CN111807387A - Potassium nitrate purification device - Google Patents

Potassium nitrate purification device Download PDF

Info

Publication number
CN111807387A
CN111807387A CN202010757771.0A CN202010757771A CN111807387A CN 111807387 A CN111807387 A CN 111807387A CN 202010757771 A CN202010757771 A CN 202010757771A CN 111807387 A CN111807387 A CN 111807387A
Authority
CN
China
Prior art keywords
potassium nitrate
bottom plate
jar body
solution
wall
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202010757771.0A
Other languages
Chinese (zh)
Inventor
孙立辉
王俊峰
高斌
刘国洪
邱刚
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shandong Wealth Chemical Engineering Co ltd
Original Assignee
Shandong Wealth Chemical Engineering Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shandong Wealth Chemical Engineering Co ltd filed Critical Shandong Wealth Chemical Engineering Co ltd
Priority to CN202010757771.0A priority Critical patent/CN111807387A/en
Publication of CN111807387A publication Critical patent/CN111807387A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D9/00Nitrates of sodium, potassium or alkali metals in general
    • C01D9/16Purification
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a potassium nitrate purifying device which comprises a bottom plate, a fixed rod, a mounting frame and a tank body, wherein support rods are welded on the outer wall of the tank body at equal intervals, the bottom ends of the support rods are welded on the upper surface of the bottom plate, a supporting seat is welded on the lower surface of the bottom plate, a discharge port is formed in the bottom end of the inner wall of the tank body, a connecting buckle is movably clamped at the upper end of the fixed rod and fixed on the outer wall of the upper end of the tank body through bolts, a power wire is arranged at one end of the fixed rod, an electric heating rod is arranged at the other end of the fixed rod, two ends of the mounting frame are welded on. The invention has compact structure and convenient use, is convenient for heating and circulating the solution, improves the purification efficiency and meets the use requirements of personnel.

Description

Potassium nitrate purification device
Technical Field
The invention relates to the technical field of substance purification, in particular to a potassium nitrate purification device.
Background
Potassium nitrate refers to nitrate of potassium, commonly called potassium nitrate or soil nitrate, is colorless transparent orthorhombic crystal or rhombic crystal or white powder, and has no odor, no toxicity, salty taste and cool feeling. The water-soluble polyurethane has the advantages of small moisture absorption in air, difficult agglomeration, easy water solubility and rapid increase of the solubility along with the temperature rise. Can be dissolved in liquid ammonia and glycerin, and can not be dissolved in absolute ethyl alcohol and ethyl ether, and the potassium nitrate is a strong oxidant, and can be contacted with organic matter to cause combustion and explosion. Therefore, the potassium nitrate should be stored in a cool and dry place away from the fire and heat sources. The materials are not mixed with reducing agent, acid, easily combustible substance and metal powder.
Because the solubility of potassium nitrate is greatly changed along with the temperature, and the solubility is smaller at low temperature, the cooling crystallization (cooling of a hot saturated solution) is the best method, the principle of the cooling crystallization is that the temperature is reduced, the solubility of a substance is reduced, the solution is saturated, and redundant solute which cannot be dissolved can be separated out. For example, alkali removal in winter is the reason (by using temperature change). The principle of evaporative crystallization is that under the condition of constant temperature or before and after evaporation, the temperature is unchanged, the solubility is unchanged, the water content is reduced, and the solution is saturated, namely redundant solute is separated out. For example, the salt is sun-dried in the salt lake in summer, the temperature is reduced for crystallization, the solution is heated and concentrated to obtain a hot saturated solution, then the hot saturated solution is filtered to remove insoluble impurities, the crystals are cooled for crystallization and filtered, the obtained crystals can contain other impurities, and the crystals are recrystallized if further purification is needed.
Traditional purification device adopts the end hot type usually, and the circulation and the transfer of inconvenient solution for this reason, and the end hot type is inconvenient being heated of solution even, reduces reaction efficiency by a wide margin, can not satisfy personnel's user demand.
Disclosure of Invention
The invention aims to provide a potassium nitrate purifying device which has the advantages of compact structure, convenience in use, convenience in heating and circulating of solution, improvement in purifying efficiency and capability of meeting the use requirements of personnel, and solves the problems that the traditional purifying device usually adopts a bottom heating type, so that the circulation and transfer of the solution are inconvenient, the bottom heating type is inconvenient, the solution is uniformly heated, the reaction efficiency is greatly reduced, and the use requirements of the personnel cannot be met.
In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides a potassium nitrate purification device, includes bottom plate, dead lever, mounting bracket and jar body, the outer wall equidistance welding of the jar body has the bracing piece, and the bottom welding of bracing piece is at the upper surface of bottom plate, the lower skin weld of bottom plate has the supporting seat, and the inner wall bottom of the jar body is equipped with the discharge port, the upper end activity joint of dead lever has the connector link, and the connector link passes through the bolt fastening at the upper end outer wall of the jar body, and the one end of dead lever is equipped with the power cord, and the other end of dead lever is equipped with the electric bar, the both ends welding of mounting bracket is at the upper surface of.
Preferably, the lower surface of the tank body is provided with a connecting pipe, a butterfly valve body is installed on the connecting pipe, and the connecting pipe corresponds to the position of the discharge port.
Preferably, a wire hole matched with the power wire is arranged in the fixing rod, and the power wire penetrates through the wire hole to be electrically connected with the electric heating rod.
Preferably, the lower end of the stirring shaft is provided with a stirring blade, and the stirring blade is positioned in the middle of the lower end of the inner wall of the tank body.
Preferably, the mounting frame is provided with a rotating hole matched with the stirring shaft, and the stirring shaft is rotatably arranged in the rotating hole.
Preferably, the number of the supporting seats is four, and the four supporting seats are distributed on the lower surface of the bottom plate in a rectangular array.
Compared with the prior art, the invention has the following beneficial effects:
during the use of the potassium nitrate purifying device, the solution and the raw materials can be poured into the tank body to dissolve the raw materials in the solution medium, the electric heating rod is electrified to work by switching on an external power supply to generate heat, the solution in the tank body is heated, the saturated solution is obtained by heating and concentrating, at the moment, the motor body is electrified to work the stirring shaft which stirs the solution to uniformly heat the solution and accelerate the material to be dissolved in the solution, when the solution tends to be saturated, the butterfly valve body can be opened to enable the solution in the tank body to fall down together with insoluble impurities, the solution enters the external heat filtering device through the connecting pipe to be filtered and purified, and then the temperature is reduced (cooled to room temperature) to separate out crystals from the saturated solution, so that the potassium nitrate purifying device has a compact structure, is convenient to use, facilitates the heating and the circulation of the solution, and improves the purifying efficiency, the use requirements of personnel are met.
Drawings
FIG. 1 is a schematic front view of the present invention;
FIG. 2 is a schematic top view of the present invention;
FIG. 3 is a schematic structural diagram of A in FIG. 1 according to the present invention.
In the figure: 1. a base plate; 2. a butterfly valve body; 3. a discharge port; 4. a connecting pipe; 5. a support bar; 6. a supporting seat; 7. an electric heating rod; 8. fixing the rod; 9. a mounting frame; 10. a motor body; 11. a tank body; 12. a stirring shaft; 13. stirring blades; 14. a power line; 15. a connecting buckle.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "front", "rear", "both ends", "one end", "the other end", and the like indicate orientations or positional relationships based on those shown in the drawings, and are only for convenience of description and simplicity of description, but do not indicate or imply that the referred device or element must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "connected," and the like are to be construed broadly, such as "connected," which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1 to 3, an embodiment of the present invention includes: the utility model provides a potassium nitrate purification device, includes bottom plate 1, dead lever 8, mounting bracket 9 and jar body 11, and the outer wall equidistance welding of jar body 11 has bracing piece 5, and the bottom welding of bracing piece 5 is at the upper surface of bottom plate 1, and the lower skin weld of bottom plate 1 has supporting seat 6, and supporting seat 6 is four altogether, and four supporting seats 6 are rectangle array distribution at the lower surface of bottom plate 1, in the use, can empty solution and raw materials and get into jar body 11 in for the raw materials dissolves in the solution medium.
The inner wall bottom of the jar body 11 is equipped with the discharge port 3, the upper end activity joint of dead lever 8 has connector link 15, connector link 15 passes through the bolt fastening at the upper end outer wall of the jar body 11, and the one end of dead lever 8 is equipped with power cord 14, the other end of dead lever 8 is equipped with electric rod 7, be equipped with the line hole with 14 looks adaptations of power cord in the dead lever 8, and power cord 14 passes the line hole and is connected with electric rod 7 electricity each other, through switch-on external power supply, make electric rod 7 circular telegram work, and then produce the heat, heat the solution in the jar body 11, obtain saturated solution through heating concentration.
It should be noted that the structure of the electric heating rod 7 is the existing mature technology, the working principle and the internal structure thereof are known to those skilled in the art, and the present invention only utilizes the function thereof and does not improve the internal structure thereof, and therefore, detailed description thereof is omitted.
The both ends welding of mounting bracket 9 is at the upper surface of bottom plate 1, and the upper surface of mounting bracket 9 is equipped with motor body 10, rotate on the motor body 10 and install (mixing) shaft 12, be equipped with the rotation hole with (mixing) shaft 12 looks adaptation on mounting bracket 9, and (mixing) shaft 12 rotates and installs in rotating the hole, the lower extreme of (mixing) shaft 12 is equipped with stirring leaf 13, and stirring leaf 13 is located the inner wall lower extreme intermediate position department of jar body 11, motor body 10 circular telegram makes (mixing) shaft 12 work, stirring shaft 12 stirs solution, make solution be heated evenly, the material dissolves in solution with higher speed.
The motor body 10 is 5IK40RGN-C, and has the advantages of low noise, high efficiency, long service life and the like.
The lower surface of the jar body 11 is equipped with connecting pipe 4, install butterfly valve body 2 on the connecting pipe 4, and connecting pipe 4 is corresponding with the position of discharge port 3, when solution tends to the saturation, can open butterfly valve body 2 and make the interior solution of jar body 11 together with insoluble impurity whereabouts, enter into external hot filter equipment through connecting pipe 4 in, filter the purification to solution, then rethread reduce temperature (cool to room temperature), make the crystal appear from saturated solution can, compact structure, it is convenient to use, make things convenient for the heating and the circulation of solution, improve purification efficiency, satisfy personnel's user demand.
The working principle is as follows: during the use of the potassium nitrate purifying device, the solution and the raw materials can be poured into the tank body 11 to be dissolved in the solution medium, the electric heating rod 7 is electrified to work by switching on an external power supply to generate heat, the solution in the tank body 11 is heated, saturated solution is obtained by heating and concentrating, at the moment, the motor body 10 is electrified to work the stirring shaft 12, the stirring shaft 12 is used for stirring the solution to uniformly heat the solution, the dissolution of the materials in the solution is accelerated, when the solution tends to be saturated, the butterfly valve body 2 can be opened to enable the solution in the tank body 11 and insoluble impurities to fall down, the solution enters an external hot filtering device through the connecting pipe 4 to be filtered and purified, and then the temperature is reduced (cooled to room temperature) to separate out crystals from the saturated solution.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.

Claims (6)

1. The utility model provides a potassium nitrate purification device, includes bottom plate (1), dead lever (8), mounting bracket (9) and jar body (11), its characterized in that: the utility model discloses a storage tank, including the jar body (11), the outer wall equidistance welding of the jar body has bracing piece (5), and the bottom welding of bracing piece (5) is at the upper surface of bottom plate (1), the lower skin weld of bottom plate (1) has supporting seat (6), and the inner wall bottom of the jar body (11) is equipped with discharge port (3), the upper end activity joint of dead lever (8) has connector link (15), and connector link (15) pass through the bolt fastening at the upper end outer wall of the jar body (11), and the one end of dead lever (8) is equipped with power cord (14), and the other end of dead lever (8) is equipped with electrical bar (7), the both ends welding of mounting bracket (9) is at the upper surface of bottom plate (1), and the upper surface of mounting bracket (9) is equipped with.
2. The potassium nitrate purifying apparatus according to claim 1, wherein: the lower surface of the tank body (11) is provided with a connecting pipe (4), the connecting pipe (4) is provided with a butterfly valve body (2), and the connecting pipe (4) corresponds to the position of the discharge port (3).
3. The potassium nitrate purifying apparatus according to claim 1, wherein: a wire hole matched with the power wire (14) is formed in the fixing rod (8), and the power wire (14) penetrates through the wire hole to be electrically connected with the electric heating rod (7).
4. The potassium nitrate purifying apparatus according to claim 1, wherein: the lower extreme of (mixing) shaft (12) is equipped with stirring leaf (13), and stirring leaf (13) are located the inner wall lower extreme intermediate position department of jar body (11).
5. The potassium nitrate purifying apparatus according to claim 1, wherein: the mounting rack (9) is provided with a rotating hole matched with the stirring shaft (12), and the stirring shaft (12) is rotatably arranged in the rotating hole.
6. The potassium nitrate purifying apparatus according to claim 1, wherein: the number of the supporting seats (6) is four, and the four supporting seats (6) are distributed on the lower surface of the bottom plate (1) in a rectangular array.
CN202010757771.0A 2020-07-31 2020-07-31 Potassium nitrate purification device Pending CN111807387A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010757771.0A CN111807387A (en) 2020-07-31 2020-07-31 Potassium nitrate purification device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202010757771.0A CN111807387A (en) 2020-07-31 2020-07-31 Potassium nitrate purification device

Publications (1)

Publication Number Publication Date
CN111807387A true CN111807387A (en) 2020-10-23

Family

ID=72863475

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202010757771.0A Pending CN111807387A (en) 2020-07-31 2020-07-31 Potassium nitrate purification device

Country Status (1)

Country Link
CN (1) CN111807387A (en)

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2011152457A (en) * 2011-12-22 2013-06-27 Федеральное Государственное Унитарное Предприятие "Государственный Ордена Трудового Красного Знамени Научно-Исследовательский Институт Химических Реактивов И Особо Чистых Химических Веществ" METHOD FOR CLEANING POTASSIUM NITRATE
CN203668013U (en) * 2013-12-06 2014-06-25 宏达光电玻璃(东莞)有限公司 Potassium nitrate purification equipment
CN104891766A (en) * 2015-06-10 2015-09-09 北京洁绿科技发展有限公司 Sludge pyrohydrolysis device and method
CN204897432U (en) * 2015-08-25 2015-12-23 浏阳市金和化工有限公司 Potassium nitrate fast reaction separator
CN205235454U (en) * 2015-12-14 2016-05-18 昆明青上化工有限公司 A reactive crystallization groove for producing potassium nitrate
CN205435743U (en) * 2016-03-28 2016-08-10 苏州美嘉汇食品科技有限公司 Reaction kettle
CN106955653A (en) * 2017-03-07 2017-07-18 中信大锰矿业有限责任公司 A kind of reactor of net cover type agitator
CN207957787U (en) * 2018-01-19 2018-10-12 江西金利达钾业有限责任公司 A kind of potassium nitrate equipment for purifying
CN108970569A (en) * 2018-09-26 2018-12-11 浙江省嘉善县第中学 A kind of reaction unit for chemical experiment
CN210825456U (en) * 2019-09-23 2020-06-23 湖南美奥钾业有限责任公司 A purification device for potassium nitrate processing
CN210825455U (en) * 2019-09-23 2020-06-23 湖南美奥钾业有限责任公司 High-efficient purification device of potassium nitrate

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2011152457A (en) * 2011-12-22 2013-06-27 Федеральное Государственное Унитарное Предприятие "Государственный Ордена Трудового Красного Знамени Научно-Исследовательский Институт Химических Реактивов И Особо Чистых Химических Веществ" METHOD FOR CLEANING POTASSIUM NITRATE
CN203668013U (en) * 2013-12-06 2014-06-25 宏达光电玻璃(东莞)有限公司 Potassium nitrate purification equipment
CN104891766A (en) * 2015-06-10 2015-09-09 北京洁绿科技发展有限公司 Sludge pyrohydrolysis device and method
CN204897432U (en) * 2015-08-25 2015-12-23 浏阳市金和化工有限公司 Potassium nitrate fast reaction separator
CN205235454U (en) * 2015-12-14 2016-05-18 昆明青上化工有限公司 A reactive crystallization groove for producing potassium nitrate
CN205435743U (en) * 2016-03-28 2016-08-10 苏州美嘉汇食品科技有限公司 Reaction kettle
CN106955653A (en) * 2017-03-07 2017-07-18 中信大锰矿业有限责任公司 A kind of reactor of net cover type agitator
CN207957787U (en) * 2018-01-19 2018-10-12 江西金利达钾业有限责任公司 A kind of potassium nitrate equipment for purifying
CN108970569A (en) * 2018-09-26 2018-12-11 浙江省嘉善县第中学 A kind of reaction unit for chemical experiment
CN210825456U (en) * 2019-09-23 2020-06-23 湖南美奥钾业有限责任公司 A purification device for potassium nitrate processing
CN210825455U (en) * 2019-09-23 2020-06-23 湖南美奥钾业有限责任公司 High-efficient purification device of potassium nitrate

Similar Documents

Publication Publication Date Title
CN111807387A (en) Potassium nitrate purification device
CN213636110U (en) High radiating lithium cell
CN113666346A (en) Short-path distillation efficient purification device and purification method for lithium bis (fluorosulfonyl) imide
CN109817992A (en) A kind of preparation method of the dedicated redox elctro-catalyst of magnesium air fuel cell
CN218291146U (en) Low-energy-consumption micro-arc oxidation power supply
CN216077733U (en) Fan is from forced air cooling structure
CN115869699A (en) Lithium hexafluorophosphate purification device and purification method
CN217489495U (en) Medical hydrogen-oxygen therapeutic apparatus
CN212085481U (en) Extension type switch board
CN210825455U (en) High-efficient purification device of potassium nitrate
CN212269459U (en) Water-cooling ozone generator
CN211026172U (en) High-efficient refrigerated graphite sulphuric acid dilutes cooler
CN217025673U (en) Rural domestic sewage integration treatment device of efficient
CN110787479A (en) Purification and crystallization device for zinc sulfate production and preparation method thereof
CN111533195A (en) Internal combustion type evaporation cylinder device used on waste water treatment equipment
CN212417134U (en) Circulating water wisdom thing allies oneself with system
CN214551308U (en) High-purity potassium purification is with freezing crystallization device
CN215601745U (en) Pure water cooling system
CN213714018U (en) Cooling tower convenient to transport
CN213984655U (en) A cooling tower spray pump pipeline structure for aqueous ammonia production
CN215723739U (en) Softened water recycling system
CN221045978U (en) Battery slurry mixing device
CN212158298U (en) Cooling tower vapor recovery device
CN212005867U (en) Wind energy heating device based on floor heating stone
CN214172683U (en) Waste heat utilization equipment for absolute ethyl alcohol production

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20201023