CN111990452A - Aquatic product coating preservation solution carrying burdock polyphenol and preparation and use methods thereof - Google Patents
Aquatic product coating preservation solution carrying burdock polyphenol and preparation and use methods thereof Download PDFInfo
- Publication number
- CN111990452A CN111990452A CN202010741507.8A CN202010741507A CN111990452A CN 111990452 A CN111990452 A CN 111990452A CN 202010741507 A CN202010741507 A CN 202010741507A CN 111990452 A CN111990452 A CN 111990452A
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- Prior art keywords
- burdock
- polyphenol
- lipid
- aquatic product
- solution
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Links
- 235000003130 Arctium lappa Nutrition 0.000 title claims abstract description 84
- 235000008078 Arctium minus Nutrition 0.000 title claims abstract description 84
- 235000013824 polyphenols Nutrition 0.000 title claims abstract description 70
- 150000008442 polyphenolic compounds Chemical class 0.000 title claims abstract description 69
- 239000011248 coating agent Substances 0.000 title claims abstract description 44
- 238000000576 coating method Methods 0.000 title claims abstract description 44
- 238000000034 method Methods 0.000 title claims abstract description 33
- 239000003761 preservation solution Substances 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 240000005528 Arctium lappa Species 0.000 title 1
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- 150000002632 lipids Chemical class 0.000 claims abstract description 83
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- 239000003995 emulsifying agent Substances 0.000 claims abstract description 21
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 20
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- OKMWKBLSFKFYGZ-UHFFFAOYSA-N 1-behenoylglycerol Chemical compound CCCCCCCCCCCCCCCCCCCCCC(=O)OCC(O)CO OKMWKBLSFKFYGZ-UHFFFAOYSA-N 0.000 claims description 4
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 4
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 4
- 239000005642 Oleic acid Substances 0.000 claims description 4
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- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 4
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 4
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- HVUMOYIDDBPOLL-XWVZOOPGSA-N Sorbitan monostearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O HVUMOYIDDBPOLL-XWVZOOPGSA-N 0.000 claims description 3
- LWZFANDGMFTDAV-BURFUSLBSA-N [(2r)-2-[(2r,3r,4s)-3,4-dihydroxyoxolan-2-yl]-2-hydroxyethyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O LWZFANDGMFTDAV-BURFUSLBSA-N 0.000 claims description 3
- 239000001110 calcium chloride Substances 0.000 claims description 3
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 3
- 239000003240 coconut oil Substances 0.000 claims description 3
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- 239000002285 corn oil Substances 0.000 claims description 3
- 235000021323 fish oil Nutrition 0.000 claims description 3
- 238000004108 freeze drying Methods 0.000 claims description 3
- 239000008172 hydrogenated vegetable oil Substances 0.000 claims description 3
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims description 3
- 235000021313 oleic acid Nutrition 0.000 claims description 3
- 239000002540 palm oil Substances 0.000 claims description 3
- 229920000136 polysorbate Polymers 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 3
- ARIWANIATODDMH-UHFFFAOYSA-N rac-1-monolauroylglycerol Chemical compound CCCCCCCCCCCC(=O)OCC(O)CO ARIWANIATODDMH-UHFFFAOYSA-N 0.000 claims description 3
- 235000011067 sorbitan monolaureate Nutrition 0.000 claims description 3
- 239000003549 soybean oil Substances 0.000 claims description 3
- 235000012424 soybean oil Nutrition 0.000 claims description 3
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- 238000004321 preservation Methods 0.000 description 9
- 241000143060 Americamysis bahia Species 0.000 description 6
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 230000001580 bacterial effect Effects 0.000 description 4
- 239000007908 nanoemulsion Substances 0.000 description 4
- 239000000341 volatile oil Substances 0.000 description 4
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- 238000007254 oxidation reaction Methods 0.000 description 3
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- RVBUGGBMJDPOST-UHFFFAOYSA-N 2-thiobarbituric acid Chemical compound O=C1CC(=O)NC(=S)N1 RVBUGGBMJDPOST-UHFFFAOYSA-N 0.000 description 2
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- 229910019142 PO4 Inorganic materials 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
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- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
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- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 2
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- XTJKNGLLPGBHHO-HNNXBMFYSA-N (2s)-5-(diaminomethylideneamino)-2-(dodecanoylamino)pentanoic acid Chemical compound CCCCCCCCCCCC(=O)N[C@H](C(O)=O)CCCN=C(N)N XTJKNGLLPGBHHO-HNNXBMFYSA-N 0.000 description 1
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 229930182827 D-tryptophan Natural products 0.000 description 1
- QIVBCDIJIAJPQS-SECBINFHSA-N D-tryptophane Chemical compound C1=CC=C2C(C[C@@H](N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-SECBINFHSA-N 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
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- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
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- 229930003268 Vitamin C Natural products 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
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- 235000010323 ascorbic acid Nutrition 0.000 description 1
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- 231100000956 nontoxicity Toxicity 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 150000007965 phenolic acids Chemical class 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920000747 poly(lactic acid) Polymers 0.000 description 1
- 239000004626 polylactic acid Substances 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000017854 proteolysis Effects 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 1
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 1
- 229940048086 sodium pyrophosphate Drugs 0.000 description 1
- 235000019832 sodium triphosphate Nutrition 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000013268 sustained release Methods 0.000 description 1
- 239000012730 sustained-release form Substances 0.000 description 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/10—Coating with a protective layer; Compositions or apparatus therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Nutrition Science (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Microbiology (AREA)
- Storage Of Fruits Or Vegetables (AREA)
Abstract
The invention discloses an aquatic product coating preservation solution carrying burdock polyphenol and a preparation and use method thereof, the preparation method comprises the steps of firstly preparing burdock polyphenol, then preparing a burdock polyphenol nanostructured lipid carrier by using the prepared burdock polyphenol, composite lipid, an emulsifying agent and water as raw materials, wherein in the composite lipid, liquid lipid accounts for 20-60% of the total mass of the composite lipid, and finally preparing the aquatic product coating preservation solution carrying burdock polyphenol by using the prepared burdock polyphenol nanostructured lipid carrier, sodium alginate, glycerol and fish skin collagen as raw materials. The nano-structure lipid carrier is in a crystalline solid sphere shape, and the carried polyphenol is positioned in internal defect lattices, so that the stability and the slow release performance are better, the antioxidant and antibacterial effects can be exerted more durably, and the effect of delaying the quality deterioration of aquatic products in links of storage, transportation, sale and the like is achieved.
Description
Technical Field
The invention relates to an aquatic product coating preservation solution carrying burdock polyphenol and a preparation method and a use method thereof, belonging to the technical field of food preservation processing.
Background
The processed aquatic products have high water activity, rich nutrient components and strong in-vivo enzyme activity, and are easy to generate the phenomena of protein degradation, fat oxidation and bacterial breeding during storage, transportation and sale, so that the putrefaction and the deterioration are caused, and the commercial value of the processed aquatic products is seriously influenced. How to adopt natural, green and safe technical means to effectively delay the decrease of the edible quality and the safe quality of processed aquatic products is a research hotspot in the field of food preservation at present.
The coating preservation takes macromolecules (such as polysaccharide, protein, lipid and the like) as materials, and plasticizers, cross-linking agents and the like are added to cover the surfaces of aquatic products in a wrapping or coating mode so as to achieve the effects of water resistance, air permeability, bacteria resistance and the like. In order to further improve the preservation effect of the composite coating, researchers usually strengthen the functions of the composite coating by natural active molecules such as essential oil, vitamin C and the like, so as to inhibit the oxidation and bacterial reproduction of aquatic products. In the practical application process, the active ingredients in the coating film are chemically degraded and easily diffused to the surrounding environment, thereby causing the loss of the efficacy of the coating film.
Patent CN201911140310.2 discloses a preservative film for biological preservation of aquatic products, which adopts D-tryptophan/polylactic acid and sodium chloride to compound, thereby destroying bacterial biofilm and inhibiting bacterial growth. However, the coating film prepared by this technique has a low content of antioxidant active substances, thereby impairing the freshness-retaining effect. Patent CN201711326317.4 discloses an aquatic product preservative mainly comprising sodium hexametaphosphate, sodium tripolyphosphate, sodium pyrophosphate, ascorbic acid, glycerol and other components. The technology relates to the use of phosphate, which is easy to migrate into the muscle tissue of aquatic products, and the ingestion of a large amount of phosphate can increase health risks. Patent CN201810431028.9 discloses a composite fresh-keeping coating liquid for aquatic products, a preparation method and a use method thereof, which comprises 0.5-2% of chitosan, 0.5-2% of lauroyl arginine ethyl ester hydrochloride, 0.5-2% of essential oil, 0.5-1% of grease and the balance of distilled water. In the method, the essential oil is not encapsulated by microencapsulation, but the oil is mixed and dispersed in the preservative film. Therefore, essential oils are easily volatilized and diffused, not taking advantage of the maintenance of their efficacy; patent CN201910162654.7 discloses a preparation method of a tea polyphenol liposome/lysozyme-chitosan slow-release coating film applied to fish slice preservation, and the related polyphenol liposome is of a double-layer film structure and has strong fluidity.
Disclosure of Invention
The nano-structure lipid carrier is a nano delivery system which takes solid/liquid mixed lipid as a matrix and generates a defect structure in the crystallization process by utilizing the mixed lipid to carry active molecules. Different from common lipid delivery systems such as nano emulsion, pickering emulsion and the like, the lipid matrix of the nano-structured lipid carrier is solid at room temperature, so that the steady protection and the sustained release control of the embedded molecules can be more effectively realized. In addition, the nano-structure lipid carrier has good degradability and biocompatibility, high safety and no toxicity to food. The burdock is a traditional economic crop for food and medicine, and has rich phenolic acid, flavonol and other polyphenol compounds and obvious antioxidant and antibacterial effects. The invention discloses a preparation method and a use method of a coating preservation solution taking a nanostructure lipid carrier carrying burdock polyphenol as a main functional component, and provides a new solution for maintaining the quality of aquatic products. The specific technical scheme of the invention is as follows:
a preparation method of an aquatic product coating preservation solution carrying burdock polyphenol comprises the following steps:
step 1: preparing the burdock polyphenol by using the raw materials,
step 2: preparing the burdock polyphenol nanostructured lipid carrier by using the burdock polyphenol prepared in the step 1, composite lipid, emulsifier and water as raw materials, wherein in the composite lipid, liquid lipid accounts for 20-60% of the total mass of the composite lipid,
and step 3: and (3) preparing the coating preservation solution for the aquatic products by taking the burdock polyphenol nanostructured lipid carrier prepared in the step (2), sodium alginate, glycerol and fish skin collagen as raw materials.
Further, the specific operation of step 1 is as follows,
step 1.1: slicing fresh radix Arctii, blanching in boiling water for 10-15s, taking out, draining,
step 1.2: drying the burdock root slices with water drained in an oven at 40-50 ℃,
step 1.3: slicing dried radix Arctii, pulverizing, sieving with 40 mesh sieve to obtain radix Arctii powder,
step 1.4: mixing burdock root powder and 40-60% ethanol according to the volume fraction of 1: (10-30) (g/mL) to obtain a mixed solution, performing reflux extraction on the mixed solution at 50-60 ℃ for 2-3h until the reflux is finished,
step 1.5: and (3) removing the organic solvent from the mixed solution in negative pressure, and freeze-drying to obtain the burdock polyphenol.
Further, the specific operation of step 2 is as follows,
step 2.1: taking the raw materials according to the following mass percentages: 0.05% -0.2%, complex lipid: 5 to 30 percent; emulsifier: 5 to 10 percent; the balance of water,
step 2.2: weighing solid lipid and liquid lipid according to a set mass ratio, mixing to obtain composite lipid, heating the composite lipid at 90 deg.C to melt the composite lipid,
step 2.3: adding Burdock polyphenol into molten compound lipid until dissolving to obtain oil phase,
step 2.4: taking the emulsifier, placing the emulsifier in water until the emulsifier is completely dissolved, then placing the emulsifier at 90 ℃ for preheating to obtain a water phase,
step 2.5: adding the water phase into the oil phase under 10000-12000rpm high-speed homogenization conditions, continuing to homogenize for 3-5min to obtain a primary emulsion,
step 2.6: carrying out high-intensity ultrasonic treatment on the primary emulsion for 10-15min to obtain the nano-structured lipid carrier, wherein the temperature of the sample is maintained at 90 ℃ in the whole operation process of the step 2.5 and the step 2.6,
step 2.7: and (3) placing the prepared nano-structured lipid carrier in an ice water bath to cool to room temperature for later use.
Further, the specific operation of step 3 is as follows,
step 3.1: dissolving sodium alginate in distilled water to prepare sodium alginate solution with mass concentration of 2-4%,
step 3.2: according to the weight percentage of sodium alginate: glycerol: the mass ratio of the fish skin collagen is 100: (30-50): (10-20) weighing glycerol and fish skin collagen,
step 3.3: adding the weighed glycerol and the fish skin collagen into the sodium alginate solution, stirring to form a film forming solution,
step 3.4: and (3) mixing the nano-structure lipid carrier prepared in the step (2) with the film forming solution according to the volume ratio of (5-10) to 100, then homogenizing at high speed to obtain the aquatic product film coating preservation solution, and degassing the aquatic product film coating preservation solution for later use.
Further, the solid lipid is one or more of glyceryl tristearate, glyceryl behenate, glyceryl monolaurate, hydrogenated vegetable oil, coconut oil and palm oil, the liquid lipid is one or more of medium-chain triglyceride, soybean oil, corn oil, fish oil, algae oil, oleic acid and palmitic acid, and the emulsifier is any one of tween 20, tween 40, tween 80, span 20, span 40 and span 60.
Further, in the step 2.6, during the high intensity ultrasonic treatment of the primary emulsion for 10-15min, the ultrasonic treatment instrument is set to be switched on/off for 2s at 200-.
The invention also discloses the coating preservation solution for aquatic products carrying the burdock polyphenol, which is prepared by any one of the methods.
The invention also comprises the application of the burdock polyphenol-carrying aquatic product coating preservative solution prepared by any one of the methods in preservation of processed aquatic products, and the method specifically comprises the following operation processes:
soaking the processed aquatic product in a film-coating preservation solution for 5-10min, draining in a sterile environment, soaking the processed aquatic product in a 3-5% calcium chloride cross-linking agent solution for 1-2min, rinsing in clear water, draining in the sterile environment, packaging, and refrigerating or freezing at low temperature.
Has the advantages that: the nano-structure lipid carrier is in a crystalline solid sphere shape, and the carried polyphenol is positioned in internal defect lattices, so that the stability and the slow release performance are better, the antioxidant and antibacterial effects can be exerted more durably, and the effect of delaying the quality deterioration of aquatic products in links of storage, transportation, sale and the like is achieved.
Drawings
Figure 1 is a schematic block diagram of the overall technical route of the present invention,
FIG. 2 is a graph showing the effect of three coating preservation solutions of example 1 on the total volatile basic nitrogen (TVB-N) content of fillets stored at 4 ℃,
FIG. 3 is a graph showing the effect of three coating preservation solutions in example 1 of the present invention on the content of thiobarbituric acid reaction substrate (TBARS) in fillets stored at 4 ℃.
Detailed Description
The present invention is further illustrated by the following figures and specific examples, which are to be understood as illustrative only and not as limiting the scope of the invention, which is to be given the full breadth of the appended claims and any and all equivalent modifications thereof which may occur to those skilled in the art upon reading the present specification.
The overall technical route schematic block diagram of the invention is shown in figure 1, and the preparation method of the coating preservative solution for aquatic products carrying burdock polyphenol comprises the following steps:
step 1: preparing the burdock polyphenol by using the raw materials,
step 1.1: slicing fresh radix Arctii, blanching in boiling water for 10-15s, taking out, draining,
step 1.2: drying the burdock root slices with water drained in an oven at 40-50 ℃,
step 1.3: slicing dried radix Arctii, pulverizing, sieving with 40 mesh sieve to obtain radix Arctii powder,
step 1.4: mixing burdock root powder and 40-60% ethanol according to the volume fraction of 1: (10-30) (g/mL) to obtain a mixed solution, performing reflux extraction on the mixed solution at 50-60 ℃ for 2-3h until the reflux is finished,
step 1.5: removing the organic solvent from the mixed solution under negative pressure, and freeze-drying to obtain burdock polyphenol;
step 2: preparing the burdock polyphenol nanostructured lipid carrier by using the burdock polyphenol prepared in the step 1, composite lipid, emulsifier and water as raw materials, wherein in the composite lipid, liquid lipid accounts for 20-60% of the total mass of the composite lipid,
step 2.1: taking the raw materials according to the following mass percentages: 0.05% -0.2%, complex lipid: 5 to 30 percent; emulsifier: 5 to 10 percent; the balance of water,
step 2.2: weighing solid lipid and liquid lipid according to a set mass ratio, mixing to obtain composite lipid, heating the composite lipid at 90 ℃ to melt the composite lipid, wherein the solid lipid is one or more of glyceryl tristearate, glyceryl behenate, lauric monoglyceride, hydrogenated vegetable oil, coconut oil and palm oil, the liquid lipid is one or more of medium chain triglyceride, soybean oil, corn oil, fish oil, algae oil, oleic acid and palmitic acid,
step 2.3: adding Burdock polyphenol into molten compound lipid until dissolving to obtain oil phase,
step 2.4: taking an emulsifier, wherein the emulsifier is one or more of tween 20, tween 40, tween 80, span 20, span 40 and span 60, placing the emulsifier in water until the emulsifier is completely dissolved, preheating at 90 ℃ to obtain a water phase,
step 2.5: adding the water phase into the oil phase under 10000-12000rpm high-speed homogenization conditions, continuing to homogenize for 3-5min to obtain a primary emulsion,
step 2.6: carrying out high-intensity ultrasonic treatment on the primary emulsion for 10-15min, wherein in the process, an ultrasonic treatment instrument is set to be switched on/off for 2s under the power of 200-400W to obtain the nano-structured lipid carrier, the temperature of the sample is maintained at 90 ℃ in the whole operation process of the step 2.5 and the step 2.6,
step 2.7: placing the prepared lipid carrier with the nano structure in ice water bath to cool to room temperature for later use;
and step 3: and (3) preparing the coating preservation solution for the aquatic products by taking the burdock polyphenol nanostructured lipid carrier prepared in the step (2), sodium alginate, glycerol and fish skin collagen as raw materials.
Step 3.1: dissolving sodium alginate in distilled water to prepare sodium alginate solution with mass concentration of 2-4%,
step 3.2: according to the weight percentage of sodium alginate: glycerol: the mass ratio of the fish skin collagen is 100: (30-50): (10-20) weighing glycerol and fish skin collagen,
step 3.3: adding the weighed glycerol and the fish skin collagen into the sodium alginate solution, stirring to form a film forming solution,
step 3.4: and (3) mixing the nano-structure lipid carrier prepared in the step (2) with the film forming solution according to the volume ratio of (5-10) to 100, then homogenizing at high speed to obtain the aquatic product film coating preservation solution, and degassing the aquatic product film coating preservation solution for later use.
The invention also comprises the aquatic product coating preservative solution prepared by any one of the methods and the application of the preservative solution in the preservation of processed aquatic products, and the specific application process comprises the following operation processes:
placing the processed aquatic products in the coating preservation solution for soaking the aquatic products carrying the burdock polyphenols for 5-10min, draining the aquatic products in a sterile environment, soaking the processed aquatic products in a 3-5% calcium chloride cross-linking agent solution for 1-2min, rinsing the processed aquatic products in clear water, continuously draining the processed aquatic products in the sterile environment, packaging the processed aquatic products, and finally refrigerating or freezing the processed aquatic products at a low temperature.
Example 1
Step 1: preparation of burdock polyphenol
Slicing fresh burdock roots, blanching in boiling water for 15s, taking out, and draining; drying the burdock root slices in an oven at 45 ℃, crushing the burdock root slices by a tissue triturator, and sieving the burdock root slices by a 40-mesh sieve for later use; mixing burdock powder according to the proportion of 1: mixing the mixture with 20 g/mL of ethanol solution with volume fraction of 50%, and reflux-extracting at 55 deg.C for 3 hr; removing the organic solvent under reduced pressure, and lyophilizing in a lyophilizer to obtain burdock polyphenol;
step 2: preparation of burdock polyphenol nanostructured lipid carrier
Weighing 5% tristearin and 5% medium chain triglyceride, mixing, heating at 90 deg.C to melt the compound lipid, adding 0.10% burdock polyphenol, and dissolving in the compound lipid; completely dissolving 5% of Tween 20 in an aqueous phase (84.90% of the total mass of the system), and preheating at 90 ℃; adding the water phase into the oil phase under the homogenization condition of 10000rpm, continuing to homogenize for 3min, treating the primary emulsion with high-intensity ultrasound for 12min (400W, 2s on/2 s off) to obtain a nanostructured lipid carrier, and maintaining the temperature of the sample at 90 ℃ by using a high-temperature circulating water tank in the whole operation process; the prepared nanostructured lipid vehicle was cooled to room temperature in an ice-water bath.
And step 3: preparation of burdock polyphenol-loaded aquatic product coating preservation solution
Dissolving sodium alginate in distilled water to prepare a solution with the mass concentration of 4%, adding glycerol accounting for 50% of the mass of the sodium alginate and fish skin collagen accounting for 15%, and stirring to form a film forming solution; mixing the nano-structure lipid carrier solution prepared in the last step with the film forming solution according to the volume ratio of 10:100, mixing under the condition of high-speed homogenization to obtain the coating preservation solution for the aquatic products carrying the burdock polyphenol, and degassing for later use.
The prepared burdock polyphenol-loaded aquatic product film-coating preservative solution is used for processing aquatic products for preservation
Soaking fresh fillets in the coating preservative solution for aquatic products carrying burdock polyphenols for 5min, and draining on sterile gauze; subsequently, soaking the fillets in 3% calcium chloride solution for 1min for full crosslinking; taking out the fillets, rinsing the fillets with clear water, and draining the fillets on sterile gauze to form a film; and (3) placing the fillets in a plastic tray, packaging the fillets by using a preservative film, and refrigerating the fillets at 4 ℃.
Example 2
Step 1: preparation of burdock polyphenol
Slicing fresh burdock roots, blanching in boiling water for 15s, taking out, and draining; drying the burdock root slices in an oven at 50 ℃, crushing the burdock root slices by a tissue triturator, and sieving the burdock root slices by a 40-mesh sieve for later use; mixing burdock powder according to the proportion of 1: mixing the mixture with ethanol with volume fraction of 60% at a feed-liquid ratio of 10(g/mL), and performing reflux extraction at 60 ℃ for 2 h; removing the organic solvent under reduced pressure, and lyophilizing in a lyophilizer to obtain burdock polyphenol;
step 2: preparation of burdock polyphenol nanostructured lipid carrier
Weighing 10% glyceryl behenate and 5% oleic acid, mixing, heating at 90 deg.C to make the composite lipid in molten state, adding 0.15% burdock polyphenol, and dissolving in the composite lipid; completely dissolving 7% of Tween 80 in an aqueous phase (77.85% of the total mass of the system), and preheating at 90 ℃; adding the water phase into the oil phase under the condition of homogenizing at 12000rpm, continuing homogenizing for 5min, treating the primary emulsion with high-intensity ultrasound for 15min (300W, 2s on/2 s off) to obtain a nanostructured lipid carrier, and maintaining the temperature of the sample at 90 ℃ by using a high-temperature circulating water tank in the whole operation process; the prepared nanostructured lipid vehicle was cooled to room temperature in an ice-water bath.
And step 3: preparation of burdock polyphenol-loaded aquatic product coating preservation solution
Dissolving sodium alginate in distilled water to prepare a solution with the mass concentration of 3%, adding glycerol accounting for 40% of the mass of the sodium alginate and fish skin collagen accounting for 20%, and stirring to form a film forming solution; mixing the nano-structure lipid carrier solution prepared in the last step with the film forming solution according to the volume ratio of 8:100, mixing under the condition of high-speed homogenization to obtain the coating preservation solution for the aquatic products carrying the burdock polyphenol, and degassing for later use.
The prepared burdock polyphenol-loaded aquatic product film-coating preservative solution is used for processing aquatic products for preservation
Soaking fresh shelled shrimps in the coating preservative solution for aquatic products carrying burdock polyphenol for 10min, and draining on sterile gauze; subsequently, soaking the shelled shrimps in 5% calcium chloride solution for 2min for full crosslinking; taking out the shelled shrimps, rinsing the shelled shrimps with clear water, and draining the shelled shrimps on sterile gauze to form a film; and quickly freezing the shelled shrimps by a tunnel type instant freezer, bagging and sealing, and transferring to a condition of-20 ℃ for freezing storage.
This experiment compares the influence of the coating preservative solution using the burdock polyphenol-loaded nanostructured lipid carrier, the burdock polyphenol-loaded nanoemulsion (replacing the quality of glyceryl tristearate and the like in step 2 of example 1 with medium-chain triglyceride) and the burdock polyphenol-unloaded nanostructured lipid carrier (no burdock polyphenol is added in step 2 of example 1) in example 1 on the quality of the fillet under the refrigeration condition of 4 ℃. As can be seen from fig. 2 and 3, the three ways of coating preservation can significantly inhibit the generation of total volatile basic nitrogen (TVB-N) and thiobarbituric acid reaction products (TBARS) during storage. The fresh-keeping effect of the nano-structured lipid carrier carrying the burdock polyphenol is stronger than that of the nano-emulsion carrying the burdock polyphenol and that of the nano-structured lipid carrier not carrying the burdock polyphenol, which shows that:
1. the burdock polyphenol plays a key role in resisting oxidation and bacteria;
2. compared with the nano emulsion in the coating film, the nano-structure lipid carrier can better realize the steady regulation and control and the controlled release of the burdock polyphenol, thereby strengthening the functional activity of the burdock polyphenol.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (8)
1. A preparation method of a burdock polyphenol-loaded aquatic product coating preservation solution is characterized by comprising the following steps:
step 1: preparing the burdock polyphenol by using the raw materials,
step 2: preparing the burdock polyphenol nanostructured lipid carrier by using the burdock polyphenol prepared in the step 1, composite lipid, emulsifier and water as raw materials, wherein in the composite lipid, liquid lipid accounts for 20-60% of the total mass of the composite lipid,
and step 3: and (3) preparing the coating preservation solution for the aquatic products by taking the burdock polyphenol nanostructured lipid carrier prepared in the step (2), sodium alginate, glycerol and fish skin collagen as raw materials.
2. The method for preparing the burdock polyphenol-loaded aquatic product coating preservation solution according to claim 1, which is characterized in that the step 1 is specifically operated as follows,
step 1.1: slicing fresh radix Arctii, blanching in boiling water for 10-15s, taking out, draining,
step 1.2: drying the burdock root slices with water drained in an oven at 40-50 ℃,
step 1.3: slicing dried radix Arctii, pulverizing, sieving with 40 mesh sieve to obtain radix Arctii powder,
step 1.4: mixing burdock root powder and 40-60% ethanol according to the volume fraction of 1: (10-30) (g/mL) to obtain a mixed solution, performing reflux extraction on the mixed solution at 50-60 ℃ for 2-3h until the reflux is finished,
step 1.5: and (3) removing the organic solvent from the mixed solution in negative pressure, and freeze-drying to obtain the burdock polyphenol.
3. The method for preparing the burdock polyphenol-loaded aquatic product coating preservation solution according to claim 1, which is characterized in that the step 2 is specifically operated as follows,
step 2.1: taking the raw materials according to the following mass percentages: 0.05% -0.2%, complex lipid: 5 to 30 percent; emulsifier: 5 to 10 percent; the balance of water,
step 2.2: weighing solid lipid and liquid lipid according to a set mass ratio, mixing to obtain composite lipid, heating the composite lipid at 90 deg.C to melt the composite lipid,
step 2.3: adding Burdock polyphenol into molten compound lipid until dissolving to obtain oil phase,
step 2.4: taking the emulsifier, placing the emulsifier in water until the emulsifier is completely dissolved, then placing the emulsifier at 90 ℃ for preheating to obtain a water phase,
step 2.5: adding the water phase into the oil phase under 10000-12000rpm high-speed homogenization conditions, continuing to homogenize for 3-5min to obtain a primary emulsion,
step 2.6: carrying out high-intensity ultrasonic treatment on the primary emulsion for 10-15min to obtain the nano-structured lipid carrier, wherein the temperature of the sample is maintained at 90 ℃ in the whole operation process of the step 2.5 and the step 2.6,
step 2.7: and (3) placing the prepared nano-structured lipid carrier in an ice water bath to cool to room temperature for later use.
4. The method for preparing the burdock polyphenol-loaded aquatic product coating preservation solution according to claim 1, which is characterized in that the step 3 is specifically operated as follows,
step 3.1: dissolving sodium alginate in distilled water to prepare sodium alginate solution with mass concentration of 2-4%,
step 3.2: according to the weight percentage of sodium alginate: glycerol: the mass ratio of the fish skin collagen is 100: (30-50): (10-20) weighing glycerol and fish skin collagen,
step 3.3: adding the weighed glycerol and the fish skin collagen into the sodium alginate solution, stirring to form a film forming solution,
step 3.4: and (3) mixing the nano-structure lipid carrier prepared in the step (2) with the film forming solution according to the volume ratio of (5-10) to 100, then homogenizing at high speed to obtain the aquatic product film coating preservation solution, and degassing the aquatic product film coating preservation solution for later use.
5. The method for preparing the burdock polyphenol-loaded aquatic product coating preservation solution according to claim 3, wherein the solid lipid is one or any more of glyceryl tristearate, glyceryl behenate, monoglycerol laurate, hydrogenated vegetable oil, coconut oil and palm oil, the liquid lipid is one or any more of medium-chain triglyceride, soybean oil, corn oil, fish oil, algae oil, oleic acid and palmitic acid, and the emulsifier is any one of Tween 20, Tween 40, Tween 80, span 20, span 40 and span 60.
6. The method for preparing the burdock polyphenol-loaded aquatic product coating preservation solution as claimed in claim 3, wherein in the step 2.6, in the process of carrying out high-intensity ultrasonic treatment on the primary emulsion for 10-15min, an ultrasonic treatment instrument is set to be switched on/off for 2s at 200-400W.
7. A coating preservation solution for aquatic products carrying burdock polyphenol, which is characterized by being prepared by the method of any one of the claims 1 to 6.
8. A use method of an aquatic product coating preservative solution carrying burdock polyphenol is characterized in that the aquatic product coating preservative solution prepared by any one of the methods of claims 1-6 is used for preserving processed aquatic products, and specifically comprises the following operation processes:
soaking the processed aquatic product in a film-coating preservation solution for 5-10min, draining in a sterile environment, soaking the processed aquatic product in a 3-5% calcium chloride cross-linking agent solution for 1-2min, rinsing in clear water, draining in the sterile environment, packaging, and refrigerating or freezing at low temperature.
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