CN112120966A - 一种可粘黏假睫毛的可撕拉粘性眼线液及其制备方法和应用 - Google Patents
一种可粘黏假睫毛的可撕拉粘性眼线液及其制备方法和应用 Download PDFInfo
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Abstract
本发明公开了一种可粘黏假睫毛的可撕拉粘性眼线液及其制备方法。可粘黏假睫毛的可撕拉粘性眼线液，包括以下重量份的原料，溶剂8‑12份，保湿剂3‑7份，着色剂2‑4份，中和剂0.5‑1.5份，乳化剂2‑4份，撕拉增粘成膜剂65‑85份，防腐剂0.2‑0.5份。其制备方法为将其组份分批加入并于不同温度下加热、搅拌均匀，密封得成品。所述可粘黏假睫毛的可撕拉粘性眼线液可应用于眼线笔。本发明中的可粘黏假睫毛的可撕拉粘性眼线液集合了眼线液和假睫毛胶水的功能，使用本发明中的可粘黏假睫毛的可撕拉粘性眼线液，卸妆时只需一步撕除，方便快捷，卸妆时不会引发过敏，不会造成眼部不适，体验感好。
Description
技术领域
本发明涉及眼线液技术领域，特别是一种可粘黏假睫毛的可撕拉粘性眼线液及其制备方法和应用。
背景技术
眼线液是广大女性生活、工作中广泛使用的美妆产品，该产品可有效提升女性气质，使其更加自信和美丽。该产品使用时，直接在眼皮边缘勾勒出线条即可，卸妆时需使用卸妆产品或直接以温水反复搓洗将眼线液去除，使用卸妆产品卸妆易使敏感肌肤者过敏，以温水反复搓洗卸妆，有时会产生黑水，使眼角周围形成黑眼圈，反复搓洗易造成眼部不适，体验感较差。而且，现有的眼线液仅能用作画眼线，产品功能较为单一。所以，现有的眼线液产品功能较为单一、卸妆不便、卸妆时易引发过敏、易造成眼部不适和体验感差。
发明内容
本发明的目的，在于提供一种可粘黏假睫毛的可撕拉粘性眼线液及其制备方法和应用。以解决上述背景技术中提到的眼线液产品功能单一，卸妆不便、卸妆时易引发过敏、易造成眼部不适和体验感差的问题。
本发明的技术方案：一种可粘黏假睫毛的可撕拉粘性眼线液，包括以下重量份的原料，溶剂8-12份，保湿剂3-7份，着色剂2-4份，中和剂0.5-1.5份，乳化剂2-4份，撕拉增粘成膜剂65-85份，防腐剂0.2-0.5份。
所述的可粘黏假睫毛的可撕拉粘性眼线液，包括以下重量份的原料，溶剂10份，保湿剂5份，着色剂3份，中和剂1份，乳化剂3份，增粘成膜剂77.7份，防腐剂0.3份。
所述溶剂为水。
所述保湿剂包括丙二醇和1,2-丁二醇，丙二醇和1,2-丁二醇的重量比为3:(1-3)。
所述保湿剂包括丙二醇和1,2-丁二醇，丙二醇和1,2-丁二醇的重量比为3:2。
所述着色剂为CI 77266。
所述中和剂为三乙醇胺，所述乳化剂为聚山梨醇酯-80。
所述增粘成膜剂包括松香丙烯酸酯、聚乙烯醇、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、聚异戊二烯、乙烯/VA共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯、聚氨酯-1，松香丙烯酸酯:聚乙烯醇:C5-6烷/环烷/萜烯共聚物:苯乙烯/异戊二烯共聚物:丙烯酸酯类/丙烯酸乙基己酯共聚物:苯乙烯/丙烯酸酯类共聚物:聚乙酸乙烯酯:聚氯乙烯:聚丙烯酸丁酯:聚异戊二烯:乙烯/VA共聚物:苯乙烯/丁二烯共聚物:乙酸乙烯酯:聚氨酯-1的重量比为(4-6):(3-5):(2-4):(3-5):(2-4):(4-6):(7-11):(5-9):(3.5-5.5):(5-9):(5.5-9.5):(4-6):(3-5):(8-12)。
所述松香丙烯酸酯:聚乙烯醇:C5-6烷/环烷/萜烯共聚物:苯乙烯/异戊二烯共聚物:丙烯酸酯类/丙烯酸乙基己酯共聚物:苯乙烯/丙烯酸酯类共聚物:聚乙酸乙烯酯:聚氯乙烯:聚丙烯酸丁酯:聚异戊二烯:乙烯/VA共聚物:苯乙烯/丁二烯共聚物:乙酸乙烯酯:聚氨酯-1的重量比为5:4:3:4:3:5:9:7:4.3:7:7.4:5:4:10。
所述防腐剂包括苯氧乙醇、辛甘醇、氯苯甘醚，所述苯氧乙醇:辛甘醇:氯苯甘醚的重量比为1:1:1。
所述的可粘黏假睫毛的可撕拉粘性眼线液的制备方法，包括以下步骤，
步骤a，将水、丙二醇、1,2-丁二醇、三乙醇胺和聚山梨醇酯-80置于乳化锅，搅拌加热至75-95℃，得A品；
步骤b，向A品中加入松香丙烯酸酯、聚乙烯醇、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、聚异戊二烯、乙烯/VA共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯、聚氨酯-1，维持温度为80-90℃，均质搅拌8-12min，得B品；
步骤c,向B品中加入CI 77266、苯氧乙醇、辛甘醇、氯苯甘醚，均质搅拌2-5min，降温至45-55℃，放料，密封储存，得成品。
所述的可粘黏假睫毛的可撕拉粘性眼线液在眼线笔中的应用。
与现有技术比较，本发明将眼线液与假睫毛胶水合二为一，本发明的眼线液既是眼线液又可作粘黏假睫毛的胶水，使用时，只需一个产品，一步解决画眼线和粘贴假睫毛的问题。本发明的松香丙烯酸酯、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物都具有较好的粘性，这些成分按本发明中的配比混合后发生协同作用，产生了比任何单一成份粘性都强的粘性，可有效粘黏假睫毛。聚氨酯-1、聚乙烯醇、聚异戊二烯、乙烯/VA共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯，这些成分自身具有粘性，同时具有成模性，使得本发明的眼线液具有可撕拉性，这些成分按本发明中的配比混合后可使本发明的眼线液干燥后具有很好的整体撕拉性，撕拉后无残胶。本发明各成分间的配比，可使可粘黏假睫毛的可撕拉粘性眼线液既具有饱满的色感，又可将假睫毛牢固粘附于眼皮且卸妆时可整体撕拉，所述可粘黏假睫毛的可撕拉粘性眼线液贴附于皮肤时无紧绷感，撕拉时无不适感，持妆时间可达12小时，雨雾天气不脱妆。本发明中的可粘黏假睫毛的可撕拉粘性眼线液集合了眼线液和假睫毛胶水的功能，使用本发明中的可粘黏假睫毛的可撕拉粘性眼线液，卸妆时只需一步撕除，方便快捷，卸妆时不会引发过敏，不会造成眼部不适，体验感好。
附图说明
图1为可粘黏假睫毛的可撕拉粘性眼线液与假睫毛的粘黏示意图；
图2为撕除假睫毛的示意图；
图3为撕除可粘黏假睫毛的可撕拉粘性眼线液的示意图。
具体实施方式
下面结合附图和实施例对本发明作进一步的说明，但并不作为对本发明限制的依据。
本发明可粘黏假睫毛的可撕拉粘性眼线液的成分表见表1。
表1可粘黏假睫毛的可撕拉粘性眼线液的成分表
本发明实施例中的各组份与成分表中物质相对应。本发明中带“/”的物质为常规的成分确定的一体混合物类化妆品原料。
实施例1。一种可粘黏假睫毛的可撕拉粘性眼线液，包括以下重量份的原料，溶剂8份，保湿剂3份，着色剂2份，中和剂0.5份，乳化剂2份，撕拉增粘成膜剂65份，防腐剂0.2份。
所述溶剂为水。
所述保湿剂包括丙二醇和1,2-丁二醇，丙二醇和1,2-丁二醇的重量比为3:1。
所述着色剂为CI 77266。
所述中和剂为三乙醇胺，所述乳化剂为聚山梨醇酯-80。
所述增粘成膜剂包括松香丙烯酸酯、聚乙烯醇、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、聚异戊二烯、乙烯/VA共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯、聚氨酯-1，松香丙烯酸酯:聚乙烯醇:C5-6烷/环烷/萜烯共聚物:苯乙烯/异戊二烯共聚物:丙烯酸酯类/丙烯酸乙基己酯共聚物:苯乙烯/丙烯酸酯类共聚物:聚乙酸乙烯酯:聚氯乙烯:聚丙烯酸丁酯:聚异戊二烯:乙烯/VA共聚物:苯乙烯/丁二烯共聚物:乙酸乙烯酯:聚氨酯-1的重量比为4:3:2:3:2:4:7:5:3.5:5:5.5:4:3:8。
所述防腐剂包括苯氧乙醇、辛甘醇、氯苯甘醚，所述苯氧乙醇:辛甘醇:氯苯甘醚的重量比为1:1:1。
所述的可粘黏假睫毛的可撕拉粘性眼线液的制备方法，包括以下步骤，
步骤a，将水、丙二醇、1,2-丁二醇、三乙醇胺和聚山梨醇酯-80置于乳化锅，搅拌加热至75℃，得A品；
步骤b，向A品中加入松香丙烯酸酯、聚乙烯醇、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、聚异戊二烯、乙烯/VA共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯、聚氨酯-1，维持温度为80℃，均质搅拌8min，得B品；
步骤c,向B品中加入CI 77266、苯氧乙醇、辛甘醇、氯苯甘醚，均质搅拌2min，降温至45℃，放料，密封储存，得成品。
所述的可粘黏假睫毛的可撕拉粘性眼线液在眼线笔中的应用。按常规制作工艺，以可粘黏假睫毛的可撕拉粘性眼线液为原料，添加制作眼线笔的其他辅料，制作成眼线液笔。
所述可粘黏假睫毛的可撕拉粘性眼线液的持妆时间为11.80h。
所述可粘黏假睫毛的可撕拉粘性眼线液符合GB/T35889-2018的要求。
实施例2。一种可粘黏假睫毛的可撕拉粘性眼线液，包括以下重量份的原料，溶剂12份，保湿剂7份，着色剂4份，中和剂1.5份，乳化剂4份，撕拉增粘成膜剂85份，防腐剂0.5份。
所述溶剂为水。
所述保湿剂包括丙二醇和1,2-丁二醇，丙二醇和1,2-丁二醇的重量比为1:1。
所述着色剂为CI 77266。
所述中和剂为三乙醇胺，所述乳化剂为聚山梨醇酯-80。
所述增粘成膜剂包括松香丙烯酸酯、聚乙烯醇、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、聚异戊二烯、乙烯/VA共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯、聚氨酯-1，松香丙烯酸酯:聚乙烯醇:C5-6烷/环烷/萜烯共聚物:苯乙烯/异戊二烯共聚物:丙烯酸酯类/丙烯酸乙基己酯共聚物:苯乙烯/丙烯酸酯类共聚物:聚乙酸乙烯酯:聚氯乙烯:聚丙烯酸丁酯:聚异戊二烯:乙烯/VA共聚物:苯乙烯/丁二烯共聚物:乙酸乙烯酯:聚氨酯-1的重量比为6:5:4:5:4:6:11:9:5.5:9:9.5:6:5:12。
所述防腐剂包括苯氧乙醇、辛甘醇、氯苯甘醚，所述苯氧乙醇:辛甘醇:氯苯甘醚的重量比为1:1:1。
所述的可粘黏假睫毛的可撕拉粘性眼线液的制备方法，包括以下步骤，
步骤a，将水、丙二醇、1,2-丁二醇、三乙醇胺和聚山梨醇酯-80置于乳化锅，搅拌加热至95℃，得A品；
步骤b，向A品中加入松香丙烯酸酯、聚乙烯醇、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、聚异戊二烯、乙烯/VA共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯、聚氨酯-1，维持温度为90℃，均质搅拌12min，得B品；
步骤c,向B品中加入CI 77266、苯氧乙醇、辛甘醇、氯苯甘醚，均质搅拌5min，降温至55℃，放料，密封储存，得成品。
所述的可粘黏假睫毛的可撕拉粘性眼线液在眼线笔中的应用。按常规制作工艺，以可粘黏假睫毛的可撕拉粘性眼线液为原料，添加制作眼线笔的其他辅料，制作成眼线液笔。
所述可粘黏假睫毛的可撕拉粘性眼线液的持妆时间为11.85h。
所述可粘黏假睫毛的可撕拉粘性眼线液符合GB/T35889-2018的要求。
实施例3。一种可粘黏假睫毛的可撕拉粘性眼线液，包括以下重量份的原料，溶剂10份，保湿剂5份，着色剂3份，中和剂1份，乳化剂3份，增粘成膜剂77.7份，防腐剂0.3份。
所述溶剂为水。
所述保湿剂包括丙二醇和1,2-丁二醇，丙二醇和1,2-丁二醇的重量比为3:2。
所述着色剂为CI 77266。
所述中和剂为三乙醇胺，所述乳化剂为聚山梨醇酯-80。
所述增粘成膜剂包括松香丙烯酸酯、聚乙烯醇、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、聚异戊二烯、乙烯/VA共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯、聚氨酯-1，松香丙烯酸酯:聚乙烯醇:C5-6烷/环烷/萜烯共聚物:苯乙烯/异戊二烯共聚物:丙烯酸酯类/丙烯酸乙基己酯共聚物:苯乙烯/丙烯酸酯类共聚物:聚乙酸乙烯酯:聚氯乙烯:聚丙烯酸丁酯:聚异戊二烯:乙烯/VA共聚物:苯乙烯/丁二烯共聚物:乙酸乙烯酯:聚氨酯-1的重量比为5:4:3:4:3:5:9:7:4.3:7:7.4:5:4:10。
所述防腐剂包括苯氧乙醇、辛甘醇、氯苯甘醚，所述苯氧乙醇:辛甘醇:氯苯甘醚的重量比为1:1:1。
所述的可粘黏假睫毛的可撕拉粘性眼线液的制备方法，包括以下步骤，
步骤a，将水、丙二醇、1,2-丁二醇、三乙醇胺和聚山梨醇酯-80置于乳化锅，搅拌加热至85℃，得A品；
步骤b，向A品中加入松香丙烯酸酯、聚乙烯醇、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、聚异戊二烯、乙烯/VA共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯、聚氨酯-1，维持温度为85℃，均质搅拌10min，得B品；
步骤c,向B品中加入CI 77266、苯氧乙醇、辛甘醇、氯苯甘醚，均质搅拌3min，降温至50℃，放料，密封储存，得成品。
所述的可粘黏假睫毛的可撕拉粘性眼线液在眼线笔中的应用。按常规制作工艺，以可粘黏假睫毛的可撕拉粘性眼线液为原料，添加制作眼线笔的其他辅料，制作成眼线液笔。
所述可粘黏假睫毛的可撕拉粘性眼线液的持妆时间为12.00h。
所述可粘黏假睫毛的可撕拉粘性眼线液符合GB/T35889-2018的要求。
当然，本发明还可有其它多种实施例，在不背离本发明精神及其实质的情况下，熟悉本领域的技术人员当可根据本发明作出各种相应的改变和变形，但这些相应的改变和变形都应属于本发明所附的权利要求的保护范围。
Claims (10)
1.一种可粘黏假睫毛的可撕拉粘性眼线液，其特征在于：包括以下重量份的原料，溶剂8-12份，保湿剂3-7份，着色剂2-4份，中和剂0.5-1.5份，乳化剂2-4份，撕拉增粘成膜剂65-85份，防腐剂0.2-0.5份。
2.根据权利要求1所述的可粘黏假睫毛的可撕拉粘性眼线液，其特征在于：包括以下重量份的原料，溶剂10份，保湿剂5份，着色剂3份，中和剂1份，乳化剂3份，增粘成膜剂77.7份，防腐剂0.3份。
3.根据权利要求1或2所述的可粘黏假睫毛的可撕拉粘性眼线液，其特征在于：所述溶剂为水。
4.根据权利要求3所述的可粘黏假睫毛的可撕拉粘性眼线液，其特征在于：所述保湿剂包括丙二醇和1,2-丁二醇，丙二醇和1,2-丁二醇的重量比为3:（1-3）。
5.根据权利要求4所述的可粘黏假睫毛的可撕拉粘性眼线液，其特征在于：所述着色剂为CI 77266。
6.根据权利要求5所述的可粘黏假睫毛的可撕拉粘性眼线液，其特征在于：所述中和剂为三乙醇胺，所述乳化剂为聚山梨醇酯-80。
7.根据权利要求6所述的可粘黏假睫毛的可撕拉粘性眼线液，其特征在于：所述增粘成膜剂包括松香丙烯酸酯、聚乙烯醇、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、聚异戊二烯、乙烯/VA共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯、聚氨酯-1，松香丙烯酸酯:聚乙烯醇:C5-6烷/环烷/萜烯共聚物:苯乙烯/异戊二烯共聚物:丙烯酸酯类/丙烯酸乙基己酯共聚物:苯乙烯/丙烯酸酯类共聚物:聚乙酸乙烯酯:聚氯乙烯:聚丙烯酸丁酯:聚异戊二烯:乙烯/VA共聚物:苯乙烯/丁二烯共聚物:乙酸乙烯酯:聚氨酯-1的重量比为（4-6）:（3-5）:（2-4）:（3-5）:（2-4）:（4-6）:（7-11）:（5-9）:（3.5-5.5）:（5-9）:（5.5-9.5）:（4-6）:（3-5）:（8-12）。
8.根据权利要求7所述的可粘黏假睫毛的可撕拉粘性眼线液，其特征在于：所述防腐剂包括苯氧乙醇、辛甘醇、氯苯甘醚，所述苯氧乙醇: 辛甘醇:氯苯甘醚的重量比为1:1:1。
9.根据权利要求8所述的可粘黏假睫毛的可撕拉粘性眼线液的制备方法，其特征在于：包括以下步骤，
步骤a，将水、丙二醇、1,2-丁二醇、三乙醇胺和聚山梨醇酯-80置于乳化锅，搅拌加热至75-95℃，得A品；
步骤b，向A品中加入松香丙烯酸酯、聚乙烯醇、C5-6烷/环烷/萜烯共聚物、苯乙烯/异戊二烯共聚物、丙烯酸酯类/丙烯酸乙基己酯共聚物、苯乙烯/丙烯酸酯类共聚物、聚乙酸乙烯酯、聚氯乙烯、聚丙烯酸丁酯、聚异戊二烯、乙烯/VA 共聚物、苯乙烯/丁二烯共聚物、乙酸乙烯酯、聚氨酯-1，维持温度为80-90℃，均质搅拌8-12min，得B品；
步骤c,向B品中加入CI 77266、苯氧乙醇、辛甘醇、氯苯甘醚，均质搅拌2-5min，降温至45-55℃，放料，密封储存，得成品。
10.根据权利要求1-8任一权利要求所述的可粘黏假睫毛的可撕拉粘性眼线液在眼线笔中的应用。
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| CN110831451A (zh) * | 2017-06-30 | 2020-02-21 | 欧莱雅 | 用于将纤维添加至天然睫毛的组件及相应的美容处理方法 |
| CN112220698A (zh) * | 2020-04-27 | 2021-01-15 | 广州桃花里生物科技有限公司 | 一种可粘黏假睫毛的可撕拉粘性眼线液及其制备方法和应用 |
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| US20120301416A1 (en) * | 2007-07-30 | 2012-11-29 | Paul Henry Marotta | Cosmetic Composition Containing A Polymer Blend |
| TW201742619A (zh) * | 2016-06-13 | 2017-12-16 | 波菲詩美妝有限公司 | 成膜配方及應用其之撕除式眼線液 |
| CN110831451A (zh) * | 2017-06-30 | 2020-02-21 | 欧莱雅 | 用于将纤维添加至天然睫毛的组件及相应的美容处理方法 |
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