CN112479226A - High-purity ammonia deep purification device and implementation method thereof - Google Patents
High-purity ammonia deep purification device and implementation method thereof Download PDFInfo
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- CN112479226A CN112479226A CN202011371768.1A CN202011371768A CN112479226A CN 112479226 A CN112479226 A CN 112479226A CN 202011371768 A CN202011371768 A CN 202011371768A CN 112479226 A CN112479226 A CN 112479226A
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- reaction tank
- wall
- air inlet
- motor
- inlet pipe
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/024—Purification
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/76—Gas phase processes, e.g. by using aerosols
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/20—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought
- B08B9/38—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought the apparatus cleaning by using scrapers, chains, grains of shot, sand or other abrasive means
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/20—Reductants
- B01D2251/206—Ammonium compounds
- B01D2251/2062—Ammonia
Abstract
The invention discloses a high-purity ammonia deep purification device and an implementation method thereof, wherein the device comprises a first motor, a stirring frame, a scraper, a discharge hole, a material receiving box, a first air inlet pipe, a second limiting block, a first through hole, a second motor, a first limiting ball, a second air inlet pipe, a third limiting block, a fourth through hole, a third motor and a second limiting ball; the automatic cleaning device is safe and reliable, and the purpose of automatically cleaning the interior of the reaction tank is realized through the matched use of the first motor, the stirring frame, the scraper, the discharge hole and the material receiving box; the first air inlet pipe, the second limiting block, the first through hole, the second motor, the first limiting ball, the second air inlet pipe, the third limiting block, the fourth through hole, the third motor and the second limiting ball are matched for use, so that the air inlet pipe is convenient to open and close, the flow rate of air introduced into the air inlet pipe is convenient to adjust, and the air inlet pipe is convenient to use; through the use of deep purification device, the purification treatment of gas is convenient for, and the purification effect is improved and the use is convenient.
Description
Technical Field
The invention relates to the technical field of ammonia gas purification devices.
Background
Because of the wide use of purification devices in gas purification, certain requirements are placed on some gas purification devices in the market; however, the existing purification devices are complex in structure and inconvenient to disassemble and maintain, most of the existing purification devices cannot automatically clean the inner wall, manual shutdown cleaning is mostly needed, the use is affected, and most of the existing purification treatment devices are not provided with an air inlet adjusting device, the purification effect is affected, and the use is inconvenient.
Disclosure of Invention
The invention aims to provide a high-purity ammonia deep purification device and an implementation method thereof, so as to solve the problems in the background technology.
The technical scheme adopted by the invention for realizing the purpose is as follows: the device comprises a reaction tank 1, a first motor 7, a rotating shaft 8, a bearing seat 9, a bearing 10, a stirring frame 11, a limiting groove 13, a telescopic rod 14, a spring 15, a scraper 16, a discharge hole 17, an air outlet pipe 24, a first air inlet pipe 25 and a second air inlet pipe 33, wherein the first motor 7 is installed at the upper part of the reaction tank 1, the output shaft of the first motor 7 is connected with the rotating shaft 8, the bearing seat 9 is fixedly connected to the inner wall of the bottom end of the reaction tank 1, the bearing 10 is installed on the bearing seat 9, and the lower end of the rotating shaft 8 is installed; a stirring frame 11 is arranged on the rotating shaft 8, a limiting groove 13 is distributed on the outer wall of the stirring frame 11, a telescopic rod 14 is fixedly connected with the limiting groove 13, a spring 15 is sleeved on the telescopic rod 14, a scraper 16 is fixedly connected with the outer end of the telescopic rod 14, and the scraper 16 is positioned on the inner wall of the reaction tank 1; the bottom end of the reaction tank 1 is provided with a discharge hole 17; the top of retort 1 is pegged graft and is had outlet duct 24, and it has first intake pipe 25 to peg graft on the outer wall of one side of retort 1, and it has second intake pipe 33 to peg graft on the opposite side outer wall of retort 1.
The bottom end of the reaction tank 1 is connected with a double-output-shaft oil cylinder 18 in an embedded mode, sliding grooves 19 are symmetrically formed in the outer wall of the bottom end of the reaction tank 1, corresponding to the outer wall of one side of an oil cylinder rod of the double-output-shaft oil cylinder 18, the oil cylinder rod of the double-output-shaft oil cylinder 18 is fixedly connected with a first limiting block 20, and the first limiting block 20 is installed in the sliding grooves 19 in a sliding mode.
The top of the reaction tank 1 is inserted with the air outlet pipe 24, the outer wall of one side of the reaction tank 1 is inserted with the first air inlet pipe 25, the inner part of the first air inlet pipe 25 is fixedly connected with the second limiting block 26, the upper part of the second limiting block 26 is penetrated with the first through hole 27, one end of the output shaft of the second motor 29 is rotatably connected with the inner part of the first air inlet pipe 25, one end of the output shaft of the second motor 29 is fixedly connected with the first limiting ball 30, the outer wall of the first limiting ball 30 is penetrated with the second through hole 31, the outer wall of the first limiting ball 30 is penetrated with the third through hole 32, the outer wall of the other side of the reaction tank 1 is inserted with the second air inlet pipe 33, the inner part of the second air inlet pipe 33 is fixedly connected with the third limiting block 34, the third limiting block 34 is penetrated with the second through hole 35, one end of the output shaft of the third motor 37 is rotatably connected with the inner part of the second air inlet pipe 33, a fifth through hole 39 is formed in the outer wall of one side of the second limiting ball 38 in a penetrating manner, and a sixth through hole 40 is formed in the outer wall of one side of the second limiting ball 38 in a penetrating manner.
And a protective layer 3 is arranged on the inner wall of one side of the reaction tank 1.
The upper portion of retort 1 is equipped with mounting panel 4, and motor cabinet 5 of first motor 7 is fixed in on mounting panel 4 through bolt 6.
And a connecting rod 12 is arranged between the stirring frames 11 at the two sides.
A material receiving box 21 is arranged below the discharge hole 17 at the bottom of the reaction tank 1, a pulley 22 is arranged at the bottom end of the material receiving box 21, and a handle 23 is fixedly connected to the outer wall of one side of the material receiving box 21.
Step one, desulfurization treatment; step two, cleaning a reaction tank; step three, treating residues;
in the first step, the desulfurization treatment comprises the following steps;
1) quantitative gas and quantitative ammonia gas which need to be desulfurized are simultaneously introduced into the reaction tank 1 through the matching of the first air inlet pipe 25 and the second air inlet pipe 33, so that the gas and the ammonia gas are reacted and desulfurized in the reaction tank 1;
2) respectively starting the second motor 29 and the third motor 37 to drive the first limiting ball 30 and the second limiting ball 38 to rotate, so that the first air inlet pipe 25 and the second air inlet pipe 33 are opened and closed, and the flow rate of the gas introduced into the reaction tank 1 is adjusted through the rotation of the first limiting ball 30 and the second limiting ball 38;
3) opening the gas outlet pipe 24, and leading out the desulfurized high-purity gas;
in the second step, the first motor 7 is started to drive the scraper 16 on the stirring frame 11 to rotate, so that the scraper 16 scrapes the inner wall of the reaction tank 1, and the high-purity gas reacts with the ammonia gas to be separated out and be condensed on the solid on the inner wall of the reaction tank 1 to be scraped;
in the third step, the double-output-shaft oil cylinder 18 is started to drive the first limiting block 20 to move, the discharge hole 17 is opened, and solid residues in the reaction tank 1 are led out and collected in the material receiving box 21 through the matching of the scraper 16 on the stirring frame 11.
Compared with the prior art, the invention has the following beneficial effects: the automatic cleaning device is safe and reliable, has a simple structure and realizes the purpose of automatically cleaning the interior of the reaction tank by matching the first motor, the stirring frame, the scraper, the discharge hole and the material receiving box; the first air inlet pipe, the second limiting block, the first through hole, the second motor, the first limiting ball, the second air inlet pipe, the third limiting block, the fourth through hole, the third motor and the second limiting ball are matched for use, so that the air inlet pipe is convenient to open and close, the flow rate of air introduced into the air inlet pipe is convenient to adjust, and the air inlet pipe is convenient to use; through the use of the purification device, the purification treatment of gas is convenient, the purification effect is improved, and the use is convenient.
Drawings
FIG. 1 is a schematic sectional view of a high purity ammonia deep purification device according to the present invention;
FIG. 2 is a side view, sectional and schematic structural view of an apparatus for deeply purifying and implementing high-purity ammonia according to the present invention;
FIG. 3 is an enlarged view of the structure of the area A in FIG. 1 according to the present invention;
FIG. 4 is an enlarged view of the structure of the area B in FIG. 2 according to the present invention;
FIG. 5 is a schematic perspective view of the blender of the present invention;
FIG. 6 is a flow chart of a method of the present invention;
in the figure: 1. a reaction tank; 2. supporting legs; 3. a protective layer; 4. mounting a plate; 5. a motor base; 6. a bolt; 7. a first motor; 8. a rotating shaft; 9. a bearing seat; 10. a bearing; 11. a stirring frame; 12. a connecting rod; 13. a limiting groove; 14. a telescopic rod; 15. a spring; 16. a scraper; 17. a discharge hole; 18. a double output shaft oil cylinder; 19. a chute; 20. a first stopper; 21. a material receiving box; 22. a pulley; 23. a handle; 24. an air outlet pipe; 25. a first intake pipe; 26. a second limiting block; 27. a first through hole; 28. a first motor case; 29. a second motor; 30. a first limit ball; 31. a second through hole; 32. a third through hole; 33. a second intake pipe; 34. a third limiting block; 35. a fourth via hole; 36. a second motor case; 37. a third motor; 38. a second limit ball; 39. a fifth through hole; 40. and a sixth through hole.
Detailed Description
Referring to fig. 1-5, a high-purity ammonia deep purification device comprises a reaction tank 1, support legs 2, a protective layer 3, a mounting plate 4, a motor base 5, bolts 6, a first motor 7, a rotating shaft 8, a bearing seat 9, a bearing 10, a stirring frame 11, a connecting rod 12, a limiting groove 13, a telescopic rod 14, a spring 15, a scraper 16, a discharge hole 17, a double-output-shaft oil cylinder 18, a sliding groove 19, a first limiting block 20, a material receiving box 21, a pulley 22, a handle 23, an air outlet pipe 24, a first air inlet pipe 25, a second limiting block 26, a first through hole 27, a first motor box 28, a second motor 29, a first limiting ball 30, a second through hole 31, a third through hole 32, a second air inlet pipe 33, a third limiting block 34, a fourth through hole 35, a second motor box 36, a third motor 37, a second limiting ball 38, a fifth through hole 39 and a sixth through hole 40, wherein the support legs 2 are fixedly connected to the outer wall of the bottom end of, the reaction tank 1 is convenient to ensure stability, the inner wall of one side of the reaction tank 1 is provided with the protective layer 3, the protection is convenient, the service life of the reaction tank 1 is prolonged, the outer wall of the top end of the reaction tank 1 is fixedly connected with the mounting plate 4, the outer wall of one side of the mounting plate 4 is fixedly connected with the motor base 5, the outer wall of one side of the motor base 5 is in threaded connection with the bolt 6, one end of the bolt 6 is in threaded connection with the inner wall of one side of the mounting plate 4, the bolt 6 is used in a matched manner, the disassembly and maintenance are convenient, the outer wall of one side of the motor base 5 is fixedly connected with the first motor 7, one end of the output shaft of the first motor 7 is rotatably connected with the inside of the reaction tank 1, the outer wall of one end of the output shaft of the first motor 7 is fixedly connected with the rotating shaft 8, one end of the rotating shaft 8 is fixedly connected to one side inner wall of the bearing 10, a stirring frame 11 is fixedly connected to one side outer wall of the rotating shaft 8, a connecting rod 12 is fixedly connected to one side inner wall of the stirring frame 11, the stability of the stirring frame 11 is improved, a limiting groove 13 is distributed on one side outer wall of the stirring frame 11, a telescopic rod 14 is fixedly connected to one side inner wall of the limiting groove 13, a spring 15 is sleeved on one side outer wall of an output shaft of the telescopic rod 14, a scraper 16 is fixedly connected to one end outer wall of an output shaft of the telescopic rod 14, a discharge hole 17 is formed in the bottom end inner wall of the reaction tank 1 in a penetrating manner, a double-output-shaft oil cylinder 18 is embedded and connected to the bottom end inner wall of the reaction tank 1, sliding grooves 19 are symmetrically formed in one side outer wall of the bottom end inner wall of the reaction tank 1 corresponding to the output, the first limiting block 20 is connected to the inner wall of one side of the sliding groove 19 in a sliding manner, the bottom end of the reaction tank 1 is provided with a material receiving box 21, the outer wall of the bottom end of the material receiving box 21 is fixedly connected with a pulley 22, the outer wall of one side of the material receiving box 21 is fixedly connected with a handle 23, the material receiving box 21 is convenient to move by the matching use of the pulley 22 and the handle 23, the outer wall of the top end of the reaction tank 1 is inserted with an air outlet pipe 24, the outer wall of one side of the reaction tank 1 is inserted with a first air inlet pipe 25, the inner wall of one side of the first air inlet pipe 25 is fixedly connected with a second limiting block 26, the inner wall of one side of the second limiting block 26 is provided with a first through hole 27 in a penetrating manner, the outer wall of one side of the reaction tank 1 corresponding to the first air inlet pipe 25 is fixedly connected with a first motor box 28, the inner wall of one, a first limiting ball 30 is fixedly connected to the outer wall of one end of an output shaft of a second motor 29, a second through hole 31 is penetrated and formed in the outer wall of one side of the first limiting ball 30, a third through hole 32 is penetrated and formed in the outer wall of one side of the first limiting ball 30, a second air inlet pipe 33 is inserted and connected to the outer wall of one side of the reaction tank 1, a third limiting block 34 is fixedly connected to the inner wall of one side of the second air inlet pipe 33, a fourth through hole 35 is penetrated and formed in the inner wall of one side of the third limiting block 34, a second motor box 36 is fixedly connected to one side of the outer wall of one side of the reaction tank 1 corresponding to the second air inlet pipe 33, a third motor 37 is fixedly connected to the inner wall of one side of the second motor box 36, one end of an output shaft of the third motor 37 is rotatably connected to the inside of the second air inlet pipe 33, a second limiting ball 38 is fixedly, a fifth through hole 39 is formed in the outer wall of one side of the second limiting ball 38 in a penetrating manner, and a sixth through hole 40 is formed in the outer wall of one side of the second limiting ball 38 in a penetrating manner.
Referring to fig. 6, an implementation method of a high-purity ammonia deep purification device includes a first step of preparing for work; step two, desulfurization treatment; step three, cleaning a reaction tank; step four, treating residues;
in the first step, the work preparation comprises the following steps;
1) debugging a first motor 7, installing the first motor 7 at the top end of the reaction tank 1, and connecting an output shaft of the first motor 7 with a rotating shaft 8;
2) manually moving an empty material receiving box 21 to the lower part of the reaction tank 1 through the matching of a pulley 22 and a handle 23, and starting a double-output-shaft oil cylinder 18 to enable a first limiting block 20 to seal a discharge hole 17;
in the second step, the desulfurization treatment comprises the following steps;
1) quantitative gas and quantitative ammonia gas which need to be desulfurized are simultaneously introduced into the reaction tank 1 through the matching of the first air inlet pipe 25 and the second air inlet pipe 33, so that the gas and the ammonia gas are reacted and desulfurized in the reaction tank 1;
2) respectively starting the second motor 29 and the third motor 37 to drive the first limiting ball 30 and the second limiting ball 38 to rotate, so that the first air inlet pipe 25 and the second air inlet pipe 33 are opened and closed, and the flow rate of the gas introduced into the reaction tank 1 is adjusted through the rotation of the first limiting ball 30 and the second limiting ball 38;
3) opening the gas outlet pipe 24, and leading out the desulfurized high-purity gas;
in the third step, the first motor 7 is started to drive the scraper 16 on the stirring frame 11 to rotate, so that the scraper 16 scrapes the inner wall of the reaction tank 1, and the high-purity gas reacts with the ammonia gas to be separated out and the solid condensed on the inner wall of the reaction tank 1 is scraped;
in the fourth step, the double-output-shaft oil cylinder 18 is started to drive the first limiting block 20 to move, the discharge hole 17 is opened, and solid residues in the reaction tank 1 are led out and collected in the material receiving box 21 through the matching of the scraper 16 on the stirring frame 11.
Based on the above, the present invention has the advantages that when the present invention is used, the first motor 7 is debugged, the first motor 7 is installed at the top end of the reaction tank 1, and the output shaft of the first motor 7 is connected with the rotating shaft 8; manually moving the empty material receiving box 21 to the lower part of the reaction tank 1 through the matching of the pulley 22 and the handle 23, starting the double-output-shaft oil cylinder 18 to drive the first limiting block 20 to move, so that the first limiting block 20 seals the discharge hole 17, simultaneously introducing quantitative gas and quantitative ammonia gas to be subjected to desulfurization treatment into the reaction tank 1 through the matching of the first air inlet pipe 25 and the second air inlet pipe 33, so that the gas is subjected to reaction desulfurization in the reaction tank 1, respectively starting the second motor 29 and the third motor 37 to drive the first limiting ball 30 and the second limiting ball 38 to rotate, so as to realize the opening and closing actions of the first air inlet pipe 25 and the second air inlet pipe 33, regulating the flow rate of the gas introduced into the reaction tank 1 through the rotation of the first limiting ball 30 and the second limiting ball 38, opening the air outlet pipe 24, leading out the desulfurized high-purity gas, starting the first motor 7 to drive the scraper 16 on the stirring frame 11 to rotate, the scraper 16 scrapes the inner wall of the reaction tank 1, so that the high-purity gas and the ammonia gas react to separate out and condense solid on the inner wall of the reaction tank 1 to scrape, the double-output-shaft oil cylinder 18 is started to drive the first limiting block 20 to move, the discharge hole 17 is opened, solid residues in the reaction tank 1 are led out through the matching of the scraper 16 on the stirring frame 11 and collected in the material receiving box 21, and the material receiving box 21 is moved to a proper position through the matching of the pulley 22 and the handle 23.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (9)
1. The utility model provides a high-purity ammonia deep purification device which characterized in that: the device comprises a reaction tank (1), a first motor (7), a rotating shaft (8), a bearing seat (9), a bearing (10), a stirring frame (11), a limiting groove (13), a telescopic rod (14), a spring (15), a scraper (16), a discharge hole (17), an air outlet pipe (24), a first air inlet pipe (25) and a second air inlet pipe (33), wherein the first motor (7) is installed at the upper part of the reaction tank (1), an output shaft of the first motor (7) is connected with the rotating shaft (8), the bearing seat (9) is fixedly connected to the inner wall of the bottom end of the reaction tank (1), the bearing (10) is installed on the bearing seat (9), and the lower end of the rotating shaft (8) is installed on; a stirring frame (11) is arranged on the rotating shaft (8), a limiting groove (13) is distributed on the outer wall of the stirring frame (11), a telescopic rod (14) is fixedly connected with the limiting groove (13), a spring (15) is sleeved on the telescopic rod (14), a scraper (16) is fixedly connected with the outer end of the telescopic rod (14), and the scraper (16) is positioned on the inner wall of the reaction tank (1); the bottom end of the reaction tank (1) is provided with a discharge hole (17); the top of retort (1) is pegged graft and is had outlet duct (24), and it has first intake pipe (25) to peg graft on the outer wall of one side of retort (1), and it has second intake pipe (33) to peg graft on the opposite side outer wall of retort (1).
2. The high-purity ammonia deep purification device according to claim 1, characterized in that: the bottom end of the reaction tank (1) is connected with a double-output-shaft oil cylinder (18) in an embedded mode, sliding grooves (19) are symmetrically formed in the outer wall of one side, corresponding to the oil cylinder rod of the double-output-shaft oil cylinder (18), of the bottom end of the reaction tank (1), first limiting blocks (20) are fixedly connected to the oil cylinder rod of the double-output-shaft oil cylinder (18), and the first limiting blocks (20) are installed in the sliding grooves (19) in a sliding mode.
3. The high-purity ammonia deep purification device according to claim 1, characterized in that: an air outlet pipe (24) is spliced at the top of the reaction tank (1), a first air inlet pipe (25) is spliced on the outer wall of one side of the reaction tank (1), a second limiting block (26) is fixedly connected in the first air inlet pipe (25), a first through hole (27) is formed in the second limiting block (26) in a penetrating way, one end of an output shaft of a second motor (29) is rotatably connected in the first air inlet pipe (25), a first limiting ball (30) is fixedly connected at one end of an output shaft of the second motor (29), a second through hole (31) is formed in the outer wall of the first limiting ball (30) in a penetrating way, a third through hole (32) is formed in the outer wall of the first limiting ball (30) in a penetrating way, a second air inlet pipe (33) is spliced in the outer wall of the other side of the reaction tank (1), a third limiting block (34) is fixedly connected in the second air inlet pipe (33), a fourth through, one end of an output shaft of the third motor (37) is rotatably connected to the inside of the second air inlet pipe (33), a second limiting ball (38) is fixedly connected to the inner wall of one side, corresponding to the second air inlet pipe (33), of the outer wall of one end of the output shaft of the third motor (37), a fifth through hole (39) is formed in the outer wall of one side of the second limiting ball (38) in a penetrating mode, and a sixth through hole (40) is formed in the outer wall of one side of the second limiting ball (38) in a penetrating mode.
4. The high-purity ammonia deep purification device according to claim 1, characterized in that: and a protective layer (3) is arranged on the inner wall of one side of the reaction tank (1).
5. The high-purity ammonia deep purification device according to claim 1, characterized in that: the reaction tank (1) is provided with a mounting plate (4) on the upper part, and a motor base (5) of a first motor (7) is fixed on the mounting plate (4) through a bolt (6).
6. The high-purity ammonia deep purification device according to claim 1, characterized in that: and a connecting rod (12) is arranged between the stirring frames (11) at the two sides.
7. The high-purity ammonia deep purification device according to claim 1, characterized in that: the material receiving box is characterized in that a material receiving box (21) is arranged below a discharge hole (17) in the bottom of the reaction tank (1), a pulley (22) is arranged at the bottom end of the material receiving box (21), and a handle (23) is fixedly connected to the outer wall of one side of the material receiving box (21).
8. The method for carrying out advanced purification of high-purity ammonia according to claim 1 to 7, wherein: step one, desulfurization treatment; step two, cleaning a reaction tank; step three, treating residues;
in the first step, the desulfurization treatment comprises the following steps;
1) quantitative gas and quantitative ammonia gas which need to be desulfurized are simultaneously introduced into the reaction tank (1) through the matching of the first air inlet pipe (25) and the second air inlet pipe (33), so that the reaction tank (1) can be used for reaction and desulfurization;
2) respectively starting a second motor (29) and a third motor (37) to drive a first limiting ball (30) and a second limiting ball (38) to rotate, so that a first air inlet pipe (25) and a second air inlet pipe (33) are opened and closed, and the flow rate of gas introduced into the reaction tank (1) is adjusted through the rotation of the first limiting ball (30) and the second limiting ball (38);
3) opening the gas outlet pipe (24) and leading out the desulfurized high-purity gas;
and in the second step, the first motor (7) is started to drive the scraper (16) on the stirring frame (11) to rotate, so that the scraper (16) scrapes the inner wall of the reaction tank (1), and the high-purity gas reacts with the ammonia gas to precipitate solids condensed on the inner wall of the reaction tank (1) and be scraped.
9. The method for implementing the advanced purification of the high-purity ammonia according to claim 8, wherein: in the third step, the double-output-shaft oil cylinder (18) is started to drive the first limiting block (20) to move, the discharge hole (17) is opened, and solid residues in the reaction tank (1) are led out and collected in the material collecting box (21) through the matching of the scraper (16) on the stirring frame (11).
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| CN202011371768.1A CN112479226B (en) | 2020-11-30 | 2020-11-30 | High-purity ammonia deep purification device and implementation method thereof |
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| CN202011371768.1A CN112479226B (en) | 2020-11-30 | 2020-11-30 | High-purity ammonia deep purification device and implementation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116874065A (en) * | 2023-08-15 | 2023-10-13 | 广州市适然环境工程技术有限公司 | Ozone oxidation treatment device and treatment process for high-concentration chemical wastewater |
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| CN116874065A (en) * | 2023-08-15 | 2023-10-13 | 广州市适然环境工程技术有限公司 | Ozone oxidation treatment device and treatment process for high-concentration chemical wastewater |
| CN116874065B (en) * | 2023-08-15 | 2024-02-13 | 广州市适然环境工程技术有限公司 | Ozone oxidation treatment device and treatment process for high-concentration chemical wastewater |
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