CN111826257A - Filling process for reducing upper substances in yellow rice wine - Google Patents

Filling process for reducing upper substances in yellow rice wine Download PDF

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CN111826257A
CN111826257A CN202010729291.3A CN202010729291A CN111826257A CN 111826257 A CN111826257 A CN 111826257A CN 202010729291 A CN202010729291 A CN 202010729291A CN 111826257 A CN111826257 A CN 111826257A
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wine
yellow
complexing
filling process
yellow wine
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孙国昌
俞志方
吕兴龙
何权
边鉴新
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Kuaijishan Shoaxing Wine Co ltd
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Kuaijishan Shoaxing Wine Co ltd
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/12Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages without precipitation
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/04Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material
    • C12H1/0408Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of inorganic added material
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/06Precipitation by physical means, e.g. by irradiation, vibrations
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/06Precipitation by physical means, e.g. by irradiation, vibrations
    • C12H1/063Separation by filtration

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  • Health & Medical Sciences (AREA)
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Abstract

The invention discloses a filling process for reducing upper substances in yellow rice wine, which is characterized by comprising the following steps of: the method comprises the following steps: wine sucking: pumping the frozen and stored yellow wine into a complexing tank through a liquid pump; and (3) oxidation: ozone generated by the ozone generator is directly introduced into the liquid pump to be mixed with yellow wine flowing through the liquid pump, and the yellow wine is oxidized; complexing: carrying out complexation reaction on the yellow wine in a complexation tank; adsorption: and adsorbing the yellow wine by using activated carbon. The invention can oxidize, complex and adsorb the yellow wine, and effectively reduce the content of the upper substances in the yellow wine.

Description

Filling process for reducing upper substances in yellow rice wine
Technical Field
The invention relates to the technical field of yellow wine processing, in particular to a filling process for reducing upper substances in yellow wine.
Background
Yellow wine is one of the oldest wines in the world, enjoys the reputation of 'national wine', is originated from China, and is called three ancient wines in the world together with beer and glucose. The yellow wine is brewed wine with low grain consumption, low alcohol content and high nutrition, and has dietotherapy and medicinal value.
The higher alcohol is a general name of alcohols containing more than 3 carbon atoms, is commonly called fusel oil, is a main byproduct generated in the fermentation process of wines, and is also one of main fragrant and taste substances of wines. The higher alcohol in the yellow wine mainly comprises isobutanol, n-butanol, tert-butanol, isoamyl alcohol, benzyl alcohol and the like. The yellow wine is endowed with special mellow, full and smooth and harmonious taste by a proper amount of higher alcohol, but the content of the higher alcohol is too high, so that foreign flavor is generated, the brain nervous system of a person is damaged, and the headache of the person who drinks the yellow wine is caused. Symptoms of dizziness.
Biogenic amines are a class of basic, low molecular weight organic compounds that are ubiquitous in everyday fermented foods. Histamine and tyramine in biogenic amine are most toxic, and toxic and allergic reactions such as headache, nausea, vomiting, palpitation, flush, breath disorder and the like can be caused when a human body takes excessive biogenic amine (especially multi-component biogenic amine is taken simultaneously), and the life can be seriously threatened; when excessive biogenic amine and alcohol are mixed and act on human bodies, the anaphylactic reaction and the toxic reaction of the biogenic amine are improved by orders of magnitude, so that the anaphylactic reaction of the biogenic amine existing in the wine to the human bodies is more severe.
Reducing the content of the top substances in the wine is the market demand for improving the comfort level, pleasure feeling, health and safety after drinking, and is also the direction for improving the wine quality of national wine enterprises.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides a filling process for reducing the top materials in yellow wine.
In order to achieve the purpose, the invention provides the following technical scheme to realize the purpose:
a filling process for reducing the content of the upper substances in yellow rice wine comprises the following steps:
1) wine sucking: pumping the frozen and stored yellow wine into a complexing tank through a liquid pump;
2) and (3) oxidation: ozone generated by the ozone generator is directly introduced into the liquid pump to be mixed with yellow wine flowing through the liquid pump, and the yellow wine is subjected to oxidation treatment, wherein the supply amount of the ozone is 50-150L/h;
3) complexing: a complexing agent supply tank supplies a complexing agent to the complexing tank, and the yellow wine is stored in the complexing tank for 30-50min to carry out a complexing reaction to generate a large amount of particle groups to form a colloidal solution;
4) photoelectric purification and aging acceleration: after the complex reaction, the yellow wine passes through a photoelectron purification device which releases photoelectrons into the yellow wine to purify impurities in the yellow wine and enable molecules in the wine body to oscillate mutually to form stable macromolecular groups;
5) adsorption: the yellow rice wine enters an adsorption tank and passes through the adsorption tank from top to bottom, and the yellow rice wine is adsorbed by the activated carbon in the adsorption tank;
6) purifying: purifying the yellow wine in a purifier;
7) filtering with diatomite and fine filter;
8) storing in a clear wine tank;
9) sterilizing at high temperature;
10) and (6) filling and sealing.
Preferably, the yellow wine treated in the step 10 is tested, packaged, stored and transported.
Preferably, the number of the complexing tanks is two, and the two complexing tanks are connected in parallel.
Preferably, the number of the optoelectronic purification devices is three, and the three optoelectronic purification devices are connected in series in a head-to-tail sequential manner.
Compared with the prior art, the invention has the beneficial effects that: ozone is a relatively active gas existing in the form of low-temperature plasma, and has strong oxidizing property and sterilization function; complexing to make the wine body form a colloidal solution, and adsorbing impurities in the wine body by using the active carbon; the yellow wine is oxidized, complexed and adsorbed, so that the contents of biogenic amine, purine and higher alcohol in the yellow wine can be effectively reduced.
Drawings
FIG. 1 is a schematic view of the structure of a treating apparatus in the present invention.
Detailed Description
An embodiment of the present invention will be described in detail below with reference to fig. 1.
A filling process for reducing the content of the upper substances in yellow rice wine comprises the following steps:
1) wine sucking: pumping the frozen and stored yellow wine into a complexing tank (2) through a liquid pump (1);
2) and (3) oxidation: ozone generated by the ozone generator (4) is directly introduced into the liquid pump (1) to be mixed with yellow wine flowing through the liquid pump, the yellow wine is oxidized, the supply amount of the ozone is 50-150L/h,
3) complexing: the complexing agent supply tank (3) supplies complexing agent into the complexing tank (2), the yellow wine is stored in the complexing tank (2) for 30-50min for complexing reaction to generate a large amount of particle groups to form colloidal solution;
4) photoelectric purification and aging acceleration: after the complex reaction, the yellow wine passes through the photoelectron purification device (5), the photoelectron purification device (5) releases photoelectrons into the yellow wine to purify impurities in the yellow wine and enable molecules in the wine body to oscillate mutually to form stable macromolecular groups;
5) adsorption: the yellow wine enters the adsorption tank (6), passes through the adsorption tank (6) from top to bottom, and is adsorbed by the activated carbon in the adsorption tank;
6) purifying: the yellow wine enters a purifier (7) for purification treatment;
7) filtering with diatomite and fine filter;
8) storing in a clear wine tank;
9) sterilizing at high temperature;
10) and (6) filling and sealing.
Preferably, the yellow wine treated in the step 10 is subjected to wine testing, packaging, storage and transportation.
Preferably, the number of the complexing tanks (2) is two, and the two complexing tanks (2) are connected in parallel.
Preferably, the number of the photoelectron purification devices (5) is three, and the three photoelectron purification devices (5) are connected in series in a head-to-tail sequential manner.
Preferably, the complexing agent is one or a combination of more of calcium sulfate, phosphoric acid and sodium hexametaphosphate.
Ozone is a very active gas existing in a low-temperature plasma form, has strong oxidizability, and can oxidize harmful components in yellow wine to generate chemical pronunciation and finally generate harmless substances. The low-temperature plasma has an excellent sterilization function, and the electric shearing force generated by the generated electrostatic action on the surfaces of various microorganisms such as bacteria, viruses, biological enzymes and the like is greater than the surface tension of cell membranes, so that the cell membranes are damaged, and the microorganisms die.
The complexing agent is added into the complexing tank to accelerate the complexing reaction taking metal ions as the core, so that a large number of particle groups are generated to form colloidal solution.
The photoelectron purification device (5) is internally provided with a light source and a photocatalyst. The photoelectron energy (hv) generated by the light source is not less than the forbidden band width (E) of the semiconductor materialg) When the light irradiates the semiconductor photocatalyst, free radicals (OH) with strong oxidation effect and the like are generated on the surface of the photocatalyst, and the ozone filled in the photocatalyst has strong oxidation property, so that foreign flavor and unsaturated compounds in the wine, such as aldehydes, sulfides, fusel oil, waste bran flavor in the wine and harmful substances, can be oxidized into water and carbon dioxide; at the same time, the surface of the catalyst also generates [ O ] with pre-reduction capability2 -]And (4) waiting for free radicals to reduce heavy metal ions in the wine so as to remove precipitates.
The wine solution has all the characteristics of a colloidal solution, and has a considerable amount of particle clusters taking metal ions and non-metal ions as cores besides dissolved gas. The longer the yellow wine is stored, the more abundant the macromolecular group particles contained in the yellow wine are, the more rich the mellow feeling and the flavor of the corresponding wine are, and the unique style of the mature Chinese yellow wine is formed. The photoelectron energy makes the molecules in the wine oscillate mutually to form stable macromolecular groups, so as to reach the maturity of wine similar to that of the year. The wine body is subjected to photoelectron catalysis to form rich metal ion gel cores, so that the volatilization speed of aroma components in the wine is greatly reduced, and the same effect as that of aged wine which is fermented for a long time and stored for a long time is achieved.
The low-temperature plasma can promote the Maillard reaction of amino acid and monosaccharide in the wine to generate pyrazine and furan substances, thereby accelerating the aging of the yellow wine.
The activated carbon can adsorb harmful substances and impurities in the yellow wine.
The wine samples before and after treatment were analyzed and compared with yellow wine aged for 5 years, and the results are shown in the following table:
Figure BDA0002602457620000051
the contents of amino acids and esters in the processed yellow wine are close to those in the yellow wine aged for 5 years, and the contents of biogenic amine, higher alcohol and purine in the processed yellow wine are obviously reduced compared with those before the processing.
The above description is only a preferred embodiment of the present invention, and the protection scope of the present invention is not limited to the above embodiments, and all technical solutions belonging to the idea of the present invention belong to the protection scope of the present invention. It should be noted that modifications and embellishments within the scope of the invention may occur to those skilled in the art without departing from the principle of the invention, and are considered to be within the scope of the invention.

Claims (5)

1. A filling process for reducing the top substances in yellow rice wine is characterized in that: the method comprises the following steps:
1) wine sucking: pumping the frozen and stored yellow wine into a complexing tank (2) through a liquid pump (1);
2) and (3) oxidation: ozone generated by the ozone generator (4) is directly introduced into the liquid pump (1) to be mixed with yellow wine flowing through the liquid pump, and the yellow wine is oxidized;
3) complexing: the complexing agent supply tank (3) supplies a complexing agent into the complexing tank (2) to carry out complexing reaction on the yellow wine, so that a large amount of particle groups are generated to form a colloidal solution;
4) photoelectric purification and aging acceleration: after the complex reaction, the yellow wine passes through the photoelectron purification device (5), the photoelectron purification device (5) releases photoelectrons into the yellow wine to purify impurities in the yellow wine and enable molecules in the wine body to oscillate mutually to form stable macromolecular groups;
5) adsorption: yellow rice wine enters the adsorption tank (6), passes through the adsorption tank (6) from top to bottom, and is adsorbed by activated carbon arranged in the adsorption tank (6);
6) purifying: the yellow wine enters a purifier (7) for purification treatment;
7) filtering with diatomite and fine filter;
8) storing in a clear wine tank;
9) sterilizing at high temperature;
10) and (6) filling and sealing.
2. The filling process for reducing the top substances in yellow rice wine according to claim 1, wherein the filling process comprises the following steps: and (4) testing, packaging, storing and transporting the yellow wine treated in the step (10).
3. The filling process for reducing the top substances in yellow rice wine according to claim 1, wherein the filling process comprises the following steps: the number of the complexing tanks is two, and the two complexing tanks are connected in parallel.
4. The filling process for reducing the top substances in yellow rice wine according to claim 1, wherein the filling process comprises the following steps: the number of the photoelectron purification devices is three, and the three photoelectron purification devices are connected in series in a head-to-tail sequential connection mode.
5. The filling process for reducing the top substances in yellow rice wine according to claim 1, wherein the filling process comprises the following steps: the complexing agent is one or more of calcium sulfate, phosphoric acid and sodium hexametaphosphate.
CN202010729291.3A 2020-07-27 2020-07-27 Filling process for reducing upper substances in yellow rice wine Pending CN111826257A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115247114A (en) * 2022-08-04 2022-10-28 李建东 Device and method for removing headache harmful ingredients under liquor rectification gaseous state
CN115261178A (en) * 2022-08-04 2022-11-01 李建东 White spirit production device and method for removing fusel oil, biogenic amine and ethyl carbamate
CN115287147A (en) * 2022-08-08 2022-11-04 李建东 Method and device for purifying harmful ingredients in white spirit by adopting plasma high-energy waves
CN115746990A (en) * 2022-08-08 2023-03-07 李建东 Method and device for producing white spirit by removing harmful substances such as fusel oil and the like

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101948732A (en) * 2010-10-14 2011-01-19 李建东 Method and device for purifying vinosity
CN103305393A (en) * 2013-06-04 2013-09-18 李光宇 Method and device for accelerating complexing and aging of wine
CN106978324A (en) * 2017-04-19 2017-07-25 吕兴龙 A kind of yellow rice wine turbidity removal filling process

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101948732A (en) * 2010-10-14 2011-01-19 李建东 Method and device for purifying vinosity
CN103305393A (en) * 2013-06-04 2013-09-18 李光宇 Method and device for accelerating complexing and aging of wine
CN106978324A (en) * 2017-04-19 2017-07-25 吕兴龙 A kind of yellow rice wine turbidity removal filling process

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
莫新良等主编: "《黄酒化学》", 30 November 2015, 中国轻工业出版社 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115247114A (en) * 2022-08-04 2022-10-28 李建东 Device and method for removing headache harmful ingredients under liquor rectification gaseous state
CN115261178A (en) * 2022-08-04 2022-11-01 李建东 White spirit production device and method for removing fusel oil, biogenic amine and ethyl carbamate
CN115287147A (en) * 2022-08-08 2022-11-04 李建东 Method and device for purifying harmful ingredients in white spirit by adopting plasma high-energy waves
CN115746990A (en) * 2022-08-08 2023-03-07 李建东 Method and device for producing white spirit by removing harmful substances such as fusel oil and the like

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Application publication date: 20201027