CN112225549A - Bionic far infrared ceramic powder material and preparation method thereof - Google Patents
Bionic far infrared ceramic powder material and preparation method thereof Download PDFInfo
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- CN112225549A CN112225549A CN202010863161.9A CN202010863161A CN112225549A CN 112225549 A CN112225549 A CN 112225549A CN 202010863161 A CN202010863161 A CN 202010863161A CN 112225549 A CN112225549 A CN 112225549A
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/26—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on ferrites
- C04B35/2608—Compositions containing one or more ferrites of the group comprising manganese, zinc, nickel, copper or cobalt and one or more ferrites of the group comprising rare earth metals, alkali metals, alkaline earth metals or lead
- C04B35/2633—Compositions containing one or more ferrites of the group comprising manganese, zinc, nickel, copper or cobalt and one or more ferrites of the group comprising rare earth metals, alkali metals, alkaline earth metals or lead containing barium, strontium or calcium
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/26—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on ferrites
- C04B35/2608—Compositions containing one or more ferrites of the group comprising manganese, zinc, nickel, copper or cobalt and one or more ferrites of the group comprising rare earth metals, alkali metals, alkaline earth metals or lead
- C04B35/2625—Compositions containing one or more ferrites of the group comprising manganese, zinc, nickel, copper or cobalt and one or more ferrites of the group comprising rare earth metals, alkali metals, alkaline earth metals or lead containing magnesium
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- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
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- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/444—Halide containing anions, e.g. bromide, iodate, chlorite
Abstract
The invention relates to the technical field of ceramic powder materials, and discloses a bionic far infrared ceramic powder material and a preparation method thereof, wherein the bionic far infrared ceramic powder material comprises the following chemical components in percentage by mass: 50-55% of ferric oxide, 15-25% of calcium carbonate, 3-8% of sodium chloride, 3-8% of phosphorus pentoxide, 3-8% of potassium carbonate, 2-7% of magnesium carbonate, 2-7% of silicon dioxide, 1-3% of zinc oxide and 1-3% of strontium carbonate; the formula of the bionic far infrared ceramic powder material is formulated according to chemical components and proportions of a human body, and a finished product of the bionic far infrared ceramic powder material is detected and tried, wherein the far infrared wavelength is between 8 and 14 microns, is similar to the frequency of water molecule vibration in biological cells, and is easily absorbed by the human body or other organisms, so that cell tissues are activated, and the bionic far infrared ceramic powder material has remarkable warming and health care physiotherapy effects; the preparation method of the bionic far infrared ceramic powder material is simple in preparation process.
Description
Technical Field
The invention relates to the technical field of ceramic materials, in particular to a bionic far infrared ceramic powder material and a preparation method thereof.
Background
The far infrared radiation ceramic material is a novel photo-thermal conversion material, has higher radiation rate and higher radiation intensity, is widely applied to manufacturing drying furnaces, baking furnaces, heat treatment furnaces, medical physiotherapy instruments, household heaters and the like, and is also widely applied to a plurality of fields of household appliances, medical treatment and the like.
The far infrared radiation ceramic material is prepared by taking carbide, oxide, nitride and the like as raw materials and adopting a pottery clay particle material processing technology, and has higher radiance and radiation intensity in a far infrared band.
In the prior art, the commonly used far infrared radiation ceramics mainly comprise black or dark far infrared radiation ceramics such as silicon carbide series, iron-manganese-nickel-cobalt-copper series, negative ion powder and the like, and white far infrared radiation ceramics such as zirconia series, aluminum-magnesium-silicon-zinc-titanium-rare earth series and the like. However, the formula and the preparation method of the existing argil particle material cause that the far infrared emissivity of the far infrared radiation ceramics is low, and the application occasions of the processed argil particle material are not flexible enough.
Disclosure of Invention
The invention aims to overcome the defects of the prior art, adapt to practical development and provide a ceramic material capable of generating bionic far infrared rays.
The invention is realized in such a way that the bionic far infrared ceramic powder material comprises the following chemical components in percentage by mass: 50-55% of ferric oxide, 15-25% of calcium carbonate, 3-8% of sodium chloride, 3-8% of phosphorus pentoxide, 3-8% of potassium carbonate, 2-7% of magnesium carbonate, 2-7% of silicon dioxide, 1-3% of zinc oxide and 1-3% of strontium carbonate.
Preferably, the ferric oxide is 53%.
Preferably, the calcium carbonate is 20%.
Preferably, the sodium chloride is 5%.
Preferably, the phosphorus pentoxide is 5%.
Preferably, the potassium carbonate is 5%.
Preferably, the magnesium carbonate is 4%.
Preferably, the silicon dioxide is 4%, the zinc oxide is 2%, and the strontium carbonate is 2%.
Compared with the prior art, the formula of the bionic far infrared ceramic powder material is formulated according to chemical components and proportions of a human body, and a finished product of the bionic far infrared ceramic powder material is detected and tried out, wherein the far infrared wavelength is between 8 and 14 microns, is similar to the frequency of water molecule vibration in biological cells, is easily absorbed by the human body or other organisms, so that cell tissues are activated, and the bionic far infrared ceramic powder material has remarkable warming and health care physiotherapy effects.
The invention also provides a preparation method of the bionic far infrared ceramic powder material, which comprises the following steps:
1) respectively weighing the ferric oxide, the calcium carbonate, the sodium chloride, the phosphorus pentoxide, the potassium carbonate, the magnesium carbonate, the silicon dioxide, the zinc oxide and the strontium carbonate in parts by weight;
2) and filling the weighed raw materials into a ball mill, and adding: water weight ratio equal to 1: 1, performing primary ball milling for 2 hours to uniformly mix;
3) dehydrating and drying the slurry subjected to the first ball milling;
4) loading the dried mixture into a high-temperature sintering furnace for calcining;
5) and loading the calcined material into a ball mill and adding: water equal to 1: carrying out secondary ball milling on 0.8 purified water for 8 hours to obtain the required material granularity;
6) and drying the slurry subjected to the secondary ball milling for later use.
Further, in the step 4), the sintering temperature of the high-temperature constant-temperature calcination is 1150-1200 ℃, and the constant-temperature time is 2 hours.
Compared with the prior art, the preparation method of the bionic far infrared ceramic powder material provided by the invention is simple in preparation process, can be applied to a physiotherapy bed or an electric heating product, has the advantages of rapid temperature rise, high heat conversion efficiency, large-amount far infrared ray release and the like, and can improve human microcirculation and human immunity.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
The bionic far infrared ceramic powder material provided by the embodiment is applied to a physiotherapy bed or an electric heating product, and is used for improving human microcirculation and human immunity.
The bionic far-infrared ceramic powder material comprises the following chemical components in percentage by mass: 50-55% of ferric oxide, 15-25% of calcium carbonate, 3-8% of sodium chloride, 3-8% of phosphorus pentoxide, 3-8% of potassium carbonate, 2-7% of magnesium carbonate, 2-7% of silicon dioxide, 1-3% of zinc oxide and 1-3% of strontium carbonate.
The formula of the bionic far infrared ceramic powder material is formulated according to chemical components and proportions of a human body, and a finished product of the bionic far infrared ceramic powder material is detected and tried, wherein the far infrared wavelength is between 8 and 14 micrometers, is similar to the frequency of water molecule vibration in biological cells, and is easily absorbed by the human body or other organisms, so that cell tissues are activated, and the bionic far infrared ceramic powder material has remarkable warming and health care physiotherapy effects.
Preferably, the ferric oxide is 53%.
Preferably, the calcium carbonate is 20%.
Preferably, the sodium chloride is 5%.
Preferably, the phosphorus pentoxide is 5%.
Preferably, the potassium carbonate is 5%.
Preferably, the magnesium carbonate is 4%.
Preferably, the silicon dioxide is 4%, the zinc oxide is 2%, and the strontium carbonate is 2%.
The embodiment also provides a preparation method of the bionic far infrared ceramic powder material, which comprises the following steps:
1) respectively weighing the raw materials of ferric oxide, calcium carbonate, sodium chloride, phosphorus pentoxide, potassium carbonate, magnesium carbonate, silicon dioxide, zinc oxide and strontium carbonate in parts by weight, and mixing to obtain powder;
2) and filling the mixed powder into a ball mill, and adding: water 1: 1, performing primary ball milling on the purified water to achieve the purpose of uniform mixing;
3) dehydrating and drying the slurry subjected to the first ball milling mixing;
4) and putting the dried material into a high-temperature sintering furnace for calcining. (ii) a
5) And filling the calcined material into a ball milling tank and adding: water 1: purified water of 0.8 was ball milled for 8 hours to obtain the desired material particle size.
The preparation method of the bionic far infrared ceramic powder material has simple preparation process, can be applied to a physiotherapy bed or an electric heating product in a coating mode, has the advantages of rapid temperature rise, high heat conversion efficiency, large-amount release of bionic far infrared rays and the like, and can improve the microcirculation of a human body and the immunity of the human body.
In the step 4), the sintering temperature of the high-temperature constant-temperature calcination is 1150-1200 ℃, and the constant-temperature time is 2 hours.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents and improvements made within the spirit and principle of the present invention are intended to be included within the scope of the present invention.
Claims (10)
1. A bionic far infrared ceramic powder material is characterized in that the mass ratio of chemical components is as follows: 50-55% of ferric oxide, 15-25% of calcium carbonate, 3-8% of sodium chloride, 3-8% of phosphorus pentoxide, 3-8% of potassium carbonate, 2-7% of magnesium carbonate, 2-7% of silicon dioxide, 1-3% of zinc oxide and 1-3% of strontium carbonate.
2. The biomimetic far-infrared ceramic powder material according to claim 1, wherein the iron sesquioxide is 53%.
3. The biomimetic far-infrared ceramic powder material according to claim 1, wherein the calcium carbonate is 20%.
4. The biomimetic far-infrared ceramic powder material according to claim 1, wherein the sodium chloride is 5%.
5. The biomimetic far-infrared ceramic powder material according to claim 1, wherein the phosphorus pentoxide is 5%.
6. The biomimetic far-infrared ceramic powder material as set forth in claim 1, wherein the potassium carbonate is 5%.
7. The biomimetic far infrared ceramic powder material as set forth in claim 1, wherein the magnesium carbonate is 4%.
8. The bionic far-infrared ceramic powder material as claimed in claim 1, characterized in that the silica is 4%, the zinc oxide is 2%, and the strontium carbonate is 2%.
9. The method for preparing a bionic far-infrared ceramic powder material according to any one of claims 1 to 8, characterized by comprising the following steps:
1) putting the ferric oxide, calcium carbonate, sodium chloride, phosphorus pentoxide, potassium carbonate, magnesium carbonate, silicon dioxide, zinc oxide and strontium carbonate raw materials in parts by weight into a ball mill, and adding 1: 1, uniformly mixing by a water ball mill to obtain mixed powder slurry;
2) drying the mixed powder slurry;
3) calcining the dried mixed powder in a sintering furnace;
4) and filling the calcined powder into a ball mill and adding: water equal to 1: carrying out secondary ball milling on 0.8 purified water;
5) and drying the slurry subjected to the second ball milling for later use.
10. The method for preparing a bionic far-infrared ceramic powder material according to claim 9, wherein in the step 3), the sintering temperature of the high-temperature constant-temperature calcination is 1150-1200 ℃, and the constant-temperature time is 2 hours.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1535931A (en) * | 2003-04-11 | 2004-10-13 | 杨洪武 | Far infrared bio-active ceramic product and its process |
| CN103979936A (en) * | 2014-05-19 | 2014-08-13 | 河北工业大学 | Iron tailing far-infrared ceramic material and preparation method thereof |
| CN106495642A (en) * | 2016-10-22 | 2017-03-15 | 王景沧 | A kind of radiative material that just can be efficiently releasing far infrared without the need for heating |
| CN108892495A (en) * | 2018-08-08 | 2018-11-27 | 陕西新容康医疗器械有限公司 | A kind of clay granular materials and preparation method thereof that can generate far infrared |
| CN111253146A (en) * | 2020-01-21 | 2020-06-09 | 江南大学 | Medium-far infrared ceramic powder and preparation method thereof |
-
2020
- 2020-08-25 CN CN202010863161.9A patent/CN112225549A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1535931A (en) * | 2003-04-11 | 2004-10-13 | 杨洪武 | Far infrared bio-active ceramic product and its process |
| CN103979936A (en) * | 2014-05-19 | 2014-08-13 | 河北工业大学 | Iron tailing far-infrared ceramic material and preparation method thereof |
| CN106495642A (en) * | 2016-10-22 | 2017-03-15 | 王景沧 | A kind of radiative material that just can be efficiently releasing far infrared without the need for heating |
| CN108892495A (en) * | 2018-08-08 | 2018-11-27 | 陕西新容康医疗器械有限公司 | A kind of clay granular materials and preparation method thereof that can generate far infrared |
| CN111253146A (en) * | 2020-01-21 | 2020-06-09 | 江南大学 | Medium-far infrared ceramic powder and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 于琦等著: "《纳米氧化锌与金刚石复合结构的研究与应用》", 31 August 2016, 北京：北京邮电大学出版社 * |
| 凌鼎钟等: "《橡胶配合剂》", 30 April 1959, 上海：上海科学技术出版社 * |
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