CN111793533A - Herbal essence silk soap and preparation method thereof - Google Patents
Herbal essence silk soap and preparation method thereof Download PDFInfo
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- CN111793533A CN111793533A CN202010702522.1A CN202010702522A CN111793533A CN 111793533 A CN111793533 A CN 111793533A CN 202010702522 A CN202010702522 A CN 202010702522A CN 111793533 A CN111793533 A CN 111793533A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/40—Proteins
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Dermatology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a herbal essence silk soap and a preparation method thereof, wherein the herbal essence silk soap comprises 100 parts of herbal essence, 550 parts of grease, 50 parts of organic amine and 50 parts of fibroin; the essence is one or more of wild chrysanthemum flower, erigeron breviscapus, dandelion, semen cuscutae, white paeony root and bitter almond extract. The herbal plant essence can help the skin to resist inflammation, relieve swelling and pain, and inhibit the breeding of bacteria on the skin; the fibroin can penetrate into the skin to provide nutrition for the skin, promote the metabolism of the skin and accelerate the repair of the skin. The invention can effectively relieve the inflammatory reaction of the skin, simultaneously help the skin to recover the elasticity and repair scars, and has good market value.
Description
Technical Field
The invention relates to the field of soaps, and particularly relates to a herbal essence silk soap and a preparation method thereof.
Background
Soap is a common cleaning and skin care product in daily life and has a long history. With the continuous development of science and technology, the continuous improvement and perfection of technological equipment, various types of toilet soaps come out one after another, and the quality and grade of products are continuously improved. At present, the variety of soap is developed from single cleaning soap into functional soap with complete variety and multiple functions.
Due to the fact that the pace of life is accelerated, the problems of irregular diet, night stay, insufficient sleep and the like commonly exist in the young people at present. These problems affect the health of the body and are collectively reflected in the face as blackheads, acne, pimples, sallow complexion, and the like.
Therefore, there is a need in the market for a soap that helps the facial skin alleviate the inflammatory symptoms and repair the facial skin.
Disclosure of Invention
The invention aims to help the face relieve inflammation symptoms, repair the face skin and improve the face skin. The scheme of the invention is as follows:
the herbal essence silk soap comprises the following components in parts by weight:
100 parts of herbal essence, 550 parts of grease, 50 parts of organic amine and 50 parts of fibroin;
the herbal essence is one or more of extractive solutions of flos Chrysanthemi Indici, flos Hibisci, herba Taraxaci, semen Cuscutae, radix Paeoniae alba, and semen Armeniacae amarum.
The invention also discloses a preparation method of the herbal essence silk soap, which comprises the following steps:
s1, extracting herbal essence;
s2, extracting fibroin;
s3, adding the herbal essence obtained in S1 and the fibroin obtained in S2 into organic amine, and uniformly stirring;
s4, heating and melting the grease, and then cooling to 45-50 ℃;
s5, mixing the soap liquid obtained in the steps S3 and S4, pouring the mixture into a mold after stirring the mixture into a viscous state, forming the mixture after saponification reaction in the mold for 12 to 36 hours, demolding, and putting the mixture into a constant temperature cabinet for heat preservation for 12 to 36 hours;
and S6, taking out, airing and packaging.
As an improvement, the herbal essence consists of the following components in parts by weight:
10 parts of wild chrysanthemum flower, 8 parts of erigeron breviscapus, 10 parts of dandelion, 8 parts of semen cuscutae, 5 parts of white paeony root and 5 parts of bitter almond.
As an improvement, the oil and fat is selected from one or more of grape seed oil, palm oil, olive oil, almond oil, coconut oil and cocoa butter.
As an improvement, the grease comprises the following components in parts by weight:
100 parts of grape seed oil, 100 parts of palm oil, 100 parts of olive oil, 100 parts of almond oil, 100 parts of coconut oil and 50 parts of cocoa butter.
In the improvement, the S1 extracted herbal essence comprises extracted semen cuscutae, radix paeoniae alba and semen armeniacae amarae essence and extracted wild chrysanthemum flower, erigeron breviscapus and dandelion essence; the essence of semen Cuscutae, radix Paeoniae alba and semen Armeniacae amarum is prepared by alcohol extraction method, and the essence of flos Chrysanthemi Indici, flos Hibisci and herba Taraxaci is prepared by distillation method.
As an improvement, the process flow of the alcohol extraction method is as follows: pulverizing, soaking in ethanol for 24-72h, filtering to obtain liquid phase, decocting the filtrate to obtain syrup, extracting with anhydrous ethanol and gelatin water solution, filtering, freezing for 12-36h, evaporating to dryness, dissolving in distilled water, decolorizing with active carbon, filtering, extracting with diethyl ether, and drying with anhydrous sodium sulfate to obtain semen Cuscutae, radix Paeoniae alba, and semen Armeniacae amarum essence; the distillation method comprises the following process flows: soaking the raw materials in water for 20-40min, decocting for 15-30min, filtering, rehydrating for 15-30min, filtering again, distilling the effective components in the filtrate, and concentrating under reflux to obtain flos Chrysanthemi Indici, herba Erigerontis and herba Taraxaci essence.
As an improvement, the silk protein extraction in S2 comprises boiling silkworm cocoon in sodium carbonate solution for degumming, separating solid phase and liquid phase to obtain sericin solution and silk fibroin fiber, extracting sericin in the sericin solution by freezing method, extracting silk fibroin from the silk fibroin fiber by enzymolysis method, and mixing the sericin and the silk fibroin.
As an improvement, the technological process for extracting sericin by a freezing method comprises the following steps: adding activated carbon into sericin solution, decolorizing at 70-90 deg.C, filtering to obtain liquid phase, concentrating the filtrate, freezing at pH 5 and-20 deg.C for 10-14h, naturally thawing, filtering to obtain solid phase to obtain sericin; the technological process for extracting the silk fibroin by the enzymolysis method comprises the following steps: adding silk fibroin into 40% calcium chloride solution, hydrolyzing at 90-100 deg.C for 1 hr, cooling, adding alkaline protease at 45 deg.C, hydrolyzing for 7-10 hr, dialyzing, and desalting to obtain silk fibroin.
As an improvement, the degumming time of the silkworm cocoons in the sodium carbonate solution by boiling is 20-40min, and the reaction pressure is 1-4 atmospheric pressures.
Flos Chrysanthemi Indici has effects of relieving swelling and pain, and has been used for treating swelling and pain and eczema since ancient times. The wild chrysanthemum contains the substances such as the feverfew alcohol, the feverfew ketone, the wild chrysanthemum lactone, the luteolin and the like, and has the effects of resisting inflammation and resisting allergy.
Herba Erigerontis has anticoagulant effect, and can improve facial microcirculation and promote metabolism of toxin in facial skin.
The dandelion has the functions of resisting bacteria and diminishing inflammation, and the taraxasterol, the choline, the inulin and the pectin in the dandelion can effectively kill the growth of staphylococcus aureus and hemolytic streptococcus, and also have better inhibiting effect on diplococcus pneumoniae, typhoid bacillus and the like. Can reduce the occurrence of facial acne.
The fibroin has strong hydrolysis and penetration capability, can enter the dermis of the skin after contacting the skin, provides nutrition for the skin, promotes skin repair, and prevents the generation of skin scar tissues.
The invention has the beneficial effects that:
according to the soap, a plurality of herbal plant essences and fibroin are added into the soap, and the herbal plant essences can help skin to resist inflammation, relieve swelling and pain and inhibit bacteria on the skin from breeding; the fibroin can penetrate into the skin to provide nutrition for the skin, promote the metabolism of the skin and accelerate the repair of the skin. The invention can effectively relieve the inflammatory reaction of the skin, simultaneously help the skin to recover the elasticity and repair scars, and has good market value.
Detailed Description
The invention is further illustrated by the following examples, which are not intended to limit the scope of the invention.
Example 1
The embodiment discloses a herbal essence silk soap, which comprises the following components in parts by weight:
100 parts of herbal essence, 550 parts of grease, 50 parts of organic amine and 50 parts of fibroin. The herbal essence consists of the following components: 21.7 parts of wild chrysanthemum flower, 17.36 parts of erigeron breviscapus, 21.7 parts of dandelion, 17.36 parts of semen cuscutae, 10.85 parts of white paeony root and 11.03 parts of bitter almond; the grease consists of the following components: 100 parts of grape seed oil, 100 parts of palm oil, 100 parts of olive oil, 100 parts of almond oil, 100 parts of coconut oil and 50 parts of cocoa butter.
Example 2
The embodiment discloses a preparation method of herbal essence silk soap, which comprises the following steps:
s1, extracting the plant essence, including extracting semen Cuscutae, radix Paeoniae alba, semen Armeniacae amarum essence and extracting flos Chrysanthemi Indici, herba Sidae Rhombifoliae, and herba Taraxaci essence.
Extracting semen Cuscutae, radix Paeoniae alba, and semen Armeniacae amarum essence by alcohol extraction method, and the process flow is: weighing 80g of semen cuscutae, 50g of radix paeoniae alba and 50g of bitter almond, crushing, soaking in ethanol for 48h, filtering in a suction filter to obtain a liquid phase, cooking the filtrate to be syrup, extracting and filtering twice by using absolute ethyl alcohol, extracting and filtering gelatin aqueous solution for 1 time, extracting and filtering once by using absolute ethyl alcohol, freezing for 24h, filtering and evaporating to dryness, dissolving by using distilled water, adding activated carbon for decoloring and filtering, extracting for 3 times by using ethyl ether, drying for 12h by using anhydrous sodium sulfate, and filtering to obtain the essence liquid of the semen cuscutae, the radix paeoniae alba and the bitter almond.
The mother chrysanthemum, erigeron breviscapus and dandelion essence liquid is extracted by a distillation method, and the process flow is as follows: weighing 100g of wild chrysanthemum, 80g of erigeron breviscapus and 100g of dandelion, soaking in water for 30min, decocting for 20min, filtering residues, carrying out secondary filtering residues after rehydration for 20min, distilling to remove active ingredients in the filtrate, and then adding a rotary evaporator for hot reflux concentration to obtain the wild chrysanthemum, erigeron breviscapus and dandelion essence.
Mixing the above two essences.
S2, extracting silk protein, adding 20g of silkworm cocoon into a sodium carbonate solution, boiling for 30min for degumming under the condition of 2 atmospheric pressures, separating a solid phase and a liquid phase to obtain a sericin solution and silk fibroin fibers, extracting the sericin in the sericin solution by a freezing method, extracting the silk fibroin from the silk fibroin fibers by an enzymatic hydrolysis method, and mixing the sericin and the silk fibroin.
The technological process for extracting sericin by a freezing method comprises the following steps: adding activated carbon into sericin solution, decolorizing at 80 deg.C for 30min, filtering to obtain liquid phase, concentrating the filtrate, freezing at pH 5 and-20 deg.C for 12h, naturally thawing, filtering to obtain solid phase to obtain sericin, and freezing, thawing, and filtering the liquid phase to improve sericin utilization rate.
The technological process for extracting the silk fibroin by the enzymolysis method comprises the following steps: adding the silk fibroin fibers into a 40% calcium chloride solution, hydrolyzing for 1h at 100 ℃, cooling, adding alkaline protease for hydrolysis for 8h at 45 ℃, dialyzing and desalting for 3h to obtain the silk fibroin.
Sericin and silk fibroin were combined.
S3, adding 100g of herbal essence obtained in S1 and 50g of fibroin obtained in S2 into 50g of organic amine, and uniformly stirring.
S4, mixing 100g of grape seed oil, 100g of palm oil, 100g of olive oil, 100g of almond oil, 100g of coconut oil and 50g of cocoa butter, heating for melting, and cooling to 45 ℃.
S5, mixing the raw materials obtained in the steps S3 and S4, stirring the mixture into a viscous state, pouring the viscous state into a mold, performing saponification reaction in the mold for 24 hours, molding, demolding, and placing the mold into a constant temperature box for heat preservation for 24 hours.
And S6, taking out, airing and packaging.
While specific embodiments of, and examples for, the invention are described in detail, these are by way of illustration only, and any equivalent modifications or alterations to this invention would be apparent to those skilled in the art and are intended to be included within the scope of this invention. Accordingly, it is intended that all equivalent alterations and modifications be included within the scope of the invention, without departing from the spirit and scope of the invention.
Claims (10)
1. The herbal essence silk soap is characterized by comprising the following components in parts by weight:
100 parts of herbal essence, 550 parts of grease, 50 parts of organic amine and 50 parts of fibroin;
the herbal essence is one or more of extractive solutions of flos Chrysanthemi Indici, flos Hibisci, herba Taraxaci, semen Cuscutae, radix Paeoniae alba, and semen Armeniacae amarum.
2. The herbal essence silk soap according to claim 1, wherein the herbal essence comprises the following components in parts by weight:
10 parts of wild chrysanthemum flower, 8 parts of erigeron breviscapus, 10 parts of dandelion, 8 parts of semen cuscutae, 5 parts of white paeony root and 5 parts of bitter almond.
3. The herbal essence silk soap according to claim 1, wherein the oil is one or more selected from grape seed oil, palm oil, olive oil, almond oil, coconut oil and cocoa butter.
4. The herbal essence silk soap according to claim 3, is further characterized in that the oil comprises the following components in parts by weight:
100 parts of grape seed oil, 100 parts of palm oil, 100 parts of olive oil, 100 parts of almond oil, 100 parts of coconut oil and 50 parts of cocoa butter.
5. A method for preparing the herbal essence silk soap according to claim 1, comprising the following steps:
s1, extracting herbal essence;
s2, extracting fibroin;
s3, adding the herbal essence obtained in S1 and the fibroin obtained in S2 into organic amine, and uniformly stirring;
s4, heating and melting the grease, and then cooling to 45-50 ℃;
s5, mixing the raw materials obtained in the steps S3 and S4, stirring the mixture into a viscous state, pouring the viscous state into a mold, performing saponification reaction in the mold for 12-36 hours, molding, demolding, and placing the mold into a constant temperature cabinet for heat preservation for 12-36 hours;
and S6, taking out, airing and packaging.
6. The preparation method of the herbal essence silk soap according to claim 5, wherein the S1 extraction of herbal essence comprises extraction of semen Cuscutae, radix Paeoniae alba, semen Armeniacae amarum essence and extraction of flos Chrysanthemi Indici, flos Hibisci, and herba Taraxaci essence; the essence of semen Cuscutae, radix Paeoniae alba and semen Armeniacae amarum is prepared by alcohol extraction method, and the essence of flos Chrysanthemi Indici, flos Hibisci and herba Taraxaci is prepared by distillation method.
7. The preparation method of herbal essence silk soap according to claim 6, wherein the alcohol extraction method comprises the following process flows: pulverizing, soaking in ethanol for 24-72h, filtering to obtain liquid phase, decocting the filtrate to obtain syrup, extracting with anhydrous ethanol and gelatin water solution, filtering, freezing for 12-36h, filtering, evaporating, dissolving in distilled water, decolorizing with active carbon, filtering, extracting with diethyl ether, and drying with anhydrous sodium sulfate to obtain semen Cuscutae, radix Paeoniae alba, and semen Armeniacae amarum essence; the distillation method comprises the following process flows: soaking the raw materials in water for 20-40min, decocting for 15-30min, filtering, rehydrating for 15-30min, filtering again, distilling the effective components in the filtrate, and concentrating under reflux to obtain flos Chrysanthemi Indici, herba Erigerontis and herba Taraxaci essence.
8. The method of claim 5, wherein the step of extracting silk protein in S2 comprises boiling silkworm cocoon in sodium carbonate solution to remove pectin, separating solid phase from liquid phase to obtain sericin solution and silk fibroin fiber, extracting sericin from the sericin solution by freezing, extracting silk fibroin from silk fibroin fiber by enzymatic hydrolysis, and mixing sericin and silk fibroin.
9. The preparation method of herbal essence silk soap according to claim 8, wherein the technical process for extracting sericin by a freezing method comprises the following steps: adding activated carbon into sericin solution, decolorizing at 70-90 deg.C, filtering to obtain liquid phase, concentrating the filtrate, freezing at pH 5 and-20 deg.C for 10-14h, naturally thawing, filtering to obtain solid phase to obtain sericin; the technological process for extracting the silk fibroin by the enzymolysis method comprises the following steps: adding silk fibroin into 40% calcium chloride solution, hydrolyzing at 90-100 deg.C for 1 hr, cooling, adding alkaline protease at 45 deg.C, hydrolyzing for 7-10 hr, dialyzing, and desalting to obtain silk fibroin.
10. The method for preparing the herbal tea essence-Hua silk soap according to claim 8, wherein the degumming time of the silkworm cocoons in the sodium carbonate solution is 20-40min, and the reaction pressure is 1-4 atm.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010702522.1A CN111793533A (en) | 2020-07-18 | 2020-07-18 | Herbal essence silk soap and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010702522.1A CN111793533A (en) | 2020-07-18 | 2020-07-18 | Herbal essence silk soap and preparation method thereof |
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Citations (9)
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|---|---|---|---|---|
| JPH09208996A (en) * | 1996-02-06 | 1997-08-12 | Kanebo Ltd | Transparent soap composition |
| CN1626062A (en) * | 2003-12-11 | 2005-06-15 | 诗丽吉皇后陛下促进副业及相关技术基金会 | Silk soap bar and processes for manufacture the same |
| CN1670154A (en) * | 2005-04-16 | 2005-09-21 | 王浩贵 | Wild chrysanthemum flower cleaning products |
| CN104745331A (en) * | 2015-04-17 | 2015-07-01 | 谢松芬 | Natural herb soap |
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-
2020
- 2020-07-18 CN CN202010702522.1A patent/CN111793533A/en active Pending
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| CN1670154A (en) * | 2005-04-16 | 2005-09-21 | 王浩贵 | Wild chrysanthemum flower cleaning products |
| CN104745331A (en) * | 2015-04-17 | 2015-07-01 | 谢松芬 | Natural herb soap |
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| CN106753917A (en) * | 2016-12-14 | 2017-05-31 | 浙江大学 | A kind of method that silk gum essential oil handmade soap is prepared with silk gum solution |
| CN107312654A (en) * | 2017-07-13 | 2017-11-03 | 芜湖慧宇商贸有限公司 | A kind of preparation method of the skin repair soap containing fibroin albumen |
| CN107699603A (en) * | 2017-11-28 | 2018-02-16 | 张夏洋 | A kind of extracting method of fibroin |
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