CN112034072A - Method for measuring content and condensation degree of citral diacetal and lauraldehyde diacetal in perfume through gas chromatography-tandem mass spectrometry - Google Patents
Method for measuring content and condensation degree of citral diacetal and lauraldehyde diacetal in perfume through gas chromatography-tandem mass spectrometry Download PDFInfo
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- CN112034072A CN112034072A CN202010956582.6A CN202010956582A CN112034072A CN 112034072 A CN112034072 A CN 112034072A CN 202010956582 A CN202010956582 A CN 202010956582A CN 112034072 A CN112034072 A CN 112034072A
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- citral
- lauraldehyde
- diacetal
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/14—Preparation by elimination of some components
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N2030/042—Standards
- G01N2030/045—Standards internal
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N2030/062—Preparation extracting sample from raw material
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N2030/067—Preparation by reaction, e.g. derivatising the sample
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/90—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation
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Abstract
Description
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010956582.6A CN112034072B (en) | 2020-09-12 | 2020-09-12 | Method for measuring content and condensation degree of citral diethyl acetal and laural diethyl acetal in perfume by gas chromatography-tandem mass spectrometry |
Applications Claiming Priority (1)
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CN202010956582.6A CN112034072B (en) | 2020-09-12 | 2020-09-12 | Method for measuring content and condensation degree of citral diethyl acetal and laural diethyl acetal in perfume by gas chromatography-tandem mass spectrometry |
Publications (2)
Publication Number | Publication Date |
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CN112034072A true CN112034072A (en) | 2020-12-04 |
CN112034072B CN112034072B (en) | 2023-05-12 |
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CN202010956582.6A Active CN112034072B (en) | 2020-09-12 | 2020-09-12 | Method for measuring content and condensation degree of citral diethyl acetal and laural diethyl acetal in perfume by gas chromatography-tandem mass spectrometry |
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CN (1) | CN112034072B (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114199986A (en) * | 2021-12-10 | 2022-03-18 | 河南牧业经济学院 | Method for simultaneously determining 3 aldehyde compounds in beer |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003089921A1 (en) * | 2002-04-15 | 2003-10-30 | The Government Of The United States Of America As Represented By The Secretary Of The Department Of Health And Human Services | Methods for separation and detection of ketosteroids and other carbonyl-containing compounds |
JP2004018474A (en) * | 2002-06-18 | 2004-01-22 | Mitsubishi Chemicals Corp | Method for producing acetal and/or ketal compound and method for producing polyhydric alcohol |
CN102393438A (en) * | 2011-11-10 | 2012-03-28 | 中国检验检疫科学研究院 | Method for simultaneously determining residual quantities of sixteen sensitized aldehyde and ketone perfumes in toy |
CN105044094A (en) * | 2015-06-30 | 2015-11-11 | 重庆市计量质量检测研究院 | Method for measuring methylal in gasoline |
-
2020
- 2020-09-12 CN CN202010956582.6A patent/CN112034072B/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003089921A1 (en) * | 2002-04-15 | 2003-10-30 | The Government Of The United States Of America As Represented By The Secretary Of The Department Of Health And Human Services | Methods for separation and detection of ketosteroids and other carbonyl-containing compounds |
JP2004018474A (en) * | 2002-06-18 | 2004-01-22 | Mitsubishi Chemicals Corp | Method for producing acetal and/or ketal compound and method for producing polyhydric alcohol |
CN102393438A (en) * | 2011-11-10 | 2012-03-28 | 中国检验检疫科学研究院 | Method for simultaneously determining residual quantities of sixteen sensitized aldehyde and ketone perfumes in toy |
CN105044094A (en) * | 2015-06-30 | 2015-11-11 | 重庆市计量质量检测研究院 | Method for measuring methylal in gasoline |
Non-Patent Citations (5)
Title |
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LI JUN LI ET AL.: "Characterization of the Aldehydes and Their Transformations Induced by UV Irradiation and Air Exposure of White Guanxi Honey Pummelo (Citrus Grandis (L.) Osbeck) Essential Oil", 《J. AGRIC. FOOD CHEM.》 * |
周巧玲 等: "HPLC间接测定电氧化合成中的茴香醛二甲基缩醛", 《分析测试学报》 * |
曲国福 等: "气相色谱-质谱联用法测定烟用香精成分", 《理化检验-化学分册》 * |
杨君 等: "超声辅助液液萃取-气相色谱-质谱指纹图谱应用于烟用香精香料的检测", 《理化检验-化学分册》 * |
黄建国 等: "直接稀释进样-气相色谱-质谱法分析烟用香精", 《理化检验-化学分册》 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114199986A (en) * | 2021-12-10 | 2022-03-18 | 河南牧业经济学院 | Method for simultaneously determining 3 aldehyde compounds in beer |
CN114199986B (en) * | 2021-12-10 | 2024-05-07 | 河南牧业经济学院 | Method for simultaneously measuring 3 aldehyde compounds in beer |
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CN112034072B (en) | 2023-05-12 |
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Inventor after: Ma Zhiwei Inventor after: Xu Jun Inventor after: Liu Zhijing Inventor after: Liu Juntao Inventor after: Wang Chuanchuan Inventor after: Ren Cong Inventor after: Ding Degang Inventor after: Hao Jinghao Inventor after: Yang Xinling Inventor after: Wang Jianling Inventor before: Liu Zhijing Inventor before: Xu Jun Inventor before: Ma Zhiwei Inventor before: Liu Juntao Inventor before: Wang Chuanchuan Inventor before: Ren Cong Inventor before: Ding Degang Inventor before: Hao Jinghao Inventor before: Yang Xinling Inventor before: Wang Jianling |
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