CN112516948A - Reaction kettle used in MOF (metal organic framework) synthesis process - Google Patents
Reaction kettle used in MOF (metal organic framework) synthesis process Download PDFInfo
- Publication number
- CN112516948A CN112516948A CN202110063346.6A CN202110063346A CN112516948A CN 112516948 A CN112516948 A CN 112516948A CN 202110063346 A CN202110063346 A CN 202110063346A CN 112516948 A CN112516948 A CN 112516948A
- Authority
- CN
- China
- Prior art keywords
- kettle
- locking
- motor
- stirring
- rod
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0073—Sealings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/087—Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention particularly relates to a reaction kettle used in a MOF synthesis procedure, which comprises a lower box body and a top plate, wherein a support rod is arranged between the lower box body and the top plate, and the reaction kettle is characterized in that: a lifting electric cylinder is arranged in the lower box body, a lower rotating motor is arranged at the output end of the lifting electric cylinder, a clamping head is arranged at the output end of the lower rotating motor, a left fixing plate and a right fixing plate are respectively arranged at the middle parts of the left side and the right side of the supporting rod, a controller is arranged on the outer side surface of the left fixing plate, a kettle body is arranged between the left fixing plate and the right fixing plate in a front-back rotating manner, a liftable kettle cover is arranged above the kettle body, and the clamping head can drive; according to the invention, the materials are stirred in a mode of combining the inner stirring fan blades and the outer stirring fan blades, so that the materials can be more fully mixed, and the materials in contact with the inner wall of the kettle body can be fully mixed and stirred; can realize cleaning the internal wall of cauldron, adopt the cauldron body and the mode that the kettle cover carries out the separation, conveniently clear up the cauldron is internal.
Description
Technical Field
The invention belongs to the technical field of chemical equipment, and particularly relates to a reaction kettle used in a MOF (metal organic framework) synthesis process.
Background
Metal-organic framework Materials (MOFs) are coordination polymers which develop rapidly in the last decade, have three-dimensional pore structures, generally take metal ions as connecting points, and organic ligands support and form space 3D extension, are another important novel porous material besides zeolite and carbon nanotubes, and are widely applied to catalysis, energy storage and separation. Currently, MOFs have become an important research direction for many chemical branches of inorganic chemistry, organic chemistry, and the like.
A reaction kettle is needed in the process of synthesizing the MOF material, the reaction kettle is broadly understood to be a container with physical or chemical reaction, and the heating, evaporation, cooling and low-speed mixing functions required by the process are realized through the structural design and parameter configuration of the container.
The reaction kettle is widely applied to pressure vessels for petroleum, chemical engineering, rubber, pesticides, dyes, medicines and foods, and is used for completing technological processes such as vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation and the like, such as a reactor, a reaction kettle, a decomposition kettle, a polymerization kettle and the like; the material is generally carbon manganese steel, stainless steel, zirconium, nickel-based (Hastelloy, Monel, Inconel) alloy and other composite materials.
A stirring device is arranged in the reaction kettle so as to stir the materials and fully and uniformly mix the materials; but present reation kettle adopts single stirring fan blade to stir the material mostly, because there is certain clearance between the cauldron body and the stirring fan blade, the in-process cauldron body that stirs again and the material between the stirring fan blade can't be by even mixing stirring, has stirring inhomogeneous problem.
In addition, in the prior art, when the reaction kettle is cleaned, the reaction kettle is washed by clean water, for example, the clean water is supplied into the reaction kettle by a water inlet pipe to complete cleaning. The cleaning mode causes incomplete cleaning of the reaction kettle, and substances are easy to remain in the reaction kettle to influence the performance of the reaction kettle.
In order to solve the problems, the reaction kettle used in the process of synthesizing the MOF is provided, which can enable the materials in the reaction kettle to be mixed more uniformly and is convenient to clean.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provide a reaction kettle used in a MOF synthesis process.
The purpose of the invention is realized as follows: the utility model provides a reation kettle who uses in synthetic MOF process, is provided with the bracing piece including lower box, roof between lower box and the roof, the lower box in be provided with the electric jar that goes up and down, the electric jar output that goes up and down is provided with down and rotates the motor, lower motor output is provided with the dop, bracing piece left and right sides middle part is provided with left fixed plate and right fixed plate respectively, left fixed plate lateral surface is provided with the controller, but front and back pivoted is provided with the cauldron body between left fixed plate and the right fixed plate, cauldron body top is provided with the kettle cover of liftable, the dop can drive the cauldron body and rotate.
Furthermore, a rotating plate is arranged on the outer side surface of the kettle body, a rotating bearing is arranged between the rotating plate and the kettle body, rotating rods are fixedly arranged at the left end and the right end of the rotating plate respectively, and the rotating rods are rotatably connected with the left fixing plate and the right fixing plate through roller bearings; the fixed driven gear that is provided with in left dwang middle part, the last swing motor that is provided with of left fixed plate, the swing motor output is provided with the driving gear, driving gear and driven gear intermeshing.
Further, the bottom of the kettle body is provided with a clamping groove, and the inner side wall of the kettle body is provided with outer stirring fan blades.
Furthermore, the kettle body is detachably connected with the kettle cover in a sealing manner.
Furthermore, a plurality of locking seats are uniformly distributed and fixed at the upper end of the outer side surface of the kettle body, a rectangular hole is formed in the middle of each locking seat, arc-shaped grooves are formed in the locking seats on two sides of the rectangular hole, a positioning groove is formed in the upper end surface of each locking seat, and a locking groove is formed in the lower end of each locking seat; the kettle cover middle part is the arc arch, kettle cover outward flange evenly distributed has a plurality of locking levers and location arch, the location arch is semi-circular, location arch and constant head tank are clearance fit, the locking lever is connected for rotating with the kettle cover, locking lever both sides face is provided with the arc round pin respectively, be clearance fit between arc round pin and the arc wall, the fixed slide bar that is provided with of terminal surface under the locking lever, slide bar slidable is connected with the slide bar seat, slide bar lower part lateral surface cover is equipped with the spring, terminal surface fixedly connected with spring holder under the slide bar, the spring is located slide bar seat lower part with spring holder slidable, slide bar seat up end is provided with the locking plate, but the joint of.
Further, the fixed annular protrusion that is provided with of kettle cover lower surface, the annular protrusion outside is provided with sealed the pad.
Further, a stirring motor is arranged above the kettle cover, the output end of the stirring motor is rotatably connected with the kettle cover, a first bearing and a sealing ring are arranged between the kettle cover and the output end of the stirring motor, a pin rod is fixedly arranged at the tail end of the output end of the stirring motor, and a locking cover is rotatably arranged at the tail end of the output end of the stirring motor; the fixed motor board that is provided with in the agitator motor outside, be connected through removing the electric jar between motor board and the roof, the motor groove has been seted up at the roof middle part, can be located the motor inslot when agitator motor rose.
Further, agitator motor output end terminal be connected with the puddler through locking lid and cotter bar, be threaded connection between locking lid and the puddler, the cotter way has been seted up to the puddler up end, cotter bar and cotter way are clearance fit, the puddler lateral surface is provided with interior stirring fan blade.
Furthermore, the tail end of the output end of the stirring motor can be further connected with a cleaning mechanism through a locking cover and a pin rod, the cleaning mechanism comprises a transmission rod, a support rod, a cleaning barrel and a brush, the transmission rod is connected with the cleaning barrel through the support rod, a plurality of strip-shaped brushes are arranged on the outer side surface and the bottom surface of the cleaning barrel, a plurality of through holes are formed in the cleaning barrel, the locking cover is in threaded connection with the transmission rod, a pin groove is formed in the upper end surface of the transmission rod, and the pin rod and the pin groove are in clearance fit.
When the reactor is used, the kettle cover is provided with a plurality of members which are required by a common reaction kettle, such as: a feed inlet, a pressure gauge, a steam pipe, a visible pipe and other conventional functions; putting the materials into the kettle body through a feeding hole in the kettle cover, controlling the stirring motor to rotate through the controller, driving the stirring rod to rotate by the stirring motor, and stirring the materials by the inner stirring fan blades on the stirring rod; the controller controls the lifting electric cylinder to move upwards to realize the upwards movement of the lower stirring electric cylinder, and a clamping head at the upper end of the lower stirring electric cylinder is clamped into a clamping groove at the lower end of the kettle body; the lower rotating motor is controlled by the controller to rotate, the lower rotating motor drives the kettle body to rotate, and when the kettle body rotates, the materials are stirred by the outer stirring fan blades, so that double stirring of the materials is realized; so that the material is stirred more uniformly. The side of the bottom of the kettle body is provided with a discharge hole, and materials in the reaction kettle body can be discharged through the discharge hole.
When the reaction kettle body needs to be cleaned, the kettle cover is opened, the sliding rod seat is pulled downwards, the spring is pressed, and the sliding rod seat moves downwards along the sliding rod, so that the stop piece is separated from the locking groove; then the sliding rod seat is pulled outwards to drive the lock rod to rotate outwards, so that the arc-shaped pin is separated from the arc-shaped groove; then the controller controls the movable electric cylinder to drive the kettle cover to move upwards, the positioning bulge is separated from the positioning groove, the stirring rod below the kettle cover is removed, the cleaning mechanism is replaced, namely, a pin groove on a transmission rod on the cleaning mechanism is matched with the pin rod, and then the locking cover is screwed with the transmission rod in a threaded matching manner, so that the installation of the cleaning mechanism is completed; and then the kettle cover and the kettle body are reset and sealed, namely the positioning bulge and the positioning groove are in positioning fit, and then the sliding rod seat is pulled to clamp the stop piece into the lock pin, so that the sealing between the kettle cover and the kettle body is realized. Clear water and detergent are added into the kettle body through the feed inlet, the stirring motor is controlled to rotate through the controller, the cleaning barrel is driven to rotate, the brush on the cleaning barrel scrapes the inner wall of the kettle body, and the kettle body is cleaned. And opening the kettle cover, controlling the swing motor to rotate through the controller, further driving the rotating plate to rotate, driving the kettle body to incline, and pouring out the sewage after the kettle body is cleaned.
Has the advantages that: the device can realize stirring the material to the two stirring of material, and the mode that stirring fan blade and outer stirring fan blade combined in adopting stirs the material, can make more abundant that the material mixes, and for single interior stirring fan blade, this equipment can carry out the intensive mixing stirring with the material that the internal wall of cauldron contacted, and single stirring fan blade then can't carry out abundant stirring with the material between interior stirring fan blade and the cauldron body and mix. The device can also realize cleaning the internal wall of cauldron, adopt the cauldron body and the mode that the kettle cover carries out the separation, the convenience is cleared up the cauldron is internal, adopt clean mechanism can realize the automatic cleanness to the internal wall of cauldron, and can discharge the sewage after cleaning, sealing method between the cauldron body and the kettle cover adopts locking lever and locking seat's cooperation locking mode can be quick seal it and open, it is more light swift that the messenger trades puddler or clean mechanism to change, the save time cost.
Drawings
Fig. 1 is a schematic perspective view of the present invention.
Fig. 2 is a cross-sectional view of the lower housing of the invention.
Fig. 3 is a partial structural schematic diagram of the invention.
FIG. 4 is a schematic view of the structure of the kettle body and the kettle cover of the invention.
FIG. 5 is a schematic view of the structure of the inventive kettle cover and stirring rod.
FIG. 6 is a schematic view of the structure of the inventive kettle cover and stirring motor.
FIG. 7 is a schematic view of a partial structure of the inventive kettle cover.
FIG. 8 is a sectional view of the inventive kettle.
Fig. 9 is a schematic view of a partial structure of the kettle and the locking seat of the invention.
Fig. 10 is a schematic structural view of the cleaning mechanism of the present invention.
Fig. 11 is a schematic view of the bottom structure of the cleaning mechanism of the present invention.
FIG. 12 is a schematic view of the structure of the stirring rod and the inner stirring blades of the present invention.
Fig. 13 is a schematic structural view of the locking seat of the present invention.
FIG. 14 is a schematic view of the partial structure of the kettle cover and kettle body of the invention when locked.
Description of reference numerals:
1. the automatic stirring device comprises a lower box body, a supporting rod, a top plate, a right fixing plate, a left fixing plate, a moving electric cylinder, a motor groove, a kettle body, a swinging motor, a rotating plate, a kettle cover, a stirring motor, a lifting electric cylinder, a lower rotating motor, a clamping head, a controller, a driven gear, a driving gear, a discharging port, a motor plate, a rotating bearing, a ring-shaped bulge, a stirring rod, a locking cover, a positioning bulge, a sealing gasket, a sliding rod seat, a bearing I, a sealing ring, a pin rod, a spring seat, a stopping sheet, a sliding rod, a locking pin, an arc-shaped pin, a locking rod, a locking blade, an outer stirring blade, a clamping groove, a locking seat, a positioning groove, a locking groove, 43. Stay bar, 44 pin slot, 45 drive bar, 46 brush, 47 through hole, 48 cleaning barrel, 49 roller bearing, 50 drive bar.
Detailed Description
Example 1, as shown in fig. 1 to 14, a reaction kettle used in a MOF synthesis process includes a lower case 1 and a top plate 3, a support rod 2 is disposed between the lower case 1 and the top plate 3, a lifting electric cylinder 13 is disposed in the lower case 1, a lower rotating motor 14 is disposed at an output end of the lifting electric cylinder 13, an output end of the lower rotating motor 14 penetrates through an upper surface of the lower case 1, a chuck 15 is disposed at an output end of the lower rotating motor 14, a left fixing plate 5 and a right fixing plate 4 are respectively disposed at a middle portion of left and right sides of the support rod 2, a controller 16 is disposed at an outer side surface of the left fixing plate 5, the controller 16 is preferably a mitsubishi FX2N-64MT-001 controller, the controller 16 is used for controlling the lifting electric cylinder 13, the lower rotating motor 14, the stirring motor 12, the swinging motor 9, the moving electric cylinder 6, the lower rotating motor 14, the stirring motor 12, the lifting electric cylinder 13 and the moving electric cylinder 6 are preferably servo electric cylinders of Eschent 80 series, a kettle body 8 is arranged between the left fixing plate 5 and the right fixing plate 4 and can rotate back and forth, a lifting kettle cover 11 is arranged above the kettle body 8, and the chuck 15 can drive the kettle body 8 to rotate.
A clamping groove 38 is formed in the bottom of the kettle body 8, the clamping head 15 can be clamped in the clamping groove 38, the clamping head 15 can drive the kettle body 8 to rotate conveniently, and an outer stirring fan blade 37 is arranged on the inner side wall of the kettle body 8; the outer stirring fan blades 37 can stir materials between the kettle body 8 and the inner stirring fan blades, the rotating plate 10 is arranged on the outer side surface of the kettle body 8, the rotating bearing 21 is arranged between the rotating plate 10 and the kettle body 8, the left end and the right end of the rotating plate 10 are respectively and fixedly provided with a rotating rod 50, and the rotating rods 50 are rotatably connected with the left fixing plate 5 and the right fixing plate 4 through roller bearings 49; the driven gear 17 is fixedly arranged in the middle of the rotating rod 50 on the left side, the swing motor 9 is arranged on the left fixing plate 5, the driving gear 18 is arranged at the output end of the swing motor 9, and the driving gear 18 is meshed with the driven gear 17.
The kettle body 8 is detachably connected with the kettle cover 11 in a sealing way; a plurality of locking seats 39 are uniformly distributed and fixed at the upper end of the outer side surface of the kettle body 8, a rectangular hole is formed in the middle of each locking seat 39, arc-shaped grooves 41 are formed in the locking seats 39 on two sides of each rectangular hole, a positioning groove 40 is formed in the upper end surface of each locking seat 39, and a locking groove 42 is formed in the lower end of each locking seat 39; the middle part of the kettle cover 11 is provided with an arc-shaped bulge, the lower surface of the kettle cover 11 is fixedly provided with an annular bulge 22, and the outer side of the annular bulge 22 is provided with a sealing gasket 26; a plurality of locking rods 36 and positioning bulges 25 are uniformly distributed on the outer edge of the kettle cover 11, the positioning bulges 25 are semicircular, the positioning bulges 25 are in clearance fit with the positioning grooves 40, the locking rods 36 are rotatably connected with the kettle cover 11, two side faces of the locking rods 36 are respectively provided with arc-shaped pins 35, the arc-shaped pins 35 are in clearance fit with the arc-shaped grooves 41, the arc-shaped pins 35 are matched with the arc-shaped grooves 41 to lock the kettle cover 11 and the kettle body 8, a sliding rod 34 is fixedly arranged on the lower end face of the locking rods 36, the sliding rod 34 is slidably connected with a sliding rod seat 27, a spring 31 is sleeved on the outer side face of the lower part of the sliding rod 34, a spring seat 32 is fixedly connected on the lower end face of the sliding rod 34, the spring 31 and the spring seat 32 are slidably positioned in the lower part of the sliding rod seat 27.
A stirring motor 12 is arranged above the kettle cover 11, the output end of the stirring motor 12 is rotatably connected with the kettle cover 11, a bearing I28 and a sealing ring 29 are arranged between the kettle cover 11 and the output end of the stirring motor 12, a pin rod 30 is fixedly arranged at the tail end of the output end of the stirring motor 12, and a locking cover 24 is rotatably arranged at the tail end of the output end of the stirring motor 12; a motor plate 20 is fixedly arranged on the outer side of the stirring motor 12, the motor plate 20 is connected with the top plate 3 through a movable electric cylinder 6, a motor groove 7 is formed in the middle of the top plate 3, and the stirring motor 12 can be located in the motor groove 7 when ascending; the terminal puddler 23 that is connected with pin rod 30 through locking lid 24 of agitator motor 12 output, be threaded connection between locking lid 24 and the puddler 23, round pin groove 44 has been seted up to puddler 23 up end, and pin rod 30 is clearance fit with round pin groove 44, and puddler 23 lateral surface is provided with interior stirring fan blade.
The tail end of the output end of the stirring motor 12 can be further connected with a cleaning mechanism through the locking cover 24 and the pin rod 30, the cleaning mechanism comprises a transmission rod 45, a support rod 43, a cleaning barrel 48 and a brush 46, the transmission rod 45 is connected with the cleaning barrel 48 through the support rod 43, a plurality of strip-shaped brushes 46 are arranged on the outer side face and the bottom face of the cleaning barrel 48, a plurality of through holes 47 are formed in the cleaning barrel 48, the locking cover 24 is in threaded connection with the transmission rod 45, the upper end face of the transmission rod 45 is provided with a pin groove 44, and the pin rod 30 is in clearance fit with the pin.
In use, the kettle cover 11 is provided with some components that a typical reaction kettle should have, for example: a feed inlet, a pressure gauge, a steam pipe, a visible pipe and other conventional functions; putting the materials into the kettle body 8 through a feeding hole on the kettle cover 11, controlling the stirring motor 12 to rotate through the controller 16, driving the stirring rod 23 to rotate by the stirring motor 12, and stirring the materials by the inner stirring fan blades on the stirring rod 23; the controller 16 controls the lifting electric cylinder 13 to move upwards to realize the upward movement of the lower stirring electric cylinder, and the clamping head 15 at the upper end of the lower stirring electric cylinder is clamped into the clamping groove 38 at the lower end of the kettle body 8; the lower rotating motor 14 is controlled by the controller 16 to rotate, the lower rotating motor 14 drives the kettle body 8 to rotate, and when the kettle body 8 rotates, the materials are stirred by the outer stirring fan blades 37, so that double stirring of the materials is realized; so that the material is stirred more uniformly. The side of the bottom of the reaction kettle body 8 is provided with a discharge hole 19, and the materials in the reaction kettle body 8 can be discharged through the discharge hole 19.
When the reaction kettle body 8 needs to be cleaned, the kettle cover 11 is opened, namely the slide rod seat 27 is pulled down, the spring 31 is pressed, and the slide rod seat 27 moves down along the slide rod 34, so that the stop piece 33 is separated from the lock groove 42; then the sliding rod seat 27 is pulled outwards to drive the locking rod 36 to rotate outwards, so that the arc-shaped pin 35 is separated from the arc-shaped groove 41; then the controller 16 controls the movable electric cylinder 6 to drive the kettle cover 11 to move upwards, the positioning bulge 25 is separated from the positioning groove 40, the stirring rod 23 below the kettle cover 11 is removed, the cleaning mechanism is replaced, namely, a pin groove 44 on a transmission rod 45 on the cleaning mechanism is matched with a pin rod 30, and then the locking cover 24 is screwed in threaded fit with the transmission rod 45, so that the installation of the cleaning mechanism is completed; and then the kettle cover 11 and the kettle body 8 are reset and sealed, namely the positioning bulge 25 is in positioning fit with the positioning groove 40, and then the sliding rod seat 27 is pulled to clamp the stop piece 33 into the lock pin, so that the sealing between the kettle cover 11 and the kettle body 8 is realized. Clear water and detergent are added into the kettle body 8 through the feeding hole, the stirring motor 12 is controlled to rotate through the controller 16, then the cleaning barrel 48 is driven to rotate, the inner wall of the kettle body 8 is scraped and brushed by the hairbrush 46 on the cleaning barrel 48, and the kettle body 8 is cleaned. And opening the kettle cover 11, controlling the swing motor 9 to rotate through the controller 16, further driving the rotating plate 10 to rotate, driving the kettle body 8 to incline, and pouring out the cleaned sewage in the kettle body 8.
In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", and the like, indicate orientations and positional relationships based on those shown in the drawings, and are used only for convenience of description and simplicity of description, and do not indicate or imply that the equipment or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be considered as limiting the present invention.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the present invention, and it will be understood by those skilled in the art that various changes and modifications may be made therein without departing from the spirit and scope of the invention.
Claims (9)
1. The utility model provides a reation kettle who uses in synthetic MOF process, is provided with bracing piece (2), its characterized in that including lower box (1), roof (3) between lower box (1) and roof (3): lower box (1) in be provided with lift electric jar (13), lift electric jar (13) output is provided with down and rotates motor (14), it is provided with dop (15) to rotate motor (14) output down, bracing piece (2) left and right sides middle part is provided with left fixed plate (5) and right fixed plate (4) respectively, left fixed plate (5) lateral surface is provided with controller (16), can fore-and-aft rotation be provided with cauldron body (8) between left fixed plate (5) and right fixed plate (4), cauldron body (8) top is provided with kettle cover (11) of liftable, dop (15) can drive cauldron body (8) and rotate.
2. A reactor according to claim 1 for use in a process for the synthesis of MOFs, wherein: a rotating plate (10) is arranged on the outer side surface of the kettle body (8), a rotating bearing (21) is arranged between the rotating plate (10) and the kettle body (8), rotating rods (50) are respectively and fixedly arranged at the left end and the right end of the rotating plate (10), and the rotating rods (50) are rotatably connected with the left fixing plate (5) and the right fixing plate (4) through roller bearings (49); a driven gear (17) is fixedly arranged in the middle of the rotating rod (50) on the left side, a swing motor (9) is arranged on the left fixing plate (5), a driving gear (18) is arranged at the output end of the swing motor (9), and the driving gear (18) is meshed with the driven gear (17).
3. A reactor according to claim 1 for use in a process for the synthesis of MOFs, wherein: the bottom of the kettle body (8) is provided with a clamping groove (38), and the inner side wall of the kettle body (8) is provided with an outer stirring fan blade (37).
4. A reactor according to claim 1 for use in a process for the synthesis of MOFs, wherein: the kettle body (8) is detachably and hermetically connected with the kettle cover (11).
5. A reactor according to claim 4 for use in a process for the synthesis of MOF, wherein: a plurality of locking seats (39) are uniformly distributed and fixed at the upper end of the outer side surface of the kettle body (8), a rectangular hole is formed in the middle of each locking seat (39), arc-shaped grooves (41) are formed in the locking seats (39) on two sides of the rectangular hole, a positioning groove (40) is formed in the upper end surface of each locking seat (39), and a locking groove (42) is formed in the lower end of each locking seat (39); kettle cover (11) middle part is the arc arch, kettle cover (11) outward flange evenly distributed has a plurality of locking levers (36) and location arch (25), locking lever (36) are connected for rotating with kettle cover (11), locking lever (36) both sides face is provided with arc round pin (35) respectively, terminal surface is fixed under locking lever (36) is provided with slide bar (34), slide bar (34) slidable is connected with slide bar seat (27), slide bar (34) lower part lateral surface cover is equipped with spring (31), terminal surface fixedly connected with spring holder (32) under slide bar (34), spring (31) and spring holder (32) slidable are located slide bar seat (27) lower part, slide bar seat (27) up end is provided with locking plate (33).
6. A reactor according to claim 5 for use in a process for the synthesis of MOF, wherein: the lower surface of the kettle cover (11) is fixedly provided with an annular bulge (22), and a sealing gasket (26) is arranged on the outer side of the annular bulge (22).
7. A reactor according to claim 1 for use in a process for the synthesis of MOFs, wherein: kettle cover (11) top be provided with agitator motor (12), for rotating between the output of agitator motor (12) and kettle cover (11) to be connected, agitator motor (12) output end terminal is fixed and is provided with pin pole (30), agitator motor (12) output end terminal is rotatable is provided with locking lid (24), agitator motor (12) outside is fixed and is provided with motor board (20), is connected through removing electric jar (6) between motor board (20) and roof (3).
8. A reactor according to claim 1 for use in a process for the synthesis of MOFs, wherein: the tail end of the output end of the stirring motor (12) is connected with a stirring rod (23) through a locking cover (24) and a pin rod (30), and inner stirring blades are arranged on the outer side surface of the stirring rod (23).
9. A reactor according to claim 1 for use in a process for the synthesis of MOFs, wherein: the tail end of the output end of the stirring motor (12) can be further connected with a cleaning mechanism through a locking cover (24) and a pin rod (30), the cleaning mechanism comprises a transmission rod (45), a support rod (43), a cleaning barrel (48) and brushes (46), the transmission rod (45) and the cleaning barrel (48) are connected through the support rod (43), a plurality of strip-shaped brushes (46) are arranged on the outer side surface and the bottom surface of the cleaning barrel (48), and a plurality of through holes (47) are formed in the cleaning barrel (48).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110063346.6A CN112516948A (en) | 2021-01-18 | 2021-01-18 | Reaction kettle used in MOF (metal organic framework) synthesis process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110063346.6A CN112516948A (en) | 2021-01-18 | 2021-01-18 | Reaction kettle used in MOF (metal organic framework) synthesis process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112516948A true CN112516948A (en) | 2021-03-19 |
Family
ID=74975352
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110063346.6A Pending CN112516948A (en) | 2021-01-18 | 2021-01-18 | Reaction kettle used in MOF (metal organic framework) synthesis process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112516948A (en) |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105170587A (en) * | 2015-09-25 | 2015-12-23 | 重庆长风化学工业有限公司 | Cleaning device for aniline reaction still |
| CN206240466U (en) * | 2016-08-26 | 2017-06-13 | 温州日胜新材料科技有限公司 | A kind of efficiently mixing polyurethane reaction kettle |
| CN207174531U (en) * | 2017-09-20 | 2018-04-03 | 温州市金榜轻工机械有限公司 | A kind of tank body cleaning plant |
| CN207592082U (en) * | 2017-11-29 | 2018-07-10 | 合肥凯石医药科技有限公司 | A kind of centrifuge of laboratory medicine research and development |
| CN110882672A (en) * | 2019-12-05 | 2020-03-17 | 朱晓喆 | Macromolecular material reation kettle |
| CN210635975U (en) * | 2019-08-30 | 2020-05-29 | 临沂明英工贸有限公司 | Fermentation cylinder is used in production of compound microbial inoculant |
| CN211027395U (en) * | 2019-10-04 | 2020-07-17 | 江山市华顺有机硅有限公司 | Chemical reaction kettle cleaning device |
| CN211190126U (en) * | 2019-11-01 | 2020-08-07 | 苏州柯仕达电子材料有限公司 | Automatic reation kettle who uncaps |
| CN111631412A (en) * | 2020-06-15 | 2020-09-08 | 吴冬冬 | Cleaning equipment for edible fungi |
| CN211754952U (en) * | 2019-12-30 | 2020-10-27 | 河北博伊德化工有限公司 | Polymerization cauldron convenient to maintain |
-
2021
- 2021-01-18 CN CN202110063346.6A patent/CN112516948A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105170587A (en) * | 2015-09-25 | 2015-12-23 | 重庆长风化学工业有限公司 | Cleaning device for aniline reaction still |
| CN206240466U (en) * | 2016-08-26 | 2017-06-13 | 温州日胜新材料科技有限公司 | A kind of efficiently mixing polyurethane reaction kettle |
| CN207174531U (en) * | 2017-09-20 | 2018-04-03 | 温州市金榜轻工机械有限公司 | A kind of tank body cleaning plant |
| CN207592082U (en) * | 2017-11-29 | 2018-07-10 | 合肥凯石医药科技有限公司 | A kind of centrifuge of laboratory medicine research and development |
| CN210635975U (en) * | 2019-08-30 | 2020-05-29 | 临沂明英工贸有限公司 | Fermentation cylinder is used in production of compound microbial inoculant |
| CN211027395U (en) * | 2019-10-04 | 2020-07-17 | 江山市华顺有机硅有限公司 | Chemical reaction kettle cleaning device |
| CN211190126U (en) * | 2019-11-01 | 2020-08-07 | 苏州柯仕达电子材料有限公司 | Automatic reation kettle who uncaps |
| CN110882672A (en) * | 2019-12-05 | 2020-03-17 | 朱晓喆 | Macromolecular material reation kettle |
| CN211754952U (en) * | 2019-12-30 | 2020-10-27 | 河北博伊德化工有限公司 | Polymerization cauldron convenient to maintain |
| CN111631412A (en) * | 2020-06-15 | 2020-09-08 | 吴冬冬 | Cleaning equipment for edible fungi |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN210815271U (en) | Reaction kettle for producing industrial water purifying agent | |
| CN211754948U (en) | Reation kettle for chemical industry convenient to wash inner wall | |
| CN220425353U (en) | Reation kettle convenient to keep pressure | |
| CN112516948A (en) | Reaction kettle used in MOF (metal organic framework) synthesis process | |
| CN215655156U (en) | Stable form chemical industry reation kettle of high-efficient stirring | |
| CN217367931U (en) | High-efficient structure of wasing of chemical industry reation kettle | |
| CN215540896U (en) | High-efficient chemical industry reation kettle that mixes | |
| CN213824755U (en) | Chemical heating reaction pot convenient to automatically scrape materials | |
| CN212632673U (en) | Improved generation chemical industry reation kettle | |
| CN211636514U (en) | Conveniently unpack apart clear chemical industry reation kettle | |
| CN211411970U (en) | Medicament reation kettle is selected in ore deposit | |
| CN211246527U (en) | Energy-saving cement reation kettle is used in cement factory | |
| CN210584949U (en) | Reaction tank with liquid adding device | |
| CN114618349A (en) | Blueberry sauce processing is with allotment jar structure | |
| CN214183073U (en) | Large capacity reation kettle is used to environmental protection preparation | |
| CN212237271U (en) | Stirring device of high-efficiency reaction kettle | |
| CN217368138U (en) | Reation kettle is used in preparation of water base emulsion cutting fluid | |
| CN220126218U (en) | Chemical industry reation kettle | |
| CN221536678U (en) | Sealed reaction kettle for aluminum hydroxide production | |
| CN213644132U (en) | Dispersant production is with reation kettle convenient to it is clean | |
| CN214486856U (en) | Chemical reaction kettle | |
| CN218131740U (en) | Prevent reation kettle discharge gate of jam | |
| CN221452241U (en) | Electric stirring mixing kettle with filtering structure | |
| CN210752687U (en) | Novel stirring reaction kettle for manufacturing antirust agent | |
| CN220919177U (en) | Chemical raw material production reaction equipment convenient to wash |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210319 |