CN112030565A - Deep thread sealing slurry line and manufacturing method and manufacturing device thereof - Google Patents
Deep thread sealing slurry line and manufacturing method and manufacturing device thereof Download PDFInfo
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 39
- 239000002002 slurry Substances 0.000 title claims abstract description 31
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- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims abstract description 33
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000006229 carbon black Substances 0.000 claims abstract description 32
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 31
- 238000004513 sizing Methods 0.000 claims abstract description 26
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 25
- 229920002545 silicone oil Polymers 0.000 claims abstract description 25
- 239000011440 grout Substances 0.000 claims abstract description 23
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 15
- 238000001125 extrusion Methods 0.000 claims description 39
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- 239000004205 dimethyl polysiloxane Substances 0.000 claims 1
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- 238000009434 installation Methods 0.000 abstract description 11
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- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 35
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- 238000010521 absorption reaction Methods 0.000 description 14
- 229910052742 iron Inorganic materials 0.000 description 14
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- AMTWCFIAVKBGOD-UHFFFAOYSA-N dioxosilane;methoxy-dimethyl-trimethylsilyloxysilane Chemical compound O=[Si]=O.CO[Si](C)(C)O[Si](C)(C)C AMTWCFIAVKBGOD-UHFFFAOYSA-N 0.000 description 8
- 230000000694 effects Effects 0.000 description 8
- 229940083037 simethicone Drugs 0.000 description 8
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- 229910052751 metal Inorganic materials 0.000 description 2
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- 239000000565 sealant Substances 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
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Images
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
- D06B3/18—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics combined with squeezing, e.g. in padding machines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/74—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon or graphite; with carbides; with graphitic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
- D06M15/09—Cellulose ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Sealing Material Composition (AREA)
Abstract
The invention is suitable for the field of deep pipeline thread sealing materials, and provides a deep thread sealing grout line and a manufacturing method and a manufacturing device thereof, wherein the manufacturing method of the deep thread sealing grout line comprises the following steps: using the sizing agent to extrude and size the chemical fiber filaments to obtain the deep thread sealing sizing line; the slurry comprises the following components in parts by weight: 40-45 parts of dimethyl silicone oil, 30-35 parts of talcum powder, 5-10 parts of white carbon black and 5-10 parts of hydroxypropyl methyl cellulose. The thread sealing size line is prepared by coating corresponding size with the chemical fiber filaments, has the characteristics of wear resistance, self-wetting property, high and low temperature resistance, aging resistance and corrosion resistance, can be used for a long time in a wider temperature range, can not be solidified in the temperature range, keeps the original viscosity and self-wetting property, and has better adhesion in installation.
Description
Technical Field
The invention belongs to the field of deep pipeline thread sealing materials, and particularly relates to a deep thread sealing grout line and a manufacturing method and a manufacturing device thereof.
Background
At present, the widely applied sealing materials in pipeline thread sealing are anaerobic pipeline thread sealing glue, polytetrafluoroethylene raw material belts and thread sealing lines.
However, anaerobic thread sealants have the following disadvantages in the actual installation process: 1. the anaerobic adhesive only has a curing effect on metal; 2. because metal pipelines need to be threaded by a thread forming machine and need to be cooled by lubricating oil or water in the process, the threads are adhered with impurities of the lubricating oil or water, oil stains need to be cleaned when anaerobic adhesive is installed, and the installation efficiency is influenced by increasing the workload; 3. anaerobic thread sealant installation requires up to 24 hours of complete curing (e.g., longer curing time at low air temperature); 4. for example, when the anaerobic thread sealing glue is used for installing the pipe fittings, the residues need to be further treated when the pipe fittings need to be disassembled so as to be installed again.
The raw material belt has the following problems: 1. the existing new pipeline with the depth has sharp tooth lines, and the thread seal tape is cut and damaged during installation, so that the installation and sealing effects of the product are influenced; 2. due to the depth and the height of the thread pitch of the existing large-caliber thread, the sealing effect of the thread seal tape is difficult to achieve and the thread seal tape is very inconvenient to wind; 3. the residues in the use process of the raw material belt are difficult to degrade in nature, so that the environment is polluted.
In contrast, thread sealing lines can avoid the above problems and deficiencies, but existing thread sealing lines also suffer from the following deficiencies: 1. the viscose glue is not uniform on the fiber line; 2. the adhesive force of the sealing line in the thread winding process is insufficient, so that the construction efficiency is influenced; 3. the wettability of the adhesive decreases with time, and the ideal use effect cannot be achieved.
Disclosure of Invention
An embodiment of the present invention provides a method for manufacturing a deep thread sealing grout line, which aims to solve the problems in the background art.
The embodiment of the invention is realized in such a way that the manufacturing method of the deep thread sealing grout line comprises the following steps:
using the sizing agent to extrude and size the chemical fiber filaments to obtain the deep thread sealing sizing line;
the slurry comprises the following components in parts by weight: 40-45 parts of dimethyl silicone oil, 30-35 parts of talcum powder, 5-10 parts of white carbon black and 5-10 parts of hydroxypropyl methyl cellulose.
As a preferable scheme of the embodiment of the invention, the slurry comprises the following components in parts by weight: 42-43 parts of dimethyl silicone oil, 32-33 parts of talcum powder, 7-8 parts of white carbon black and 7-8 parts of hydroxypropyl methyl cellulose.
As another preferable scheme of the embodiment of the invention, the viscosity of the simethicone at 25 ℃ is 8000-12000 cSt.
As another preferable scheme of the embodiment of the invention, the viscosity of the hydroxypropyl methyl cellulose at 25 ℃ is 80000-120000 cSt.
As another preferable scheme of the embodiment of the present invention, the preparation method of the slurry comprises the following steps:
weighing dimethyl silicone oil, talcum powder, white carbon black and hydroxypropyl methyl cellulose according to the weight parts of the components;
mixing talcum powder, white carbon black and hydroxypropyl methyl cellulose to obtain powder;
and mixing the powder material and the dimethyl silicone oil, and homogenizing to obtain the slurry.
As another preferable scheme of the embodiment of the invention, the denier of the chemical fiber filament is 1000-2000D.
As another preferred scheme of the embodiment of the present invention, the chemical fiber filaments are polyester filaments or nylon filaments.
Another object of the present invention is to provide a deep thread sealing grout line manufactured by the above manufacturing method.
As another preferable scheme of the embodiment of the invention, the sealing pressure of the deep thread sealing grout line is not lower than 2.5 MPa.
Another object of an embodiment of the present invention is to provide a manufacturing apparatus for a deep thread sealing grout line, which includes the following steps:
the extrusion die is used for extruding and sizing the chemical fiber filaments;
the paying-off mechanism is used for feeding the chemical fiber filaments into the extrusion die;
the pulp supply mechanism is used for conveying pulp into the extrusion die so as to size the chemical fiber filaments being extruded;
the slurry comprises the following components in parts by weight: 40-45 parts of dimethyl silicone oil, 30-35 parts of talcum powder, 5-10 parts of white carbon black and 5-10 parts of hydroxypropyl methyl cellulose.
According to the manufacturing method of the deep thread sealing grout line provided by the embodiment of the invention, the thread sealing grout line with high viscosity, high strength and excellent sealing property is prepared by coating corresponding grout with chemical fiber filaments, has the characteristics of wear resistance, self-lubricating property, high and low temperature resistance, aging resistance and corrosion resistance, can be used for a long time at the high temperature of 200 ℃ and the low temperature of-50 ℃, can not be solidified in the temperature range, keeps the original viscosity and self-lubricating property, has better adhesion in installation, and is more convenient to install. In addition, the slurry adopted by the invention has strong adhesive force, permeability and good tensile strength, can prevent thread sealing leakage, and the sealing element of the product can be adjusted back within the range of 45 degrees, so that the one-time installation and construction are simple and convenient; meanwhile, the stability can be kept in a vibration environment and the anti-loosening effect is achieved. In addition, the slurry can form a layer of film on the threads, and the film is uniformly filled in the openings of the threads, so that the effect of the current deep tight threads is particularly better, and the method has the advantages of raw material reduction, low cost, high energy efficiency and environmental protection.
Drawings
Fig. 1 is a schematic structural diagram of a manufacturing apparatus for a deep thread sealing grout line according to an embodiment of the present invention.
In the figure, 1-a paying-off mechanism, 2-a guide wheel, 3-a pulp supply high-pressure pipe, 4-an extrusion die, 5-a pulp supply mechanism and 6-a take-up mechanism.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
The experimental methods mentioned in the following examples are all conventional methods unless otherwise specified; the materials and equipment involved, unless otherwise specified, are commercially available.
Example 1
As shown in fig. 1, a schematic structural diagram of a manufacturing apparatus for deep thread sealing grout line provided in an embodiment of the present invention includes:
the extrusion die 4 is used for extruding and sizing the chemical fiber filaments;
the paying-off mechanism 1 is used for feeding the chemical fiber filaments into the extrusion die 4;
and the size supply mechanism 5 is used for conveying size to the extrusion die 4 so as to size the chemical fiber filaments being extruded.
The slurry supply mechanism 5 can comprise a slurry supply barrel and a plunger pump, and the slurry supply barrel can be communicated with the extrusion die 4 through the plunger pump and the slurry supply high-pressure pipe 3; a guide wheel 2 can be arranged between the pay-off mechanism 1 and the extrusion die 4, so that the chemical fiber filaments can be stably conveyed to the extrusion die 4 for extrusion sizing.
In addition, the manufacturing device can also comprise a take-up mechanism 6 for taking up the deep thread sealing slurry wire after the extrusion sizing treatment. In practical application, through admission machine 6, paying out machine constructs 1 and leading wheel 2 can make chemical fibre filament move and be extruded in extrusion die 4, simultaneously, can be with thick liquids propelling movement to extrusion die 4 in through supplying thick liquids mechanism 5, whole chemical fibre filament is in thick liquids center cladding filament and passes through 1.0 mm's die nozzle again, the die nozzle plays the outside of thick liquids full circle extrusion thick liquids cladding in filament, and then makes thick liquids firmly the cladding around chemical fibre filament to form degree of depth thread sealing thick liquid line.
Example 2
This embodiment provides a method of manufacturing a deep thread sealing compound line using the manufacturing apparatus provided in embodiment 1 above, comprising the steps of:
s1, weighing 42.5kg of simethicone, 3.25kg of talcum powder, 0.75kg of white carbon black and hydroxypropyl methyl fiber0.75kg of vitamin for standby. Wherein the viscosity of the dimethyl silicone oil at 25 ℃ is 10000cSt, the appearance is colorless transparent oily liquid, and the relative density is 0.971-0.976; acid-insoluble substance of pulvis Talci no less than 90.0%, and acid-soluble iron (in the form of Fe)2O3Calculated) is less than or equal to 0.02 percent, the ignition loss (1000 ℃) is less than or equal to 6.00 percent, the magnet absorption is less than or equal to 0.04 percent, the water content is less than or equal to 0.5 percent, the granularity is 5000 meshes, and the whiteness is>93, the pH value is 8-10; SiO in white carbon black2The content (dry product) is more than or equal to 90 percent, the screen residue (45 mu m) is less than or equal to 0.5 percent, the heating decrement is 4.0 to 8.0 percent, the ignition decrement (dry product) is less than or equal to 7.0 percent, the pH value is 5.0 to 8.0, the total copper content is less than or equal to 30mg/kg, the total manganese content is less than or equal to 50mg/kg, the total iron content is less than or equal to 1000mg/kg, and the DBP absorption value is 2.00 to 3.50 cm/g; particle size of hydroxypropylmethylcellulose: the 100-mesh passing rate is more than 98.5 percent, the 80-mesh passing rate is 100 percent, the pH value is 5.0-8.0, and the viscosity at 25 ℃ is 100000 cSt.
S2, placing the weighed talcum powder, white carbon black and hydroxypropyl methyl cellulose into a mixer to be stirred and mixed to obtain powder.
And S3, mixing the powder and the dimethyl silicone oil in a high-speed dispersion mixer, centrifugally extruding a liquid layer through strong centrifugal force, blending, homogenizing, and fully dispersing and stirring to obtain the slurry.
S4, as shown in the attached drawing 1, the 2000D chemical fiber filament is sent to the extrusion die 4 for extrusion through the guide wheel 2 of the pay-off mechanism 1, meanwhile, the pulp is sent to the extrusion die 4 through the pulp supply mechanism 5, so that the pulp is firmly coated on the chemical fiber filament, and then, the take-up mechanism 6 is used for taking up the thread, so that the deep thread sealing pulp thread can be obtained. Wherein, the chemical fiber filament is a polyester filament with the strength of 8.2G/D.
Example 3
This embodiment provides a method of manufacturing a deep thread sealing compound line using the manufacturing apparatus provided in embodiment 1 above, comprising the steps of:
s1, weighing 4kg of simethicone, 3.5kg of talcum powder, 1kg of white carbon black and 1kg of hydroxypropyl methyl cellulose for later use. Wherein the viscosity of the dimethyl silicone oil at 25 ℃ is 8000cSt, the appearance is colorless transparent oily liquid, and the relative density is 0.971-0.976; talcum powderAcid-insoluble substance of not less than 90.0%, and acid-soluble iron (in the form of Fe)2O3Calculated) is less than or equal to 0.02 percent, the ignition loss (1000 ℃) is less than or equal to 6.00 percent, the magnet absorption is less than or equal to 0.04 percent, the water content is less than or equal to 0.5 percent, the granularity is 5000 meshes, and the whiteness is>93, the pH value is 8-10; SiO in white carbon black2The content (dry product) is more than or equal to 90 percent, the screen residue (45 mu m) is less than or equal to 0.5 percent, the heating decrement is 4.0 to 8.0 percent, the ignition decrement (dry product) is less than or equal to 7.0 percent, the pH value is 5.0 to 8.0, the total copper content is less than or equal to 30mg/kg, the total manganese content is less than or equal to 50mg/kg, the total iron content is less than or equal to 1000mg/kg, and the DBP absorption value is 2.00 to 3.50 cm/g; particle size of hydroxypropylmethylcellulose: the 100-mesh passing rate is more than 98.5 percent, the 80-mesh passing rate is 100 percent, the pH value is 5.0-8.0, and the viscosity at 25 ℃ is 80000 cSt.
S2, placing the weighed talcum powder, white carbon black and hydroxypropyl methyl cellulose into a mixer to be stirred and mixed to obtain powder.
And S3, mixing the powder and the dimethyl silicone oil in a high-speed dispersion mixer, centrifugally extruding a liquid layer through strong centrifugal force, blending, homogenizing, and fully dispersing and stirring to obtain the slurry.
S4, as shown in the attached drawing 1, sending 1000D chemical fiber filaments to an extrusion die 4 for extrusion through a guide wheel 2 of a pay-off mechanism 1, sending sizing agent to the extrusion die 4 through a sizing agent supply mechanism 5 so that the sizing agent is firmly coated on the chemical fiber filaments, and then taking up through a take-up mechanism 6 to obtain the deep thread sealing sizing agent line. Wherein, the chemical fiber filament is a nylon filament, and the strength of the nylon filament is 8.2G/D.
Example 4
This embodiment provides a method of manufacturing a deep thread sealing compound line using the manufacturing apparatus provided in embodiment 1 above, comprising the steps of:
s1, weighing 4.5kg of simethicone, 3kg of talcum powder, 0.5kg of white carbon black and 0.5kg of hydroxypropyl methyl cellulose for later use. Wherein the viscosity of the dimethyl silicone oil at 25 ℃ is 12000cSt, the appearance is colorless transparent oily liquid, and the relative density is 0.971-0.976; acid-insoluble substance of pulvis Talci no less than 90.0%, and acid-soluble iron (in the form of Fe)2O3Is less than or equal to 0.02 percent, the ignition loss (1000 ℃) is less than or equal to 6.00 percent, the magnet absorption is less than or equal to 0.04 percent, and the water contentNot more than 0.5%, granularity of 5000 meshes, whiteness>93, the pH value is 8-10; SiO in white carbon black2The content (dry product) is more than or equal to 90 percent, the screen residue (45 mu m) is less than or equal to 0.5 percent, the heating decrement is 4.0 to 8.0 percent, the ignition decrement (dry product) is less than or equal to 7.0 percent, the pH value is 5.0 to 8.0, the total copper content is less than or equal to 30mg/kg, the total manganese content is less than or equal to 50mg/kg, the total iron content is less than or equal to 1000mg/kg, and the DBP absorption value is 2.00 to 3.50 cm/g; particle size of hydroxypropylmethylcellulose: the 100-mesh passing rate is more than 98.5 percent, the 80-mesh passing rate is 100 percent, the pH value is 5.0-8.0, and the viscosity at 25 ℃ is 120000 cSt.
S2, placing the weighed talcum powder, white carbon black and hydroxypropyl methyl cellulose into a mixer to be stirred and mixed to obtain powder.
And S3, mixing the powder and the dimethyl silicone oil in a high-speed dispersion mixer, centrifugally extruding a liquid layer through strong centrifugal force, blending, homogenizing, and fully dispersing and stirring to obtain the slurry.
S4, as shown in the attached drawing 1, the 2000D chemical fiber filament is sent to the extrusion die 4 for extrusion through the guide wheel 2 of the pay-off mechanism 1, meanwhile, the pulp is sent to the extrusion die 4 through the pulp supply mechanism 5, so that the pulp is firmly coated on the chemical fiber filament, and then, the take-up mechanism 6 is used for taking up the thread, so that the deep thread sealing pulp thread can be obtained. Wherein, the chemical fiber filament is a nylon filament, and the strength of the nylon filament is 8.2G/D.
Example 5
This embodiment provides a method of manufacturing a deep thread sealing compound line using the manufacturing apparatus provided in embodiment 1 above, comprising the steps of:
s1, weighing 4.2kg of simethicone, 3.3kg of talcum powder, 0.8kg of white carbon black and 0.8kg of hydroxypropyl methyl cellulose for later use. Wherein the viscosity of the dimethyl silicone oil at 25 ℃ is 10000cSt, the appearance is colorless transparent oily liquid, and the relative density is 0.971-0.976; acid-insoluble substance of pulvis Talci no less than 90.0%, and acid-soluble iron (in the form of Fe)2O3Calculated) is less than or equal to 0.02 percent, the ignition loss (1000 ℃) is less than or equal to 6.00 percent, the magnet absorption is less than or equal to 0.04 percent, the water content is less than or equal to 0.5 percent, the granularity is 5000 meshes, and the whiteness is>93, the pH value is 8-10; SiO in white carbon black2The content (dry product) is more than or equal to 90 percent, the residue on sieve (45 mu m) is less than or equal to 0.5 percent, and the mixture is heatedThe decrement is 4.0-8.0%, the ignition decrement (dry product) is less than or equal to 7.0%, the pH value is 5.0-8.0, the total copper content is less than or equal to 30mg/kg, the total manganese content is less than or equal to 50mg/kg, the total iron content is less than or equal to 1000mg/kg, and the DBP absorption value is 2.00-3.50 cm/g; particle size of hydroxypropylmethylcellulose: the 100-mesh passing rate is more than 98.5 percent, the 80-mesh passing rate is 100 percent, the pH value is 5.0-8.0, and the viscosity at 25 ℃ is 100000 cSt.
S2, placing the weighed talcum powder, white carbon black and hydroxypropyl methyl cellulose into a mixer to be stirred and mixed to obtain powder.
And S3, mixing the powder and the dimethyl silicone oil in a high-speed dispersion mixer, centrifugally extruding a liquid layer through strong centrifugal force, blending, homogenizing, and fully dispersing and stirring to obtain the slurry.
S4, as shown in the attached drawing 1, sending 1500D chemical fiber filaments to an extrusion die 4 for extrusion through a guide wheel 2 of a pay-off mechanism 1, sending sizing agent to the extrusion die 4 through a sizing agent supply mechanism 5 so that the sizing agent is firmly coated on the chemical fiber filaments, and then taking up through a take-up mechanism 6 to obtain the deep thread sealing sizing agent line. Wherein, the chemical fiber filament is a polyester filament with the strength of 8.2G/D.
Example 6
This embodiment provides a method of manufacturing a deep thread sealing compound line using the manufacturing apparatus provided in embodiment 1 above, comprising the steps of:
s1, weighing 4.3kg of simethicone, 3.2kg of talcum powder, 0.7kg of white carbon black and 0.7kg of hydroxypropyl methyl cellulose for later use. Wherein the viscosity of the dimethyl silicone oil at 25 ℃ is 10000cSt, the appearance is colorless transparent oily liquid, and the relative density is 0.971-0.976; acid-insoluble substance of pulvis Talci no less than 90.0%, and acid-soluble iron (in the form of Fe)2O3Calculated) is less than or equal to 0.02 percent, the ignition loss (1000 ℃) is less than or equal to 6.00 percent, the magnet absorption is less than or equal to 0.04 percent, the water content is less than or equal to 0.5 percent, the granularity is 5000 meshes, and the whiteness is>93, the pH value is 8-10; SiO in white carbon black2The content (dry product) is more than or equal to 90 percent, the screen residue (45 mu m) is less than or equal to 0.5 percent, the heating decrement is 4.0 to 8.0 percent, the ignition decrement (dry product) is less than or equal to 7.0 percent, the pH value is 5.0 to 8.0, the total copper content is less than or equal to 30mg/kg, the total manganese content is less than or equal to 50mg/kg, and the total iron content is less than or equal to 1000mg/kgKg, the DBP absorption value is 2.00-3.50 cm/g; particle size of hydroxypropylmethylcellulose: the 100-mesh passing rate is more than 98.5 percent, the 80-mesh passing rate is 100 percent, the pH value is 5.0-8.0, and the viscosity at 25 ℃ is 100000 cSt.
S2, placing the weighed talcum powder, white carbon black and hydroxypropyl methyl cellulose into a mixer to be stirred and mixed to obtain powder.
And S3, mixing the powder and the dimethyl silicone oil in a high-speed dispersion mixer, centrifugally extruding a liquid layer through strong centrifugal force, blending, homogenizing, and fully dispersing and stirring to obtain the slurry.
S4, as shown in the attached drawing 1, sending 1500D chemical fiber filaments to an extrusion die 4 for extrusion through a guide wheel 2 of a pay-off mechanism 1, sending sizing agent to the extrusion die 4 through a sizing agent supply mechanism 5 so that the sizing agent is firmly coated on the chemical fiber filaments, and then taking up through a take-up mechanism 6 to obtain the deep thread sealing sizing agent line. Wherein, the chemical fiber filament is a polyester filament with the strength of 8.2G/D.
Comparative example 1
This comparative example provides a method of manufacturing a thread sealing compound line using the manufacturing apparatus provided in example 1 above, comprising the steps of:
s1, weighing 58kg of simethicone, 12kg of talcum powder, 0.75kg of white carbon black and 0.75kg of hydroxypropyl methyl cellulose for later use. Wherein the viscosity of the dimethyl silicone oil at 25 ℃ is 10000cSt, the appearance is colorless transparent oily liquid, and the relative density is 0.971-0.976; acid-insoluble substance of pulvis Talci no less than 90.0%, and acid-soluble iron (in the form of Fe)2O3Calculated) is less than or equal to 0.02 percent, the ignition loss (1000 ℃) is less than or equal to 6.00 percent, the magnet absorption is less than or equal to 0.04 percent, the water content is less than or equal to 0.5 percent, the granularity is 5000 meshes, and the whiteness is>93, the pH value is 8-10; SiO in white carbon black2The content (dry product) is more than or equal to 90 percent, the screen residue (45 mu m) is less than or equal to 0.5 percent, the heating decrement is 4.0 to 8.0 percent, the ignition decrement (dry product) is less than or equal to 7.0 percent, the pH value is 5.0 to 8.0, the total copper content is less than or equal to 30mg/kg, the total manganese content is less than or equal to 50mg/kg, the total iron content is less than or equal to 1000mg/kg, and the DBP absorption value is 2.00 to 3.50 cm/g; particle size of hydroxypropylmethylcellulose: the 100-mesh passing rate is more than 98.5 percent, the 80-mesh passing rate is 100 percent, and the pH value of the solution is 5.0-80, viscosity at 25 ℃ of 100000 cSt.
S2, placing the weighed talcum powder, white carbon black and hydroxypropyl methyl cellulose into a mixer to be stirred and mixed to obtain powder.
And S3, mixing the powder and the dimethyl silicone oil in a high-speed dispersion mixer, centrifugally extruding a liquid layer through strong centrifugal force, blending, homogenizing, and fully dispersing and stirring to obtain the slurry.
S4, as shown in the attached drawing 1, the 2000D chemical fiber filament is sent to the extrusion die 4 for extrusion through the guide wheel 2 of the pay-off mechanism 1, meanwhile, the pulp is sent to the extrusion die 4 through the pulp supply mechanism 5, so that the pulp is firmly coated on the chemical fiber filament, and then, the thread sealing pulp line can be obtained through the take-up mechanism 6 for taking up. Wherein, the chemical fiber filament is a polyester filament with the strength of 8.2G/D.
Comparative example 2
This comparative example provides a method of manufacturing a thread sealing compound line using the manufacturing apparatus provided in example 1 above, comprising the steps of:
s1, weighing 37kg of simethicone, 23kg of talcum powder, 0.75kg of white carbon black and 0.75kg of hydroxypropyl methyl cellulose for later use. Wherein the viscosity of the dimethyl silicone oil at 25 ℃ is 10000cSt, the appearance is colorless transparent oily liquid, and the relative density is 0.971-0.976; acid-insoluble substance of pulvis Talci no less than 90.0%, and acid-soluble iron (in the form of Fe)2O3Calculated) is less than or equal to 0.02 percent, the ignition loss (1000 ℃) is less than or equal to 6.00 percent, the magnet absorption is less than or equal to 0.04 percent, the water content is less than or equal to 0.5 percent, the granularity is 5000 meshes, and the whiteness is>93, the pH value is 8-10; SiO in white carbon black2The content (dry product) is more than or equal to 90 percent, the screen residue (45 mu m) is less than or equal to 0.5 percent, the heating decrement is 4.0 to 8.0 percent, the ignition decrement (dry product) is less than or equal to 7.0 percent, the pH value is 5.0 to 8.0, the total copper content is less than or equal to 30mg/kg, the total manganese content is less than or equal to 50mg/kg, the total iron content is less than or equal to 1000mg/kg, and the DBP absorption value is 2.00 to 3.50 cm/g; particle size of hydroxypropylmethylcellulose: the 100-mesh passing rate is more than 98.5 percent, the 80-mesh passing rate is 100 percent, the pH value is 5.0-8.0, and the viscosity at 25 ℃ is 100000 cSt.
S2, placing the weighed talcum powder, white carbon black and hydroxypropyl methyl cellulose into a mixer to be stirred and mixed to obtain powder.
And S3, mixing the powder and the dimethyl silicone oil in a high-speed dispersion mixer, centrifugally extruding a liquid layer through strong centrifugal force, blending, homogenizing, and fully dispersing and stirring to obtain the slurry.
S4, as shown in the attached drawing 1, the 2000D chemical fiber filament is sent to the extrusion die 4 for extrusion through the guide wheel 2 of the pay-off mechanism 1, meanwhile, the pulp is sent to the extrusion die 4 through the pulp supply mechanism 5, so that the pulp is firmly coated on the chemical fiber filament, and then, the thread sealing pulp line can be obtained through the take-up mechanism 6 for taking up. Wherein, the chemical fiber filament is a polyester filament with the strength of 8.2G/D.
Experimental example:
firstly, the sizing rate of the thread sealing grout lines prepared in the example 1 and the comparative examples 1 to 2 is tested, and the physical and chemical properties of the grout prepared in the example 1 and the comparative examples 1 to 2 are tested, and the test results are shown in table 1.
TABLE 1
Secondly, the thread sealing grout line prepared in the embodiment 1 has the following characteristics:
1. under the twisting acting force of the installation connecting thread, the slurry of the slurry line flows in the tooth wall of the threaded pipe to form a layer of stable sealing film, and the good flexible sealing filling effect is achieved on the tooth line gap. The resultant force of the slurry and the components is uniform, the lubricating property is good, the elasticity is good, the vibration is resistant, the slurry is uniform and firm, the slurry is stable and can not be solidified, and the pipeline can not be blocked.
2. The product is wide in application applicability, has no material requirement on pipeline thread materials, can be used as long as the pipeline threads meeting the national standard, is simple and convenient to construct, does not need to clean standard workpieces in a complicated way before installation, is simple to operate, can be installed by using an ordinary wrench and pipeline tools, is simple to install and construct, is not controlled by operation time, and is time-saving, labor-saving and convenient to install and use.
3. After the product is installed stably, the product can be adjusted back within the range of 45 degrees, leakage cannot occur, and the installation and the use are convenient.
4. The main materials and the ingredients of the product are environment-friendly and nontoxic, the product is oil-resistant, water-resistant and medium-resistant, safe and sanitary, does not pollute the environment and pipeline media, does not corrode pipeline pipe fittings, can be used for a long time at the high temperature of 200 ℃ and the low temperature of 50 ℃ below zero, can be widely applied to the industries of heating ventilation, gas, water supply and the like, and has wide adaptability.
5. The simple production process is energy-saving and environment-friendly.
6. The product has high sealing pressure, can resist more than 2.5MPa, and meets the requirements of water and gas supply pipelines (the fire-fighting pressure test standard is 1.6MPa, and the water pressure test standard is 1.0 MPa).
7. The product integrates the advantages of hemp thread, lead oil, raw material belt and anaerobic adhesive in the current market, and has more reliable sealing effect and more convenient installation.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the present invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (10)
1. A manufacturing method of a deep thread sealing grout line is characterized by comprising the following steps:
using the sizing agent to extrude and size the chemical fiber filaments to obtain the deep thread sealing sizing line;
the slurry comprises the following components in parts by weight: 40-45 parts of dimethyl silicone oil, 30-35 parts of talcum powder, 5-10 parts of white carbon black and 5-10 parts of hydroxypropyl methyl cellulose.
2. The method of claim 1, wherein the slurry comprises the following components in parts by weight: 42-43 parts of dimethyl silicone oil, 32-33 parts of talcum powder, 7-8 parts of white carbon black and 7-8 parts of hydroxypropyl methyl cellulose.
3. The method of claim 1, wherein the dimethicone has a viscosity of 8000 to 12000cSt at 25 ℃.
4. The method for manufacturing the deep thread sealing sizing wire according to claim 1, wherein the viscosity of the hydroxypropyl methyl cellulose at 25 ℃ is 80000-120000 cSt.
5. The method for manufacturing the deep thread sealing grout line according to any one of claims 1 to 4, wherein the preparation method of the grout comprises the following steps:
weighing dimethyl silicone oil, talcum powder, white carbon black and hydroxypropyl methyl cellulose according to the weight parts of the components;
mixing talcum powder, white carbon black and hydroxypropyl methyl cellulose to obtain powder;
and mixing the powder material and the dimethyl silicone oil, and homogenizing to obtain the slurry.
6. The method for manufacturing the deep thread sealing sizing thread according to claim 1, wherein the denier of the chemical fiber filament is 1000-2000D.
7. The method for manufacturing the deep thread sealing size thread according to claim 1 or 6, wherein the chemical fiber filament is a polyester filament or a nylon filament.
8. A deep thread sealing grout line prepared by the manufacturing method according to any one of claims 1 to 7.
9. A deep thread sealing grout line according to claim 8, wherein the sealing pressure of the deep thread sealing grout line is not less than 2.5 MPa.
10. A manufacturing device of a deep thread sealing grout line is characterized by comprising the following steps:
the extrusion die is used for extruding and sizing the chemical fiber filaments;
the paying-off mechanism is used for feeding the chemical fiber filaments into the extrusion die;
the pulp supply mechanism is used for conveying pulp into the extrusion die so as to size the chemical fiber filaments being extruded;
the slurry comprises the following components in parts by weight: 40-45 parts of dimethyl silicone oil, 30-35 parts of talcum powder, 5-10 parts of white carbon black and 5-10 parts of hydroxypropyl methyl cellulose.
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| CN1826276A (en) * | 2003-07-18 | 2006-08-30 | 菲尔福莱克斯有限公司 | Novel system for the gasket sealing of screwed connections in pipes for the conveyance of fluids and applicator device for same |
| CN101696551A (en) * | 2009-10-30 | 2010-04-21 | 曾燕飞 | Method for making high-intensity thread seal thread |
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| CN107109708A (en) * | 2014-10-31 | 2017-08-29 | 约瑟夫·巴赫迈尔 | Encapsulant for threaded connection |
| CN109027223A (en) * | 2018-06-15 | 2018-12-18 | 岱山县联合汽车配件制造有限公司 | High-performance rubber composite seal and its manufacturing method |
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|---|---|---|---|---|
| CN1826276A (en) * | 2003-07-18 | 2006-08-30 | 菲尔福莱克斯有限公司 | Novel system for the gasket sealing of screwed connections in pipes for the conveyance of fluids and applicator device for same |
| CN201502703U (en) * | 2009-10-16 | 2010-06-09 | 房全力 | Thread sealing string |
| CN101696551A (en) * | 2009-10-30 | 2010-04-21 | 曾燕飞 | Method for making high-intensity thread seal thread |
| CN107109708A (en) * | 2014-10-31 | 2017-08-29 | 约瑟夫·巴赫迈尔 | Encapsulant for threaded connection |
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