CN111892300A - High-strength spray-painting crystalline ceramic glaze and preparation method thereof - Google Patents
High-strength spray-painting crystalline ceramic glaze and preparation method thereof Download PDFInfo
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- CN111892300A CN111892300A CN202010791882.3A CN202010791882A CN111892300A CN 111892300 A CN111892300 A CN 111892300A CN 202010791882 A CN202010791882 A CN 202010791882A CN 111892300 A CN111892300 A CN 111892300A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Abstract
The invention discloses a high-strength spray-painting crystalline ceramic glaze and a preparation method thereof, wherein the high-strength spray-painting crystalline ceramic glaze is prepared from the following raw materials in parts by mass: 38-58 parts of feldspar, 12-16 parts of quartz, 10-16 parts of calcite, 5-8 parts of barium carbonate, 7-10 parts of talcum, 10-15 parts of silver oxide, 3-6 parts of kaolin, 8-10 parts of titanium oxide, 14-18 parts of zinc oxide, 6-8 parts of aluminum oxide, 1-4 parts of sodium dodecyl benzene sulfonate, 2-5 parts of lanthanum boride, 0.1-1.2 parts of niobium diselenide and conductive antibacterial powder. Has the advantages that: can improve the strength performance and the anti ability of falling of ceramic, improve ceramic's practicality, the glaze smoothness is good, the glaze slip performance is good, the firing range is wide, the goods outward appearance is regular, easily clean and produce higher aesthetic feeling, makes the consumer have bigger use vision sense organ, receives the good comment of customer favor.
Description
Technical Field
The invention relates to the technical field of ceramics, in particular to a high-strength color-spraying crystalline ceramic glaze and a preparation method thereof.
Background
Both daily-use ceramics and furnishing art ceramics belong to the domestic ceramics. The pottery is decorated by ceramic glaze basically, so that the pottery is beautiful and sanitary and is easy to clean. The porcelain glaze used for the ceramic ware comprises transparent glaze, opaque glaze, colored glaze and the like. Among the special kinds of glaze materials, there is a kind of glaze material called crystal glaze, which is used on the surface of ceramic products, after firing, the glaze layer is transformed into crystal by kiln, and these crystal patterns produce decorative effect. The surface of a ceramic product is often required to be coated with a layer of smooth glaze, and the glaze can not only prevent water, but also prevent adhesion and has good cleaning performance. Because most of ceramic products are manufactured into articles for daily use, the requirement on the surface hardness of the ceramic products is very high, the existing glaze coating has no higher hardness, and overglaze with different colors is sprayed on a proper place to form the spraying color effect with different colors, the formed crystal patterns can be uniformly distributed, so that the crystal glaze layer generates higher aesthetic feeling, which provides a popular research topic for the ceramic industry.
An effective solution to the problems in the related art has not been proposed yet.
Disclosure of Invention
Aiming at the problems in the related art, the invention provides a high-strength color-spraying crystalline ceramic glaze and a preparation method thereof, so as to overcome the technical problems in the prior related art.
Therefore, the invention adopts the following specific technical scheme:
according to one aspect of the present invention, a high strength spray-painted crystalline ceramic glaze is provided.
The high-strength ceramic glaze is prepared from the following raw materials in parts by mass:
38-58 parts of feldspar, 12-16 parts of quartz, 10-16 parts of calcite, 5-8 parts of barium carbonate, 7-10 parts of talcum, 10-15 parts of silver oxide, 3-6 parts of kaolin, 8-10 parts of titanium oxide, 14-18 parts of zinc oxide, 6-8 parts of aluminum oxide, 1-4 parts of sodium dodecyl benzene sulfonate, 2-5 parts of lanthanum boride, 0.1-1.2 parts of niobium diselenide and conductive antibacterial powder;
the color spraying glaze comprises the following raw materials in parts by weight: 30-50 parts of feldspar, 8-12 parts of calcite, 15-17 parts of quartz, 3-6 parts of zinc oxide and 3-4 parts of strontium carbonate; 2-6 parts of Suzhou soil, 2-4 parts of barium carbonate, 11-13 parts of zirconium silicate, 5-10 parts of talc and 10-14 parts of chromophore.
Further, the high-strength ceramic glaze comprises the following raw material components: 58 parts of feldspar, 16 parts of quartz, 16 parts of calcite, 8 parts of barium carbonate, 10 parts of talcum, 15 parts of silver oxide, 6 parts of kaolin, 10 parts of titanium oxide, 18 parts of zinc oxide, 8 parts of aluminum oxide, 4 parts of sodium dodecyl benzene sulfonate, 5 parts of lanthanum boride, 1.2 parts of niobium diselenide and conductive antibacterial powder.
Further, the color spraying glaze comprises the following raw materials in parts by weight: 50 parts of feldspar, 12 parts of calcite, 17 parts of quartz, 6 parts of zinc oxide and 4 parts of strontium carbonate; 6 parts of Suzhou soil, 4 parts of barium carbonate, 13 parts of zirconium silicate, 10 parts of talc and 14 parts of chromophore.
Further, the high-strength ceramic glaze comprises the following raw material components: 38 parts of feldspar, 12 parts of quartz, 10 parts of calcite, 5 parts of barium carbonate, 7 parts of talcum, 10 parts of silver oxide, 3 parts of kaolin, 8 parts of titanium oxide, 14 parts of zinc oxide, 6 parts of aluminum oxide, 1 part of sodium dodecyl benzene sulfonate, 2 parts of lanthanum boride, 0.1 part of niobium diselenide and conductive antibacterial powder.
Further, the color spraying glaze comprises the following raw materials in parts by weight: 30 parts of feldspar, 8 parts of calcite, 15 parts of quartz, 3 parts of zinc oxide and 3 parts of strontium carbonate; 2 parts of Suzhou soil, 2 parts of barium carbonate, 11 parts of zirconium silicate, 5 parts of talc and 10 parts of chromophore.
Further, the conductive antibacterial powder comprises the following raw materials: 1-5 parts of nano graphene, 1-5 parts of graphite, 7-10 parts of phenolic resin, 7-10 parts of epoxy resin, 1-3 parts of quartz, 2-5 parts of calcite, 15-20 parts of titanium dioxide, 10-30 parts of silver molybdate and 30-50 parts of ammonium dihydrogen phosphate.
According to another aspect of the invention, a method for preparing a high-strength spray-painted crystalline ceramic glaze is provided
The preparation method of the high-strength spray painting crystal ceramic glaze comprises the following steps:
taking raw materials according to the weight parts, sequentially adding feldspar, quartz, calcite, barium carbonate, talcum, silver oxide, kaolin, titanium oxide, zinc oxide, aluminum oxide, sodium dodecyl benzene sulfonate, lanthanum boride, niobium diselenide and conductive antibacterial powder into a ball mill, grinding and uniformly mixing;
adding a certain amount of water into the ground material to obtain a block glaze, carrying out wet ball milling on the block glaze, and treating under a mesh sieve to obtain a high-strength glaze for later use;
taking raw materials according to the weight parts, sequentially adding feldspar, calcite, quartz, zinc oxide, strontium carbonate, Suzhou soil, barium carbonate, zirconium silicate, talc and chromophore into a ball mill, grinding and uniformly mixing;
adding a certain amount of water into the ground material to obtain a color spraying glaze material, carrying out wet ball milling on the massive color spraying glaze material, and treating under a mesh sieve to obtain the color spraying glaze material for later use;
soaking the high-strength glaze on the surface of the ceramic body, storing the soaked ceramic body in a drying place for drying, then calcining, and cooling to obtain the high-strength ceramic glaze;
uniformly spraying the color-spraying glaze material on the soaked and dried ceramic blank by using a spray gun, and storing the ceramic blank after color spraying in a drying place for drying after color spraying is finished;
firing the ceramic blank body which is sprayed with colors and dried in a kiln, firing at high temperature in the nitrogen atmosphere, and finally preparing the high-strength sprayed crystalline ceramic glaze ceramic utensil under the conditions of heat preservation, fire stopping and temperature reduction.
Furthermore, the mesh number of the mesh sieve is 150-220 meshes.
Further, the ceramic body is placed into a kiln to be fired for 10-16h at the high temperature of 1100-1300 ℃.
The invention has the beneficial effects that: the high-strength spray-painting crystal ceramic glaze is prepared by combining ceramic glaze of feldspar, quartz, calcite, barium carbonate, talc, silver oxide, kaolin, titanium oxide, zinc oxide, aluminum oxide, sodium dodecyl benzene sulfonate, lanthanum boride, niobium diselenide and conductive antibacterial powder, and spray-painting color glaze matched with the feldspar, the calcite, the quartz, the zinc oxide, the strontium carbonate, Suzhou soil, barium carbonate, zirconium silicate, talc and a color base, wherein the spray-painting color glaze has raised and uniformly distributed crystal glaze points on the surface of a glaze layer, the surface of the glaze points is smooth, the crystal effect is good, the spray-painting color glaze has stereoscopic impression, the high-strength ceramic glaze can improve the strength performance and the anti-falling capacity of a ceramic product, the practicability of the ceramic product is improved, the glaze surface smoothness is good, the glaze slurry performance is good, the firing range is wide, the appearance of the product is regular and clean, and higher aesthetic feeling is generated, the consumers have larger visual sense of use and are favored by the customers.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings needed in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings without creative efforts.
Fig. 1 is a flow chart of a high-strength spray-painted crystalline ceramic glaze and a preparation method thereof according to an embodiment of the present invention.
Detailed Description
For further explanation of the various embodiments, the drawings which form a part of the disclosure and which are incorporated in and constitute a part of this specification, illustrate embodiments and, together with the description, serve to explain the principles of operation of the embodiments, and to enable others of ordinary skill in the art to understand the various embodiments and advantages of the invention, and, by reference to these figures, reference is made to the accompanying drawings, which are not to scale and wherein like reference numerals generally refer to like elements.
According to an embodiment of the present invention, there is provided a high-strength spray-painted crystalline ceramic glaze.
According to the embodiment of the invention, the high-strength spray painting crystal ceramic glaze is prepared from the following raw materials in parts by mass:
38-58 parts of feldspar, 12-16 parts of quartz, 10-16 parts of calcite, 5-8 parts of barium carbonate, 7-10 parts of talcum, 10-15 parts of silver oxide, 3-6 parts of kaolin, 8-10 parts of titanium oxide, 14-18 parts of zinc oxide, 6-8 parts of aluminum oxide, 1-4 parts of sodium dodecyl benzene sulfonate, 2-5 parts of lanthanum boride, 0.1-1.2 parts of niobium diselenide and conductive antibacterial powder;
the color spraying glaze comprises the following raw materials in parts by weight: 30-50 parts of feldspar, 8-12 parts of calcite, 15-17 parts of quartz, 3-6 parts of zinc oxide and 3-4 parts of strontium carbonate; 2-6 parts of Suzhou soil, 2-4 parts of barium carbonate, 11-13 parts of zirconium silicate, 5-10 parts of talc and 10-14 parts of chromophore.
In order to clearly understand the technical scheme of the invention, the technical scheme of the invention is described in detail through specific examples.
Example one
The high-strength ceramic glaze comprises the following raw material components: 58 parts of feldspar, 16 parts of quartz, 16 parts of calcite, 8 parts of barium carbonate, 10 parts of talcum, 15 parts of silver oxide, 6 parts of kaolin, 10 parts of titanium oxide, 18 parts of zinc oxide, 8 parts of aluminum oxide, 4 parts of sodium dodecyl benzene sulfonate, 5 parts of lanthanum boride, 1.2 parts of niobium diselenide and conductive antibacterial powder;
the color spraying glaze comprises the following raw materials in parts by weight: 50 parts of feldspar, 12 parts of calcite, 17 parts of quartz, 6 parts of zinc oxide and 4 parts of strontium carbonate; 6 parts of Suzhou soil, 4 parts of barium carbonate, 13 parts of zirconium silicate, 10 parts of talc and 14 parts of chromophore.
Example two
The high-strength ceramic glaze comprises the following raw material components: 38 parts of feldspar, 12 parts of quartz, 10 parts of calcite, 5 parts of barium carbonate, 7 parts of talcum, 10 parts of silver oxide, 3 parts of kaolin, 8 parts of titanium oxide, 14 parts of zinc oxide, 6 parts of aluminum oxide, 1 part of sodium dodecyl benzene sulfonate, 2 parts of lanthanum boride, 0.1 part of niobium diselenide and conductive antibacterial powder;
the color spraying glaze comprises the following raw materials in parts by weight: 30 parts of feldspar, 8 parts of calcite, 15 parts of quartz, 3 parts of zinc oxide and 3 parts of strontium carbonate; 2 parts of Suzhou soil, 2 parts of barium carbonate, 11 parts of zirconium silicate, 5 parts of talc and 10 parts of chromophore.
In one embodiment, the conductive antibacterial powder comprises the following raw material components: 1-5 parts of nano graphene, 1-5 parts of graphite, 7-10 parts of phenolic resin, 7-10 parts of epoxy resin, 1-3 parts of quartz, 2-5 parts of calcite, 15-20 parts of titanium dioxide, 10-30 parts of silver molybdate and 30-50 parts of ammonium dihydrogen phosphate.
As shown in fig. 1, according to an embodiment of the present invention, there is also provided a method for preparing a high-strength spray-painted crystalline ceramic glaze.
The method comprises the following steps:
step S101, taking raw materials according to parts by weight, sequentially adding feldspar, quartz, calcite, barium carbonate, talc, silver oxide, kaolin, titanium oxide, zinc oxide, aluminum oxide, sodium dodecyl benzene sulfonate, lanthanum boride, niobium diselenide and conductive antibacterial powder into a ball mill, grinding and mixing uniformly;
step S103, adding quantitative water into the ground material to obtain a block glaze, carrying out wet ball milling on the block glaze, and treating under a mesh sieve to obtain a high-strength glaze for later use;
step S105, taking the raw materials according to the weight parts, sequentially adding feldspar, calcite, quartz, zinc oxide, strontium carbonate, Suzhou clay, barium carbonate, zirconium silicate, talc and chromophore into a ball mill, grinding and uniformly mixing;
step S107, adding a certain amount of water into the ground material to obtain a sprayed color glaze, carrying out wet ball milling on the massive sprayed color glaze, and treating under a mesh sieve to obtain the sprayed color glaze for later use;
step S109, soaking the high-strength glaze on the surface of the ceramic body, storing the soaked ceramic body in a drying place for drying, then calcining, and cooling to obtain the high-strength ceramic glaze;
step S111, uniformly spraying color on the soaked and dried ceramic blank by using a spray gun to spray color glaze, and storing the ceramic blank sprayed with color in a drying place for drying after the color spraying is finished;
and S113, firing the ceramic blank subjected to color spraying and drying in a kiln, firing at a high temperature in a nitrogen atmosphere, and finally preparing the high-strength color-spraying crystalline ceramic glaze ceramic appliance under the conditions of heat preservation, fire stopping and temperature reduction.
In one embodiment, the mesh size of the mesh screen is 150-220 mesh.
In one embodiment, the ceramic body is placed into a kiln to be fired at the high temperature of 1100-1300 ℃ for 10-16 h.
For the convenience of understanding the technical solutions of the present invention, the following detailed description will be made on the working principle or the operation mode of the present invention in the practical process.
In conclusion, by means of the technical scheme of the invention, the high-strength spray-painting crystal ceramic glaze is prepared by combining the ceramic glaze of feldspar, quartz, calcite, barium carbonate, talc, silver oxide, kaolin, titanium oxide, zinc oxide, aluminum oxide, sodium dodecyl benzene sulfonate, lanthanum boride, niobium diselenide and conductive antibacterial powder, and the spray-painting color glaze matched with feldspar, calcite, quartz, zinc oxide, strontium carbonate, Suzhou clay, barium carbonate, zirconium silicate, talc and a chromophore, the surface of the ceramic glaze layer is provided with raised and uniformly distributed crystal glaze points, the surface of the glaze points is smooth, the crystallization effect is good, the spray-painting color glaze has stereoscopic impression, the high-strength ceramic glaze can improve the strength performance and the anti-falling capability of the ceramic product, the practicability of the ceramic product is improved, the glaze smoothness is good, the glaze slurry performance is good, the range is wide, the product has regular appearance, is easy to clean, generates higher aesthetic feeling, enables consumers to have larger visual sense of use, and is favored by customers.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (9)
1. The high-strength spray-painting crystalline ceramic glaze is characterized by being prepared from the following raw materials in parts by mass:
38-58 parts of feldspar, 12-16 parts of quartz, 10-16 parts of calcite, 5-8 parts of barium carbonate, 7-10 parts of talcum, 10-15 parts of silver oxide, 3-6 parts of kaolin, 8-10 parts of titanium oxide, 14-18 parts of zinc oxide, 6-8 parts of aluminum oxide, 1-4 parts of sodium dodecyl benzene sulfonate, 2-5 parts of lanthanum boride, 0.1-1.2 parts of niobium diselenide and conductive antibacterial powder;
the color spraying glaze comprises the following raw materials in parts by weight: 30-50 parts of feldspar, 8-12 parts of calcite, 15-17 parts of quartz, 3-6 parts of zinc oxide and 3-4 parts of strontium carbonate; 2-6 parts of Suzhou soil, 2-4 parts of barium carbonate, 11-13 parts of zirconium silicate, 5-10 parts of talc and 10-14 parts of chromophore.
2. The high-strength spray-painting crystalline ceramic glaze according to claim 1, wherein the high-strength ceramic glaze is prepared from the following raw materials in parts by mass: 58 parts of feldspar, 16 parts of quartz, 16 parts of calcite, 8 parts of barium carbonate, 10 parts of talcum, 15 parts of silver oxide, 6 parts of kaolin, 10 parts of titanium oxide, 18 parts of zinc oxide, 8 parts of aluminum oxide, 4 parts of sodium dodecyl benzene sulfonate, 5 parts of lanthanum boride, 1.2 parts of niobium diselenide and conductive antibacterial powder.
3. The high-strength color-spraying crystalline ceramic glaze according to claim 1, wherein the color-spraying glaze is prepared from the following raw materials in parts by mass: 50 parts of feldspar, 12 parts of calcite, 17 parts of quartz, 6 parts of zinc oxide and 4 parts of strontium carbonate; 6 parts of Suzhou soil, 4 parts of barium carbonate, 13 parts of zirconium silicate, 10 parts of talc and 14 parts of chromophore.
4. The high-strength spray-painting crystalline ceramic glaze according to claim 1, wherein the high-strength ceramic glaze is prepared from the following raw materials in parts by mass: 38 parts of feldspar, 12 parts of quartz, 10 parts of calcite, 5 parts of barium carbonate, 7 parts of talcum, 10 parts of silver oxide, 3 parts of kaolin, 8 parts of titanium oxide, 14 parts of zinc oxide, 6 parts of aluminum oxide, 1 part of sodium dodecyl benzene sulfonate, 2 parts of lanthanum boride, 0.1 part of niobium diselenide and conductive antibacterial powder.
5. The method for preparing the high-strength color-spraying crystalline ceramic glaze according to claim 1, wherein the color-spraying glaze is prepared from the following raw materials in parts by mass: 30 parts of feldspar, 8 parts of calcite, 15 parts of quartz, 3 parts of zinc oxide and 3 parts of strontium carbonate; 2 parts of Suzhou soil, 2 parts of barium carbonate, 11 parts of zirconium silicate, 5 parts of talc and 10 parts of chromophore.
6. The high-strength spray-painting crystalline ceramic glaze according to claim 1, wherein the conductive antibacterial powder comprises the following raw materials: 1-5 parts of nano graphene, 1-5 parts of graphite, 7-10 parts of phenolic resin, 7-10 parts of epoxy resin, 1-3 parts of quartz, 2-5 parts of calcite, 15-20 parts of titanium dioxide, 10-30 parts of silver molybdate and 30-50 parts of ammonium dihydrogen phosphate.
7. The method for preparing a high-strength spray-painted crystalline ceramic glaze according to claim 1, wherein the method for preparing a high-strength spray-painted crystalline ceramic glaze according to claim 1 comprises the following steps:
taking raw materials according to the weight parts, sequentially adding feldspar, quartz, calcite, barium carbonate, talcum, silver oxide, kaolin, titanium oxide, zinc oxide, aluminum oxide, sodium dodecyl benzene sulfonate, lanthanum boride, niobium diselenide and conductive antibacterial powder into a ball mill, grinding and uniformly mixing;
adding a certain amount of water into the ground material to obtain a block glaze, carrying out wet ball milling on the block glaze, and treating under a mesh sieve to obtain a high-strength glaze for later use;
taking raw materials according to the weight parts, sequentially adding feldspar, calcite, quartz, zinc oxide, strontium carbonate, Suzhou soil, barium carbonate, zirconium silicate, talc and chromophore into a ball mill, grinding and uniformly mixing;
adding a certain amount of water into the ground material to obtain a color spraying glaze material, carrying out wet ball milling on the massive color spraying glaze material, and treating under a mesh sieve to obtain the color spraying glaze material for later use;
soaking the high-strength glaze on the surface of the ceramic body, storing the soaked ceramic body in a drying place for drying, then calcining, and cooling to obtain the high-strength ceramic glaze;
uniformly spraying the color-spraying glaze material on the soaked and dried ceramic blank by using a spray gun, and storing the ceramic blank after color spraying in a drying place for drying after color spraying is finished;
firing the ceramic blank body which is sprayed with colors and dried in a kiln, firing at high temperature in the nitrogen atmosphere, and finally preparing the high-strength sprayed crystalline ceramic glaze ceramic utensil under the conditions of heat preservation, fire stopping and temperature reduction.
8. The method as claimed in claim 7, wherein the mesh size of the mesh screen is 150-220 meshes.
9. The method as claimed in claim 7, wherein the ceramic body is fired at a high temperature of 1100-1300 ℃ for 10-16 h.
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| CN112408797A (en) * | 2020-12-04 | 2021-02-26 | 湖南华联瓷业股份有限公司 | Crystalline glaze and preparation method thereof |
| CN113636866A (en) * | 2021-08-10 | 2021-11-12 | 广东易成陶瓷实业有限公司 | Preparation method of sand glaze ceramic |
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| CN112408797A (en) * | 2020-12-04 | 2021-02-26 | 湖南华联瓷业股份有限公司 | Crystalline glaze and preparation method thereof |
| CN113636866A (en) * | 2021-08-10 | 2021-11-12 | 广东易成陶瓷实业有限公司 | Preparation method of sand glaze ceramic |
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Application publication date: 20201106 |