CN111944485A - Ceramic tile surface anti-slip agent and preparation method thereof - Google Patents
Ceramic tile surface anti-slip agent and preparation method thereof Download PDFInfo
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- CN111944485A CN111944485A CN202010961294.XA CN202010961294A CN111944485A CN 111944485 A CN111944485 A CN 111944485A CN 202010961294 A CN202010961294 A CN 202010961294A CN 111944485 A CN111944485 A CN 111944485A
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- tile surface
- silicone oil
- slip agent
- surface anti
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/14—Anti-slip materials; Abrasives
- C09K3/149—Antislip compositions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5018—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with fluorine compounds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a tile surface anti-slip agent and a preparation method thereof, wherein the tile surface anti-slip agent comprises the following components in percentage by weight: 2-10% of organic acid, 10-25% of ammonium bifluoride, 0.5-2% of humectant, 0.1-1.5% of surfactant, 2-6% of silane coupling agent, 1-10% of silicone oil, 0.1-1.5% of dispersion stabilizer, 0.5-6% of OP emulsifier, 0.1-1.5% of defoaming agent, 0.2-2.5% of disinfectant, 3-7% of stain remover and the balance of deionized water. This ceramic tile surface anti-skid agent is water-soluble liquid, and is nontoxic harmless, has superstrong osmotic force, can effectively permeate ceramic tile capillary channel, through with the chemical action on ceramic tile surface, make this pipeline widen, with the sucking disc effect that the sole contact energy formed physics when meeting water or oil stain, make the ceramic tile surface after the processing have fine antiskid and antifouling effect, and the persistence is good, safety ring protects, can simplify ceramic tile surface antiskid processing technology simultaneously.
Description
Technical Field
The invention belongs to the technical field of ceramic tile surface antiskid, and particularly relates to a ceramic tile surface antiskid agent and a preparation method thereof.
Background
The anti-slip agent is a liquid for increasing the surface friction of the ground, and can be used on the surfaces of natural stone, hard ceramic tiles and wood floors, such as ceramic tiles, large floor tiles, mosaic floor tiles, terrazzo, slate, granite, marble, glazed tiles, ceramic and ceramic bathtubs, bathroom floors and other stone or inorganic materials.
Along with the needs of modern construction of cities and towns and the continuous improvement of living standard of people, ceramic tiles are more and more widely applied to places such as families, hotels, hospitals, restaurants, supermarkets, office buildings, business centers, health clubs, bathrooms, swimming pools and the like. Meanwhile, the slip accident caused by the smooth ground is frequent, especially for the special people who are old, weak, sick, disabled, pregnant and the like. Therefore, tile anti-slip agents have come into play and more enterprises are beginning to produce tile anti-slip agents to overcome this drawback. However, the prior tile anti-slip agent mostly uses toxic and harmful substances such as strong acid and the like as raw materials, causes environmental pollution while corroding the ground after use, and has poor environmental protection property. And the traditional tile anti-skid agent has the problems of low anti-skid coefficient, poor anti-skid durability and the like.
Disclosure of Invention
The invention aims to make up the defects of the prior art and provides an anti-slip agent for the surface of a ceramic tile and a preparation method thereof.
In order to achieve the above object, the present invention provides the following technical solutions:
the tile surface anti-slip agent comprises the following components in percentage by weight:
2-10% of organic acid;
10-25% of ammonium bifluoride;
0.5 to 2 percent of humectant;
0.1 to 1.5 percent of surfactant;
2-6% of a silane coupling agent;
1-10% of silicone oil;
0.1 to 1.5 percent of dispersion stabilizer;
OP emulsifier 0.5-6%;
0.1 to 1.5 percent of defoaming agent;
0.2 to 2.5 percent of bactericidal disinfectant;
3-7% of a stain remover;
the balance being deionized water.
Further, the organic acid is any one or a mixture of more of fruit acid, citric acid and acetic acid.
Further, the humectant is butanetriol, polyethylene glycol, glycerol and polypropylene glycol in a weight ratio of 0.8: (0.1-2): (0.6-0.9): 1, in a mixture of the components.
Further, the surfactant is sodium dodecyl sulfate, sodium dodecyl sulfate and esterquat in a weight ratio of 0.8: (0.3-0.6): (0.5-0.8).
Further, the silane coupling agent is methyl trimethoxy silane and methyl triacetoxy silane in a weight ratio of (1.0-1.6): 0.9 of the composition.
Further, the silicone oil is any one or a mixture of more of methyl silicone oil, organic modified silicone oil, methyl hydrogen-containing silicone oil, methyl ethoxy silicone oil and ethyl silicone oil.
Further, the dispersion stabilizer is diethylene glycol dimethyl ether, isomeric tridecanol polyoxyethylene ether and an allyl ether-acrylamide copolymer in a weight ratio (0.6-1): (0.9-1.5): 1, in a mixture of the components.
Further, the defoaming agent is any one or a mixture of more of polydimethylsiloxane, polyether modified polysiloxane, organic silicone oil, polyoxypropylene glycerol ether and polyoxypropylene polyoxyethylene glycerol ether.
Further, the bactericidal disinfectant is alkylphenol ethoxylates or dodecyl dimethyl benzyl ammonium chloride.
Further, the stain remover is any one of sodium tripolyphosphate, polyoxyethylene ether and sodium alkyl benzene sulfonate.
The preparation method of the tile surface anti-slip agent comprises the following steps:
(1) weighing organic acid, ammonium bifluoride and humectant in specified weight, dissolving in deionized water, and stirring at 25 deg.C at 1000r/min for 30min to obtain mixed solution A;
(2) weighing a surfactant, a silane coupling agent and silicone oil in specified weight, adding the surfactant, the silane coupling agent and the silicone oil into the mixed solution A, and stirring the mixture for 30min at 25 ℃ at the rotating speed of 800r/min to obtain a mixed solution B;
(3) weighing the dispersion stabilizer, the OP emulsifier and the defoaming agent in specified weight, adding the dispersion stabilizer, the OP emulsifier and the defoaming agent into the mixed solution B, and stirring the mixture for 30min at the rotating speed of 600r/min at 25 ℃ to obtain a mixed solution C;
(4) and weighing the sterilizing disinfectant and the stain remover in specified weight, adding the sterilizing disinfectant and the stain remover into the mixed solution C, and stirring the mixture for 30min at 25 ℃ at the rotating speed of 400r/min to obtain the anti-slip agent for the surface of the ceramic tile.
The invention has the advantages that:
this ceramic tile surface anti-skid agent is water-soluble liquid, and is nontoxic harmless, has superstrong osmotic force, can effectively permeate ceramic tile capillary channel, through with the chemical action on ceramic tile surface, make this pipeline widen, with the sucking disc effect that the sole contact energy formed physics when meeting water or oil stain, make the ceramic tile surface after the processing have fine antiskid and antifouling effect, and the persistence is good, safety ring protects, can simplify ceramic tile surface antiskid processing technology simultaneously.
Detailed Description
The technical scheme of the invention is further explained by combining the specific examples as follows:
example 1
The tile surface anti-slip agent comprises the following components in percentage by weight:
2% of organic acid;
10% of ammonium bifluoride;
0.5% of humectant;
0.1% of surfactant;
2% of a silane coupling agent;
1% of silicone oil;
0.1% of dispersion stabilizer;
OP emulsifier 0.5%;
0.1% of defoaming agent;
0.2% of bactericidal disinfectant;
3% of a stain remover;
the balance being deionized water.
The organic acid is one or more of fruit acid, citric acid and acetic acid.
The humectant is butanetriol, polyethylene glycol, glycerol and polypropylene glycol in a weight ratio of 0.8: (0.1-2): (0.6-0.9): 1, in a mixture of the components.
The surfactant is sodium dodecyl sulfate, sodium dodecyl sulfate and esterquat in a weight ratio of 0.8: (0.3-0.6): (0.5-0.8).
The silane coupling agent is methyl trimethoxy silane and methyl triacetoxy silane in a weight ratio of (1.0-1.6): 0.9 of the composition.
The silicone oil is any one or a mixture of more of methyl silicone oil, organic modified silicone oil, methyl hydrogen-containing silicone oil, methyl ethoxy silicone oil and ethyl silicone oil.
The dispersion stabilizer is diethylene glycol dimethyl ether, isomeric tridecanol polyoxyethylene ether and an allyl ether-acrylamide copolymer in a weight ratio (0.6-1): (0.9-1.5): 1, in a mixture of the components.
The defoaming agent is any one or a mixture of more of polydimethylsiloxane, polyether modified polysiloxane, organic silicone oil, polyoxypropylene glycerol ether and polyoxypropylene polyoxyethylene glycerol ether.
The disinfectant is alkylphenol polyoxyethylene or dodecyl dimethyl benzyl ammonium chloride.
The dirt remover is any one of sodium tripolyphosphate, polyoxyethylene ether and sodium alkyl benzene sulfonate.
The preparation method of the tile surface anti-slip agent comprises the following steps:
(1) weighing organic acid, ammonium bifluoride and humectant in specified weight, dissolving in deionized water, and stirring at 25 deg.C at 1000r/min for 30min to obtain mixed solution A;
(2) weighing a surfactant, a silane coupling agent and silicone oil in specified weight, adding the surfactant, the silane coupling agent and the silicone oil into the mixed solution A, and stirring the mixture for 30min at 25 ℃ at the rotating speed of 800r/min to obtain a mixed solution B;
(3) weighing the dispersion stabilizer, the OP emulsifier and the defoaming agent in specified weight, adding the dispersion stabilizer, the OP emulsifier and the defoaming agent into the mixed solution B, and stirring the mixture for 30min at the rotating speed of 600r/min at 25 ℃ to obtain a mixed solution C;
(4) and weighing the sterilizing disinfectant and the stain remover in specified weight, adding the sterilizing disinfectant and the stain remover into the mixed solution C, and stirring the mixture for 30min at 25 ℃ at the rotating speed of 400r/min to obtain the anti-slip agent for the surface of the ceramic tile.
Example 2
The tile surface anti-slip agent comprises the following components in percentage by weight:
6% of organic acid;
17% of ammonium bifluoride;
1.2% of a humectant;
0.8% of surfactant;
4.1% of a silane coupling agent;
6% of silicone oil;
0.8% of dispersion stabilizer;
OP emulsifier 3%;
0.8 percent of defoaming agent;
1.2 percent of bactericidal disinfectant;
5.6 percent of stain remover;
the balance being deionized water.
The other steps are the same as in example 1.
Example 3
The tile surface anti-slip agent comprises the following components in percentage by weight:
8% of organic acid;
21% of ammonium bifluoride;
1.8% of a humectant;
1.3% of a surfactant;
5.2% of a silane coupling agent;
9% of silicone oil;
1.3 percent of dispersion stabilizer;
4.5 percent of OP emulsifier;
1.3 percent of defoaming agent;
2.1 percent of bactericidal disinfectant;
6% of a stain remover;
the balance being deionized water.
The other steps are the same as in example 1.
Example 4
The tile surface anti-slip agent comprises the following components in percentage by weight:
10% of organic acid;
25% of ammonium bifluoride;
2% of a humectant;
1.5% of a surfactant;
6% of a silane coupling agent;
10% of silicone oil;
1.5 percent of dispersion stabilizer;
OP emulsifier 6%;
1.5 percent of defoaming agent;
2.5 percent of bactericidal disinfectant;
7% of a stain remover;
the balance being deionized water.
The other steps are the same as in example 1.
Example 5
The tile surface anti-slip agent comprises the following components in percentage by weight:
4% of organic acid;
14% of ammonium bifluoride;
0.8% of humectant;
0.4% of surfactant;
3% of a silane coupling agent;
3% of silicone oil;
0.4% of dispersion stabilizer;
OP emulsifier 1.5%;
0.4 percent of defoaming agent;
0.8% of bactericidal disinfectant;
4.5 percent of stain remover;
the balance being deionized water.
The other steps are the same as in example 1.
In order to verify the anti-slip effect of the anti-slip agent for tile surface according to the present invention, the inventors applied the anti-slip agent prepared in examples 1 to 5 to the tile surface and performed the measurement of the friction coefficient, and the results are shown in table 1:
TABLE 1
The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (11)
1. The tile surface anti-slip agent is characterized by comprising the following components in percentage by weight:
2-10% of organic acid;
10-25% of ammonium bifluoride;
0.5 to 2 percent of humectant;
0.1 to 1.5 percent of surfactant;
2-6% of a silane coupling agent;
1-10% of silicone oil;
0.1 to 1.5 percent of dispersion stabilizer;
OP emulsifier 0.5-6%;
0.1 to 1.5 percent of defoaming agent;
0.2 to 2.5 percent of bactericidal disinfectant;
3-7% of a stain remover;
the balance being deionized water.
2. The tile surface anti-slip agent according to claim 1, wherein the organic acid is any one or a mixture of more of fruit acid, citric acid and acetic acid.
3. The tile surface anti-slip agent according to claim 1, wherein the humectant is butanetriol, polyethylene glycol, glycerol, and polypropylene glycol in a weight ratio of 0.8: (0.1-2): (0.6-0.9): 1, in a mixture of the components.
4. The tile surface anti-slip agent according to claim 1, wherein the surfactant is sodium dodecyl sulfate, sodium dodecyl sulfate and esterquat in a weight ratio of 0.8: (0.3-0.6): (0.5-0.8).
5. The tile surface anti-slip agent according to claim 1, wherein the silane coupling agent is methyltrimethoxysilane and methyltriacetoxysilane in a weight ratio of (1.0-1.6): 0.9 of the composition.
6. The tile surface anti-slip agent according to claim 1, wherein the silicone oil is any one or a mixture of methyl silicone oil, organic modified silicone oil, methyl hydrogen-containing silicone oil, methyl ethoxy silicone oil and ethyl silicone oil.
7. The tile surface anti-slip agent according to claim 1, wherein the dispersion stabilizer is diethylene glycol dimethyl ether, isotridecanol polyoxyethylene ether, propylene ether-acrylamide copolymer in the weight ratio (0.6-1): (0.9-1.5): 1, in a mixture of the components.
8. The tile surface anti-slip agent according to claim 1, wherein the defoaming agent is any one or a mixture of polydimethylsiloxane, polyether modified polysiloxane, silicone oil, polyoxypropylene glycerol ether and polyoxypropylene polyoxyethylene glycerol ether.
9. The tile surface anti-slip agent according to claim 1, wherein the bactericidal disinfectant is alkylphenol ethoxylates or dodecyl dimethyl benzyl ammonium chloride.
10. The tile surface anti-slip agent according to claim 1, wherein the stain remover is any one of sodium tripolyphosphate, polyoxyethylene ether and sodium alkyl benzene sulfonate.
11. A process for the preparation of a tile surface anti-slip agent according to any one of claims 1 to 10, comprising the steps of:
(1) weighing organic acid, ammonium bifluoride and humectant in specified weight, dissolving in deionized water, and stirring at 25 deg.C at 1000r/min for 30min to obtain mixed solution A;
(2) weighing a surfactant, a silane coupling agent and silicone oil in specified weight, adding the surfactant, the silane coupling agent and the silicone oil into the mixed solution A, and stirring the mixture for 30min at 25 ℃ at the rotating speed of 800r/min to obtain a mixed solution B;
(3) weighing the dispersion stabilizer, the OP emulsifier and the defoaming agent in specified weight, adding the dispersion stabilizer, the OP emulsifier and the defoaming agent into the mixed solution B, and stirring the mixture for 30min at the rotating speed of 600r/min at 25 ℃ to obtain a mixed solution C;
(4) and weighing the sterilizing disinfectant and the stain remover in specified weight, adding the sterilizing disinfectant and the stain remover into the mixed solution C, and stirring the mixture for 30min at 25 ℃ at the rotating speed of 400r/min to obtain the anti-slip agent for the surface of the ceramic tile.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010961294.XA CN111944485A (en) | 2020-09-14 | 2020-09-14 | Ceramic tile surface anti-slip agent and preparation method thereof |
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| CN202010961294.XA CN111944485A (en) | 2020-09-14 | 2020-09-14 | Ceramic tile surface anti-slip agent and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113004868A (en) * | 2021-02-26 | 2021-06-22 | 郝士军 | Anti-slip agent and preparation method thereof |
| CN113636870A (en) * | 2021-07-13 | 2021-11-12 | 广东富强陶瓷有限公司 | Production process of antibacterial wear-resistant anti-skid glazed ceramic tile |
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