind of reactor of quick blend feedstock |
| CN206793660U (en) * | 2017-05-18 | 2017-12-26 | 佛山市尚峰高分子科技有限公司 | A kind of vertical response kettle |
| CN107313746B (en) * | 2017-08-07 | 2023-05-26 | 南充西南石油大学设计研究院有限责任公司 | Double-channel rotary mixing spray head |
| CN109772234B (en) * | 2017-11-14 | 2024-01-05 | 中国石油化工股份有限公司 | Feed gas feed system for propylene ammoxidation reactor |
| CN207838991U (en) * | 2017-12-29 | 2018-09-11 | 常州瑞明药业有限公司 | Controllably multi-purpose uniform feeding reaction kettle |
| CN210045113U (en) * | 2019-10-28 | 2020-02-11 | 海南紫杉园制药有限公司 | Liquid preparation tank |
| CN211988090U (en) * | 2019-11-21 | 2020-11-24 | 云南昆船电子设备有限公司 | Flexible stirring device |
-
2020
- 2020-12-25 CN CN202011565543.XA patent/CN112705144B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109966939A (en) * | 2019-03-27 | 2019-07-05 | 浙江大学 | A kind of Venturi type microbubble generator and gas-liquid producer |
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