CN111808692A

CN111808692A - Chinese herbal medicine cow milk soap composition and preparation method thereof

Info

Publication number: CN111808692A
Application number: CN202010791562.8A
Authority: CN
Inventors: 石国凤; 王天兰; 柴艺汇; 李丽; 张璐姣; 苏芬菊; 饶柳
Original assignee: Guizhou University of Traditional Chinese Medicine
Current assignee: Guizhou University of Traditional Chinese Medicine
Priority date: 2020-08-07
Filing date: 2020-08-07
Publication date: 2020-10-23

Abstract

The invention relates to a Chinese herbal medicine cow milk soap composition, which comprises raw materials and auxiliary materials, wherein the raw materials and the auxiliary materials specifically comprise: 300-500 g of fibroin soap base, 50-150 ml of cow milk, 3-18 ml of chamomile extract or 3-18 g of chamomile powder, 0.002-0.005 ml of pigment, 0.002-0.005 ml of essence, 0.002-0.005 ml of foaming agent and 0.5-4 ml of vegetable oil. The invention combines traditional Chinese medicine chamomile and milk, develops the handmade soap suitable for middle-dry skin people to wash hands and baths and for people with non-sensitive skin to clean faces, and has the advantages of fashion, health, environmental protection and the like.

Description

Chinese herbal medicine cow milk soap composition and preparation method thereof

Technical Field

The invention relates to the field of washing and caring products, in particular to a Chinese herbal medicine cow milk soap composition and a preparation method thereof.

Background

Along with the increasing importance of people on the sanitation, the demand of skin cleaning products is also increasing, products such as hand sanitizer, soap, perfumed soap and the like are sold in the market, the perfumed soap of the existing brand contains a large amount of chemical components and is not good for the health of human bodies, and the development of a green environment-friendly skin cleaning product is urgently needed.

Prior art application No. CN201610963634.6, title of invention: the invention discloses a traditional Chinese medicine whitening perfumed soap and a preparation method thereof, and belongs to the technical field of washing products. The soap is prepared by mixing a traditional Chinese medicine composition and a soap base according to the mass ratio of 1:1 and then pressing, wherein the traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 10-20 parts of chamomile, 8-18 parts of spina gleditsiae, 10-20 parts of glossy privet fruit, 8-18 parts of liquorice, 6-12 parts of holy basil, 4-10 parts of evodia rutaecarpa, 4-10 parts of suberect spatholobus stem, 8-18 parts of rhizoma typhonii, 4-12 parts of divaricate saposhnikovia root, 6-12 parts of amur corktree bark, 3-9 parts of mint, 4-10 parts of selfheal and 4-10 parts of centella. The invention can effectively treat skin diseases such as acne, pimple, whelk, chloasma, freckle, dry peeling and the like, can effectively remove free radicals in skin, inhibit peroxide substances and remove the generation of brown pigment in the skin, and has the effects of moistening skin, beautifying, whitening and brightening the face and removing freckles.

Application No. CN201610963634.6 has the following drawbacks: 1. the medicine has more medicine flavor and high cost; 2. mainly aiming at skin diseases, the face cleaning effect needs to be further researched.

Application numberCN201811131809.2，Acne removing and whitening perfumed soap and preparation method thereofThe invention discloses acne-removing whitening perfumed soap and preparation thereofThe method belongs to the technical field of washing products. The acne-removing whitening perfumed soap is prepared by mixing a traditional Chinese medicine composition and a soap base according to the mass ratio of 1:1 and then pressing, wherein the traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 5-15 parts of chamomile, 6-18 parts of bighead atractylodes rhizome, 6-12 parts of glossy privet fruit, 4-12 parts of liquorice, 5-15 parts of patrinia, 6-12 parts of pinellia ternate, 4-12 parts of white morning glory, 5-15 parts of centella, 4-12 parts of paper mulberry fruit and 6-12 parts of cinnamomum camphora leaves. The invention also discloses a preparation method of the acne-removing whitening soap. The invention can effectively treat skin diseases such as acne, pimple, whelk, chloasma, freckle, dry peeling and the like, can effectively remove free radicals in skin, inhibit peroxide substances and remove the generation of brown pigment in the skin, and has the effects of moistening skin, beautifying, whitening and brightening the face and removing freckles.

But application numberCN201811131809.2The following drawbacks exist: 1. the medicine has more medicine flavor and high cost; 2. mainly aiming at skin diseases, the face cleaning effect needs to be further researched.

The traditional Chinese medicine chamomile is pungent, sweet and bitter in taste and slightly cold in nature, and enters lung and liver meridians. The Chinese medicinal composition is well known for having obvious effects of cooling, diminishing inflammation, sterilizing and relieving pain and calming nerves; beautifying, balancing the secretion of oil on the surface of the skin, replenishing water, moisturizing, resisting aging, moistening the skin, refining pores, dispelling wind, clearing heat, detoxifying, reducing swelling, improving eczema, pimple, herpes, psoriasis and general allergic phenomena and the like.

Cow milk is commonly called 'milk', is neutral in nature, sweet in taste, can tonify deficiency, tonify lung and stomach, promote the production of body fluid, moisten intestines, and moisten skin by external use.

In order to solve the problems, the invention combines traditional Chinese medicine chamomile with milk to develop the handmade soap which is suitable for middle-dry skin people to wash hands and baths and for people with insensitive skin to clean faces, is fashionable, healthy, green and environment-friendly.

Disclosure of Invention

The invention aims to provide a Chinese herbal medicine cow milk soap composition.

The invention also aims to provide a preparation method of the Chinese herbal medicine cow milk soap composition.

The Chinese herbal medicine cow milk soap composition comprises the following raw materials and auxiliary materials: 300-500 g of fibroin soap base, 50-150 ml of cow milk, 3-18 ml of chamomile extract or 3-18 g of chamomile powder.

Preferably, the raw materials of the invention consist of the following components: 330-480 g of fibroin soap base, 60-140 ml of cow milk, 5-16 ml of chamomile extract or 5-16 g of chamomile powder.

Further preferably, the raw materials of the invention consist of the following components: 350-460 g of fibroin soap base, 70-130 ml of cow milk, 7-13 ml of chamomile extract or 7-13 g of chamomile powder.

Further preferably, the raw materials of the invention consist of the following components: the raw materials consist of the following components: 380-430 g of fibroin soap base, 85-120 ml of cow milk, 9-11 ml of chamomile extract or 9-11 g of chamomile powder.

Further preferably, the raw materials of the invention consist of the following components: 400g of fibroin soap base, 100ml of cow milk juice, 10ml of chamomile extract or 10g of chamomile powder.

The auxiliary materials of the invention are: 0.002-0.005 ml of pigment, 0.002-0.005 ml of essence, 0.002-0.005 ml of foaming agent and 0.5-4 ml of vegetable oil.

Further preferred auxiliary materials of the invention are: 0.003ml of pigment, 0.003ml of essence, 0.003ml of foaming agent and 2ml of vegetable oil.

The preparation method of the Chinese herbal medicine cow milk soap composition comprises the following steps:

1) cutting the fibroin soap base into small pieces, putting the small pieces into a beaker, heating and melting the fibroin soap base, and cooling the fibroin soap base to 30-60 ℃ at normal temperature for later use after the fibroin soap base is completely melted;

2) uniformly mixing and blending chamomile extract or chamomile powder with unfrozen milk, and mixing the mixture for later use;

3) pouring the mixed solution into soap solution, and stirring for 15-55 minutes by using a constant-temperature magnetic stirrer to fully mix the mixed solution;

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

5) quickly pouring the prepared solution into a cleaning mould to wait for mould entering, and scraping surface bubbles by using a scraper to ensure that the surface of a soap product is smoother and more attractive;

6) standing for 1-5 hours at normal temperature after mold entering; or freezing the semi-solidified mixture in a refrigerator for 5 to 25 minutes;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Preferably, the preparation method comprises the following steps:

1) cutting the fibroin soap base into small pieces, putting the small pieces into a beaker, heating and melting the fibroin soap base, and cooling the fibroin soap base to 35-55 ℃ at normal temperature for later use after the fibroin soap base is completely melted;

3) pouring the mixed solution into soap solution, and stirring for 20-40 minutes by using a constant-temperature magnetic stirrer to fully and uniformly mix the mixed solution;

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

6) standing for 1-4 hours at normal temperature after mold entering; or after the semi-solidified state, putting the semi-solidified state into a refrigerator for freezing for 10 to 20 minutes;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Further preferably, the preparation method of the invention comprises the following steps:

1) cutting the fibroin soap base into small pieces, putting the small pieces into a beaker, heating and melting the fibroin soap base, and cooling the fibroin soap base to 40-50 ℃ at normal temperature for later use after the fibroin soap base is completely melted;

3) pouring the mixed solution into soap solution, and stirring for 30 minutes by using a constant-temperature magnetic stirrer to fully and uniformly mix the mixed solution;

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

6) standing for 1-3 hours at normal temperature after mold entering; or freezing for 15 minutes in a refrigerator after the semi-solidified state;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

The milk of the invention can also be replaced by other animal milks such as sheep milk, donkey milk and the like.

The chamomile extract can be a ready-made extract (cosmetic grade) purchased from the market, and can also be obtained by extracting according to a conventional reflux extraction method or an immersion method.

The vegetable oil of the present invention may be jojoba oil, olive oil, etc.

Has the advantages that:

1. the invention overcomes the problems of the prior art, and the traditional Chinese medicine chamomile is combined with milk to develop the handmade soap suitable for washing hands and bathing of people with dry and moderate skin and cleaning faces of people with non-sensitive skin.

2. The application numbers CN201610963634.6 and CN201811131809.2 in the prior art have the following defects: firstly, the medicine has more medicinal flavor and high cost; ② the cleansing effect is needed to be further studied mainly for dermatosis. The invention overcomes the defects of the prior art, adds milk into a single medicine, has low cost, and is suitable for hand washing, bath and face cleaning of people with dry skin.

3. Effectively care the skin, is fashionable and healthy, and is green and environment-friendly.

4. The preparation process can provide DIY experience for handmade soap makers, and has the advantages of simple process, easy learning of the method, safety and quick finished product yield.

5. Experiments prove that the skin feel and the moisturizing feel of the invention are good, the cleanliness reaches 9.6 minutes to the maximum, and the moisturizing performance reaches 9.0 minutes.

Detailed Description

The technical solution of the present invention will be further specifically described below by way of specific examples.

Example 1

The formula is as follows: 400g of fibroin soap base, 100ml of cow milk, 10ml of chamomile extract or chamomile powder, 0.003ml of pigment, 0.003ml of essence, 0.003ml of foaming agent and 2ml of vegetable oil.

The preparation method comprises the following steps:

1) cutting fibroin soap base into small pieces, putting the small pieces into a beaker, heating and melting, and cooling to 50 ℃ at normal temperature for later use after the fibroin soap base is completely melted;

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

6) standing for 3 hours at normal temperature after mold filling; or freezing for 15 minutes in a refrigerator after the semi-solidified state;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 2

The preparation method comprises the following steps:

1) cutting fibroin soap base into small pieces, putting the small pieces into a beaker, heating and melting, and cooling to 40 ℃ at normal temperature for later use after the fibroin soap base is completely melted;

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

6) standing for 1 hour at normal temperature after mold filling; or freezing for 15 minutes in a refrigerator after the semi-solidified state;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 3

The preparation method comprises the following steps:

1) cutting fibroin soap base into small pieces, putting the small pieces into a beaker, heating and melting, and cooling to 35 ℃ at normal temperature for later use after the fibroin soap base is completely melted;

3) pouring the mixed solution into soap solution, and stirring with a constant-temperature magnetic stirrer for 20 days to fully mix the mixed solution;

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

6) standing for 1 hour at normal temperature after mold filling; or freezing in refrigerator for 10 min after the semi-solidified state;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 4

The preparation method comprises the following steps:

1) cutting fibroin soap base into small pieces, putting the small pieces into a beaker, heating and melting, and cooling to 55 ℃ at normal temperature for later use after the fibroin soap base is completely melted;

3) pouring the mixed solution into soap solution, and stirring for 40 minutes by using a constant-temperature magnetic stirrer to fully and uniformly mix the mixed solution;

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

6) standing for 4 hours at normal temperature after mold filling; or freezing in refrigerator for 20 min after the semi-solidified state;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 5

The formula is as follows: 380g of fibroin soap base, 85ml of cow milk juice, 9ml of chamomile extract or 9g of chamomile powder, 0.002ml of pigment, 0.002ml of essence, 0.002ml of foaming agent and 0.5ml of vegetable oil.

The process comprises the following steps:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 6

The formula is as follows: 430g of fibroin soap base, 120ml of cow milk juice, 11ml of chamomile extract or 11g of chamomile powder, 0.005ml of pigment, 0.005ml of essence, 0.005ml of foaming agent and 4ml of vegetable oil.

The process comprises the following steps:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 7

The formula is as follows: 350g of fibroin soap base, 70ml of cow milk, 7ml of chamomile extract or 7g of chamomile powder, 0.003ml of pigment, 0.003ml of essence, 0.003ml of foaming agent and 2ml of vegetable oil.

The process comprises the following steps:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 8

The formula is as follows: 460g of fibroin soap base, 130ml of cow milk, 13ml of chamomile extract or 13g of chamomile powder, 0.003ml of pigment, 0.003ml of essence, 0.003ml of foaming agent and 2ml of vegetable oil.

The process comprises the following steps:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 9

The formula is as follows: 330g of fibroin soap base, 60ml of cow milk, 5ml of chamomile extract or 5g of chamomile powder, 0.003ml of pigment, 0.003ml of essence, 0.003ml of foaming agent and 2ml of vegetable oil.

The process comprises the following steps:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 10

The formula is as follows: 480g of fibroin soap base, 140ml of cow milk, 16ml of chamomile extract or 16g of chamomile powder, 0.003ml of pigment, 0.003ml of essence, 0.003ml of foaming agent and 2ml of vegetable oil.

The process comprises the following steps:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 11

The formula is as follows: 300g of fibroin soap base, 50ml of cow milk, 3ml of chamomile extract or 3g of chamomile powder, 0.003ml of pigment, 0.003ml of essence, 0.003ml of foaming agent and 2ml of vegetable oil.

The process comprises the following steps:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

Example 12

The formula is as follows: 500g of fibroin soap base, 150ml of cow milk, 18ml of chamomile extract or 18g of chamomile powder, 0.003ml of pigment, 0.003ml of essence, 0.003ml of foaming agent and 2ml of vegetable oil.

The process comprises the following steps:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

To further verify the feasibility of the present invention, the inventors performed the following experiments:

test example

First, sensory index detection

The standard requires that: appearance: the soap shape is regular and uniform in color and luster, and has no obvious impurities or stains; odor: has stable fragrance and no bad odor such as rancidity of oil and fat.

The sensory evaluation of examples 1 to 4 of the present invention was conducted, and the results are shown in Table 1

As a result: as is clear from Table 1, the sensory tests of examples 1 to 4 were all acceptable.

Second, other requirements and tests

The results of the detection of other indexes such as total free alkali and the like in examples 1 to 4 of the present invention according to the existing detection method are shown in Table 2

TABLE 2 tables of other items of examination results

As is clear from Table 2, the indexes of the experimental examples 1 to 4 were all checked and were all acceptable.

Third, cleaning effect test

Description of the test: selecting 40 subjects, randomly dividing into 4 groups, and using the product of example 1, evaluating skin feel and lubrication feel well, generally and poorly; the indexes of cleanliness and moisture retention are given 1-10 points, 10 points represent the most satisfactory, 0 point represents the unsatisfactory, and the test results are shown in Table 3.

TABLE 3 cleaning Effect table

As can be seen from Table 3, the skin feel and moisturized feel of the present invention were good, the cleanliness reached 9.6 minutes at the maximum, and the moisture retention reached 9.0 minutes.

Although the invention has been described in detail above with reference to a general description, specific embodiments and test examples, it will be apparent to those skilled in the art that modifications and improvements can be made based on the invention. Accordingly, such modifications and improvements are intended to be within the scope of the invention as claimed.

Claims

1. The Chinese herbal medicine cow milk soap composition is characterized by comprising raw materials and auxiliary materials, wherein the raw materials comprise the following components: 300-500 g of fibroin soap base, 50-150 ml of cow milk, 3-18 ml of chamomile extract or 3-18 g of chamomile powder.

2. The composition of claim 1, wherein the raw material consists of: 330-480 g of fibroin soap base, 60-140 ml of cow milk, 5-16 ml of chamomile extract or 5-16 g of chamomile powder.

3. The composition according to claim 2, characterized in that the raw material consists of: 350-460 g of fibroin soap base, 70-130 ml of cow milk, 7-13 ml of chamomile extract or 7-13 g of chamomile powder.

4. The composition of claim 3, wherein the raw material consists of: 380-430 g of fibroin soap base, 85-120 ml of cow milk, 9-11 ml of chamomile extract or 9-11 g of chamomile powder.

5. The composition according to claim 4, characterized in that the raw material consists of: 400g of fibroin soap base, 100ml of cow milk juice, 10ml of chamomile extract or 10g of chamomile powder.

6. The composition according to any one of claims 1 to 5, wherein the excipient is: 0.002-0.005 ml of pigment, 0.002-0.005 ml of essence, 0.002-0.005 ml of foaming agent and 0.5-4 ml of vegetable oil.

7. The composition according to claim 6, wherein the excipient is: 0.003ml of pigment, 0.003ml of essence, 0.003ml of foaming agent and 2ml of vegetable oil.

8. The method of preparing a herbal cow's milk soap composition as claimed in claim 1, wherein said method comprises the steps of:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

9. The method for preparing according to claim 8, characterized in that it comprises the following steps:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.

10. The method for preparing according to claim 9, characterized in that it comprises the following steps:

4) adding auxiliary materials, and stirring again to fully and uniformly mix;

7) demolding;

8) and (5) demolding, standing for 3-5 minutes, and packaging the product.