CN112137075B - Compound emulsifier fine powder and preparation method thereof - Google Patents

Compound emulsifier fine powder and preparation method thereof Download PDF

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Publication number
CN112137075B
CN112137075B CN202010939568.5A CN202010939568A CN112137075B CN 112137075 B CN112137075 B CN 112137075B CN 202010939568 A CN202010939568 A CN 202010939568A CN 112137075 B CN112137075 B CN 112137075B
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fine powder
emulsifier
fatty acid
acid ester
compound emulsifier
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CN112137075A (en
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孟宪伟
姜黎黎
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Fujian Yile Baobao Biotechnology Co ltd
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Fujian Yile Baobao Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/10Foods or foodstuffs containing additives; Preparation or treatment thereof containing emulsifiers
    • AHUMAN NECESSITIES
    • A21BAKING; EDIBLE DOUGHS
    • A21DTREATMENT, e.g. PRESERVATION, OF FLOUR OR DOUGH, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS; PRESERVATION THEREOF
    • A21D15/00Preserving finished, partly finished or par-baked bakery products; Improving
    • AHUMAN NECESSITIES
    • A21BAKING; EDIBLE DOUGHS
    • A21DTREATMENT, e.g. PRESERVATION, OF FLOUR OR DOUGH, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS; PRESERVATION THEREOF
    • A21D2/00Treatment of flour or dough by adding materials thereto before or during baking
    • A21D2/08Treatment of flour or dough by adding materials thereto before or during baking by adding organic substances
    • A21D2/14Organic oxygen compounds
    • A21D2/16Fatty acid esters
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Bakery Products And Manufacturing Methods Therefor (AREA)

Abstract

The invention discloses compound emulsifier fine powder and a preparation method thereof, and belongs to the field of emulsifier compounding. The compound emulsifier fine powder comprises the following components in percentage by weight: polyglycerin fatty acid ester: 0% -10% of mono-diglyceride fatty acid ester: 65% -100%, sucrose fatty acid ester: 0% -5% of sodium stearoyl lactylate or diacetyl tartaric acid mono-diglyceride: 0-20%. The preparation method comprises mixing one or more of polyglycerol fatty acid ester, mono-diglycerol fatty acid ester, sucrose fatty acid ester, sodium stearoyl lactylate or diacetyl tartaric acid mono-diglycerol ester, heating and melting, and cooling with cold air to obtain compound emulsifier fine powder with particle size of more than 80 mesh. The compound emulsifier fine powder can prolong the shelf life of starch products and increase the chewy mouthfeel.

Description

Compound emulsifier fine powder and preparation method thereof
Technical Field
The invention relates to compound emulsifier fine powder and a preparation method thereof, belonging to the field of emulsifier compounding.
Background
The emulsifier is an important food additive and is widely applied to the preparation of starch foods such as cakes, breads and the like. The two ends of the molecule are composed of hydrophilic and oleophilic groups, and an adsorption layer can be formed at the interface of water and oil to connect the two groups, so that the emulsification effect is achieved. Emulsifiers can also interact specifically with carbohydrates, proteins, lipids, etc. in starch based foods to exhibit a variety of functions. The starch product is added with a proper amount of emulsifying agent to fully emulsify the ingredients, uniformly mix, improve the flavor of the product, achieve the effects of softening, preserving freshness, increasing the chewy taste and prolonging the shelf life, and improve the product quality.
The mono-diglyceride fatty acid ester and the polyglycerol fatty acid ester have excellent emulsifying property, have the double characteristics of hydrophilicity and lipophilicity, have the functions of improving the viscosity of starch and preventing the aging of starch, can be decomposed in the metabolic process of human bodies, and have high safety.
The sucrose fatty acid ester can enlarge the dough, and can interact with proteins in the flour, in particular can form a compound with gluten proteins, the gliadin in the starch is combined with hydrophilic groups of the emulsifier, and the glutenin is combined with lipophilic groups of the emulsifier, so that more proteins are combined with each other to form a macromolecular gluten network, the gluten strength is enhanced, the extensibility and gas retention of the gluten are improved, and the volume of the dough and a finished product is enlarged.
Sodium stearyl lactate can be combined with starch to form a spiral complex, and prevent amylose from agglomerating from the interior of starch granules to prevent starch from aging; and it can also form a complex with gluten proteins, forming a smooth film structure between gluten and starch, binding the gluten to reduce the viscosity of the dough, thereby improving the extensibility of the gluten.
The diacetyl tartaric acid mono-diglyceride has stronger emulsification, anti-aging and other effects, can effectively enhance the elasticity, toughness and gas holding property of dough, reduce the weakening degree of the dough, increase the volume of bread and improve the tissue structure of the bread.
In the technical data disclosed in the prior art, the used compound emulsifier contains filling agents such as water, sorbitol, maltodextrin and the like, and the particles of the used emulsifier are larger, such as mono-diglyceride fatty acid ester, polyglycerol fatty acid ester and the like, generally have a size of 30-60 meshes, can not form good combination with starch particles (130 meshes) in starch products such as flour and the like, can not achieve the aim of well preventing starch aging, and reduces the use effect of the emulsifier. In the technical data disclosed in the prior art, the used emulsifier is mostly dried by adopting a hot air type spray drying method, so that the performance of the emulsifier is affected to a certain extent.
Based on the prior art, a compound emulsifier which can be fully combined with starch, can well prevent starch from aging, prolong the shelf life of starch finished products and increase the chewy mouthfeel is needed in the field.
Disclosure of Invention
In order to solve the problems, the invention aims to provide the compound emulsifier fine powder and the preparation method thereof, and the compound emulsifier prepared by the invention can prolong the shelf life of starch finished products and increase the chewy mouthfeel.
The first object of the invention is to provide a method for preparing the compound emulsifier fine powder, which comprises the following steps:
step one, mixing one or more of polyglycerol fatty acid ester, mono-diglycerol fatty acid ester (C16:0/C18:0), sucrose fatty acid ester, sodium stearoyl lactylate or diacetyl tartaric acid mono-diglycerol ester, heating to 70-80 ℃, and preserving heat for 10-20min;
step two, carrying out cold air spray cooling on the melted mixed emulsifier obtained in the step one, wherein the inlet temperature of the mixed emulsifier is 65-70 ℃, and the pressure of a pressure spray nozzle is 5-150 kg/cm 2 The inlet temperature of cold air/nitrogen is 0-10deg.C, and the wind pressure is 10-20 kg/cm 2 The compound emulsifier fine powder with the 80-mesh passing rate of more than or equal to 90 percent can be obtained.
In one embodiment of the invention, the compounded emulsifier fine powder comprises the following components in percentage by weight:
polyglycerin fatty acid ester: 0% -10%;
mono-di-glycerol fatty acid ester (c16:0/c18:0): 65% -100%;
sucrose fatty acid ester: 0% -5%;
sodium stearoyl lactylate or diacetyl tartaric acid mono-diglyceride: 0-20%.
In one embodiment of the invention, the polyglycerin fatty acid ester is preferably a polyglycerin fatty acid ester E475; the mono-di-glycerin fatty acid ester (C16:0/C18:0) is preferably a mono-di-glycerin fatty acid ester E471; the sucrose fatty acid ester is preferably sucrose fatty acid ester E473; the sodium stearoyl lactylate is preferably sodium stearoyl lactylate E481i; the diacetyl tartaric acid mono-diglyceride is preferably diacetyl tartaric acid mono-diglyceride E472.
In one embodiment of the present invention, preferably, the content of polyglycerin fatty acid ester and sucrose fatty acid ester in the compound emulsifier fine powder is more than 0%; the content of the sodium stearoyl lactylate or diacetyl tartaric acid mono-diglyceride in the compound emulsifier fine powder is more than 0%.
In one embodiment of the present invention, in the first step, stirring is required during the heating and heat preservation, and the stirring speed is 5-30rpm.
In one embodiment of the present invention, in step one, the optimal stirring speed is 25rpm and the optimal incubation time is 15min.
In one embodiment of the invention, step two, the optimum inlet temperature of the mixed emulsifier is 70 ℃.
In one embodiment of the invention, step two, the optimum pressure spray nozzle pressure is 60 kg/cm 2
In one embodiment of the invention, step two, the optimal cold air/nitrogen inlet temperature is 0 ℃.
In one embodiment of the present invention, in the second step, the optimal wind pressure is 15 kg/cm 2
The second purpose of the invention is to provide the compound emulsifier fine powder prepared by the method.
It is a third object of the present invention to provide a food product, preferably a starch-based product, more preferably a baked flour product, comprising the above-described formulated emulsifier fine powder.
The fourth object of the invention is to provide the application of the compound emulsifier fine powder in the food field.
The invention provides a compound emulsifier fine powder and a preparation method thereof, which have the following advantages compared with the prior art:
the compound emulsifier fine powder provided by the invention is prepared by adopting a cold air spray cooling method, so that the fine powder compound emulsifier with the 80-mesh passing rate of more than or equal to 90% is obtained, the compound emulsifier does not contain filler, can be fully combined with starch particles, and has synergistic interaction with each other, so that the compound emulsifier fine powder has the advantages of well preventing starch from aging, prolonging the shelf life of starch finished products, improving the extensibility and gas retention of gluten, and increasing the chewy mouthfeel.
Detailed Description
Bread texture (hardness, elasticity, chewiness): the texture analyzer adopts a P/25 test probe, the speed before, during and after the test is 1.5mm/s, the compression rate is 50%, the triggering type is automatic, and the starting point induction force is 5g.
Mesh number measurement of the components: and (5) a 80-mesh standard sieve, measuring the weight of the undersize material, and calculating the passing rate.
Examples 1-5 preparation of formulated emulsifier fines
Step one, the polyglycerin fatty acid ester (E475), the mono-di-glycerin fatty acid ester (C16:0/C18:0) (E471), the sucrose fatty acid ester (E473) and the sodium stearoyl lactylate (E481 i) are weighed according to the weight percentage of the following table 1, then heated to 75 ℃, and kept at the temperature for 15 minutes, wherein stirring is required in the heating and the heat-preserving processes, and the stirring speed is 25rpm.
And step two, carrying out cold air type spray cooling on the melted and mixed emulsifier obtained in the step one. The inlet temperature of the mixed emulsifier is 70 ℃, and the pressure of the pressure spray nozzle is 60 kg/cm 2 Cold air/nitrogen inlet temperature is 0 ℃, wind pressure: 15 kg/cm 2 . Obtaining the compound emulsifier fine powder with the 80-mesh passing rate of more than or equal to 90 percent.
Table 1: each component of the compound emulsifier fine powder and the weight percentage thereof
Comparative example 1
The polyglycerin fatty acid ester (E475), the mono-di-glycerin fatty acid ester (C16:0/C18:0) (E471), the sucrose fatty acid ester (E473) and the sodium stearoyl lactylate (E481 i) were weighed according to the ratio of comparative example 1 in Table 1, and directly mixed to obtain a compound emulsifier. The component mesh number of the compound emulsifier is 30-60 meshes as shown by measurement.
Comparative example 2
According to the proportion of comparative example 2 in Table 1, the polyglycerin fatty acid ester (E475), the mono-di glycerin fatty acid ester (C16:0/C18:0) (E471), the sucrose fatty acid ester (E473) and the sodium stearoyl lactylate (E481 i) are weighed, mixed and then directly subjected to mechanical grinding, and the study shows that the emulsifier is softened during the grinding process to cause difficult grinding and cannot be normally carried out, and the obtained compound emulsifier is serious in caking and cannot be used in the subsequent application process.
Example 6
Bread was made using the compounded emulsifier from comparative example 1 and the compounded emulsifier fines from examples 1-5 in weight fractions using the following formulation and manufacturing method:
the formula of the bread is as follows: 1000g of high gluten wheat flour, 120g of white granulated sugar, 14g of salt, 80g of butter, 12g of yeast, 575g of water, 1g of calcium propionate, 0.3g of sodium dehydroacetate and 10g of compound emulsifying agent (fine powder).
The preparation method of the bread comprises the following steps: stirring procedure: firstly, slowly stirring and then rapidly stirring for 11min; segmentation shaping: 150 g/dough; relaxing at room temperature for 15min; proofing temperature (deg.c): 35 ℃; relative humidity (%): 80%; proofing time (min): 100min; baking temperature (deg.c): heating to 180 deg.c, heating to 200 deg.c and stoving for 25 min. The prepared bread was tested for hardness, elasticity and chewiness by a texture tester. The results of the performance test are shown in Table 2.
TABLE 2 results of various Performance tests for comparative example 1 and examples 1-5
From the above table, the hardness, elasticity and chewiness of the bread of examples 1 to 5 are better than those of comparative example 1, because the compound emulsifier of examples 1 to 5 is finely pulverized by the preparation method of the present invention, and can be better combined with starch particles in flour, promote sufficient interaction between protein and lipid compounds in the bread and each emulsifier component, maintain the network structure of gluten, and improve softness, elasticity and chewiness of the bread. The bread has improved moisture retention, good taste and other edible properties, and the compound emulsifier fine powder is fully combined with amylose, so that the active alpha-crystal form is maintained for a long time, and the shelf life is prolonged.
In addition, at present, the shelf life of the commercially available compound emulsifier is generally 12-18 months. The storage performance of the compound emulsifier fine powder is tested, and researches show that the shelf life of the compound emulsifier fine powder can reach 24 months, the phenomenon of caking of the existing compound emulsifier can not occur under the conventional storage condition, and the bread tissue structure and taste prepared within the shelf life are not changed.
While the invention has been described with reference to the preferred embodiments, it is not limited thereto, and various changes and modifications can be made therein by those skilled in the art without departing from the spirit and scope of the invention as defined in the appended claims.

Claims (8)

1. The preparation method of the compound emulsifier fine powder for improving the mouthfeel of starch foods is characterized by comprising the following steps of:
step one, polyglycerin fatty acid ester, namely, polyglycerin fatty acid ester C16 with the weight percentages of 5-10%, 65-80%, 1-5% and 10-20% respectively: 0/C18: 0. mixing sucrose fatty acid ester and sodium stearoyl lactylate, heating to 70-80deg.C, and maintaining for 10-20min;
step two, carrying out cold air spray cooling on the melted mixed emulsifier obtained in the step one, wherein the inlet temperature of the mixed emulsifier is 65-70 ℃, and the pressure of a pressure spray nozzle is 5-150 kg/cm 2 The inlet temperature of cold air/nitrogen is 0-10deg.C, and the wind pressure is 10-20 kg/cm 2 The compound emulsifier fine powder with the 80-mesh passing rate of more than or equal to 90 percent can be obtained.
2. The method for preparing the fine powder of the compound emulsifier according to claim 1, wherein stirring is required in the heating and heat preservation process, and the stirring speed is 5-30rpm.
3. The method for preparing the fine powder of the compound emulsifier according to claim 1 or 2, wherein in the second step, the inlet temperature of the mixed emulsifier is 70 ℃.
4. The method for preparing the compound emulsifier fine powder according to claim 1 or 2, wherein in the second step, the pressure of the pressure spray nozzle is 60 kg/cm 2
5. The method for preparing the fine powder of the compound emulsifier according to claim 1 or 2, wherein in the second step, the cold air/nitrogen inlet temperature is 0 ℃; the wind pressure is 15 kg/cm 2
6. The formulated emulsifier fine powder produced by the method for producing formulated emulsifier fine powder according to claim 1 or 2.
7. A starch-based food product comprising the compounded emulsifier fine powder of claim 6.
8. The use of the compounded emulsifier fine powder of claim 6 in the field of starch-based foods.
CN202010939568.5A 2020-09-09 2020-09-09 Compound emulsifier fine powder and preparation method thereof Active CN112137075B (en)

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CN112137075B true CN112137075B (en) 2023-07-25

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Publication number Priority date Publication date Assignee Title
CN113424926A (en) * 2021-06-17 2021-09-24 江苏邦臣生物科技股份有限公司 Compound emulsifier fine powder and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0556757A (en) * 1991-08-29 1993-03-09 Taiyo Kagaku Co Ltd Production of emulsifiable foaming agent powder
JP2000279786A (en) * 1998-11-05 2000-10-10 Hayashibara Biochem Lab Inc Production of powdery emulsifier and apparatus for production therefor
CN101684984A (en) * 2008-09-28 2010-03-31 赵君哲 Spray drying method and device thereof
CN104543626A (en) * 2014-12-26 2015-04-29 山东圣琪生物有限公司 Compound emulsifier
CN108184945A (en) * 2017-11-27 2018-06-22 安徽乐锦记食品有限公司 A kind of bread emulsifiers formula

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0556757A (en) * 1991-08-29 1993-03-09 Taiyo Kagaku Co Ltd Production of emulsifiable foaming agent powder
JP2000279786A (en) * 1998-11-05 2000-10-10 Hayashibara Biochem Lab Inc Production of powdery emulsifier and apparatus for production therefor
CN101684984A (en) * 2008-09-28 2010-03-31 赵君哲 Spray drying method and device thereof
CN104543626A (en) * 2014-12-26 2015-04-29 山东圣琪生物有限公司 Compound emulsifier
CN108184945A (en) * 2017-11-27 2018-06-22 安徽乐锦记食品有限公司 A kind of bread emulsifiers formula

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
粉末油脂生产过程分析与喷雾冷却塔设计探讨;张彬,郑为完,游海,李岂凡;《南昌大学学报(工程技术版)》;19940630(第02期);第1-6页 *
粉状硬脂酸单甘油酯的工艺研究;齐凯琴;《化学工程师》;19940426(第02期);第16-18页 *
高彦祥.复配乳化剂.《食品添加剂》.中国轻工业出版社,2019,第250页. *

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