CN112137902B - Moisturizing, concealer and anti-wrinkle composition and preparation method thereof - Google Patents
Moisturizing, concealer and anti-wrinkle composition and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention relates to a moisturizing, concealer and anti-wrinkle composition, which comprises, by weight, 26.3% -35.8% of a polyol humectant, 6.6% -9.2% of porous titanium dioxide modified nano pearl powder particles, 25.3% -36.2% of a silicone oil-based oil aqueous phase, 0.1% -0.5% of a nonionic surfactant, 0.1% -0.5% of a thickening agent, 0.2% -0.3% of a pH regulator triethanolamine, and the balance of distilled water; the polyhydric alcohol humectant consists of the following substances in parts by weight: 20-60 parts of sodium hyaluronate, 100 parts of propylene glycol, 400 parts of glycerol and 10-50 parts of ascorbyl glucoside. The titanium glycol salt is irradiated on the porous titanium dioxide modified nano pearl powder particles through ultraviolet light, a nano-scale porous titanium dioxide structure is formed on the surface of the nano pearl powder, and a structure that the nano pearl powder is partially coated by the porous titanium dioxide structure is obtained.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a moisturizing, concealer and anti-wrinkle composition and a preparation method thereof.
Background
With age, the skin undergoes a gradual aging after a prolonged period of time, and a dry cortex, wrinkles, spots, etc. appear on the skin surface. Beauty-conscious encourages people to always present their best aspect to the public, and thus there is a need to mask these skin surface imperfections.
The intrinsic causes of skin aging are mainly weakening of differentiation ability of epidermal cells and reduction of sebum secretion of epidermis, reduction of collagen substance in dermis, reduction of water retention ability, reduction of skin elasticity, relaxation, dryness, and further appearance of cortex and wrinkles. In addition, under the irradiation of external ultraviolet rays, oxygen radicals and lipid peroxides are formed in the skin, and combined with dopaquinone produced by tyrosinase in the skin, brown pigment spots are easily formed in the skin, so that the differentiation capability and the sebum secretion capability of skin cells are affected, and spots and wrinkles appear.
Therefore, in order to cover various defects on the skin surface, the moisture retention, the concealer, the wrinkle resistance and the like are mainly considered. At present, various products such as foundation, moisturizing lotion, whitening cream, freckle removing cream and the like are on the market. Some of the products have the defects of unobvious moisturizing effect and non-persistence; some defects of excessive whitening effect and unnatural appearance exist; some defects have insufficient spot-shading effect; the defects of heavy concealer trace and poor softness exist.
The most ideal cosmetic should have good and lasting effect, while concealer, whiten naturally, soft-burnt effects excellent, have no obvious covering trace, look natural from all angles. In terms of optical or visual effects, in order to obtain a more natural concealing effect, i.e. a high soft focus index, cosmetics applied to the surface of human skin need to exhibit: high and uniform transmittance, extremely low absorption of visible light, and uniform light reflected by the skin after transmission; low or very low reflectivity, especially specular reflectivity; extremely high scattering power and uniform reflection effect caused by scattering.
In order to obtain a desired soft-focus effect, inorganic powders having a high refractive index, such as titanium dioxide, zinc oxide, silica, etc., are generally used in conventional cosmetics, however, the actual soft-focus effect is not desired due to insufficient transparency and poor scattering properties of these materials. Meanwhile, the combination effect of these materials with a moisturizing agent is poor, so that the moisturizing effect of the cosmetic composition is not ideal.
Therefore, a cosmetic composition having excellent soft-focus effect, natural concealer effect and good moisture retention is desired.
Disclosure of Invention
In order to solve the problems of unnatural concealing and anti-wrinkle effects and insufficient moisture retention in the existing products, the invention provides a moisturizing and concealing anti-wrinkle composition containing porous titanium dioxide modified nano pearl powder particles, which takes sodium hyaluronate, propylene glycol, glycerol and ascorbyl glucoside as humectants, and is added with the porous titanium dioxide modified nano pearl powder particles, so that the concealing and anti-wrinkle effects of the composition are improved, the soft-focus effect of the composition is enhanced, and the natural concealing and anti-wrinkle effects are presented.
The invention is realized by the following technical scheme:
a moisturizing, concealer and anti-wrinkle composition comprises, by weight, 26.3% -35.8% of a polyol humectant, 6.6% -9.2% of porous titanium dioxide modified nano pearl powder particles, 25.3% -36.2% of a silicone oil-based aqueous phase, 0.1% -0.5% of a nonionic surfactant, 0.1% -0.5% of a thickener, 0.2% -0.3% of a pH regulator triethanolamine, and the balance of distilled water; the polyhydric alcohol humectant consists of the following substances in parts by weight: 20-60 parts of sodium hyaluronate, 100 parts of propylene glycol, 400 parts of glycerol and 10-50 parts of ascorbyl glucoside.
The porous titanium dioxide modified nano pearl powder particles are prepared by the following preparation method:
(1) pre-crushing pearl raw materials: pre-pulverizing high-quality fresh water pearl into pearl powder with particle size less than 50 um;
(2) nano-crushing: dispersing the pearl powder with the granularity of less than 50um obtained in the step (1) in deionized water, adding a proper amount of dispersant to obtain micron pearl powder dispersion liquid,
in the dispersion liquid, the concentration of the dispersant is 10-20g/L, the concentration of the pearl powder is 100-200g/L,
pulverizing the micrometer Margarita powder dispersion with nanometer pulverizer for 1-2 hr to obtain nanometer Margarita powder dispersion with particle size of 20-100 nm;
(3) preparing a mixed dispersion liquid: taking 100ml of the nano pearl powder dispersion liquid obtained in the step (2), adding 5-8g of titanium glycol salt, and then shearing at high speed in a high-speed shearing machine to obtain uniform titanium glycol salt and nano pearl powder dispersion liquid;
(4) ultraviolet light irradiation: and (4) carrying out ultraviolet irradiation on the titanium glycol salt and the nano pearl powder dispersion liquid obtained in the step (3) for 2-4h to form porous titanium dioxide nano particles on the surface of the nano pearl powder, and standing, centrifugally separating and washing with deionized water to obtain the porous titanium dioxide modified nano pearl powder particles.
Wherein the porous titanium dioxide nanoparticles have a pore size of about 1 to 5 nm.
The dispersing agent is a non-release dispersing agent and is selected from one or more of sorbitan monooleate, polyoxyethylene lauryl ether, polyoxyethylene monopalmitate, polyoxyethylene monolaurate, polyoxyethylene fatty alcohol, polyethylene glycol monopalmitate, polyoxyethylene cetyl alcohol, polyoxyethylene sorbitan monopalmitate, polyoxyethylene sorbitan monolaurate, polyoxyethylene alkyl aryl ether and polyoxyethylene vegetable oil.
For the moisturizing concealer anti-wrinkle composition of the present invention, further, the silicone based oily phase is selected from one or more of polydimethylsiloxane, phenyltrimethicone, phenyltrimethylsiloxydiphenylsiloxane, diphenyldimethylsiloxane, (2-phenylethyl) trimethylsiloxysilicate.
Further, the nonionic surfactant is selected from one or more of glycerol laurate, glycerol ricinoleate, soybean lecithin, fatty alcohol-polyoxyethylene ether, sucrose cocoate and sorbitan stearate.
Further, the thickening agent is selected from one or more of carbomer, polyacrylamide, ammonium polyacryloyldimethyl taurate, xanthan gum and acrylic polysiloxane.
Further, the moisturizing concealer and anti-wrinkle composition can also contain various additives such as an anti-wrinkle agent, an anti-aging agent, an antibacterial agent, a delustering agent, an antioxidant and the like.
The invention also relates to a preparation method of the cosmetic composition consisting of the moisturizing concealer and wrinkle-resistant composition, which comprises the following steps of (1) mixing all components in the polyalcohol moisturizing agent according to a ratio in advance to prepare the polyalcohol moisturizing agent; (2) stirring and mixing the polyalcohol humectant, the silicone oil-based oil phase, the defoaming agent and water uniformly; (3) sequentially adding nonionic surfactant, porous titanium dioxide modified nanometer pearl powder particles, thickener and triethanolamine, and stirring at 60 deg.C and 3000 rpm.
Detailed Description
The present invention will be described below with reference to specific examples, but these are not intended to be all the invention.
Example 1
Preparing porous titanium dioxide modified nano pearl powder particles:
(1) pre-crushing pearl raw materials: pre-pulverizing high-quality fresh water pearl into pearl powder with particle size less than 50 um;
(2) nano-crushing: dispersing the pearl powder with the granularity of less than 50um obtained in the step (1) in deionized water, adding a proper amount of sorbitan monooleate to obtain micron pearl powder dispersion liquid,
in the dispersion, the concentration of sorbitan monooleate is 18g/L, the concentration of pearl powder is 160g/L,
pulverizing the micrometer Margarita powder dispersion with nanometer pulverizer for 2 hr to obtain nanometer Margarita powder dispersion with particle size of 20-100 nm;
(3) preparing a mixed dispersion liquid: taking 100ml of the nano pearl powder dispersion liquid obtained in the step (2), adding 8g of titanium glycol salt, and then shearing at high speed in a high-speed shearing machine to obtain uniform titanium glycol salt and nano pearl powder dispersion liquid;
(4) ultraviolet light irradiation: and (4) carrying out ultraviolet irradiation on the titanium glycol salt and the nano pearl powder dispersion liquid obtained in the step (3) for 4 hours to form porous titanium dioxide nano particles on the surface of the nano pearl powder, and standing, centrifugally separating and washing with deionized water to obtain the porous titanium dioxide modified nano pearl powder particles.
The porous titanium dioxide nanoparticles were determined to have a pore size of about 1-5 nm.
Example 2
Based on the defined weight percentages and weight part ranges:
26.3 to 35.8 percent of polyalcohol humectant,
6.6 to 9.2 percent of porous titanium dioxide modified nano pearl powder particles,
25.3 to 36.2 percent of silicone oil-based oily phase,
0.1 to 0.5 percent of nonionic surfactant,
0.1 to 0.5 percent of thickening agent,
0.2 to 0.3 percent of pH regulator triethanolamine,
The balance of distilled water;
20-60 parts of sodium hyaluronate,
100 portions of propylene glycol and 300 portions of,
100 portions of glycerin,
10-50 parts of ascorbic acid glucoside. Selecting a certain amount of each component, and preparing a corresponding cosmetic composition according to the following steps: (1) mixing all components in the polyalcohol humectant according to a ratio to prepare the polyalcohol humectant; (2) stirring and mixing the polyalcohol humectant, the silicone oil-based oil phase, the defoaming agent and water uniformly; (3) sequentially adding nonionic surfactant, porous titanium dioxide modified nanometer pearl powder particles, thickener and triethanolamine, and stirring at 60 deg.C and 3000 rpm. See table 1 for the specific compositions of the examples.
Meanwhile, in order to better embody the effects of the present invention, corresponding comparative examples are provided, and see table 1 specifically. In a comparative example 1, titanium glycol salt is irradiated by ultraviolet light in the embodiment 1 in a manner that tetrabutyl titanate is hydrolyzed at 60 ℃, so that the structure of micron-sized titanium dioxide densely-coated nano pearl powder is obtained, the soft-focus effect of the nano pearl powder is relatively weak, and meanwhile, the micron-sized titanium dioxide densely-coats the inside nano pearl powder, so that the anti-wrinkle and whitening effects of the pearl powder cannot be embodied. In comparative example 2, the mixture of titanium dioxide powder and pearl powder was directly substituted for the porous titanium dioxide modified nano pearl powder particles prepared in example 1, and the soft focus effect was poor and the concealing effect was unnatural.
The composition of each example was coated on the surface of a transparent polyester film to a thickness of about 50um, and after drying at room temperature, the transparency, haze and whitening effect of the surface were visually observed, and the detailed results are shown in table 1.
TABLE 1
| Components | Example 1 | Example 2 | Example 3 | Comparative example 1 | Comparative example 2 |
| Propylene glycol | 12% | 10% | 12% | 12% | 12% |
| Glycerol | 13.2% | 18% | 12% | 13.2% | 13.2% |
| Hyaluronic acid sodium salt | 3% | 2.5% | 3% | 3% | 3% |
| Ascorbic acid glucoside | 1.8% | 1.5% | 3% | 1.8% | 1.8% |
| Example 1 porous titanium dioxide modified Nano Pearl powder particles | 8% | 8% | 8% | 0 | 0 |
| Hydrolyzing tetrabutyl titanate on the surface of the nano pearl powder to form titanium dioxide | 0 | 0 | 0 | 8% | 0 |
| Pearl powder and titanium dioxide nanopowder | 0 | 0 | 0 | 0 | 3% of titanium dioxide and 5% of pearl powder |
| Polydimethylsiloxane | 18% | 12% | 15% | 18% | 18% |
| Phenyl trimethicone | 6% | 12% | 5% | 6% | 6% |
| (2-phenylethyl) trimethylsiloxysilicate | 6% | 6% | 10% | 6% | 6% |
| Sorbitan stearate | 0.5% | 0.4% | 0.3% | 0.5% | 0.5% |
| Carbomer | 0.4% | 0.5% | 0.5% | 0.4% | 0.4% |
| Triethanolamine | 0.3% | 0.3% | 0.3% | 0.3% | 0.3% |
| Distilled water | Balance of | Balance of | Balance of | Balance of | Balance of |
| Whitening effect | Bright and smooth | Bright and smooth | Bright and smooth | Over-whitening and slightly rough surface | Bright and slightly rough surface |
| Transparency | 89.92 | 90.28 | 89.46 | 78.52 | 91.02 |
| Haze degree | 91.26 | 90.88 | 91.30 | 68.46 | 75.86 |
Wherein, the haze value is more than 85, namely the haze is extremely good, and the corresponding soft-focus effect is excellent. As can be seen from the results of table 1, the moisturizing concealer anti-wrinkle composition of the present invention has excellent whitening effect, and has excellent haze and soft-focus effect. In the whitening effect of the comparative example 1, whitening is excessive, and the surface is slightly rough, which may be caused by the structure of the added micron-sized titanium dioxide densely-coated nano pearl powder, the micron-sized titanium dioxide densely-coated nano pearl powder is white, has large particles, easily shows an excessive whitening effect, and has insufficient soft focus scattering to light, so that the rough structure of the surface is shown. The whitening effect of comparative example 2 is bright and has a slightly rough surface, the bright whitening effect is caused by the nano pearl powder and the nano titanium dioxide powder inside the composition, the nano powder size is uniformly dispersed in the composition, the displayed whitening effect is bright and moderate, and the soft focus scattering effect of the nano particles on light is promoted to display the bright whitening effect due to the micro particles. In the embodiment of the invention, titanium glycol salt is irradiated by ultraviolet light to form a nano-scale porous titanium dioxide structure on the surface of the nano pearl powder, so that the structure that the nano pearl powder is partially coated by the porous titanium dioxide structure is obtained. In the structure, a porous structure with the aperture of about 1-5nm exists in the porous titanium dioxide on the surface, nano-scale gaps also exist among the porous titanium dioxide attached to the surface of the nano pearl powder, and the nano-pores and the nano-scale gaps enrich soft focus scattering of light, so that the composition has more prominent soft focus scattering effect on the light, is bright visually, cannot observe the situation of a rough surface structure, and promotes the bright and smooth whitening effect. Meanwhile, the nano-scale gaps among the porous titanium dioxide can ensure that the anti-wrinkle and whitening effects of the pearl powder in the pearl powder are effectively exerted.
Claims (7)
1. A moisturizing, concealer and anti-wrinkle composition comprises, by weight, 26.3% -35.8% of a polyol humectant, 6.6% -9.2% of porous titanium dioxide modified nano pearl powder particles, 25.3% -36.2% of a silicone oil-based aqueous phase, 0.1% -0.5% of a nonionic surfactant, 0.1% -0.5% of a thickener, 0.2% -0.3% of a pH regulator triethanolamine, and the balance of distilled water; the polyhydric alcohol humectant consists of the following substances in parts by weight: 20-60 parts of sodium hyaluronate, 100 parts of propylene glycol, 400 parts of glycerol and 10-50 parts of ascorbyl glucoside; the porous titanium dioxide modified nano pearl powder particles are prepared by the following preparation method:
(1) pre-crushing pearl raw materials: pre-pulverizing high-quality fresh water pearl into pearl powder with particle size less than 50 um;
(2) nano-crushing: dispersing the pearl powder with the granularity of less than 50um obtained in the step (1) in deionized water, adding a proper amount of dispersant to obtain micron pearl powder dispersion liquid,
in the dispersion liquid, the concentration of the dispersant is 10-20g/L, the concentration of the pearl powder is 100-200g/L,
pulverizing the micrometer Margarita powder dispersion with nanometer pulverizer for 1-2 hr to obtain nanometer Margarita powder dispersion with particle size of 20-100 nm;
(3) preparing a mixed dispersion liquid: taking 100ml of the nano pearl powder dispersion liquid obtained in the step (2), adding 5-8g of titanium glycol salt, and then shearing at high speed in a high-speed shearing machine to obtain uniform titanium glycol salt and nano pearl powder dispersion liquid;
(4) ultraviolet light irradiation: and (4) carrying out ultraviolet irradiation on the titanium glycol salt and the nano pearl powder dispersion liquid obtained in the step (3) for 2-4h to form porous titanium dioxide nano particles on the surface of the nano pearl powder, and standing, centrifugally separating and washing with deionized water to obtain the porous titanium dioxide modified nano pearl powder particles.
2. The moisturizing concealer anti-wrinkle composition according to claim 1, wherein: the pore diameter of the porous titanium dioxide nano-particles is 1-5 nm.
3. The moisturizing concealer anti-wrinkle composition according to claim 1, wherein: the dispersing agent is a nonionic dispersing agent and is selected from one or more of sorbitan monooleate, polyoxyethylene lauryl ether, polyoxyethylene monopalmitate, polyoxyethylene monolaurate, polyoxyethylene cetyl alcohol, polyoxyethylene sorbitan monopalmitate, polyoxyethylene sorbitan monolaurate, polyoxyethylene alkyl aryl ether and polyoxyethylene vegetable oil.
4. The moisturizing concealer anti-wrinkle composition according to claim 1, wherein: the silicone oil-based oily phase is selected from one or more of polydimethylsiloxane, phenyl trimethicone and diphenyl dimethylsiloxane.
5. The moisturizing concealer anti-wrinkle composition according to claim 1, wherein: the nonionic surfactant is selected from one or more of glycerol laurate, ricinoleic acid glyceride, soybean lecithin, fatty alcohol-polyoxyethylene ether, sucrose cocoate and sorbitan stearate.
6. The moisturizing concealer anti-wrinkle composition according to claim 1, wherein: the thickening agent is selected from one or more of carbomer, polyacrylamide dimethyl taurinate, xanthan gum and acrylic polysiloxane.
7. A method for preparing a cosmetic composition consisting of the moisturizing concealer and anti-wrinkle composition as claimed in any one of claims 1 to 6, comprising (1) preparing a polyhydric alcohol humectant by mixing each component of the polyhydric alcohol humectant in advance according to a ratio; (2) stirring and mixing the polyalcohol humectant, the silicone oil-based oil phase and distilled water uniformly; (3) sequentially adding nonionic surfactant, porous titanium dioxide modified nanometer pearl powder particles, thickener and triethanolamine, and stirring at 60 deg.C and 3000 rpm.
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| CN1300246C (en) * | 2003-12-19 | 2007-02-14 | 上海交通大学 | Method for preparing uvioresistant polyester by nanometer titania generated in situ |
| CN101874811B (en) * | 2009-12-11 | 2012-10-31 | 天津兆阳纳米科技有限公司 | Preparation method of silica modified nano pearl powder |
| CN101734717B (en) * | 2010-03-19 | 2012-06-13 | 上海交通大学 | Method for preparing porous titanium dioxide based on light assistance |
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Effective date of registration: 20210708 Address after: 528000 no.50-3, area a, Datang Town, Sanshui District, Foshan City, Guangdong Province Applicant after: Foshan baizhixiu Cosmetics Co., Ltd Address before: Room 309, 3 / F, No.2 building, Qianwan bonded port area, Qingdao area, China (Shandong) pilot Free Trade Zone, Qingdao, Shandong Province Applicant before: Qingdao zizhiyan cosmetics technology Co.,Ltd. |
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