CN112190530A - Preparation method of cod roe essence mask - Google Patents

Preparation method of cod roe essence mask Download PDF

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Publication number
CN112190530A
CN112190530A CN202011192856.5A CN202011192856A CN112190530A CN 112190530 A CN112190530 A CN 112190530A CN 202011192856 A CN202011192856 A CN 202011192856A CN 112190530 A CN112190530 A CN 112190530A
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cylinder
cod roe
enzymolysis device
filter
pressure column
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CN112190530B (en
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朱永会
李彩虹
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YANTAI NEW ERA HEALTH INDUSTRY DAILY CHEMICAL Co.,Ltd.
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Shenzhen Luoqi Electromechanical Technology Co ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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    • C12M33/00—Means for introduction, transport, positioning, extraction, harvesting, peeling or sampling of biological material in or from the apparatus
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    • C12M33/00—Means for introduction, transport, positioning, extraction, harvesting, peeling or sampling of biological material in or from the apparatus
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    • C12M47/00—Means for after-treatment of the produced biomass or of the fermentation or metabolic products, e.g. storage of biomass
    • C12M47/20—Heating or cooling

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Abstract

The invention relates to the technical field of cosmetic processing, in particular to a preparation method of a cod roe essence mask, which is prepared by the following steps: (1) cleaning fresh cod roe, adding deionized water and protease, and performing enzymolysis at 30-35 deg.C for 12-15 hr to obtain cod roe slurry; (2) carrying out solid-liquid separation on the cod roe slurry, taking the separated liquid, and adding nipagin ester and hyaluronic acid to obtain a mixed solution; (3) and introducing gas into the mixed solution, reducing the temperature to 8-15 ℃ under the pressure of 3-8MPa, stirring for 2-3h, filtering the crystallized solid, taking the filtered liquid, heating the liquid to 30-35 ℃, and sterilizing to obtain a finished product.

Description

Preparation method of cod roe essence mask
Technical Field
The invention relates to the technical field of cosmetic processing, in particular to a preparation method of a cod roe essence mask.
Background
The cod is cod fish, the cold water fish living in the bottom layer and middle and lower layers of the ocean is distributed in all oceans in the world, the cod fish is fresh and tender in meat quality and high in nutritional value and is favored by people, however, in production and processing, processing personnel often only take and cut the cod fish meat for sale, the viscera and roe of the cod fish are discarded, however, roe contains a large amount of protein, unsaturated fatty acid, phospholipid, inorganic elements and various vitamins, and the nutrient substances cannot be fully utilized at all, so that the prior art needs further improvement.
Disclosure of Invention
The invention aims to provide a preparation method of a cod roe essence mask which is good in moisturizing effect and can adjust the balance of skin moisture and oil.
A preparation method of a cod roe essence mask comprises the following steps: (1) cleaning fresh cod roe, adding deionized water and protease, and performing enzymolysis at 30-35 deg.C for 12-15 hr to obtain cod roe slurry; (2) carrying out solid-liquid separation on the cod roe slurry, taking the separated liquid, and adding nipagin ester and hyaluronic acid to obtain a mixed solution; (3) introducing gas into the mixed solution, reducing the temperature to 8-15 deg.C under 3-8MPa, stirring for 2-3h, filtering the crystallized solid, collecting the filtered liquid, heating to 30-35 deg.C, and sterilizing to obtain the final product.
Further, the mass-volume ratio of the cod roes, the deionized water, the protease, the nipagin ester and the hyaluronic acid is as follows: 20-50 g: 30-50 ml: 1-2 g: 2-5 ml.
Further, the gas in the step (3) is N2。
A processing system used in a preparation method of a cod roe essence mask comprises an enzymolysis device, wherein a discharge hole of the enzymolysis device is communicated with a feed inlet of a solid-liquid separator, a liquid outlet of the solid-liquid separator is communicated with a feed inlet of a heating tank, a discharge hole of the heating tank is communicated with a feed inlet of a microwave sterilizer, and a discharge hole of the microwave sterilizer is communicated with a bottling system.
Furthermore, the enzymolysis device comprises a shell, the shell is a sealed cavity, the shell is divided into an upper decomposition cavity and a lower hydration cavity by a baffle, the surface of the baffle is parallel to the bottom surface of the shell, a top wall in the shell is provided with a rotating base, a hydraulic cylinder is arranged below the rotating base, a telescopic rod of the hydraulic cylinder is connected with a pressure column, the baffle is provided with a through hole for the pressure column to pass through, the through hole is connected with a filter cylinder in a sliding way through a bearing, a crushing cylinder is sleeved in the filter cylinder, the diameter of the cylinder of the crushing cylinder is larger than the circular diameter of the pressure column, when the pressure column enters the crushing cylinder, the outer side wall of the pressure column is mutually attached to the inner side wall of the crushing cylinder, the length direction of the pressure column is the same as that of the crushing cylinder, the length directions of the filter cylinder and the crushing cylinder are the same as that of the shell, a plurality of cutting steel wires are arranged on the perforation, the upper opening edge of the crushing cylinder is connected with the upper opening edge of the filter cylinder through an annular plate, the lower openings of the crushing cylinder and the filter cylinder are fixedly connected with a rotary table, the disc surface of the rotary table is vertical to the length direction of the crushing cylinder and the filter cylinder, a rotary motor is connected below the rotary table, the base of the rotary motor is fixed at the bottom of the shell, the output end of the rotary motor is connected with the lower surface of the rotary table, a plurality of heaters are arranged above the baffle, a refrigerator is arranged below the baffle, the shell is also provided with an enzymolysis device steam outlet, an enzymolysis device first feed inlet, an enzymolysis, the first feed inlet and the steam outlet of the enzymolysis device are positioned above the separation baffle and arranged at the top of the shell, the second feed inlet of the enzymolysis device is positioned below the separation baffle, the air inlet of the enzymolysis device is positioned at the bottom of the shell, and the air outlet is communicated with the vacuum pump.
Furthermore, the outer side wall of the filter cartridge is provided with a plurality of shifting plates, and the plate surfaces of the shifting plates are perpendicular to the outer side wall of the filter cartridge.
Furthermore, the length direction of the poking plate is the same as that of the filter cylinder.
Furthermore, the plurality of cutting steel wires are arranged in the through hole in a crossed mode.
Furthermore, the pressure column comprises two layers, the outer layer is a rubber layer, and the inner layer column body is made of stainless steel.
The cod roe essence mask prepared by the invention can adjust the balance of moisture and oil of the skin, and has good moisturizing effect and good water holding effect.
Drawings
FIG. 1 is a diagram of a processing system of the present invention;
FIG. 2 is a schematic structural diagram of an enzymolysis device;
FIG. 3 is a view showing the positional relationship between the crushing cylinder and the perforations;
FIG. 4 is a diagram illustrating the position of the filter cartridge and the filter openings;
FIG. 5 is a view showing the positional relationship between the through-hole and the filter cartridge;
fig. 6 is a diagram showing a positional relationship between the rotating base and the hydraulic cylinder.
Detailed Description
The foregoing and other technical and scientific aspects, features and utilities of the present invention will be apparent from the following detailed description of the embodiments, which is to be read in connection with the accompanying drawings of fig. 1-6. The structural contents mentioned in the following embodiments are all referred to the attached drawings of the specification.
Example 1:
a preparation method of a cod roe essence mask comprises the following steps: (1) cleaning fresh cod roe, adding deionized water and protease, and performing enzymolysis at 30 deg.C for 12 hr to obtain cod roe slurry; (2) carrying out solid-liquid separation on the cod roe slurry, taking the separated liquid, and adding nipagin ester and hyaluronic acid to obtain a mixed solution; (3) introducing gas into the mixed solution, reducing the temperature to 8 ℃ under the pressure of 3MPa, stirring for 2h, filtering the crystallized solid, taking the filtered liquid, heating the liquid to 30 ℃, and sterilizing to obtain the finished product.
The mass-volume ratio of the cod roes, the deionized water, the protease, the nipagin ester and the hyaluronic acid is as follows: 20 g: 30 ml: 1 g: 2 ml. SaidThe gas in the step (3) is N2。
The processing system used in the preparation method of the cod roe essence mask comprises an enzymolysis device 1, wherein a discharge hole 101 of the enzymolysis device is communicated with a feed inlet 201 of a solid-liquid separator, a liquid outlet 202 of the solid-liquid separator is communicated with a feed inlet 301 of a heating tank, a discharge hole 302 of the heating tank is communicated with a feed inlet 401 of a microwave sterilizer, and a discharge hole 402 of the microwave sterilizer is communicated with a bottling system 5.
The enzymolysis device 1 comprises a shell 102, the shell 102 is a sealed cavity, the shell 102 is divided into an upper decomposition cavity 103 and a lower hydration cavity 104 by a baffle 105, the surface of the baffle 105 is parallel to the bottom of the shell 102, a top wall in the shell 102 is provided with a rotating base 106, a hydraulic cylinder 107 is arranged below the rotating base 106, the hydraulic cylinder 107 is connected with a pressure column 108 through a telescopic rod, the baffle 105 is provided with a through hole 109 for the pressure column 108 to pass through, the through hole 109 is connected with a filter cylinder 111 through a bearing 110 in a sliding way, the filter cylinder 111 is sleeved with a crushing cylinder 112, the cylinder diameter of the crushing cylinder 112 is larger than the circular diameter of the pressure column 108, when the pressure column 108 enters the crushing cylinder 112, the outer side wall of the pressure column 108 is mutually attached to the inner side wall of the crushing cylinder 112, the length direction of the pressure column 108 is the same as the length direction of the crushing cylinder 112, and the, the pressure column 108, the filter cylinder 111 and the crushing cylinder 112 are all cylindrical, filter holes 114 are uniformly distributed on the side wall of the filter cylinder 111, filter cloth covers the filter holes 114, through holes 115 are uniformly distributed on the crushing cylinder 112, a plurality of cutting steel wires 116 are arranged on the through holes 115, the diameter of each through hole 115 is smaller than that of a conventional cod roe, the crushing cylinder 112 is connected with the upper opening edge of the filter cylinder 111 through an annular plate 113, the crushing cylinder 112 is fixedly connected with a turntable 117 with the lower opening of the filter cylinder 111, the disc surface of the turntable 117 is vertical to the length direction of the crushing cylinder 112 and the filter cylinder 111, a rotary motor 118 is connected below the turntable 117, the base of the rotary motor 118 is fixed at the bottom of the shell 102, the output end of the rotary motor 118 is connected with the lower surface of the turntable 117, two heaters 119 are arranged above the baffle 105, a refrigerator 120 is, The first feed inlet 122 of enzymolysis device, enzymolysis device second feed inlet 123, enzymolysis device discharge gate 101, enzymolysis device air inlet 124 and enzymolysis device gas outlet 125, this first feed inlet 122 of enzymolysis device and steam outlet are located and separate baffle 105 top and set up in casing 102 top, and enzymolysis device second feed inlet 123 is located and separates baffle 105 below, and enzymolysis device air inlet 124 is located casing 102 bottom, and enzymolysis device gas outlet 125 communicates vacuum pump 126. The outer side wall of the filter cartridge 111 is provided with three shifting plates 127, and the plate surface of the shifting plates 127 is perpendicular to the outer side wall of the filter cartridge 111. The length direction of the dial plate 127 is the same as the length direction of the filter cartridge 111. The two cutter wires 116 are arranged crosswise in the perforation 115. The pressure column 108 comprises two layers, wherein the outer layer is a rubber layer 1081, and the inner layer column 1082 is made of stainless steel.
During processing, the hydraulic cylinder 107 is opened, the telescopic rod of the hydraulic cylinder 107 is extended, the through hole 109 is sealed by the pressure column 108, fresh cod roes are cleaned and enter the decomposition cavity 103 from the first feed port 122 of the enzymolysis device 1, deionized water and protease are added into the first feed port 122 of the enzymolysis device 1, the heater 119 is opened for heating to 30 ℃, after enzymolysis is carried out for 12 hours, the heater 119 is closed, the hydraulic cylinder 107 is adjusted to shrink the hydraulic cylinder 107, the pressure column 108 is pulled out from the through hole 109, the cod roes slurry after enzymolysis enters the crushing cylinder 112, the hydraulic cylinder 107 is adjusted again, the hydraulic cylinder 107 is extended, the cod roes are extruded by the pressure column 108, the cod roes which are subjected to enzymolysis enter the filter cylinder 111 through the perforation 115, the cod roes which are not subjected to enzymolysis enter the filter cylinder 111 after being crushed by the cutting steel wire 116, and are filtered by the filter hole 114 of the filter cylinder 111, obtaining cod roe slurry, introducing the cod roe slurry between the shell 102 and the filter cylinder 111, introducing the nipagin ester and the hyaluronic acid into a second inlet 123 of the enzymolysis device, then opening the refrigerator 120, and introducing the N from an air inlet 124 of the enzymolysis device2Simultaneously, the vacuum pump 126 pumps out gas and pumps the inside to 8MPa, when the temperature is reduced to 8 ℃, part of cod roe slurry is condensed into crystals, the crystals flow out of the discharge port 101 of the enzymolysis device, enter the solid-liquid separator 2 to separate solids, the separated liquid is discharged from the liquid outlet 202 of the solid-liquid separator, and the liquid enters the feed port 301 of the heating tank to be added with the waterHeating to 30 deg.C, discharging a part of gas, sterilizing in microwave sterilizer 4, introducing into bottling system 5, and bottling. Wherein rotating electrical machines 118 can also rotate, drives broken section of thick bamboo 112 and cartridge filter 111 and rotates, dials board 127 and can stirs the liquid between cartridge filter 111 and the casing.
Example 2:
a preparation method of a cod roe essence mask comprises the following steps: (1) cleaning fresh cod roe, adding deionized water and protease, and performing enzymolysis at 32 deg.C for 13 hr to obtain cod roe slurry; (2) carrying out solid-liquid separation on the cod roe slurry, taking the separated liquid, and adding nipagin ester and hyaluronic acid to obtain a mixed solution; (3) introducing gas into the mixed solution, reducing the temperature to 10 ℃ under the pressure of 5MPa, stirring for 2.5h, filtering the crystallized solid, taking the filtered liquid, heating the liquid to 32 ℃, and sterilizing to obtain the finished product.
The mass-volume ratio of the cod roes, the deionized water, the protease, the nipagin ester and the hyaluronic acid is as follows: 30 g: 40 ml: 1.5 g: 3 ml. The gas in the step (3) is N2。
Example 3:
a preparation method of a cod roe essence mask comprises the following steps: (1) cleaning fresh cod roe, adding deionized water and protease, and performing enzymolysis at 35 deg.C for 15 hr to obtain cod roe slurry; (2) carrying out solid-liquid separation on the cod roe slurry, taking the separated liquid, and adding nipagin ester and hyaluronic acid to obtain a mixed solution; (3) introducing gas into the mixed solution, reducing the temperature to 15 ℃ under the pressure of 8MPa, stirring for 3h, filtering the crystallized solid, taking the filtered liquid, heating the liquid to 35 ℃, and sterilizing to obtain the finished product.
The mass-volume ratio of the cod roes, the deionized water, the protease, the nipagin ester and the hyaluronic acid is as follows: 50 g: 50 ml: 2 g: 5 ml. The gas in the step (3) is N2。
Test example 1:
inviting 10 female subjects without allergic conditions, wherein 10 females are 20 years old and have good health conditions, cleaning the face by using facial cleanser, testing the moisture and the oil content of the skin by using a skin moisture tester, uniformly covering the face by using the cod roe essence mask prepared in the embodiment 1, covering the face for 20min, keeping the face in the air for 30min after cleaning, and testing the moisture and the oil content of the skin again, wherein the test results are as follows:
Figure 434155DEST_PATH_IMAGE002
therefore, after the cod roe essence mask prepared by the invention is used, the facial moisture of a user can be effectively improved, the balance of the moisture and the grease of the skin can be adjusted, the balance of the moisture and the grease can be effectively kept, and the skin is moisturized and smooth.

Claims (9)

1. The preparation method of the cod roe essence mask is characterized by comprising the following steps: (1) cleaning fresh cod roe, adding deionized water and protease, and performing enzymolysis at 30-35 deg.C for 12-15 hr to obtain cod roe slurry; (2) carrying out solid-liquid separation on the cod roe slurry, taking the separated liquid, and adding nipagin ester and hyaluronic acid to obtain a mixed solution; (3) introducing gas into the mixed solution, reducing the temperature to 8-15 deg.C under 3-8MPa, stirring for 2-3h, filtering the crystallized solid, collecting the filtered liquid, heating to 30-35 deg.C, and sterilizing to obtain the final product.
2. The preparation method of the cod roe essence mask according to claim 1, wherein the mass-to-volume ratio of the cod roe, the deionized water, the protease, the nipagin ester and the hyaluronic acid is as follows: 20-50 g: 30-50 ml: 1-2 g: 2-5 ml.
3. The method for preparing a cod roe essence mask according to claim 1, wherein the gas in the step (3) is N2。
4. The processing system for the preparation method of the cod roe essence mask, according to claim 1, is characterized by comprising an enzymolysis device, wherein a discharge hole of the enzymolysis device is communicated with a feed hole of a solid-liquid separator, a liquid outlet of the solid-liquid separator is communicated with a feed hole of a heating tank, a discharge hole of the heating tank is communicated with a feed hole of a microwave sterilizer, and a discharge hole of the microwave sterilizer is communicated with a bottling system.
5. The processing system of claim 1, wherein the enzymolysis device comprises a housing, the housing is a sealed cavity, the housing is divided into an upper decomposition chamber and a lower hydration chamber by a baffle, the surface of the baffle is parallel to the bottom surface of the housing, a rotating base is arranged on the top wall in the housing, a hydraulic cylinder is arranged below the rotating base, a telescopic rod of the hydraulic cylinder is connected with a pressure column, the baffle is provided with a through hole for the pressure column to pass through, the through hole is connected with a filter cylinder through a bearing in a sliding manner, the filter cylinder is sleeved with a crushing cylinder, the diameter of the cylinder of the crushing cylinder is larger than the circular diameter of the pressure column, when the pressure column enters the crushing cylinder, the outer side wall of the pressure column is mutually attached to the inner side wall of the crushing cylinder, the length direction of the pressure column is the same as the length direction of the crushing cylinder, the length directions of the filter cylinder and, the filter holes are covered with filter cloth, perforations are uniformly distributed on the crushing cylinder, a plurality of cutting steel wires are arranged on the perforations, the crushing cylinder is connected with the upper opening edge of the filter cylinder through an annular plate, the crushing cylinder and the lower opening of the filter cylinder are fixedly connected with a rotary disc, the disc surface of the rotary disc is vertical to the length direction of the crushing cylinder and the filter cylinder, a rotary motor is connected below the rotary disc, a base of the rotary motor is fixed at the bottom of the shell, the output end of the rotary motor is connected with the lower surface of the rotary disc, a plurality of heaters are arranged above the baffle, a refrigerator is arranged below the baffle, the shell is also provided with an enzymolysis device steam outlet, a first feed inlet of the enzymolysis device, a second feed inlet of the enzymolysis device, an enzymolysis device discharge outlet, an enzymolysis device air inlet and an enzymolysis device air outlet, the first feed, the air inlet of the enzymolysis device is positioned at the bottom of the shell, and the air outlet is communicated with the vacuum pump.
6. The processing system as claimed in claim 1, wherein the outer sidewall of the filter cartridge is provided with a plurality of dial plates, and the plate surfaces of the dial plates are perpendicular to the outer sidewall of the filter cartridge.
7. The tooling system of claim 1 wherein the length of the dial plate is the same as the length of the filter cartridge.
8. A tooling system according to claim 1 wherein said plurality of cutter wires are interleaved within said perforations.
9. The tooling system of claim 1 wherein the pressure column comprises two layers, an outer layer of rubber and an inner layer of cylinder made of stainless steel.
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