CN112662240A - Preparation process of fragrance lamp - Google Patents

Preparation process of fragrance lamp Download PDF

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Publication number
CN112662240A
CN112662240A CN202011454450.XA CN202011454450A CN112662240A CN 112662240 A CN112662240 A CN 112662240A CN 202011454450 A CN202011454450 A CN 202011454450A CN 112662240 A CN112662240 A CN 112662240A
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hollow microspheres
coating
preparation process
water
fragrance lamp
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CN202011454450.XA
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陈惠敏
陈国冻
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Quanzhou Quanxing Hardware Art Co ltd
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Quanzhou Quanxing Hardware Art Co ltd
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Abstract

The application relates to the field of lamps and particularly discloses a preparation process of a fragrance lamp. The preparation process of the fragrance lamp comprises the following steps: s1, carrying out primary stirring dispersion on styrene-acrylic emulsion, epoxy resin, a defoaming agent and water for 5-20 min, then adding polymethyl silsesquioxane and hollow microspheres for secondary stirring dispersion for 20-50 min, and then adding a film-forming assistant for tertiary stirring dispersion for 5-15 min to obtain a heat-insulating coating; s2, coating the heat insulation coating on the surface of the lamp housing, and drying to form a coating, wherein the thickness of the coating is 0.5-2 mm; s3, smearing glass cement on the edge of the glass, bonding the glass with the edge of a preset observation port of the lamp shell, curing at 50-60 ℃, and mounting a base, thereby preparing the fragrance lamp. This application has the heat-proof quality that improves the fragrance lamp body, improves the advantage of using experience.

Description

Preparation process of fragrance lamp
Technical Field
The application relates to the field of lamps, in particular to a preparation process of a fragrance lamp.
Background
Along with the continuous improvement of the social and economic levels, people pay more and more attention to the living quality, and the development of the aromatherapy industry is promoted; the aromatherapy industry mainly has two related directions, namely aromatherapy beauty treatment and aromatherapy, people realize the volatilization of the essential oil by heating the essential oil, and the aromatherapy has the functions of beautifying the environment, removing peculiar smell, refreshing the mind, nourishing the health, removing diseases and the like, so that the aromatherapy is widely welcomed by people.
The instrument that is generally used for heating essential oil is the champignon lamp, and the champignon lamp includes the base and encloses the lamp body of locating the base, and the base is used for holding essential oil and heating essential oil, and essential oil volatilizees through the opening at lamp body top, plays the effect of champignon.
Because the lamp body is generally made by iron plate, the heat-proof quality of iron plate is poor, and at the in-process of fragrant lamp heating essential oil, on the heat can transmit the lamp body, if the user touches the lamp body, the phenomenon that the hand scalds appears very easily, influences the use experience of fragrant lamp.
Disclosure of Invention
In order to improve the heat-proof quality of the fragrance lamp housing and improve the use experience, the application provides a preparation process of the fragrance lamp.
The preparation process of the fragrance lamp adopts the following technical scheme:
a preparation process of a fragrance lamp comprises the following steps:
s1, carrying out primary stirring dispersion on styrene-acrylic emulsion, epoxy resin, a defoaming agent and water for 5-20 min, then adding polymethyl silsesquioxane and hollow microspheres for secondary stirring dispersion for 20-50 min, and then adding a film-forming assistant for tertiary stirring dispersion for 5-15 min to obtain a heat-insulating coating;
s2, coating the heat insulation coating on the surface of the lamp housing, and drying to form a coating, wherein the thickness of the coating is 0.5-2 mm;
s3, smearing glass cement on the edge of the glass, bonding the glass with the edge of a preset observation port of the lamp shell, curing at 50-60 ℃, and mounting a base, thereby preparing the fragrance lamp.
By adopting the technical scheme, the lamp housing is provided with the observation window and the glass, a user can observe the heating condition of the essential oil conveniently, the heat insulation coating is formed on the lamp housing by adopting the styrene-acrylic emulsion coating containing the polymethylsilsesquioxane and the cenospheres, the heat insulation performance of the lamp housing is improved, the polymethylsilsesquioxane and the cenospheres are arranged more stably and dispersedly under the action of the epoxy resin, the adhesive force of the coating is improved, the durability of the lamp housing is improved, and therefore the lamp housing has good heat insulation performance and longer service life.
Preferably, in the step S1, the weight ratio of the styrene-acrylic emulsion, the epoxy resin, the polymethylsilsesquioxane, the cenosphere, the defoaming agent, the film-forming assistant and the water is 60 (2-6): 4-8): 6-12): 0.7-1.2: (1.5-1.9): 30-36.
By adopting the technical scheme, the coating with the proportion has better effect on improving the heat-insulating property and the service life of the lamp shell.
Preferably, the defoaming agent comprises dimethyl silicone oil, liquid paraffin, span 60 and water, and the weight ratio of the dimethyl silicone oil to the liquid paraffin to the span 60 to the water is 10 (2-5) to (1-3) to (30-40).
By adopting the technical scheme, the defoaming agent can reduce the surface tension of the coating, promote the coating to uniformly cover the surface of the lamp housing and improve the film forming quality.
Preferably, the coalescent is selected from dipropylene glycol n-butyl ether.
Preferably, before the step of S1, the method further comprises the step of S1A: mixing and stirring the hollow microspheres, sodium hydroxide and water for 2-4 hours, wherein the weight ratio of the hollow microspheres to the sodium hydroxide to the water is 10 (15-20) to (40-50), filtering, washing with water, and drying the solid to obtain the pretreated hollow microspheres.
By adopting the technical scheme, the surface defects of the hollow microspheres are increased, the heat entering the coating is promoted to be repeatedly reflected and scattered in the defects, the heat passing through the coating is reduced, and the heat insulation performance is improved.
Preferably, after the step of S1A and before the step of S1, the method further includes the step of S1B: mixing and stirring hollow microspheres, KH-570, ethanol and water at 60-70 ℃ for 1-2 h, wherein the weight ratio of the hollow microspheres to the KH-570 to the ethanol to the water is 10 (0.8-1.5) to (30-40) to (5-10), filtering, washing with water, and drying the solid to obtain the modified hollow microspheres.
By adopting the technical scheme, the KH-570 is utilized to modify the surface of the hollow microspheres, so that the dispersibility of the hollow microspheres is improved, and the KH-570 is utilized to enhance the combination of the coating and the glass cement, so that the stability of the glass bonded to the lamp shell is improved.
Preferably, in the step S1, zinc gray iron titanium powder is further added during the second stirring and dispersing, and the weight ratio of the styrene-acrylic emulsion to the zinc gray iron titanium powder is 60 (3-6).
By adopting the technical scheme, the zinc-ash-iron-titanium powder can improve the antirust and anticorrosive performances of the coating and improve the durability of the lamp shell.
Preferably, in the step S1, before the zinc gray iron titanium powder is added, the zinc gray iron titanium powder and the hollow microspheres are mixed and stirred for 10-30 min.
By adopting the technical scheme, the zinc ash iron titanium powder is partially doped into the defects of the hollow microspheres, so that the heat insulation capability of the hollow microspheres is improved, and the heat insulation performance of the lamp shell is improved.
Preferably, the particle size of the zinc gray iron titanium powder is 15-20 mu m.
By adopting the technical scheme, the zinc ash iron titanium powder has good rust prevention and corrosion prevention effects.
Preferably, the particle size of the hollow microsphere is 250-280 μm.
By adopting the technical scheme, the zinc ash iron titanium powder can be better doped into the defects of the hollow microspheres, and the heat-insulating property is further improved.
Preferably, the glass cement is neutral silicone glass cement.
By adopting the technical scheme, the neutral silicone glass adhesive has a good bonding effect on metal and glass.
In summary, the present application has the following beneficial effects:
1. because this application adopts the styrene-acrylic emulsion, and polymethylsilsesquioxane and cenosphere cooperation use, form thermal barrier coating on the lamp body, improved the heat-proof quality of lamp body, under epoxy's effect, improved the adhesive force of coating, consequently make the lamp body have good heat-proof quality and longer life.
2. The hollow microspheres are preferably pretreated by using sodium hydroxide, and the zinc gray iron titanium powder is added, so that the heat-insulating property of the hollow microspheres is improved, and further, the heat-insulating property of the coating is improved.
Drawings
Fig. 1 is a schematic perspective view of the fragrance lamp of the present application.
Description of reference numerals: 1. a lamp housing; 2. glass; 3. a base.
Detailed Description
The present application will be described in further detail with reference to the following drawings and examples.
The styrene-acrylic emulsion is purchased from Jinchuan chemical industry Co., Ltd, Jinan, and has a solid content of 40%;
epoxy resin was purchased from the new materials of jenno showy ltd, model E21;
neutral silicone glass cement was purchased from dow corning.
The zinc-ash-iron-titanium powder was purchased from Heizhou Fengsho chemical Co.
Preparation example
Preparation example 1
Preparing a defoaming agent:
1kg of dimethyl silicone oil, 0.2kg of liquid paraffin, 0.1kg of span 60 and 3kg of water are mixed and stirred for 10min to obtain the defoaming agent.
Preparation example 2
Preparing a defoaming agent:
1kg of dimethyl silicone oil, 0.5kg of liquid paraffin, 0.3kg of span 60 and 4kg of water are mixed and stirred for 10min to obtain the defoaming agent.
Examples
Example 1
As shown in fig. 1, a preparation process of a fragrance lamp comprises the following steps:
s1, adding 6kg of styrene-acrylic emulsion, 0.2kg of epoxy resin, 0.1kg of defoaming agent of preparation example 1 and 3kg of water into a dispersion machine for primary stirring dispersion at a stirring speed of 200r/min for 5min, then adding 0.4kg of polymethylsilsesquioxane and 0.6kg of hollow microspheres for secondary stirring dispersion at a stirring speed of 800r/min for 20min, and then adding 0.15kg of dipropylene glycol n-butyl ether for tertiary stirring dispersion for 5min to obtain a heat-insulating coating;
s2, coating the heat insulation coating on the surface of a lamp shell made of an iron plate, drying at 50 ℃, and forming a coating on the surface of the lamp shell, wherein the thickness of the coating is 0.5 mm;
s3, presetting an observation port on the lamp housing, smearing neutral silicone glass cement on the edge of the glass, then adhering the glass and the edge of the lamp housing, which is positioned at the observation port, curing at 50 ℃, and then installing a base at the bottom of the lamp housing, thereby preparing the fragrance lamp.
Examples 2 to 3
Examples 2 to 3 differ from example 1 only in the raw material ratios and the reaction parameters, and are specifically shown in table 1.
TABLE 1
Example 1 Example 2 Example 3
Styrene-acrylic emulsion (kg) 6 6 6
Epoxy resin (kg) 0.2 0.6 0.4
Defoaming agent (kg) 0.1 0.07 0.12
Water (kg) 3 3.3 3.6
Polymethylsilsesquioxane (kg) 0.4 0.8 0.6
Hollow micro-bead (kg) 0.6 1.2 0.9
Dipropylene glycol n-butyl ether (kg) 0.15 0.19 0.17
First time stirring time (min) in S1 5 20 20
Second stirring time (min) in S1 20 50 50
Third stirring time (min) in S1 5 5 15
S2 middle coating thickness (mm) 0.5 1 2
Curing temperature (. degree.C.) in S3 50 60 60
Example 4
The present example is different from example 3 only in that, in step S1, 0.3kg of zinc gray ferrotitanium powder is further added during the second stirring dispersion, and the zinc gray ferrotitanium powder and the hollow microspheres are mixed and stirred for 10min before the zinc gray ferrotitanium powder is added.
Example 5
The present example is different from example 3 only in that, in step S1, 0.6kg of zinc gray ferrotitanium powder is further added during the second stirring dispersion, and the zinc gray ferrotitanium powder and the hollow microspheres are mixed and stirred for 30min before the zinc gray ferrotitanium powder is added.
Example 6
The present embodiment differs from embodiment 3 only in that, before the step of S1, a step of S1A is further included: adding 2kg of hollow microspheres, 3kg of sodium hydroxide and 8kg of water into a reaction bottle, mixing and stirring for 4 hours, filtering, taking out the hollow microspheres, washing the hollow microspheres with water, and drying in a 50 ℃ oven to obtain the pretreated hollow microspheres.
Example 7
The present embodiment differs from embodiment 3 only in that, before the step of S1, a step of S1A is further included: adding 2kg of hollow microspheres, 4kg of sodium hydroxide and 10kg of water into a reaction bottle, mixing and stirring for 2 hours, filtering, taking out the hollow microspheres, washing the hollow microspheres with water, and drying in a 50 ℃ oven to obtain the pretreated hollow microspheres.
Example 8
The present embodiment differs from embodiment 5 only in that, before the step of S1, a step of S1A is further included: adding 2kg of hollow microspheres, 4kg of sodium hydroxide and 10kg of water into a reaction bottle, mixing and stirring for 2 hours, filtering, taking out the hollow microspheres, washing the hollow microspheres with water, and drying in a 50 ℃ oven to obtain the pretreated hollow microspheres.
Example 9
The present embodiment differs from embodiment 8 only in that after the step of S1A and before the step of S1, the present embodiment further includes a step of S1B: adding 1kg of hollow microspheres, 0.08kg of KH-570, 3kg of ethanol and 0.5kg of water into a stirring tank at 60 ℃, mixing and stirring for 2 hours, filtering, taking out the hollow microspheres, washing the hollow microspheres with water, and drying in a 50 ℃ drying oven to obtain the modified hollow microspheres.
Example 10
The present embodiment differs from embodiment 8 only in that after the step of S1A and before the step of S1, the present embodiment further includes a step of S1B: adding 1kg of hollow microspheres, 0.15kg of KH-570, 4kg of ethanol and 1kg of water into a stirring tank at 70 ℃, mixing and stirring for 1h, filtering, taking out the hollow microspheres, washing the hollow microspheres with water, and drying in a 50 ℃ oven to obtain the modified hollow microspheres.
Comparative example
Comparative example 1
This comparative example differs from example 3 only in that, in the step of S1, the polymethylsilsesquioxane and the cenospheres were replaced with an equal amount of styrene-acrylic emulsion.
Comparative example 2
This comparative example differs from example 3 only in that in the step of S1, the same amount of styrene-acrylic emulsion was used instead of the polymethylsilsesquioxane.
Comparative example 3
This comparative example differs from example 3 only in that, in the step of S1, the cenospheres were replaced with an equal amount of styrene-acrylic emulsion.
Comparative example 4
This comparative example differs from example 3 only in that in the step of S1, an equal amount of styrene-acrylic emulsion was used instead of the epoxy resin.
Performance test
Taking an iron plate for manufacturing a lamp housing, wherein the thickness of the iron plate is 6mm, the two sides of the iron plate are coated with the heat insulation coating in the step S1 of each embodiment and each comparative example, the coating thickness and the drying temperature are set according to the step S2, a YBF-3 heat conductivity coefficient tester is used for testing the heat conductivity coefficient of each iron plate, and the test results are shown in Table 2.
Taking an iron plate for lamp housing manufacture, the thickness of the iron plate was 6mm, both sides of the iron plate were coated with the thermal barrier coating in step S1 of each of examples and comparative examples of the present application, and the coating thickness and baking temperature were set in accordance with step S2, and each iron plate was subjected to adhesion test in accordance with GB 1720-.
Taking an iron plate and glass for manufacturing a lamp housing, wherein the thicknesses of the iron plate and the glass are both 6mm, the two surfaces of the iron plate are coated with the heat insulation coating in the step S1 of each example and each comparative example, the coating thickness and the drying temperature are set according to the step S2, then the iron plate and the glass are bonded through a neutral silicone glass adhesive, and the iron plate and the glass are subjected to tensile shear strength tests according to the determination of tensile shear strength of the adhesive (rigid material to rigid material) in GB/T7124 & 2008, and the test results are shown in Table 2.
TABLE 2
Thermal conductivity W/(m.K) Grade of adhesion Tensile shear strength Mpa
Example 1 3.9 First stage 1.6
Example 2 4.0 First stage 1.8
Example 3 3.7 First stage 1.6
Example 4 4.2 Second stage 1.7
Example 5 4.3 Second stage 1.9
Example 6 3.4 First stage 1.4
Example 7 3.3 First stage 1.5
Example 8 2.7 First stage 1.6
Example 9 2.2 First stage 3.2
Example 10 2.3 First stage 3.5
Comparative example 1 11.8 Second stage 1.5
Comparative example 2 10.5 Second stage 1.2
Comparative example 3 9.8 First stage 1.4
Comparative example 4 8.8 Three-stage 1.4
As can be seen from table 2, the thermal conductivity of comparative examples 1 and 4 is higher than that of example 3, and the adhesion rating is lower than that of example 3, which indicates that the addition of polymethylsilsesquioxane and cenospheres can improve the heat-insulating property and durability of the coating on the premise of the addition of epoxy resin, because the styrene-acrylic emulsion and epoxy resin form an interpenetrating network for stable arrangement and dispersion of the cenospheres and polymethylsilsesquioxane in the network, and both the cenospheres and polymethylsilsesquioxane have good strength, thereby improving the film-forming strength of the styrene-acrylic emulsion, improving the adhesion of the coating, improving the protection degree of the iron plate, and prolonging the service life of the lamp housing.
The thermal conductivity of comparative example 2 and comparative example 3 is higher than that of example 3, namely the thermal insulation performance of example 3 is better, which shows that the effect of the combination of the cenospheres and the polymethylsilsesquioxane is better than the effect of the single use of the cenospheres or the single use of the polymethylsilsesquioxane.
The heat conductivity coefficients of the examples 4-5 are all higher than that of the example 3, and the adhesion rating is lower than that of the example 3, namely the heat insulation performance and the durability of the coating of the example 3 are better, probably because the addition of the zinc gray iron titanium powder as an antirust filler can improve the antirust effect of the coating, but the heat conductivity of the zinc gray iron titanium powder is high, so the heat insulation performance of the coating is influenced, and in addition, the zinc gray iron titanium powder is not good in dispersibility in a system consisting of the styrene-acrylic emulsion and the epoxy resin, so the adhesion of the coating is reduced.
The thermal conductivity of examples 6-7 was lower than that of example 3, i.e., the coatings of examples 6-7 had better thermal insulation performance, probably because the sodium hydroxide etched the surface of the cenospheres, resulting in increased defects on the surface of the cenospheres, which caused repeated reflection and scattering of heat entering the coating, thereby reducing the amount of heat passing through the coating and improving the thermal insulation performance.
Example 8 has a lower thermal conductivity than example 5 and a higher adhesion level than example 5, i.e., the coating of example 8 has better thermal insulation performance and durability, probably because the zinc gray ferrotitanium powder is doped into the defects of the cenospheres, and the thermal conductivity of the zinc gray ferrotitanium powder further promotes the repeated reflection and scattering of heat entering the coating in the defects of the cenospheres, thereby improving the thermal insulation performance; in addition, the hollow microspheres provide attachment for the zinc-gray iron-titanium powder, and the dispersibility of the zinc-gray iron-titanium powder is improved, so that the adhesive force of the coating is improved.
The examples 9-10 have a lower thermal conductivity than example 8, and the tensile shear strength of the iron plate and the glass is higher than that of the coating of example 8, i.e., the coatings of examples 9-10 have better thermal insulation performance and adhesion to neutral silicone glass cement, probably because the KH-570 modifies the surface of the hollow microspheres to improve the dispersibility of the hollow microspheres, thereby improving the thermal insulation effect, and in addition, when the neutral silicone glass cement is cured, the end of the KH-570 is bonded to the neutral silicone glass cement to improve the adhesion strength of the coating to the neutral silicone glass cement, thereby further improving the structural stability and durability of the lamp envelope.
The present embodiment is only for explaining the present application, and it is not limited to the present application, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present application.

Claims (10)

1. The preparation process of the fragrance lamp is characterized by comprising the following steps of:
s1, carrying out primary stirring dispersion on styrene-acrylic emulsion, epoxy resin, a defoaming agent and water for 5-20 min, then adding polymethyl silsesquioxane and hollow microspheres for secondary stirring dispersion for 20-50 min, and then adding a film-forming assistant for tertiary stirring dispersion for 5-15 min to obtain a heat-insulating coating;
s2, coating the heat insulation coating on the surface of the lamp housing, and drying to form a coating, wherein the thickness of the coating is 0.5-2 mm;
s3, smearing glass cement on the edge of the glass, bonding the glass with the edge of a preset observation port of the lamp shell, curing at 50-60 ℃, and mounting a base, thereby preparing the fragrance lamp.
2. The preparation process of the fragrance lamp according to claim 1, characterized in that: in step S1, the weight ratio of the styrene-acrylic emulsion, the epoxy resin, the polymethylsilsesquioxane, the cenosphere, the defoaming agent, the film-forming assistant and the water is 60 (2-6): 4-8): 6-12): 0.7-1.2): 1.5-1.9): 30-36.
3. The preparation process of the fragrance lamp according to claim 1, characterized in that: the defoaming agent comprises dimethyl silicone oil, liquid paraffin, span 60 and water, wherein the weight ratio of the dimethyl silicone oil to the liquid paraffin to the span 60 to the water is 10 (2-5) to (1-3) to (30-40).
4. The preparation process of the fragrance lamp according to claim 1, characterized in that: before the step of S1, the method also comprises the step of S1A: mixing and stirring the hollow microspheres, sodium hydroxide and water for 2-4 hours, wherein the weight ratio of the hollow microspheres to the sodium hydroxide to the water is 10 (15-20) to (40-50), filtering, washing with water, and drying the solid to obtain the pretreated hollow microspheres.
5. The preparation process of the fragrance lamp according to claim 4, characterized in that: after the step of S1A and before the step of S1, the method further includes a step of S1B: mixing and stirring hollow microspheres, KH-570, ethanol and water at 60-70 ℃ for 1-2 h, wherein the weight ratio of the hollow microspheres to the KH-570 to the ethanol to the water is 10 (0.8-1.5) to (30-40) to (5-10), filtering, washing with water, and drying the solid to obtain the modified hollow microspheres.
6. The preparation process of the fragrance lamp according to claim 4, characterized in that: in the step S1, zinc gray iron titanium powder is added during the second stirring and dispersing, and the weight ratio of the styrene-acrylic emulsion to the zinc gray iron titanium powder is 60 (3-6).
7. The preparation process of the fragrance lamp according to claim 6, characterized in that: in the step S1, before the zinc gray iron titanium powder is added, the zinc gray iron titanium powder and the hollow microspheres are mixed and stirred for 10-30 min.
8. The preparation process of the fragrance lamp according to claim 6, characterized in that: the particle size of the zinc gray iron titanium powder is 15-20 mu m.
9. The preparation process of the fragrance lamp according to claim 1, characterized in that: the particle size of the hollow microspheres is 250-280 mu m.
10. The preparation process of the fragrance lamp according to claim 1, characterized in that: the glass cement is neutral silicone glass cement.
CN202011454450.XA 2020-12-10 2020-12-10 Preparation process of fragrance lamp Pending CN112662240A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202020715U (en) * 2011-04-30 2011-11-02 曾礼秀 Fragrance lamp
CN104974581A (en) * 2014-04-11 2015-10-14 中国科学院苏州纳米技术与纳米仿生研究所 Super-hydrophobic heat-insulating coating and preparation method thereof
CN109456653A (en) * 2017-09-02 2019-03-12 成都乐沸科技有限责任公司 A kind of environmental protection heat insulation type building energy-saving heat-insulating material
WO2019095398A1 (en) * 2017-11-17 2019-05-23 苏州锐特捷化工制品有限公司 Thermally insulating, anti-static and weather-resistant coating for metal surface and preparation method therefor

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202020715U (en) * 2011-04-30 2011-11-02 曾礼秀 Fragrance lamp
CN104974581A (en) * 2014-04-11 2015-10-14 中国科学院苏州纳米技术与纳米仿生研究所 Super-hydrophobic heat-insulating coating and preparation method thereof
CN109456653A (en) * 2017-09-02 2019-03-12 成都乐沸科技有限责任公司 A kind of environmental protection heat insulation type building energy-saving heat-insulating material
WO2019095398A1 (en) * 2017-11-17 2019-05-23 苏州锐特捷化工制品有限公司 Thermally insulating, anti-static and weather-resistant coating for metal surface and preparation method therefor

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