CN112075562A - Solid beverage of probiotics and prebiotics composite micromolecule pectin - Google Patents
Solid beverage of probiotics and prebiotics composite micromolecule pectin Download PDFInfo
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- CN112075562A CN112075562A CN202010735777.8A CN202010735777A CN112075562A CN 112075562 A CN112075562 A CN 112075562A CN 202010735777 A CN202010735777 A CN 202010735777A CN 112075562 A CN112075562 A CN 112075562A
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- 229920001277 pectin Polymers 0.000 title claims abstract description 91
- 239000001814 pectin Substances 0.000 title claims abstract description 91
- 235000013361 beverage Nutrition 0.000 title claims abstract description 55
- 239000007787 solid Substances 0.000 title claims abstract description 46
- 235000013406 prebiotics Nutrition 0.000 title claims abstract description 43
- 239000006041 probiotic Substances 0.000 title claims abstract description 43
- 235000018291 probiotics Nutrition 0.000 title claims abstract description 43
- 239000002131 composite material Substances 0.000 title claims abstract description 11
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- 238000011282 treatment Methods 0.000 claims abstract description 18
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- 230000000529 probiotic effect Effects 0.000 claims abstract description 11
- 238000002360 preparation method Methods 0.000 claims abstract description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 30
- 239000000243 solution Substances 0.000 claims description 29
- 239000000843 powder Substances 0.000 claims description 20
- 229930003231 vitamin Natural products 0.000 claims description 16
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 239000011259 mixed solution Substances 0.000 claims description 14
- 150000003384 small molecules Chemical class 0.000 claims description 14
- 239000000126 substance Substances 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 11
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 10
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 10
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 10
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 10
- 108010059820 Polygalacturonase Proteins 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 108010093305 exopolygalacturonase Proteins 0.000 claims description 10
- 239000008101 lactose Substances 0.000 claims description 10
- 238000007873 sieving Methods 0.000 claims description 10
- -1 compound vitamin Chemical class 0.000 claims description 9
- 239000007864 aqueous solution Substances 0.000 claims description 8
- 241000207199 Citrus Species 0.000 claims description 7
- 235000020971 citrus fruits Nutrition 0.000 claims description 7
- 150000003722 vitamin derivatives Chemical class 0.000 claims description 6
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims description 5
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 5
- 229930003451 Vitamin B1 Natural products 0.000 claims description 5
- 229930003268 Vitamin C Natural products 0.000 claims description 5
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- 239000001569 carbon dioxide Substances 0.000 claims description 5
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 5
- 238000004806 packaging method and process Methods 0.000 claims description 5
- 238000009417 prefabrication Methods 0.000 claims description 5
- 229960003495 thiamine Drugs 0.000 claims description 5
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 claims description 5
- 235000010374 vitamin B1 Nutrition 0.000 claims description 5
- 239000011691 vitamin B1 Substances 0.000 claims description 5
- 235000019154 vitamin C Nutrition 0.000 claims description 5
- 239000011718 vitamin C Substances 0.000 claims description 5
- 235000019165 vitamin E Nutrition 0.000 claims description 5
- 239000011709 vitamin E Substances 0.000 claims description 5
- 229940046009 vitamin E Drugs 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 238000001291 vacuum drying Methods 0.000 claims description 2
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- 230000007935 neutral effect Effects 0.000 description 3
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- 241000675108 Citrus tangerina Species 0.000 description 2
- 206010028980 Neoplasm Diseases 0.000 description 2
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- 238000011161 development Methods 0.000 description 2
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- 208000026310 Breast neoplasm Diseases 0.000 description 1
- 241000193171 Clostridium butyricum Species 0.000 description 1
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- 241000186660 Lactobacillus Species 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/135—Bacteria or derivatives thereof, e.g. probiotics
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/20—Reducing nutritive value; Dietetic products with reduced nutritive value
- A23L33/21—Addition of substantially indigestible substances, e.g. dietary fibres
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention provides a solid beverage of probiotics and prebiotics composite micromolecule pectin, and relates to the technical field of solid beverage processing. The preparation method of the solid beverage of probiotic and prebiotics compounded with micromolecule pectin mainly comprises the steps of prefabricating the micromolecule pectin, preparing the micromolecule pectin, carrying out high-pressure micro-jet treatment, mixing and stirring at high pressure, concentrating, freeze-drying, mixing and grinding and the like. The invention overcomes the defects of the prior art, improves the nutritive value of the solid beverage, and simultaneously effectively improves the dissolubility of the solid beverage, so that the solid beverage has the advantages of high nutritive value, good stability, good flavor and taste and the like.
Description
Technical Field
The invention relates to the technical field of solid beverage processing, in particular to a solid beverage of probiotics and prebiotics composite micromolecule pectin.
Background
The small Molecule (MCP) pectin is a natural high molecular food material, can reduce blood viscosity, inhibit platelet coagulation and vasodilatation, keep blood smooth, prevent cancer occurrence and development, and has effects of preventing and treating atherosclerosis, coronary heart disease, ischemic heart disease, and hyperlipemia. The tumor inhibiting effect also has estrogen-like effect, and can be used for treating diseases such as breast cancer.
Probiotics is a kind of active microorganisms beneficial to a host, and is a general term for active beneficial microorganisms which are planted in the intestinal tract and the reproductive system of a human body and can generate definite health efficacy so as to improve the micro-ecological balance of the host and play beneficial roles. The beneficial bacteria or fungi in human bodies and animal bodies are mainly as follows: clostridium butyricum, lactobacillus, bifidobacterium, actinomycete, saccharomycete, etc. The products with the strongest research functions in the world at present mainly comprise the composite active probiotics consisting of various microorganisms, and are widely applied to the fields of bioengineering, industry and agriculture, food safety and life health.
Prebiotics are non-digestible food ingredients that improve host health by selectively stimulating the growth and activity of one or a small number of bacteria in a colony to beneficially affect the host. Successful prebiotics should be largely undigested and fermented by the gut flora when passing through the upper gut. Most importantly, it stimulates the growth of beneficial bacterial flora and not harmful bacteria with potentially pathogenic or putrefactive activity.
With the development of economy and the improvement of social living standard, people seek high-quality life more and more, the requirement of people on daily diet is higher and higher, and the pursuit of healthy and concise life becomes the habit of people. In the aspect of daily drinking beverages, people are more and more inclined to the selection of solid beverages due to the inconvenience of carrying liquid beverages, but most of the existing beverages are pursuing excellent mouthfeel, the positioning of health components contained in the existing beverages is not strict, and the existing solid beverages rarely appear in mouthfeel and nutritional components and can meet the requirements of people
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides the solid beverage of probiotics and prebiotics compounded with micromolecular pectin, which improves the nutritive value of the solid beverage and effectively improves the dissolubility of the solid beverage at the same time, so that the solid beverage has the advantages of high nutritive value, good stability, good flavor and taste and the like.
In order to achieve the above purpose, the technical scheme of the invention is realized by the following technical scheme:
the solid beverage of the probiotics and the prebiotics compounded with the small molecular pectin is characterized in that the preparation method of the solid beverage of the probiotics and the prebiotics compounded with the small molecular pectin comprises the following steps:
(1) prefabrication of small molecule pectin: dissolving conventional pectin in water, adding pectinase, and performing enzymolysis at 28-30 deg.C for 2-3 hr to obtain mixed pectin solution;
(2) preparing micromolecule pectin: adjusting the pH of the mixed pectin solution to 2.5-3.5, rapidly stirring in a high-pressure environment for 1-2h, taking out, adjusting the pH to neutrality, and vacuum drying to obtain micromolecule pectin for later use;
(3) high-pressure micro-jet treatment: mixing the micromolecular pectin, the probiotic powder and the prebiotics, grinding in a grinding machine, adding deionized water, stirring uniformly, carrying out high-pressure micro-jet treatment, and circulating for 1-3 times to obtain a mixed aqueous solution for later use;
(4) high-pressure mixing and stirring: adding lactose and vitamin complex into the mixed water solution, stirring in a stirrer, placing in a high-pressure reaction kettle, introducing carbon dioxide into the reaction kettle, increasing the pressure to 12-16MPa, and standing for 1.5-2h to obtain a mixed solution for later use;
(5) concentration and freeze-drying: taking out the mixed solution, concentrating in vacuum to 1/5-1/8 of the original volume, and freeze-drying in a low-temperature environment to obtain a freeze-dried material for later use;
(6) mixing and grinding: adding citric acid and citrus powder into the freeze-dried material, mixing, grinding in a grinder, sieving, weighing, and packaging to obtain the fixed beverage.
Preferably, the addition amount of the pectinase in the step (1) is 0.2-0.3% of the conventional pectin.
Preferably, the pressure of the rapid stirring in the high-pressure environment in the step (2) is 15-18MPa, and the rotation speed of the stirring is 600-.
Preferably, the pressure of the high-pressure micro-jet treatment in the step (3) is 12000-18000 psi.
Preferably, the vitamin complex in the step (4) comprises the following substances in parts by weight: vitamin C: 1-5 parts, vitamin E: 0.5-1.5 parts, vitamin B1: 0.1 to 0.5 portion.
Preferably, the temperature of the low-temperature freeze-drying in the step (5) is 5 ℃ below zero to 8 ℃ below zero.
Preferably, the step (6) is carried out by sieving with an 80-mesh sieve.
Preferably, the solid beverage of the probiotics and prebiotics composite micromolecule pectin comprises the following substances in parts by weight: 2-8 parts of micromolecular pectin, 5-15 parts of probiotic powder, 10-30 parts of prebiotics, 1-5 parts of lactose, 1-5 parts of citric acid, 4-12 parts of citrus powder and 1.6-7 parts of compound vitamin.
The invention provides a solid beverage of probiotics and prebiotics composite micromolecule pectin, which has the advantages compared with the prior art that:
(1) the solid beverage adopts micromolecule pectin mixed prebiotics and probiotics as main raw materials, effectively improves the nutritive value of the solid beverage, protects intestines and stomach, promotes digestion health, is rich in various vitamins, has balanced nutrition, has low calorie and reduces obesity troubles;
(2) according to the invention, the micromolecular pectin, the prebiotics and the probiotics are subjected to high-pressure micro-jet treatment and mixed with other substances for high-pressure treatment, so that the dissolubility of the substances is effectively improved, the precipitate of the solid beverage is reduced, and the taste requirements of the public are met.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention are clearly and completely described below in conjunction with the embodiments of the present invention, and it is obvious that the described embodiments are some embodiments of the present invention, but not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
the solid beverage of the probiotics and the prebiotics compounded with the small molecular pectin is characterized in that the preparation method of the solid beverage of the probiotics and the prebiotics compounded with the small molecular pectin comprises the following steps:
(1) prefabrication of small molecule pectin: dissolving conventional pectin in water, adding pectinase, and performing enzymolysis at 28 deg.C for 2 hr to obtain mixed pectin solution;
(2) preparing micromolecule pectin: adjusting the pH of the mixed pectin solution to 2.5, then placing the mixed pectin solution in a high-pressure environment, quickly stirring the mixed pectin solution for 1 hour, taking out the mixed pectin solution, adjusting the pH to be neutral, and drying the mixed pectin solution in vacuum to obtain micromolecule pectin for later use;
(3) high-pressure micro-jet treatment: mixing the micromolecular pectin, the probiotic powder and the prebiotics, grinding in a grinding machine, adding deionized water, stirring uniformly, carrying out high-pressure micro-jet treatment, and circulating for 1-3 times to obtain a mixed aqueous solution for later use;
(4) high-pressure mixing and stirring: adding lactose and vitamin complex into the mixed aqueous solution, uniformly stirring in a stirrer, placing in a high-pressure reaction kettle, introducing carbon dioxide into the reaction kettle, boosting the pressure to 12MPa, and standing for 1.5h to obtain a mixed solution for later use;
(5) concentration and freeze-drying: taking out the mixed solution, concentrating the mixed solution in vacuum to 1/5 of the original volume, and freeze-drying the mixed solution in a low-temperature environment to obtain a freeze-dried material for later use;
(6) mixing and grinding: adding citric acid and citrus powder into the freeze-dried material, mixing, grinding in a grinder, sieving, weighing, and packaging to obtain the fixed beverage.
Wherein the addition amount of the pectinase in the step (1) is 0.2 percent of that of the conventional pectin; the pressure intensity of rapid stirring in the high-pressure environment in the step (2) is 15MPa, and the stirring rotating speed is 600 r/min; the pressure of the high-pressure micro-jet treatment in the step (3) is 12000 psi; the compound vitamin in the step (4) comprises the following substances in parts by weight: vitamin C: 1 part, vitamin E: 0.5 part, vitamin B1: 0.1 part; the temperature of low-temperature freeze-drying in the step (5) is 5 ℃ below zero; sieving with a 80-mesh sieve after grinding in the step (6); the solid beverage of the probiotics and prebiotics composite micromolecule pectin comprises the following substances in parts by weight: 2 parts of micromolecular pectin, 5 parts of probiotic powder, 10 parts of prebiotics, 1 part of lactose, 1 part of citric acid, 4 parts of orange powder and 1.6 parts of compound vitamin.
Example 2:
the solid beverage of the probiotics and the prebiotics compounded with the small molecular pectin is characterized in that the preparation method of the solid beverage of the probiotics and the prebiotics compounded with the small molecular pectin comprises the following steps:
(1) prefabrication of small molecule pectin: dissolving conventional pectin in water, adding pectinase, and performing enzymolysis at 30 deg.C for 3 hr to obtain mixed pectin solution;
(2) preparing micromolecule pectin: adjusting the pH of the mixed pectin solution to 3.5, then placing the mixed pectin solution in a high-pressure environment, quickly stirring the mixed pectin solution for 2 hours, taking out the mixed pectin solution, adjusting the pH to be neutral, and drying the mixed pectin solution in vacuum to obtain micromolecule pectin for later use;
(3) high-pressure micro-jet treatment: mixing the micromolecular pectin, the probiotic powder and the prebiotics, grinding in a grinding machine, adding deionized water, stirring uniformly, carrying out high-pressure micro-jet treatment, and circulating for 1-3 times to obtain a mixed aqueous solution for later use;
(4) high-pressure mixing and stirring: adding lactose and vitamin complex into the mixed aqueous solution, uniformly stirring in a stirrer, placing in a high-pressure reaction kettle, introducing carbon dioxide into the reaction kettle, boosting the pressure to 16MPa, and standing for 2 hours to obtain a mixed solution for later use;
(5) concentration and freeze-drying: taking out the mixed solution, concentrating the mixed solution in vacuum to 1/8 of the original volume, and freeze-drying the mixed solution in a low-temperature environment to obtain a freeze-dried material for later use;
(6) mixing and grinding: adding citric acid and citrus powder into the freeze-dried material, mixing, grinding in a grinder, sieving, weighing, and packaging to obtain the fixed beverage.
Wherein the addition amount of the pectinase in the step (1) is 0.3 percent of that of the conventional pectin; the pressure intensity of rapid stirring in the high-pressure environment in the step (2) is 18MPa, and the stirring rotating speed is 800 r/min; the pressure of the high-pressure micro-jet treatment in the step (3) is 18000 psi; the compound vitamin in the step (4) comprises the following substances in parts by weight: vitamin C: 5 parts, vitamin E: 1.5 parts, vitamin B1: 0.5 part; the temperature of low-temperature freeze-drying in the step (5) is below 8 ℃; sieving with a 80-mesh sieve after grinding in the step (6); the solid beverage of the probiotics and prebiotics composite micromolecule pectin comprises the following substances in parts by weight: 8 parts of micromolecular pectin, 15 parts of probiotic powder, 30 parts of prebiotics, 5 parts of lactose, 5 parts of citric acid, 12 parts of tangerine powder and 7 parts of compound vitamin.
Example 3:
the solid beverage of the probiotics and the prebiotics compounded with the small molecular pectin is characterized in that the preparation method of the solid beverage of the probiotics and the prebiotics compounded with the small molecular pectin comprises the following steps:
(1) prefabrication of small molecule pectin: dissolving conventional pectin in water, adding pectinase, and performing enzymolysis at 28-30 deg.C for 2-3 hr to obtain mixed pectin solution;
(2) preparing micromolecule pectin: adjusting the pH of the mixed pectin solution to 3, then placing the mixed pectin solution in a high-pressure environment, quickly stirring the mixed pectin solution for 1.5h, taking out the mixed pectin solution, adjusting the pH to be neutral, and drying the mixed pectin solution in vacuum to obtain micromolecule pectin for later use;
(3) high-pressure micro-jet treatment: mixing the micromolecular pectin, the probiotic powder and the prebiotics, grinding in a grinding machine, adding deionized water, stirring uniformly, carrying out high-pressure micro-jet treatment, and circulating for 1-3 times to obtain a mixed aqueous solution for later use;
(4) high-pressure mixing and stirring: adding lactose and vitamin complex into the mixed aqueous solution, uniformly stirring in a stirrer, placing in a high-pressure reaction kettle, introducing carbon dioxide into the reaction kettle, boosting the pressure to 14MPa, and standing for 1.8h to obtain a mixed solution for later use;
(5) concentration and freeze-drying: taking out the mixed solution, concentrating in vacuum to 1/5-1/8 of the original volume, and freeze-drying in a low-temperature environment to obtain a freeze-dried material for later use;
(6) mixing and grinding: adding citric acid and citrus powder into the freeze-dried material, mixing, grinding in a grinder, sieving, weighing, and packaging to obtain the fixed beverage.
Wherein the addition amount of the pectinase in the step (1) is 0.25 percent of that of the conventional pectin; the pressure intensity of rapid stirring in the high-pressure environment in the step (2) is 16MPa, and the stirring rotating speed is 700 r/min; the pressure of the high-pressure micro-jet treatment in the step (3) is 16000 psi; the compound vitamin in the step (4) comprises the following substances in parts by weight: vitamin C: 3.5 parts, vitamin E: 1 part, vitamin B1: 0.3 part; the temperature of low-temperature freeze-drying in the step (5) is below 6 ℃; sieving with a 80-mesh sieve after grinding in the step (6); the solid beverage of the probiotics and prebiotics composite micromolecule pectin comprises the following substances in parts by weight: 5 parts of micromolecular pectin, 10 parts of probiotic powder, 20 parts of prebiotics, 3 parts of lactose, 3.5 parts of citric acid, 8 parts of tangerine powder and 4.2 parts of compound vitamin.
Example 4:
the solid beverages obtained in the above examples 1-3 and the common solid beverage of the control group were tested for their dissolution rate and presence or absence of precipitates at the water temperatures of 0 ℃, 10 ℃, 25 ℃, 45 ℃ and 80 ℃, and the brewing method was to take 25g of the solid beverage, add 200ml of clean water at the corresponding temperature, mix them and observe the dissolution by stirring clockwise with a spoon, and the results are shown in the following table:
the table shows that the solid beverage prepared by the invention has good solubility, is easy to brew in water with lower temperature, is not easy to precipitate, and has good mouthfeel.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in a process, method, article, or apparatus that comprises the element.
The above examples are only intended to illustrate the technical solution of the present invention, but not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and such modifications or substitutions do not depart from the spirit and scope of the corresponding technical solutions of the embodiments of the present invention.
Claims (8)
1. The solid beverage of the probiotics and the prebiotics compounded with the small molecular pectin is characterized in that the preparation method of the solid beverage of the probiotics and the prebiotics compounded with the small molecular pectin comprises the following steps:
(1) prefabrication of small molecule pectin: dissolving conventional pectin in water, adding pectinase, and performing enzymolysis at 28-30 deg.C for 2-3 hr to obtain mixed pectin solution;
(2) preparing micromolecule pectin: adjusting the pH of the mixed pectin solution to 2.5-3.5, rapidly stirring in a high-pressure environment for 1-2h, taking out, adjusting the pH to neutrality, and vacuum drying to obtain micromolecule pectin for later use;
(3) high-pressure micro-jet treatment: mixing the micromolecular pectin, the probiotic powder and the prebiotics, grinding in a grinding machine, adding deionized water, stirring uniformly, carrying out high-pressure micro-jet treatment, and circulating for 1-3 times to obtain a mixed aqueous solution for later use;
(4) high-pressure mixing and stirring: adding lactose and vitamin complex into the mixed water solution, stirring in a stirrer, placing in a high-pressure reaction kettle, introducing carbon dioxide into the reaction kettle, increasing the pressure to 12-16MPa, and standing for 1.5-2h to obtain a mixed solution for later use;
(5) concentration and freeze-drying: taking out the mixed solution, concentrating in vacuum to 1/5-1/8 of the original volume, and freeze-drying in a low-temperature environment to obtain a freeze-dried material for later use;
(6) mixing and grinding: adding citric acid and citrus powder into the freeze-dried material, mixing, grinding in a grinder, sieving, weighing, and packaging to obtain the fixed beverage.
2. The solid beverage of probiotics and prebiotics compounded with small molecule pectin according to claim 1, characterized in that: the addition amount of the pectinase in the step (1) is 0.2-0.3% of that of the conventional pectin.
3. The solid beverage of probiotics and prebiotics compounded with small molecule pectin according to claim 1, characterized in that: the pressure intensity of rapid stirring in the high-pressure environment in the step (2) is 15-18MPa, and the stirring rotating speed is 600-800 r/min.
4. The solid beverage of probiotics and prebiotics compounded with small molecule pectin according to claim 1, characterized in that: the pressure of the high-pressure micro-jet treatment in the step (3) is 12000-18000 psi.
5. The solid beverage of probiotics and prebiotics compounded with small molecule pectin according to claim 1, characterized in that: the compound vitamin in the step (4) comprises the following substances in parts by weight: vitamin C: 1-5 parts, vitamin E: 0.5-1.5 parts, vitamin B1: 0.1 to 0.5 portion.
6. The solid beverage of probiotics and prebiotics compounded with small molecule pectin according to claim 1, characterized in that: the temperature of low-temperature freeze-drying in the step (5) is 5 ℃ below zero to 8 ℃ below zero.
7. The solid beverage of probiotics and prebiotics compounded with small molecule pectin according to claim 1, characterized in that: and (4) sieving with a 80-mesh sieve after grinding in the step (6).
8. The solid beverage of probiotics and prebiotics compounded with small molecule pectin according to claim 1, characterized in that: the solid beverage of the probiotics and prebiotics composite micromolecule pectin comprises the following substances in parts by weight: 2-8 parts of micromolecular pectin, 5-15 parts of probiotic powder, 10-30 parts of prebiotics, 1-5 parts of lactose, 1-5 parts of citric acid, 4-12 parts of citrus powder and 1.6-7 parts of compound vitamin.
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