CN112144297A - Pure plant blue dyeing ancient vat building formula and method - Google Patents
Pure plant blue dyeing ancient vat building formula and method Download PDFInfo
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- CN112144297A CN112144297A CN202011006976.1A CN202011006976A CN112144297A CN 112144297 A CN112144297 A CN 112144297A CN 202011006976 A CN202011006976 A CN 202011006976A CN 112144297 A CN112144297 A CN 112144297A
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- 238000004043 dyeing Methods 0.000 title claims abstract description 42
- 238000000034 method Methods 0.000 title claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 74
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims abstract description 44
- 239000004744 fabric Substances 0.000 claims abstract description 35
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 claims abstract description 23
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims abstract description 22
- 235000000177 Indigofera tinctoria Nutrition 0.000 claims abstract description 22
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims abstract description 22
- 235000012255 calcium oxide Nutrition 0.000 claims abstract description 22
- 239000000292 calcium oxide Substances 0.000 claims abstract description 22
- 229940097275 indigo Drugs 0.000 claims abstract description 22
- 235000019991 rice wine Nutrition 0.000 claims abstract description 22
- 241000196324 Embryophyta Species 0.000 claims abstract description 20
- 239000012459 cleaning agent Substances 0.000 claims abstract description 18
- 235000009508 confectionery Nutrition 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 235000014101 wine Nutrition 0.000 claims abstract description 12
- 239000000975 dye Substances 0.000 claims description 93
- 238000003756 stirring Methods 0.000 claims description 63
- 238000002156 mixing Methods 0.000 claims description 23
- 238000004140 cleaning Methods 0.000 claims description 16
- 238000002791 soaking Methods 0.000 claims description 15
- 238000005406 washing Methods 0.000 claims description 15
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 229940034610 toothpaste Drugs 0.000 claims description 10
- 239000000606 toothpaste Substances 0.000 claims description 10
- 239000002699 waste material Substances 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 239000000919 ceramic Substances 0.000 claims description 5
- 235000013339 cereals Nutrition 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 5
- 238000000576 coating method Methods 0.000 claims description 5
- 239000003599 detergent Substances 0.000 claims description 5
- 239000006260 foam Substances 0.000 claims description 5
- 239000001046 green dye Substances 0.000 claims description 5
- 230000001590 oxidative effect Effects 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 5
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 5
- 235000021419 vinegar Nutrition 0.000 claims description 5
- 239000000052 vinegar Substances 0.000 claims description 5
- 239000002351 wastewater Substances 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 2
- 230000008569 process Effects 0.000 abstract description 8
- 239000012535 impurity Substances 0.000 abstract description 6
- 239000000463 material Substances 0.000 abstract description 6
- QQILFGKZUJYXGS-UHFFFAOYSA-N Indigo dye Chemical compound C1=CC=C2C(=O)C(C3=C(C4=CC=CC=C4N3)O)=NC2=C1 QQILFGKZUJYXGS-UHFFFAOYSA-N 0.000 abstract description 5
- 230000009286 beneficial effect Effects 0.000 abstract description 5
- 230000002829 reductive effect Effects 0.000 abstract description 5
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 239000003086 colorant Substances 0.000 abstract description 2
- 239000004474 valine Substances 0.000 description 8
- KZSNJWFQEVHDMF-BYPYZUCNSA-N L-valine Chemical compound CC(C)[C@H](N)C(O)=O KZSNJWFQEVHDMF-BYPYZUCNSA-N 0.000 description 7
- KZSNJWFQEVHDMF-UHFFFAOYSA-N Valine Natural products CC(C)C(N)C(O)=O KZSNJWFQEVHDMF-UHFFFAOYSA-N 0.000 description 7
- 230000009471 action Effects 0.000 description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- 241000191398 Kalanchoe blossfeldiana Species 0.000 description 1
- 241000205407 Polygonum Species 0.000 description 1
- 244000152045 Themeda triandra Species 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000012173 estrus Effects 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- COHYTHOBJLSHDF-BUHFOSPRSA-N indigo dye Chemical compound N\1C2=CC=CC=C2C(=O)C/1=C1/C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-BUHFOSPRSA-N 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/22—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using vat dyestuffs including indigo
- D06P1/228—Indigo
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention discloses an ancient vat building formula of pure plant blue dyeing and a method thereof, wherein the formula comprises the following steps: the indigo naturalis, quicklime, high-alcohol wine, rice wine, candy, maltose, hot water and cool boiled water, wherein the raw materials comprise the following components in parts by weight: 9.9 to 10.1 portions of indigo, 1.9 to 2.1 portions of quicklime, 1.9 to 2.1 portions of high-alcohol, 3.9 to 4.1 portions of rice wine, 5.9 to 6.1 portions of sweets, 0.9 to 1.1 portions of maltose, 9.9 to 10.1 portions of hot water and 64.9 to 65.1 portions of cool boiled water, the invention has the advantages that the materials needed in the process of building the cylinder are easy to find, the material searching time is shortened, the cylinder building cost is reduced, meanwhile, the efficiency of building the vat is improved, the time for building the vat is greatly shortened, the method is beneficial to environmental protection, meanwhile, the method for building the vat is not influenced by the temperature and the humidity of the environment, the dye is stable, and the dye vat is cleaned by using a cleaning agent before the dye vat is built, which is beneficial to removing the residual impurities on the inner wall of the dye vat, thereby avoiding the color difference between the colors of the dye caused by the residual impurities in the dye vat and improving the quality of the dyed cloth.
Description
Technical Field
The invention relates to the technical field of blue dyeing, in particular to an ancient vat building formula and method for pure plant blue dyeing.
Background
Blue dyeing is an ancient process, and has a history of more than 3000 years till now, and the traditional blue dyeing techniques in China mainly comprise four-valine (wax valine, twisting valine, clip valine and gray valine), wherein the wax valine (wax dyeing), twisting valine (tie dyeing), clip dyeing and gray valine (blue printed cloth). The traditional Chinese plant blue dyeing comprises the following main raw materials: the stem leaves of the kalanchoe and the indigo polygonum blue are soaked and added with lime to be fermented into the indigo, the indigo belongs to a reductive dye, the indigo mud is prepared from the picked bluegrass, and then the indigo mud is reduced into the indigo dye solution through fermentation, so that the process is very complicated and fussy.
Disclosure of Invention
The invention aims to provide an ancient vat building formula for pure plant blue dyeing and a method thereof, so as to solve the problems in the background technology.
In order to solve the technical problems, the invention provides the following technical scheme: an ancient vat building formula adopting pure plant blue dyeing comprises the following components: the indigo naturalis, quicklime, high-alcohol wine, rice wine, candy, maltose, hot water and cool boiled water, wherein the raw materials comprise the following components in parts by weight: 9.9-10.1 parts of indigo, 1.9-2.1 parts of quicklime, 1.9-2.1 parts of high-alcohol, 3.9-4.1 parts of rice wine, 5.9-6.1 parts of sweets, 0.9-1.1 parts of maltose, 9.9-10.1 parts of hot water and 64.9-65.1 parts of cool boiled water.
An ancient vat building method of pure plant blue dyeing comprises the following steps of firstly, selecting raw materials; step two, cleaning a dye vat; step three, mixing the raw materials; step four, selecting and soaking; step five, stirring and blending; step six, mixing and stirring; step seven, stirring and standing; step eight, trial dyeing and standing;
in the first step, 9.9-10.1 parts of indigo, 1.9-2.1 parts of quicklime, 1.9-2.1 parts of strong liquor, 3.9-4.1 parts of rice wine, 5.9-6.1 parts of sweets, 0.9-1.1 parts of maltose, 9.9-10.1 parts of hot water and 64.9-65.1 parts of cool boiled water are respectively selected according to the weight parts of the components;
pouring a proper amount of cleaning agent into the dye vat, pouring proper amount of water into the dye vat, then placing waste cloth into the dye vat, then cleaning the inner surface of the dye vat by using the waste cloth, pouring out waste water after the cleaning is finished, then washing the dye vat once by using clear water, then uniformly coating toothpaste on the inner surface of the dye vat, standing for 5-10min, then washing for 2-3 times by using the clear water to ensure that no toothpaste residue is left on the inner surface of the dye vat, and then draining, wherein the ratio of the cleaning agent to the water is 2: 1;
in the third step, a part of the cool boiled water in the first step is selected and poured into a dye vat after draining treatment, and then indigo is poured into the dye vat and uniformly stirred for 10min, wherein the stirring speed is 100-;
in the fourth step, the rest of cold boiled water is selected and poured into a container, and then the quick lime selected in the first step is poured into the container for soaking;
in the fifth step, the estrus sugar and the maltose selected in the third step are placed in a container in the third step to be stirred and blended to obtain a mixture;
wherein in the sixth step, the mixture obtained in the fourth step is put into a dye vat together with the high-alcohol wine and the rice wine selected in the first step and uniformly stirred, the stirring time is 3-5min, and the stirring speed is 150-;
in the seventh step, after stirring, pouring the hot boiled water selected in the first step into a dye vat for uniform stirring, wherein the stirring time is 10min, the stirring speed is 300-;
in the eighth step, after standing is completed, fermenting the solution in the dye vat into dark green dye liquor, enabling 8-15cm of bluish-purple bright foam to float on the surface, then carrying out trial dyeing and soaking for 3min by using a test cloth strip, enabling the cloth strip to be yellow-green at the moment of taking out the cloth strip, slowly oxidizing the dye liquor on the cloth strip into blue by contacting with air, namely successfully reducing, then standing, and carrying out dyeing treatment in the next day.
According to the technical scheme, the alcohol content of the high-alcohol-content grain liquor is 55-60 degrees.
According to the technical scheme, the temperature of the hot water is 95-100 ℃.
According to the technical scheme, in the second step, the cleaning agent is formed by mixing 20-22 parts by weight of edible vinegar, 0.5-0.6 part by weight of washing powder, 0.5-0.6 part by weight of liquid detergent and 1-2 parts by weight of baking soda
According to the technical scheme, in the second step, the dye vat is a ceramic dye vat.
According to the technical scheme, in the fifth step, the stirring time is 8-10min, and the stirring speed is 200-250 r/min.
Compared with the prior art, the invention has the following beneficial effects: according to the method, materials required in the process of building the vat are easy to find, the material searching time is shortened, the cost of building the vat is reduced, the vat building efficiency is improved, the vat building time is greatly shortened, the method is beneficial to environmental protection, the method for building the vat is not influenced by the temperature and the humidity of the environment, the dye is stable, the cleaning agent is used for cleaning the vat before the vat is built, the impurities remained on the inner wall of the vat are removed, the color difference among the colors of the dye caused by the impurities remained in the vat is avoided, and the quality of the dyed cloth is improved.
Drawings
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention. In the drawings:
FIG. 1 is a flow chart of the method of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1, the present invention provides a technical solution:
example 1:
an ancient vat building formula adopting pure plant blue dyeing comprises the following components: the indigo naturalis, quicklime, high-alcohol wine, rice wine, candy, maltose, hot water and cool boiled water, wherein the raw materials comprise the following components in parts by weight: 9.9 to 10.1 portions of indigo, 1.9 to 2.1 portions of quicklime, 1.9 to 2.1 portions of high-alcohol, 3.9 to 4.1 portions of rice wine, 5.9 to 6.1 portions of sweets, 0.9 to 1.1 portions of maltose, 9.9 to 10.1 portions of hot water and 64.9 to 65.1 portions of cool boiled water, wherein the alcohol content of the high-alcohol is 55 to 60 degrees of grain liquor, and the temperature of the hot water is 95 to 100 ℃.
An ancient vat building method of pure plant blue dyeing comprises the following steps of firstly, selecting raw materials; step two, cleaning a dye vat; step three, mixing the raw materials; step four, selecting and soaking; step five, stirring and blending; step six, mixing and stirring; step seven, stirring and standing; step eight, trial dyeing and standing;
in the first step, 9.9 parts of indigo, 1.9 parts of quicklime, 1.9 parts of high-alcohol, 3.9 parts of rice wine, 5.9 parts of candy, 0.9 part of maltose, 9.9 parts of hot water and 64.9 parts of cool boiled water are respectively selected according to the weight parts of the components;
pouring a proper amount of cleaning agent into a dye vat, pouring proper water into the dye vat, placing waste cloth into the dye vat, cleaning the inner surface of the dye vat by using the waste cloth, pouring waste water after cleaning, washing the dye vat once by using clear water, uniformly coating toothpaste on the inner surface of the dye vat, standing for 5-10min, washing for 2-3 times by using the clear water to ensure that no toothpaste residue exists on the inner surface of the dye vat, draining, wherein the ratio of the cleaning agent to the water is 2: 1, the cleaning agent is formed by mixing 20 parts by weight of edible vinegar, 0.5 part by weight of washing powder, 0.5 part by weight of detergent and 1 part by weight of baking soda, and the dye vat is a ceramic dye vat;
in the third step, a part of the cool boiled water in the first step is selected and poured into a dye vat after draining treatment, and then indigo is poured into the dye vat and uniformly stirred for 10min, wherein the stirring speed is 100-;
in the fourth step, the rest of cold boiled water is selected and poured into a container, and then the quick lime selected in the first step is poured into the container for soaking;
in the fifth step, the candy and the maltose selected in the first step are placed in a container in the third step for stirring and blending to obtain a mixture, wherein the stirring time is 8-10min, and the stirring speed is 200-250 r/min;
wherein in the sixth step, the mixture obtained in the fourth step is put into a dye vat together with the high-alcohol wine and the rice wine selected in the first step and uniformly stirred, the stirring time is 3-5min, and the stirring speed is 150-;
in the seventh step, after stirring, pouring the hot boiled water selected in the first step into a dye vat for uniform stirring, wherein the stirring time is 10min, the stirring speed is 300-;
in the eighth step, after standing is completed, fermenting the solution in the dye vat into dark green dye liquor, enabling 8-15cm of bluish-purple bright foam to float on the surface, then carrying out trial dyeing and soaking for 3min by using a test cloth strip, enabling the cloth strip to be yellow-green at the moment of taking out the cloth strip, slowly oxidizing the dye liquor on the cloth strip into blue by contacting with air, namely successfully reducing, then standing, and carrying out dyeing treatment in the next day.
Example 2:
an ancient vat building formula adopting pure plant blue dyeing comprises the following components: the indigo naturalis, quicklime, high-alcohol wine, rice wine, candy, maltose, hot water and cool boiled water, wherein the raw materials comprise the following components in parts by weight: 9.9 to 10.1 portions of indigo, 1.9 to 2.1 portions of quicklime, 1.9 to 2.1 portions of high-alcohol, 3.9 to 4.1 portions of rice wine, 5.9 to 6.1 portions of sweets, 0.9 to 1.1 portions of maltose, 9.9 to 10.1 portions of hot water and 64.9 to 65.1 portions of cool boiled water, wherein the alcohol content of the high-alcohol is 55 to 60 degrees of grain liquor, and the temperature of the hot water is 95 to 100 ℃.
An ancient vat building method of pure plant blue dyeing comprises the following steps of firstly, selecting raw materials; step two, cleaning a dye vat; step three, mixing the raw materials; step four, selecting and soaking; step five, stirring and blending; step six, mixing and stirring; step seven, stirring and standing; step eight, trial dyeing and standing;
in the first step, 10.1 parts of indigo, 2.1 parts of quicklime, 2.1 parts of high-alcohol, 4.1 parts of rice wine, 6.1 parts of lovose, 1.1 parts of maltose, 10.1 parts of hot water and 65.1 parts of cool boiled water are respectively selected according to the weight parts of the components;
pouring a proper amount of cleaning agent into a dye vat, pouring proper water into the dye vat, placing waste cloth into the dye vat, cleaning the inner surface of the dye vat by using the waste cloth, pouring waste water after cleaning, washing the dye vat once by using clear water, uniformly coating toothpaste on the inner surface of the dye vat, standing for 5-10min, washing for 2-3 times by using the clear water to ensure that no toothpaste residue exists on the inner surface of the dye vat, draining, wherein the ratio of the cleaning agent to the water is 2: 1, the cleaning agent is formed by mixing 22 parts by weight of edible vinegar, 0.6 part by weight of washing powder, 0.6 part by weight of detergent and 2 parts by weight of baking soda, and the dye vat is a ceramic dye vat;
in the third step, a part of the cool boiled water in the first step is selected and poured into a dye vat after draining treatment, and then indigo is poured into the dye vat and uniformly stirred for 10min, wherein the stirring speed is 100-;
in the fourth step, the rest of cold boiled water is selected and poured into a container, and then the quick lime selected in the first step is poured into the container for soaking;
in the fifth step, the candy and the maltose selected in the first step are placed in a container in the third step for stirring and blending to obtain a mixture, wherein the stirring time is 8-10min, and the stirring speed is 200-250 r/min;
wherein in the sixth step, the mixture obtained in the fourth step is put into a dye vat together with the high-alcohol wine and the rice wine selected in the first step and uniformly stirred, the stirring time is 3-5min, and the stirring speed is 150-;
in the seventh step, after stirring, pouring the hot boiled water selected in the first step into a dye vat for uniform stirring, wherein the stirring time is 10min, the stirring speed is 300-;
in the eighth step, after standing is completed, fermenting the solution in the dye vat into dark green dye liquor, enabling 8-15cm of bluish-purple bright foam to float on the surface, then carrying out trial dyeing and soaking for 3min by using a test cloth strip, enabling the cloth strip to be yellow-green at the moment of taking out the cloth strip, slowly oxidizing the dye liquor on the cloth strip into blue by contacting with air, namely successfully reducing, then standing, and carrying out dyeing treatment in the next day.
Example 3:
an ancient vat building formula adopting pure plant blue dyeing comprises the following components: the indigo naturalis, quicklime, high-alcohol wine, rice wine, candy, maltose, hot water and cool boiled water, wherein the raw materials comprise the following components in parts by weight: 9.9 to 10.1 portions of indigo, 1.9 to 2.1 portions of quicklime, 1.9 to 2.1 portions of high-alcohol, 3.9 to 4.1 portions of rice wine, 5.9 to 6.1 portions of sweets, 0.9 to 1.1 portions of maltose, 9.9 to 10.1 portions of hot water and 64.9 to 65.1 portions of cool boiled water, wherein the alcohol content of the high-alcohol is 55 to 60 degrees of grain liquor, and the temperature of the hot water is 95 to 100 ℃.
An ancient vat building method of pure plant blue dyeing comprises the following steps of firstly, selecting raw materials; step two, cleaning a dye vat; step three, mixing the raw materials; step four, selecting and soaking; step five, stirring and blending; step six, mixing and stirring; step seven, stirring and standing; step eight, trial dyeing and standing;
in the first step, 10 parts of indigo, 2 parts of quicklime, 2 parts of high-alcohol wine, 4 parts of rice wine, 6 parts of loving sugar, 1 part of maltose, 1 part of hot water and 65 parts of cold boiled water are respectively selected according to the weight parts of the components;
pouring a proper amount of cleaning agent into a dye vat, pouring proper water into the dye vat, placing waste cloth into the dye vat, cleaning the inner surface of the dye vat by using the waste cloth, pouring waste water after cleaning, washing the dye vat once by using clear water, uniformly coating toothpaste on the inner surface of the dye vat, standing for 5-10min, washing for 2-3 times by using the clear water to ensure that no toothpaste residue exists on the inner surface of the dye vat, draining, wherein the ratio of the cleaning agent to the water is 2: 1, the cleaning agent is formed by mixing 21 parts by weight of edible vinegar, 0.5 part by weight of washing powder, 0.6 part by weight of detergent and 1 part by weight of baking soda, and the dye vat is a ceramic dye vat;
in the third step, a part of the cool boiled water in the first step is selected and poured into a dye vat after draining treatment, and then indigo is poured into the dye vat and uniformly stirred for 10min, wherein the stirring speed is 100-;
in the fourth step, the rest of cold boiled water is selected and poured into a container, and then the quick lime selected in the first step is poured into the container for soaking;
in the fifth step, the candy and the maltose selected in the first step are placed in a container in the third step for stirring and blending to obtain a mixture, wherein the stirring time is 8-10min, and the stirring speed is 200-250 r/min;
wherein in the sixth step, the mixture obtained in the fourth step is put into a dye vat together with the high-alcohol wine and the rice wine selected in the first step and uniformly stirred, the stirring time is 3-5min, and the stirring speed is 150-;
in the seventh step, after stirring, pouring the hot boiled water selected in the first step into a dye vat for uniform stirring, wherein the stirring time is 10min, the stirring speed is 300-;
in the eighth step, after standing is completed, fermenting the solution in the dye vat into dark green dye liquor, enabling 8-15cm of bluish-purple bright foam to float on the surface, then carrying out trial dyeing and soaking for 3min by using a test cloth strip, enabling the cloth strip to be yellow-green at the moment of taking out the cloth strip, slowly oxidizing the dye liquor on the cloth strip into blue by contacting with air, namely successfully reducing, then standing, and carrying out dyeing treatment in the next day.
The cylinder building time of the above embodiment is compared with the cylinder building time of the conventional method, and the obtained data are as follows:
| example 1 | Example 2 | Example 3 | Comparative example | |
| Time for building cylinder | 1 day | 1 day | 1 day | 10 days |
Based on the above, the method has the advantages that the dye vat is cleaned by using the cleaning agent in the process of building the dye vat, so that the impurities remained in the dye vat can be cleaned, the color difference of the dyed cloth caused by the impurities remained in the dye vat is avoided, the quality of the dyed cloth is improved, meanwhile, the materials required in the process of building the dye vat are easy to find, the material searching time is shortened, the cost for building the dye vat is reduced, the efficiency for building the dye vat is improved, the time for building the dye vat is greatly shortened, the method is beneficial to environmental protection, the method for building the dye vat is not influenced by the temperature and the humidity of the environment, and the dye is stable.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (7)
1. An ancient vat building formula adopting pure plant blue dyeing comprises the following components: indigo, quick lime, high-alcohol wine, rice wine, loving sugar, maltose, hot water and cool boiled water, its characterized in that: the weight parts of the components are respectively as follows: 9.9-10.1 parts of indigo, 1.9-2.1 parts of quicklime, 1.9-2.1 parts of high-alcohol, 3.9-4.1 parts of rice wine, 5.9-6.1 parts of sweets, 0.9-1.1 parts of maltose, 9.9-10.1 parts of hot water and 64.9-65.1 parts of cool boiled water.
2. An ancient vat building method of pure plant blue dyeing comprises the following steps of firstly, selecting raw materials; step two, cleaning a dye vat; step three, mixing the raw materials; step four, selecting and soaking; step five, stirring and blending; step six, mixing and stirring; step seven, stirring and standing; step eight, trial dyeing and standing; the method is characterized in that:
in the first step, 9.9-10.1 parts of indigo, 1.9-2.1 parts of quicklime, 1.9-2.1 parts of strong liquor, 3.9-4.1 parts of rice wine, 5.9-6.1 parts of sweets, 0.9-1.1 parts of maltose, 9.9-10.1 parts of hot water and 64.9-65.1 parts of cool boiled water are respectively selected according to the weight parts of the components;
pouring a proper amount of cleaning agent into the dye vat, pouring proper amount of water into the dye vat, then placing waste cloth into the dye vat, then cleaning the inner surface of the dye vat by using the waste cloth, pouring out waste water after the cleaning is finished, then washing the dye vat once by using clear water, then uniformly coating toothpaste on the inner surface of the dye vat, standing for 5-10min, then washing for 2-3 times by using the clear water to ensure that no toothpaste residue is left on the inner surface of the dye vat, and then draining, wherein the ratio of the cleaning agent to the water is 2: 1;
in the third step, a part of the cool boiled water in the first step is selected and poured into a dye vat after draining treatment, and then indigo is poured into the dye vat and uniformly stirred for 10min, wherein the stirring speed is 100-;
in the fourth step, the rest of cold boiled water is selected and poured into a container, and then the quick lime selected in the first step is poured into the container for soaking;
in the fifth step, the candy and the maltose selected in the first step are placed in a container in the third step to be stirred and blended to obtain a mixture;
wherein in the sixth step, the mixture obtained in the fourth step is put into a dye vat together with the high-alcohol wine and the rice wine selected in the first step and uniformly stirred, the stirring time is 3-5min, and the stirring speed is 150-;
in the seventh step, after stirring, pouring the hot boiled water selected in the first step into a dye vat for uniform stirring, wherein the stirring time is 10min, the stirring speed is 300-;
in the eighth step, after standing is completed, fermenting the solution in the dye vat into dark green dye liquor, enabling 8-15cm of bluish-purple bright foam to float on the surface, then carrying out trial dyeing and soaking for 3min by using a test cloth strip, enabling the cloth strip to be yellow-green at the moment of taking out the cloth strip, slowly oxidizing the dye liquor on the cloth strip into blue by contacting with air, namely successfully reducing, then standing, and carrying out dyeing treatment in the next day.
3. The ancient vat building formula for pure plant blue dyeing according to claim 1, which is characterized in that: the alcohol content of the high-alcohol-content liquor is 55-60 degrees of grain liquor.
4. The ancient vat building formula for pure plant blue dyeing according to claim 1, which is characterized in that: the temperature of the hot water is 95-100 ℃.
5. The ancient vat building method by pure plant blue dyeing according to claim 2, which is characterized in that: in the second step, the cleaning agent is prepared by mixing 20-22 parts by weight of edible vinegar, 0.5-0.6 part by weight of washing powder, 0.5-0.6 part by weight of liquid detergent and 1-2 parts by weight of baking soda.
6. The ancient vat building method by pure plant blue dyeing according to claim 2, which is characterized in that: in the second step, the dye vat is a ceramic dye vat.
7. The ancient vat building method by pure plant blue dyeing according to claim 2, which is characterized in that: in the fifth step, the stirring time is 8-10min, and the stirring speed is 200-250 r/min.
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