CN112679091A - Formula and method of vanadium yellow matte decorative glaze for ceramic wine bottles - Google Patents
Formula and method of vanadium yellow matte decorative glaze for ceramic wine bottles Download PDFInfo
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Abstract
The invention discloses a vanadium yellow matte decorative glaze formula for ceramic wine bottles and a method, wherein the formula comprises the following steps: the paint comprises potassium feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate, kaolin, a black pigment, a vanadium yellow pigment, a praseodymium yellow pigment and zirconium iron red, wherein the mass percentages of the components are as follows: 30-40 parts of potassium feldspar, 10-20 parts of quartz, 5-10 parts of calcite, 10-15 parts of wollastonite, 15-20 parts of talcum, 5-10 parts of alumina, 3-7 parts of zirconium silicate, 10-15 parts of kaolin, 0.5-1 part of black pigment, 5-10 parts of vanadium yellow pigment, 3-6 parts of praseodymium yellow pigment and 1-3 parts of ferrozirconium red; according to the invention, after the porcelain is fired at 1260-1280 ℃, the glaze color is pure, the glaze surface is smooth, no fading exists, no heavy metal exceeds the standard, the porcelain is resistant to chemical corrosion, wear resistant, good in product quality, high in grade, as jade and as good as a product, and the porcelain is practical, safe and guaranteed as a wine container; the enamel is fine and smooth, the glaze is as smooth as jade, the pressure resistance is high, and the hardness of the glaze is good.
Description
Technical Field
The invention relates to the technical field of a formula of a vanadium yellow matte decorative glaze for a ceramic wine bottle, in particular to a formula and a method of the vanadium yellow matte decorative glaze for the ceramic wine bottle.
Background
The ceramic is the essence of China of Chinese nationality and is famous all over the world since ancient times. In the field of this traditional process, there are hundreds of different forms and raw material formulations. There are various ceramic artwork in Jiangxi Jingdezhen, Guangdong Chaozhou, Fujian German, Shandong Zibo, Hunan carinling, etc.; all flowers are put together, and are bright and dazzling, so that the intelligent crystals of China nationality are shown;
the colored glaze is one of ceramic decorative glaze materials and can not decay for thousands of years; the market is very common today, and the presentation form and decoration type are the best. The multifunctional water cup is similar to the multifunctional water cup in the field of life, and can be used as a utensil for eating and drinking; quite common and very practical; compared with plastic and metal tools, the material has the obvious advantages of being healthier and safer; in the current market, some existing ceramic colored glazes have defects, such as low firing temperature, fading, excessive heavy metal and the like, and it is necessary to design a formula and a method of a vanadium yellow matte decorative glaze for ceramic wine bottles.
Disclosure of Invention
The invention aims to provide a formula and a method of a vanadium yellow matte decorative glaze for a ceramic wine bottle, so as to solve the problems in the background technology.
In order to solve the technical problems, the invention provides the following technical scheme: a formula of vanadium yellow matte decorative glaze for ceramic wine bottles comprises the following components: the paint comprises potassium feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate, kaolin, a black pigment, a vanadium yellow pigment, a praseodymium yellow pigment and zirconium iron red, wherein the mass percentages of the components are as follows: 30-40 parts of potassium feldspar, 10-20 parts of quartz, 5-10 parts of calcite, 10-15 parts of wollastonite, 15-20 parts of talcum, 5-10 parts of alumina, 3-7 parts of zirconium silicate, 10-15 parts of kaolin, 0.5-1 part of black pigment, 5-10 parts of vanadium yellow pigment, 3-6 parts of praseodymium yellow pigment and 1-3 parts of ferrozirconium red.
A method for preparing a vanadium yellow matte decorative glaze formula for a ceramic wine bottle comprises the following steps of firstly, selecting materials; step two, mixing and ball milling; step three, screening and processing; step four, glazing and kiln loading; step five, storing and placing;
in the first step, the contents of the components are as follows: selecting 30-40 parts of potassium feldspar, 10-20 parts of quartz, 5-10 parts of calcite, 10-15 parts of wollastonite, 15-20 parts of talcum, 5-10 parts of alumina, 3-7 parts of zirconium silicate, 10-15 parts of kaolin, 0.5-1 part of black pigment, 5-10 parts of vanadium yellow pigment, 3-6 parts of praseodymium yellow pigment and 1-3 parts of ferrozirconium red, and weighing;
in the second step, the mixing and ball milling comprises the following steps:
1) manually preparing a reaction kettle, adding potash feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate and kaolin into the reaction kettle, stirring for 10-20min, and then standing;
2) adding black pigment, vanadium yellow pigment, praseodymium yellow pigment and zirconium iron red into the reaction kettle, stirring for 10-20min again, pouring the mixture into a ball mill, adding water and high alumina ball stone, and starting the ball mill for ball milling for 20-30 h;
in the third step, the screening process comprises the following steps:
1) manually taking out the mixture subjected to ball milling in the step two 2), mixing and stirring for 10-20min, and then standing for 1-2 h;
2) pouring the mixture into a screen mesh for screening, and continuously screening for 2-3 times, wherein the screen residue is 0.01% -0.03%;
wherein in the fourth step, the glazing and kiln loading comprises the following steps:
1) artificially glazing the mixture screened in the step three 2) to obtain a glaze with the glazing concentration of 35-45 Baume degrees;
2) glazing the biscuit, then placing the biscuit in a kiln, raising the temperature, and sintering the oxidizing flame at a high temperature of 1260-1280 ℃ to obtain a smooth glazed surface of the porcelain, thus obtaining a finished product;
in the fifth step, the finished products obtained in the fourth step 2) are manually checked, boxed and stored in a shady and cool place after being checked to be qualified.
According to the technical scheme, the contents of the components are respectively as follows: 35 parts of potassium feldspar, 15 parts of quartz, 5 parts of calcite, 10 parts of wollastonite, 15 parts of talc, 5 parts of alumina, 5 parts of zirconium silicate, 10 parts of kaolin, 1 part of black pigment, 5 parts of vanadium yellow pigment, 3 parts of praseodymium yellow pigment and 1 part of ferrozirconium red.
According to the technical scheme, the medium-high alumina ball stone in the step two 2) is an alumina ball.
According to the technical scheme, the mass ratio of the raw materials, the high-alumina ball stone and the water in the second step 2) is 1: 1.5: 0.8.
According to the technical scheme, the screen mesh in the step three 2) is 200 meshes.
According to the technical scheme, in the fifth step, disinfection treatment is required before boxing.
Compared with the prior art, the invention has the following beneficial effects: according to the invention, after the porcelain is fired at 1260-1280 ℃, the glaze color is pure, the glaze surface is smooth, no fading exists, no heavy metal exceeds the standard, the porcelain is resistant to chemical corrosion, wear resistant, good in product quality, high in grade, as jade and as good as a product, and the porcelain is practical, safe and guaranteed as a wine container; the enamel is fine and smooth, the glaze is as smooth as jade, the pressure resistance is high, the hardness of the glaze is good, and the decorative effect is unique.
Drawings
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention. In the drawings:
FIG. 1 is a process flow diagram of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1, the present invention provides a technical solution: a formula and a method of a vanadium yellow matte decorative glaze for ceramic wine bottles are as follows:
example 1:
a formula of vanadium yellow matte decorative glaze for ceramic wine bottles comprises the following components: the paint comprises potassium feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate, kaolin, a black pigment, a vanadium yellow pigment, a praseodymium yellow pigment and zirconium iron red, wherein the mass percentages of the components are as follows: 30 parts of potassium feldspar, 20 parts of quartz, 5 parts of calcite, 10 parts of wollastonite, 15 parts of talc, 5 parts of alumina, 5 parts of zirconium silicate, 10 parts of kaolin, 1 part of black pigment, 5 parts of vanadium yellow pigment, 3 parts of praseodymium yellow pigment and 1 part of ferrozirconium red.
A method for preparing a vanadium yellow matte decorative glaze formula for a ceramic wine bottle comprises the following steps of firstly, selecting materials; step two, mixing and ball milling; step three, screening and processing; step four, glazing and kiln loading; step five, storing and placing;
in the first step, the contents of the components are as follows: selecting 30 parts of potassium feldspar, 20 parts of quartz, 5 parts of calcite, 10 parts of wollastonite, 15 parts of talcum, 5 parts of alumina, 5 parts of zirconium silicate, 10 parts of kaolin, 1 part of black pigment, 5 parts of vanadium yellow pigment, 3 parts of praseodymium yellow pigment and 1 part of ferrozirconium red, and weighing;
in the second step, the mixing and ball milling comprises the following steps:
1) manually preparing a reaction kettle, adding potash feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate and kaolin into the reaction kettle, stirring for 10-20min, and then standing;
2) adding black pigment, vanadium pigment, praseodymium yellow pigment and zirconium iron red into the reaction kettle, stirring for 10-20min again, pouring the mixture into a ball mill, adding water and high alumina ball stone, wherein the high alumina ball stone is alumina balls, the mass ratio of the raw materials, the high alumina ball stone and the water is 1: 1.5: 0.8, and starting the ball mill for ball milling for 20-30 h;
in the third step, the screening process comprises the following steps:
1) manually taking out the mixture subjected to ball milling in the step two 2), mixing and stirring for 10-20min, and then standing for 1-2 h;
2) pouring the mixture into a screen mesh for screening, wherein the screen mesh is 200 meshes, and continuously screening for 2-3 times, and the screen residue is 0.01% -0.03%;
wherein in the fourth step, the glazing and kiln loading comprises the following steps:
1) artificially glazing the mixture screened in the step three 2) to obtain a glaze with the glazing concentration of 35-45 Baume degrees;
2) glazing the biscuit, then placing the biscuit in a kiln, raising the temperature, and sintering the oxidizing flame at a high temperature of 1260-1280 ℃ to obtain a smooth glazed surface of the porcelain, thus obtaining a finished product;
in the fifth step, the finished products obtained in the fourth step 2) are manually checked, boxed and stored in a cool place after being checked to be qualified, and disinfection treatment is required before boxing.
Example 2:
a formula of vanadium yellow matte decorative glaze for ceramic wine bottles comprises the following components: the paint comprises potassium feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate, kaolin, a black pigment, a vanadium yellow pigment, a praseodymium yellow pigment and zirconium iron red, wherein the mass percentages of the components are as follows: 35 parts of potassium feldspar, 15 parts of quartz, 5 parts of calcite, 10 parts of wollastonite, 15 parts of talc, 5 parts of alumina, 5 parts of zirconium silicate, 10 parts of kaolin, 1 part of black pigment, 5 parts of vanadium yellow pigment, 3 parts of praseodymium yellow pigment and 1 part of ferrozirconium red.
A method for preparing a vanadium yellow matte decorative glaze formula for a ceramic wine bottle comprises the following steps of firstly, selecting materials; step two, mixing and ball milling; step three, screening and processing; step four, glazing and kiln loading; step five, storing and placing;
in the first step, the contents of the components are as follows: selecting 35 parts of potassium feldspar, 15 parts of quartz, 5 parts of calcite, 10 parts of wollastonite, 15 parts of talcum, 5 parts of alumina, 5 parts of zirconium silicate, 10 parts of kaolin, 1 part of black pigment, 5 parts of vanadium yellow pigment, 3 parts of praseodymium yellow pigment and 1 part of ferrozirconium red, and weighing;
in the second step, the mixing and ball milling comprises the following steps:
1) manually preparing a reaction kettle, adding potash feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate and kaolin into the reaction kettle, stirring for 10-20min, and then standing;
2) adding black pigment, vanadium pigment, praseodymium yellow pigment and zirconium iron red into the reaction kettle, stirring for 10-20min again, pouring the mixture into a ball mill, adding water and high alumina ball stone, wherein the high alumina ball stone is alumina balls, the mass ratio of the raw materials, the high alumina ball stone and the water is 1: 1.5: 0.8, and starting the ball mill for ball milling for 20-30 h;
in the third step, the screening process comprises the following steps:
1) manually taking out the mixture subjected to ball milling in the step two 2), mixing and stirring for 10-20min, and then standing for 1-2 h;
2) pouring the mixture into a screen mesh for screening, wherein the screen mesh is 200 meshes, and continuously screening for 2-3 times, and the screen residue is 0.01% -0.03%;
wherein in the fourth step, the glazing and kiln loading comprises the following steps:
1) artificially glazing the mixture screened in the step three 2) to obtain a glaze with the glazing concentration of 35-45 Baume degrees;
2) glazing the biscuit, then placing the biscuit in a kiln, raising the temperature, and sintering the oxidizing flame at a high temperature of 1260-1280 ℃ to obtain a smooth glazed surface of the porcelain, thus obtaining a finished product;
in the fifth step, the finished products obtained in the fourth step 2) are manually checked, boxed and stored in a cool place after being checked to be qualified, and disinfection treatment is required before boxing.
Example 3:
a formula of vanadium yellow matte decorative glaze for ceramic wine bottles comprises the following components: the paint comprises potassium feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate, kaolin, a black pigment, a vanadium yellow pigment, a praseodymium yellow pigment and zirconium iron red, wherein the mass percentages of the components are as follows: 40 parts of potassium feldspar, 10 parts of quartz, 5 parts of calcite, 10 parts of wollastonite, 15 parts of talc, 5 parts of alumina, 5 parts of zirconium silicate, 10 parts of kaolin, 1 part of black pigment, 5 parts of vanadium yellow pigment, 3 parts of praseodymium yellow pigment and 1 part of ferrozirconium red.
A method for preparing a vanadium yellow matte decorative glaze formula for a ceramic wine bottle comprises the following steps of firstly, selecting materials; step two, mixing and ball milling; step three, screening and processing; step four, glazing and kiln loading; step five, storing and placing;
in the first step, the contents of the components are as follows: selecting 40 parts of potassium feldspar, 10 parts of quartz, 5 parts of calcite, 10 parts of wollastonite, 15 parts of talc, 5 parts of alumina, 5 parts of zirconium silicate, 10 parts of kaolin, 1 part of black pigment, 5 parts of vanadium yellow pigment, 3 parts of praseodymium yellow pigment and 1 part of ferrozirconium red, and weighing;
in the second step, the mixing and ball milling comprises the following steps:
1) manually preparing a reaction kettle, adding potash feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate and kaolin into the reaction kettle, stirring for 10-20min, and then standing;
2) adding black pigment, vanadium pigment, praseodymium yellow pigment and zirconium iron red into the reaction kettle, stirring for 10-20min again, pouring the mixture into a ball mill, adding water and high alumina ball stone, wherein the high alumina ball stone is alumina balls, the mass ratio of the raw materials, the high alumina ball stone and the water is 1: 1.5: 0.8, and starting the ball mill for ball milling for 20-30 h;
in the third step, the screening process comprises the following steps:
1) manually taking out the mixture subjected to ball milling in the step two 2), mixing and stirring for 10-20min, and then standing for 1-2 h;
2) pouring the mixture into a screen mesh for screening, wherein the screen mesh is 200 meshes, and continuously screening for 2-3 times, and the screen residue is 0.01% -0.03%;
wherein in the fourth step, the glazing and kiln loading comprises the following steps:
1) artificially glazing the mixture screened in the step three 2) to obtain a glaze with the glazing concentration of 35-45 Baume degrees;
2) glazing the biscuit, then placing the biscuit in a kiln, raising the temperature, and sintering the oxidizing flame at a high temperature of 1260-1280 ℃ to obtain a smooth glazed surface of the porcelain, thus obtaining a finished product;
in the fifth step, the finished products obtained in the fourth step 2) are manually checked, boxed and stored in a cool place after being checked to be qualified, and disinfection treatment is required before boxing.
The properties of the above examples are compared in the following table:
heavy metal content | Chemical resistance/(grade) | Compressive strength/(grade) | |
Example 1 | Qualified | 3 | 2 |
Example 2 | Qualified | 3 | 3 |
Example 3 | Qualified | 2 | 3 |
Based on the above, the invention has the advantages that after the porcelain is fired at 1260-1280 ℃, the glaze color is pure, the glaze surface is smooth, has no fading, no heavy metal exceeding standard, chemical corrosion resistance, abrasion resistance, good product quality, high grade, and is as warm as jade and has a product level, thereby being practical, safe and guaranteed as a wine container; the enamel is fine and smooth, the glaze is as smooth as jade, the pressure resistance is high, the hardness of the glaze is good, and the decorative effect is unique.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (7)
1. The formula of the vanadium yellow matte decorative glaze for the ceramic wine bottle is characterized in that: the formula comprises the following components: the paint comprises potassium feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate, kaolin, a black pigment, a vanadium yellow pigment, a praseodymium yellow pigment and zirconium iron red, wherein the mass percentages of the components are as follows: 30-40 parts of potassium feldspar, 10-20 parts of quartz, 5-10 parts of calcite, 10-15 parts of wollastonite, 15-20 parts of talcum, 5-10 parts of alumina, 3-7 parts of zirconium silicate, 10-15 parts of kaolin, 0.5-1 part of black pigment, 5-10 parts of vanadium yellow pigment, 3-6 parts of praseodymium yellow pigment and 1-3 parts of ferrozirconium red.
2. A method for preparing a vanadium yellow matte decorative glaze formula for a ceramic wine bottle comprises the following steps of firstly, selecting materials; step two, mixing and ball milling; step three, screening and processing; step four, glazing and kiln loading; step five, storing and placing; the method is characterized in that:
in the first step, the contents of the components are as follows: selecting 30-40 parts of potassium feldspar, 10-20 parts of quartz, 5-10 parts of calcite, 10-15 parts of wollastonite, 15-20 parts of talcum, 5-10 parts of alumina, 3-7 parts of zirconium silicate, 10-15 parts of kaolin, 0.5-1 part of black pigment, 5-10 parts of vanadium yellow pigment, 3-6 parts of praseodymium yellow pigment and 1-3 parts of ferrozirconium red, and weighing;
in the second step, the mixing and ball milling comprises the following steps:
1) manually preparing a reaction kettle, adding potash feldspar, quartz, calcite, wollastonite, talc, alumina, zirconium silicate and kaolin into the reaction kettle, stirring for 10-20min, and then standing;
2) adding black pigment, vanadium yellow pigment, praseodymium yellow pigment and zirconium iron red into the reaction kettle, stirring for 10-20min again, pouring the mixture into a ball mill, adding water and high alumina ball stone, and starting the ball mill for ball milling for 20-30 h;
in the third step, the screening process comprises the following steps:
1) manually taking out the mixture subjected to ball milling in the step two 2), mixing and stirring for 10-20min, and then standing for 1-2 h;
2) pouring the mixture into a screen mesh for screening, and continuously screening for 2-3 times, wherein the screen residue is 0.01% -0.03%;
wherein in the fourth step, the glazing and kiln loading comprises the following steps:
1) artificially glazing the mixture screened in the step three 2) to obtain a glaze with the glazing concentration of 35-45 Baume degrees;
2) glazing the biscuit, then placing the biscuit in a kiln, raising the temperature, and sintering the oxidizing flame at a high temperature of 1260-1280 ℃ to obtain a smooth glazed surface of the porcelain, thus obtaining a finished product;
in the fifth step, the finished products obtained in the fourth step 2) are manually checked, boxed and stored in a shady and cool place after being checked to be qualified.
3. The vanadium yellow matte decorative glaze formula for ceramic wine bottles according to claim 1, wherein the formula comprises the following components in percentage by weight: the contents of the components are respectively as follows: 35 parts of potassium feldspar, 15 parts of quartz, 5 parts of calcite, 10 parts of wollastonite, 15 parts of talc, 5 parts of alumina, 5 parts of zirconium silicate, 10 parts of kaolin, 1 part of black pigment, 5 parts of vanadium yellow pigment, 3 parts of praseodymium yellow pigment and 1 part of ferrozirconium red.
4. The method for preparing the vanadium yellow matte decorative glaze formula for the ceramic wine bottles according to claim 1, wherein the method comprises the following steps: and in the second step 2), the medium-high alumina ball stone is an alumina ball.
5. The method for preparing the vanadium yellow matte decorative glaze formula for the ceramic wine bottles according to claim 2, wherein the method comprises the following steps: the mass ratio of the raw materials, the high alumina ball stone and the water in the step 2) is 1: 1.5: 0.8.
6. The method for preparing the vanadium yellow matte decorative glaze formula for the ceramic wine bottles according to claim 2, wherein the method comprises the following steps: and in the third step 2), the sieve mesh is 200 meshes.
7. The method for preparing the vanadium yellow matte decorative glaze formula for the ceramic wine bottles according to claim 2, wherein the method comprises the following steps: and in the fifth step, disinfection treatment is required before boxing.
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Cited By (2)
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CN115745404A (en) * | 2022-11-28 | 2023-03-07 | 浙江大学温州研究院 | High-solid-content glaze suitable for direct-writing 3D printing and preparation method thereof |
JP7382046B1 (en) | 2023-05-11 | 2023-11-16 | ハクスイテック株式会社 | glaze composition |
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2020
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Cited By (2)
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CN115745404A (en) * | 2022-11-28 | 2023-03-07 | 浙江大学温州研究院 | High-solid-content glaze suitable for direct-writing 3D printing and preparation method thereof |
JP7382046B1 (en) | 2023-05-11 | 2023-11-16 | ハクスイテック株式会社 | glaze composition |
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