CN215743392U

CN215743392U - Reaction kettle device convenient for separating liquid

Info

Publication number: CN215743392U
Application number: CN202121421892.4U
Authority: CN
Inventors: 刘荣
Original assignee: Changzhou Watson Fine Chemical Co ltd
Current assignee: Changzhou Watson Fine Chemical Co ltd
Priority date: 2021-06-25
Filing date: 2021-06-25
Publication date: 2022-02-08
Anticipated expiration: 2031-06-25

Abstract

The utility model discloses a reaction kettle device convenient for liquid separation, which comprises a reaction kettle, wherein the top of the reaction kettle is provided with a feed inlet, a drainage device capable of extending into the reaction kettle is arranged at the feed inlet, the drainage device comprises a telescopic drainage tube and a flow collecting barrel, the outlet end of the drainage tube extends out of the feed inlet, and the inlet end of the drainage tube extends into the reaction kettle and is communicated with the bottom of the flow collecting barrel. According to the utility model, the layered liquid in the reaction kettle can be easily transferred out one by one through the drainage device, and meanwhile, the next layer of liquid is not influenced, so that the separation time is short, and the post-treatment time of production is greatly shortened.

Description

Reaction kettle device convenient for separating liquid

Technical Field

The utility model relates to the technical field of reaction kettles, in particular to a reaction kettle device convenient for liquid separation.

Background

The reaction kettle is widely applied to petroleum, chemical engineering, rubber, pesticides, dyes, medicines and foods, and is a pressure container for completing technological processes such as vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation and the like, such as a reactor, a reaction kettle, a decomposition kettle, a polymerization kettle and the like; the material is carbon manganese steel, stainless steel and other composite materials.

After the reaction in the reaction kettle is finished, substances in the reaction kettle need to be discharged, when one solid-liquid mixture or a plurality of liquid mixtures are injected into the reaction kettle, the mixtures can be slowly layered in the reaction process, solid-liquid separation or one-by-one separation of a plurality of liquids is needed when the solid-liquid mixture or the plurality of liquid mixtures are discharged after the reaction is finished, so as to extract the liquid reactant with higher purity, but when the existing reaction kettle is used for discharging, other separation devices are used for separating solid from liquid or a plurality of liquids, but the separation is carried out, so that not only is the separation incomplete, but also other liquids or solids are mixed together, the time is wasted, and the subsequent manufacturing cost and the processing time are increased.

Disclosure of Invention

The utility model aims to overcome the defects of the prior art and provide a reaction kettle device which is convenient for quickly separating well-layered solid-liquid mixture or a plurality of liquid mixtures and is convenient for separating liquid.

The technical scheme adopted by the utility model is as follows:

the utility model provides a reation kettle device convenient to separate liquid, it includes reation kettle, and reation kettle's top is equipped with the charge door, and charge door department installs the drainage device that can stretch into in the reation kettle, and drainage device includes telescopic drainage tube and mass flow bucket, and the exit end of drainage tube stretches out the charge door, and the entrance point of drainage tube stretches into in the reation kettle and communicates with the bottom of mass flow bucket.

The drainage tube of the device is formed by sequentially sleeving a plurality of sleeves with polygonal cross sections, and the inner wall of the upper end of each sleeve is fixedly provided with a limiting sleeve.

The outlet end of the drainage tube of the device is connected with a vacuum pump.

The top of the collecting barrel of the device inclines towards the direction of the drainage tube, wherein the bottom of the collecting barrel forms an inclination angle of 5-10 degrees with the horizontal plane.

The size of the collecting barrel of the device is matched with the size of the charging opening.

The outer wall of the reaction kettle of the device is provided with a visible window.

The bottom of the reaction kettle of the device is provided with a support frame with a shockproof pad.

The device also comprises a stirring system, wherein the stirring system comprises a driving motor, a coupler and a stirring shaft extending into the reaction kettle, and the stirring shaft is connected with the driving motor through the coupler.

The stirring shaft of the device is provided with a detachable stirrer.

The utility model has the following beneficial effects: according to the utility model, the layered liquid in the reaction kettle can be easily transferred out one by one through the drainage device, an operator extends the drainage device into the liquid to be moved out in the reaction kettle through the charging opening, the liquid firstly flows into the collecting barrel, the bottom of the collecting through is communicated with the drainage tube extending out of the charging opening, so that the liquid is moved out along the drainage tube under the action of the vacuum pump, when the height of the liquid to be moved out in the reaction kettle is lower than that of the collecting barrel, the operator can press the collecting barrel downwards through the drainage tube, so that the residual liquid does not influence the next layer of liquid while flowing into the collecting barrel, thus the separation time is short, and the post-production treatment time is greatly shortened.

Drawings

FIG. 1 is a schematic structural diagram of the present invention;

FIG. 2 is another schematic structural view of the present invention;

FIG. 3 is a schematic view of the drainage device according to the present invention;

in the figure 1, a reaction kettle; 2. a feed inlet; 3. a drainage device; 4. a drainage tube; 5. a collecting barrel; 6. a drive motor; 7. a coupling; 8. a stirring shaft; 9. a sleeve; 10. a limiting sleeve; 11. a vacuum pump; 12. a visible window; 13. a stirrer; 14. a support frame.

Detailed Description

The utility model will be further described with reference to the accompanying drawings in which:

as shown in fig. 1-3, the utility model comprises a reaction kettle 1, a feed inlet 2 is arranged at the top of the reaction kettle 1, a drainage device 3 which can extend into the reaction kettle 1 is arranged at the feed inlet 2, the drainage device 3 comprises a telescopic drainage tube 4 and a collecting barrel 5, and the size of the collecting barrel 5 is matched with the size of the feed inlet 2; the outlet end of the drainage tube 4 extends out of the charging opening 2, the inlet end of the drainage tube 4 extends into the reaction kettle 1 and is communicated with the bottom of the collecting barrel 5, so that the liquid to be moved out can flow into the collecting barrel 5 firstly and then move out of the reaction kettle 1 along the drainage tube 4.

The drainage tube 4 of the device is formed by sequentially sleeving a plurality of sleeves 9 with polygonal cross sections, and the inner wall of the upper end of each sleeve 9 is fixedly provided with a limiting sleeve 10, so that the vertically adjacent sleeves 9 cannot be separated, and the drainage tube has sealing performance, and prevents liquid to be moved out from the fixed positions of the adjacent sleeves 9. Because the cross section of sleeve pipe 9 is the polygon for the in-process of operating personnel manual extension or withdrawal drainage tube 4, the phenomenon that every sleeve pipe 9 rotates relative to other sleeve pipes 9 can not appear, after the height control of drainage tube 4 targets in place, collecting bucket 5 can not squint the original position, and operating personnel need not worry that the liquid that the layering is good is stirred and is mixed, and it is very convenient to use.

The top of the collecting barrel 5 of the device can be parallel to the horizontal plane and can also be inclined towards the drainage tube 4, the bottom of the collecting barrel 5 when the collecting barrel is inclined forms an inclined angle of 5-10 degrees with the horizontal plane, so that liquid flowing into the collecting barrel 5 can quickly enter the drainage tube 4 and then is pumped out through a vacuum pump 11 connected with the outlet end of the drainage tube 4.

This device still includes the mixing system, and this mixing system includes driving motor 6, shaft coupling 7 and stretches into (mixing) shaft 8 in reation kettle 1, and (mixing) shaft 8 passes through shaft coupling 7 and is connected with driving motor 6, is equipped with detachable agitator 13 on the (mixing) shaft 8.

The visible window 12 is arranged on the outer wall of the reaction kettle 1 of the device, so that an operator can conveniently operate the drainage device 3 to transfer out liquid within the stroke range of the visible window 12 without worrying about moving out the next layer of liquid; the bottom of the reaction kettle 1 is provided with a support frame 14 with a shockproof pad.

The using process of the utility model is as follows:

when the device is used, one end of the drainage tube 4 communicated with the collecting barrel 5 extends into the reaction kettle 1 from the feeding port 2, the other end of the drainage tube extends out of the feeding port 2 and is connected with the vacuum pump 11, then an operator determines the position of liquid to be moved out through the visible window 12, the drainage tube 4 is manually elongated, the collecting barrel 5 is slowly immersed into the liquid to be moved out, the liquid flows into the collecting barrel 5, the liquid entering the collecting barrel 5 directly flows into the drainage tube 4, and then the vacuum pump 11 completely moves out the liquid entering the drainage tube 4; when the height of the liquid to be removed in the reaction kettle 1 is lower than that of the collecting barrel 5, an operator can continuously pull out the drainage tube 4 to press the collecting barrel 5 towards the direction of the next layer of liquid, so that the remaining liquid flows into the collecting barrel 5 without influencing the next layer of liquid, the purity of the removed liquid is very high, and the time of post-production treatment is greatly shortened.

Other undescribed portions of the present invention are the same as the prior art.

Claims

1. The utility model provides a reation kettle device convenient to separate liquid, characterized by it includes reation kettle (1), the top of reation kettle (1) is equipped with charge door (2), charge door (2) department installs drainage device (3) that can stretch into reation kettle (1), drainage device (3) include telescopic drainage tube (4) and mass flow bucket (5), charge door (2) are stretched out to the exit end of drainage tube (4), the entrance point of drainage tube (4) stretch into in reation kettle (1) and communicate with the bottom of mass flow bucket (5).

2. The reactor device convenient for separating liquid according to claim 1, wherein the drainage tube (4) is formed by sequentially sleeving a plurality of sleeves (9) with polygonal cross sections, and a limiting sleeve (10) is fixedly arranged on the inner wall of the upper end of each sleeve (9).

3. A reactor vessel arrangement for facilitating the separation of liquids according to claim 1, characterized in that the outlet end of the draft tube (4) is connected to a vacuum pump (11).

4. The reactor device convenient for separating liquid as claimed in claim 1, wherein the top of the collecting barrel (5) is inclined towards the drainage tube (4), and the bottom of the collecting barrel (5) forms an inclined angle of 5-10 degrees with the horizontal plane.

5. The reactor apparatus for facilitating the separation of liquid according to claim 1, wherein the size of the collecting barrel (5) is matched with the size of the feed inlet (2).

6. The reactor device convenient for separating liquid as claimed in claim 1, wherein the outer wall of the reactor (1) is provided with a visible window (12).

7. The reactor device convenient for separating liquid as claimed in claim 1, wherein the bottom of the reactor (1) is provided with a support frame (14) with a shock-proof pad.

8. The reaction kettle device convenient for separating liquid according to claim 1, characterized in that the reaction kettle device comprises a stirring system, the stirring system comprises a driving motor (6), a coupler (7) and a stirring shaft (8) extending into the reaction kettle (1), and the stirring shaft (8) is connected with the driving motor (6) through the coupler (7).

9. The reactor apparatus for facilitating the separation of liquid according to claim 8, wherein the stirring shaft (8) is provided with a detachable stirrer (13).