CN112402269A - 一种保湿修复面膜及其制备方法 - Google Patents
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Abstract
本发明公开了一种保湿修复面膜及其制备方法,它是由下述重量份的原料组成的,蓖麻酸钙0.1‑0.3、抗坏血酸棕榈酸酯10‑14、玻尿酸5‑7、壳聚糖1‑2、油相溶液40‑50、分散剂1‑2、黄原胶1‑2、乙二胺四乙酸0.9‑2、复合蛋白3‑5,本发明加入的钙离子在皮肤细胞分裂分化、皮脂的合成分泌、皮肤屏障再生自律中有着重要的作用,适当浓度的钙离子能够修复皮肤表皮损伤;钙离子具有天然抗氧化活性,能够有效人体自由基,延缓皮肤衰老组织皱纹产生。
Description
技术领域
本发明属于面膜领域,具体涉及一种保湿修复面膜及其制备方法。
背景技术
随着经济不断增长,人民生活水平日益提升,大家对美的要求也越来越高越来越关注,大量的护肤产品层出不穷、涌入市场,虽然给许多爱美人士带来了福音,但随之而来因护肤产品,尤其是美白产品,引起的皮肤问题的报道逐渐引起了人们的警惕。面膜是集清洁、护肤、美容为一体的多用途化妆品,涂覆在肌肤上,经过一定时间干燥后,在肌肤表面形成一层膜状物,将该膜去掉后,能够达到清洁肌肤的目的。面膜在使用过程中,其对肌肤存在一定的吸附作用,使得肌肤分泌旺盛,在去掉面膜时,能够将残留在肌肤表层的分泌物等除去,达到清洁的目的;同时,面膜还具有覆盖在肌肤表面,抑制水分蒸发,达到软化皮角质层,扩张毛孔和汗腺口,促进汗腺分泌与新陈代谢,使肌肤的含氧量上升,促进血液循环,使得肌肤吸收面膜中的活性营养成分,进而达到良好的护肤效果。
玻尿酸,又称糖醛酸、透明质酸,基本结构是由两个双糖单位D~葡萄糖醛酸及N~乙酰葡糖胺组成的大型多糖类。与其它粘多糖不同,它不含硫。它的透明质分子能携带500倍以上的水分,为当今所公认的最佳保湿成分,广泛的应用在保养品和化妆品中;
抗坏血酸棕榈酸酯是一种有效的抗氧化剂,是非酸性、稳定的维他命C。它具有维生素C的全部生理活性,能够起到抗炎、减少黑色素生成、促进免疫球蛋白合成,防治外伤、晒伤、痤疮等所致的色素沉着,能美白皮肤,维持皮肤弹性,减轻皱纹,改善皮肤粗糙、苍白、松弛等现象,延缓皮肤自然老化及光老化,是一种高效的抗氧化剂和氧自由基清除剂酸碱值呈中性,安定度中等;
目前市售的面膜品种繁多,但是质量参差不齐,尤其是主打中药类的面膜,其使用效果以及是否会对面部造成一定影响,都有待进一步考究,本发明的目的就是提供一种富含蛋白的,使用效果稳定,保湿修复效果好,贮存稳定性高的面膜产品。
发明内容
本发明的目的是提供一种保湿修复面膜及其制备方法。
为实现上述目的,本发明采用以下技术方案:
一种保湿修复面膜,它是由下述重量份的原料组成的:
蓖麻酸钙0.1-0.3、抗坏血酸棕榈酸酯10-14、玻尿酸5-7、壳聚糖1-2、油相溶液40-50、分散剂1-2、黄原胶1-2、乙二胺四乙酸0.9-2、复合蛋白3-5。
所述复合蛋白的制备方法,包括以下步骤:
(1)取3-5重量份的青蒿,加100-130倍水,打浆,超声,过滤,得滤液;
(2)取30-40重量份的黄豆,加20-30倍水,打浆,加氢氧化钠,调节pH为9-10,加入1-2重量份的茶皂素,离心分离,在上清液中加入醋酸,调节pH为3-4,加入到上述滤液中,搅拌均匀,喷雾干燥,即得所述复合蛋白。
所述分散剂为卵磷脂、羧甲基纤维素钠中的一种。
所述油相溶液的制备方法,包括以下步骤:
(1)取2-3重量份的尼泊金甲酯,加入到27-30重量份的甘草精油中,搅拌均匀,得精油溶液;
(2)取0.1-0.4重量份的硬脂酸钙,加入到上述精油溶液中,在40-50℃下保温搅拌10-20分钟,冷却至常温,即得。
一种保湿修复面膜的制备方法,包括以下步骤:
(1)取壳聚糖、玻尿酸混合,加入到混合料重量90-100倍的去离子水中,搅拌均匀,得水分散液;
(2)取抗坏血酸棕榈酸酯,加入到油相溶液中,搅拌均匀,与上述水分散液混合,搅拌均匀,加入分散剂,超声10-20分钟,加入复合蛋白,乳化,得o/w溶液;
(3)取蓖麻酸钙,加入到上述o/w溶液中,搅拌均匀,升高温度为65-70℃,加入乙二胺四乙酸,保温搅拌1-2小时,加入黄原胶,搅拌至常温,得浸渍液;
(4)取载体,加入到浸渍液中,浸渍3-5小时,出料,包装,即得。
步骤(1)中所述的超声频率为30-35kHz。
步骤(4)中所述载体为蚕丝面膜。
本发明的优点:
本发明的有益效果在于,本发明加入的复合蛋白,还有多糖和蛋白成品,青蒿多糖具有很好的抗氧化效果,能够有效的改善肌肤变黄,可以避免斑点的产生,蛋白则能够滋润肌肤,使得肌肤弹性更好,美白保湿性强,本发明还配合了尼泊金甲酯的精油溶液,具有很好的修复效果,本发明通过将油相与壳聚糖的水溶液共混,形成水包油溶液,在其中加入钙离子作为稳定剂,再通过乙二胺四乙酸进行螯合,得到稳定的钙离子掺杂水包油溶液,提高了成品有效物质的稳定性;
本发明加入的钙离子在皮肤细胞分裂分化、皮脂的合成分泌、皮肤屏障再生自律中有着重要的作用,适当浓度的钙离子能够修复皮肤表皮损伤;钙离子具有天然抗氧化活性,能够有效人体自由基,延缓皮肤衰老组织皱纹产生;钙离子与蛋白质螯合作用,作用于深层肌肤,改善肌肤微循环、细胞自我修复功能,再生嫩滑滋润弹性肌肤;钙离子与天然植物提取物复合作用,深度清洁,补水滋养,修复细胞活性,使得肌肤更光泽水润。
具体实施方式
实施例1
一种保湿修复面膜,它是由下述重量份的原料组成的:
蓖麻酸钙0.1、抗坏血酸棕榈酸酯10、玻尿酸5、壳聚糖1、油相溶液40、分散剂1、黄原胶1、乙二胺四乙酸0.9、复合蛋白3。
所述复合蛋白的制备方法,包括以下步骤:
(1)取3重量份的青蒿,加100倍水,打浆,超声,过滤,得滤液;
(2)取30重量份的黄豆,加20倍水,打浆,加氢氧化钠,调节pH为9,加入1重量份的茶皂素,离心分离,在上清液中加入醋酸,调节pH为3,加入到上述滤液中,搅拌均匀,喷雾干燥,即得所述复合蛋白。
所述分散剂为卵磷脂。
所述油相溶液的制备方法,包括以下步骤:
(1)取2重量份的尼泊金甲酯,加入到27重量份的甘草精油中,搅拌均匀,得精油溶液;
(2)取0.1重量份的硬脂酸钙,加入到上述精油溶液中,在40℃下保温搅拌10分钟,冷却至常温,即得。
一种保湿修复面膜的制备方法,包括以下步骤:
(1)取壳聚糖、玻尿酸混合,加入到混合料重量90倍的去离子水中,搅拌均匀,得水分散液;
(2)取抗坏血酸棕榈酸酯,加入到油相溶液中,搅拌均匀,与上述水分散液混合,搅拌均匀,加入分散剂,超声10分钟,加入复合蛋白,乳化,得o/w溶液;
(3)取蓖麻酸钙,加入到上述o/w溶液中,搅拌均匀,升高温度为65℃,加入乙二胺四乙酸,保温搅拌1小时,加入黄原胶,搅拌至常温,得浸渍液;
(4)取载体,加入到浸渍液中,浸渍3小时,出料,包装,即得。
步骤(1)中所述的超声频率为30kHz。
步骤(4)中所述载体为蚕丝面膜。
实施例2
一种保湿修复面膜,它是由下述重量份的原料组成的:
蓖麻酸钙0.3、抗坏血酸棕榈酸酯14、玻尿酸7、壳聚糖2、油相溶液50、分散剂2、黄原胶2、乙二胺四乙酸2、复合蛋白5。
所述复合蛋白的制备方法,包括以下步骤:
(1)取5重量份的青蒿,加130倍水,打浆,超声,过滤,得滤液;
(2)取40重量份的黄豆,加30倍水,打浆,加氢氧化钠,调节pH为10,加入2重量份的茶皂素,离心分离,在上清液中加入醋酸,调节pH为4,加入到上述滤液中,搅拌均匀,喷雾干燥,即得所述复合蛋白。
所述分散剂为羧甲基纤维素钠。
所述油相溶液的制备方法,包括以下步骤:
(1)取3重量份的尼泊金甲酯,加入到30重量份的甘草精油中,搅拌均匀,得精油溶液;
(2)取0.4重量份的硬脂酸钙,加入到上述精油溶液中,在50℃下保温搅拌20分钟,冷却至常温,即得。
一种保湿修复面膜的制备方法,包括以下步骤:
(1)取壳聚糖、玻尿酸混合,加入到混合料重量100倍的去离子水中,搅拌均匀,得水分散液;
(2)取抗坏血酸棕榈酸酯,加入到油相溶液中,搅拌均匀,与上述水分散液混合,搅拌均匀,加入分散剂,超声20分钟,加入复合蛋白,乳化,得o/w溶液;
(3)取蓖麻酸钙,加入到上述o/w溶液中,搅拌均匀,升高温度为70℃,加入乙二胺四乙酸,保温搅拌2小时,加入黄原胶,搅拌至常温,得浸渍液;
(4)取载体,加入到浸渍液中,浸渍5小时,出料,包装,即得。
步骤(1)中所述的超声频率为35kHz。
步骤(4)中所述载体为蚕丝面膜。
实施例3
一种保湿修复面膜,它是由下述重量份的原料组成的:
蓖麻酸钙0.2、抗坏血酸棕榈酸酯12、玻尿酸6、壳聚糖1、油相溶液44、分散剂1、黄原胶1、乙二胺四乙酸1、复合蛋白4。
所述复合蛋白的制备方法,包括以下步骤:
(1)取4重量份的青蒿,加110倍水,打浆,超声,过滤,得滤液;
(2)取34重量份的黄豆,加25倍水,打浆,加氢氧化钠,调节pH为9,加入1重量份的茶皂素,离心分离,在上清液中加入醋酸,调节pH为3,加入到上述滤液中,搅拌均匀,喷雾干燥,即得所述复合蛋白。
所述分散剂为卵磷脂。
所述油相溶液的制备方法,包括以下步骤:
(1)取2重量份的尼泊金甲酯,加入到27-30重量份的甘草精油中,搅拌均匀,得精油溶液;
(2)取0.3重量份的硬脂酸钙,加入到上述精油溶液中,在46℃下保温搅拌15分钟,冷却至常温,即得。
一种保湿修复面膜的制备方法,包括以下步骤:
(1)取壳聚糖、玻尿酸混合,加入到混合料重量95倍的去离子水中,搅拌均匀,得水分散液;
(2)取抗坏血酸棕榈酸酯,加入到油相溶液中,搅拌均匀,与上述水分散液混合,搅拌均匀,加入分散剂,超声13分钟,加入复合蛋白,乳化,得o/w溶液;
(3)取蓖麻酸钙,加入到上述o/w溶液中,搅拌均匀,升高温度为68℃,加入乙二胺四乙酸,保温搅拌1小时,加入黄原胶,搅拌至常温,得浸渍液;
(4)取载体,加入到浸渍液中,浸渍4小时,出料,包装,即得。
步骤(1)中所述的超声频率为32kHz。
步骤(4)中所述载体为蚕丝面膜。
实施例测试:
选取40例肌肤健康,无肌肤病过敏史的受试志愿者,20-40岁,随机分为4组,每组10人,对本发明实施例1-3和市售玻尿酸面膜(韩国snp)进行使用功效实验。
受试志愿者每晚洗净脸后,使用本发明实施例1-3和市售玻尿酸面膜(韩国snp)的产品,20min去掉面膜,再用手轻柔按摩5min至营养成分完全吸收为止。测试周期为5周,隔一天使用一次面膜。受试者根据自己的感受对肌肤改善进行评分,评分采用5分制,1分为最差,3分为适中,5分为最好。
以上所述仅是对本发明的实施方式的举例展示,并非对本发明作任何形式上的限制。本发明保护范围以权利要求书为准且不由上述具体实施例所限,凡是依据本发明的技术实质对以上实施方式所作的任何简单修改或等同变化与修饰均属于本发明的保护范围。
Claims (7)
1.一种保湿修复面膜,其特征在于,它是由下述重量份的原料组成的:
蓖麻酸钙0.1-0.3、抗坏血酸棕榈酸酯10-14、玻尿酸5-7、壳聚糖1-2、油相溶液40-50、分散剂1-2、黄原胶1-2、乙二胺四乙酸0.9-2、复合蛋白3-5。
2.根据权利要求1所述的一种保湿修复面膜,其特征在于,所述复合蛋白的制备方法,包括以下步骤:
(1)取3-5重量份的青蒿,加100-130倍水,打浆,超声,过滤,得滤液;
(2)取30-40重量份的黄豆,加20-30倍水,打浆,加氢氧化钠,调节pH为9-10,加入1-2重量份的茶皂素,离心分离,在上清液中加入醋酸,调节pH为3-4,加入到上述滤液中,搅拌均匀,喷雾干燥,即得所述复合蛋白。
3.根据权利要求1所述的一种保湿修复面膜,其特征在于,所述分散剂为卵磷脂、羧甲基纤维素钠中的一种。
4.根据权利要求1所述的一种保湿修复面膜,其特征在于,所述油相溶液的制备方法,包括以下步骤:
(1)取2-3重量份的尼泊金甲酯,加入到27-30重量份的甘草精油中,搅拌均匀,得精油溶液;
(2)取0.1-0.4重量份的硬脂酸钙,加入到上述精油溶液中,在40-50℃下保温搅拌10-20分钟,冷却至常温,即得。
5.一种如权利要求1所述保湿修复面膜的制备方法,其特征在于,包括以下步骤:
(1)取壳聚糖、玻尿酸混合,加入到混合料重量90-100倍的去离子水中,搅拌均匀,得水分散液;
(2)取抗坏血酸棕榈酸酯,加入到油相溶液中,搅拌均匀,与上述水分散液混合,搅拌均匀,加入分散剂,超声10-20分钟,加入复合蛋白,乳化,得o/w溶液;
(3)取蓖麻酸钙,加入到上述o/w溶液中,搅拌均匀,升高温度为65-70℃,加入乙二胺四乙酸,保温搅拌1-2小时,加入黄原胶,搅拌至常温,得浸渍液;
(4)取载体,加入到浸渍液中,浸渍3-5小时,出料,包装,即得。
6.根据权利要求2所述的保湿修复面膜的制备方法,其特征在于,步骤(1)中所述的超声频率为30-35kHz。
7.根据权利要求5所述的保湿修复面膜的制备方法,其特征在于,步骤(4)中所述载体为蚕丝面膜。
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