CN106619456A - Magnolia figo prickly-heat-removing shower gel and preparation method thereof - Google Patents

Magnolia figo prickly-heat-removing shower gel and preparation method thereof Download PDF

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Publication number
CN106619456A
CN106619456A CN201611174125.1A CN201611174125A CN106619456A CN 106619456 A CN106619456 A CN 106619456A CN 201611174125 A CN201611174125 A CN 201611174125A CN 106619456 A CN106619456 A CN 106619456A
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extract
chinese medicine
parts
michelia figo
miliaria
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尹海全
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Harbin Lingcaoshu Biotechnology Co Ltd
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Harbin Lingcaoshu Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
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    • A61K31/35Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having six-membered rings with one oxygen as the only ring hetero atom
    • A61K31/352Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having six-membered rings with one oxygen as the only ring hetero atom condensed with carbocyclic rings, e.g. methantheline 
    • A61K31/3533,4-Dihydrobenzopyrans, e.g. chroman, catechin
    • A61K31/355Tocopherols, e.g. vitamin E
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    • A61K36/185Magnoliopsida (dicotyledons)
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K36/18Magnoliophyta (angiosperms)
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    • A61K36/21Amaranthaceae (Amaranth family), e.g. pigweed, rockwort or globe amaranth
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    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/47Euphorbiaceae (Spurge family), e.g. Ricinus (castorbean)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/57Magnoliaceae (Magnolia family)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/59Menispermaceae (Moonseed family), e.g. hyperbaena or coralbead
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/888Araceae (Arum family), e.g. caladium, calla lily or skunk cabbage
    • A61K36/8888Pinellia
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    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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    • A61K2800/81Preparation or application process involves irradiation
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82Preparation or application process involves sonication or ultrasonication

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Abstract

The invention provides magnolia figo prickly-heat-removing shower gel and a preparation method thereof. The magnolia figo prickly-heat-removing shower gel is prepared by taking magnolia figo extracting liquid as a main material, taking traditional Chinese medicine extracting liquid, honey extract and glycerol as auxiliary materials, and adding vitamin E; a preparation process comprises the following steps: (1) preparing the magnolia figo extracting liquid; (2) preparing the traditional Chinese medicine extracting liquid; (3) preparing honey essence; (4) mixing and sterilizing. The magnolia figo prickly-heat-removing shower gel provided by the invention does not contain any chemical additive; a pure natural plant formula is adopted and magnolia figo essence is sufficiently extracted; a plurality of traditional Chinese medicinal materials are matched with the magnolia figo essence; meanwhile, the glycerol and the vitamin E are utilized for assistance, so that the magnolia figo prickly-heat-removing shower gel has the effect of cleaning skin dirt and can also be used for removing prickly heat, and has a very good prickly-heat-removing effect.

Description

One kind has spent miliaria shower cream and preparation method thereof with a smile
Technical field
The present invention relates to a kind of shower cream, more particularly to a kind of to have spent miliaria shower cream and preparation method thereof with a smile.
Background technology
Shower cream has been increasingly becoming the maximum class commodity of the most frequently used in people's daily life, consumption, with people Growth in the living standard, people for the requirement also more and more higher of shower cream, at present, common shower cream on the market, great majority Containing more chemical composition, frequently use, moisture of skin balance can be destroyed, easily cause pachylosis, cause dry skin, rise The problem of prickly heat, Long-Time Service is unfavorable for the skin health of people.
A kind of shower cream of Application No. CN201310268629.X, discloses a kind of shower cream, by following percentage Raw material is made:Surfactant 12 ~ 30%, FOS 0.1 ~ 5%, thickener 0.2 ~ 0.5%, water is surplus, the shower cream PH value is 5.5 to 7.0.A kind of shower cream of the disclosure of the invention, though cleaning, the purpose of skin care can be reached, it is constituted into Divide and do not possess miliaria composition, be unfavorable for baby's Long-Time Service, be unfavorable for infant skin health.
Based on the problems referred to above, the present invention adopts pure plant formula, is prepared for a kind of going miliaria effect good, skin care Miliaria shower cream has been spent with a smile, with Michelia figo as major ingredient, and Chinese medicine and its compatibility has been added, and can also effectively have been gone while cleaning skin Miliaria, is that baby and adult bring more comfortable shower to experience.
The content of the invention
It is an object of the invention to provide a kind of spent miliaria shower cream and preparation method thereof with a smile, without any chemistry addition Agent, using pure plant formula, fully extracts Michelia figo elite, and chooses kinds of traditional Chinese medicines material and its compatibility, while being aided with sweet Oil and vitamin E, while cleaning skin dirt, moreover it is possible to effectively remove miliaria, with good miliaria effect are gone.
The purpose of the present invention is achieved through the following technical solutions:
One kind has spent with a smile miliaria shower cream, described to have spent miliaria shower cream with a smile, with Michelia figo extract as major ingredient, with traditional Chinese medicine extraction Liquid, Mel extract, glycerine are auxiliary material, add vitamin E to make, and its preparation process is:
(1)Prepare Michelia figo extract:
A. distill:By weight, high-quality, fresh Michelia figo are chosen, after cleaning stalk, is placed in boiler, injection water steams Gas, distillation processes to obtain Michelia figo distillate;
B. microwave abstracting:Take Michelia figo distillate to be placed in Microwave Extraction Apparatus, microwave treatment 10-15min, filter Michelia figo carries Take liquid;
(2)Prepare Chinese medicine extract:
A. ultrasonic extraction:By weight, the water intaking tuber of pinellia, the root of gansui, Cocculus trilobus, Balsamiferou Blumea Herb, Spiny Amarauth Herb or Root, Chinese coriaria root, after cleaning, Section or silk, add 3-5 times of distilled water, after immersion 3-5h, are placed in ultrasonic extraction instrument, add 1-2 times of distilled water, ultrasonic wave 20-40min is processed, Chinese medicine extract is filtered to obtain;
B. concentrate:Chinese medicine extract is taken, moisture is concentrated in vacuo to below 15%, Chinese medicine extract is obtained;
(3)Prepare honey Essence:
By weight, high-quality propolis is taken, 80-100 mesh sieves is crossed after crushing, obtain bee glue powder, and 3-5 times of the addition into bee glue powder Distillation water termostat stirring, as solubility > 90%, is placed in ultrasonic extraction instrument, using ultrasonication 15- of 400-600W After 30min, moisture is concentrated in vacuo to below 8%, obtain honey Essence;
(4)Mixing, sterilizing:
By weight, Michelia figo extract, Chinese medicine extract, honey Essence are taken, glycerine, vitamin E is added, mixing is placed in After being well mixed in machine, Jing after sterilization processing, packaging gets product.
The step(1)The temperature that process is distilled in preparation Michelia figo extract is 85-100 DEG C, distills the time for processing For 2-3h;The temperature of microwave treatment is 60-70 DEG C, and the microwave power of microwave treatment is 300-450W.
The step(2)The temperature for preparing ultrasonication in Chinese medicine extract is 40-65 DEG C, the ultrasound of ultrasonication Wave power is 300-800W.
The step(3)The temperature for preparing constant temperature stirring in honey Essence is 40-50 DEG C, and the time of constant temperature stirring is 2- 3h。
The step(4)In mixing, sterilizing the sterilization mode that adopts of sterilization processing can for ultraviolet disinfection, pasteurization, Any one in high-temperature short-time sterilization.
The Michelia figo extract, Chinese medicine extract, Mel extract, glycerine, the weight proportion of composing of vitamin E are 10:3-5:2-4:1-3:0.5-1;
The Chinese medicine extract is made up of raw material by following parts by weight, RHIZOMA TYPHONII FLAGELLIFORMIS 3-4 parts, root of gansui 2-3 parts, Cocculus trilobus 1-3 parts, Balsamiferou Blumea Herb 1-2.5 parts, Spiny Amarauth Herb or Root 1-1.5 parts, Chinese coriaria root 0.5-1.5 parts.
It is described it is a kind of spent miliaria shower cream with a smile, the Michelia figo extract, Chinese medicine extract, Mel extract, glycerine, The optimum weight proportion of composing of vitamin E is 10:4:3:1:0.8.
Described one kind has spent miliaria shower cream with a smile, and raw material presses optimum weight number, RHIZOMA TYPHONII FLAGELLIFORMIS 3 in the Chinese medicine extract Part, 2.5 parts of the root of gansui, 2 parts of Cocculus trilobus, 1.4 parts of Balsamiferou Blumea Herb, 1.25 parts of Spiny Amarauth Herb or Root, 0.8 part of Chinese coriaria root.
In selected raw material of the invention, effect of each raw material is respectively:
Michelia figo, not only with menoxenia is controlled, effect that menorrhagia also goes miliaria effect, Michelia figo with distinguished In rich in abundant vitamin, volatile oil, with the multiple efficacies such as anti-oxidant, calm, dispelling fatigue, it is adaptable to all skin quality, Especially baby skin.
In Chinese medicine, Rhizoma pinelliae cordatae extract can effectively reduce skin oxidation rate, skin-protecting face nursing, the god of the anxiety that relaxes Jing, deep layer nourish skin, eliminating dampness, resolving sputum, cough-relieving, for coughing with a lot of sputum, bronchitis, external application fresh goods controls ulcerative carbuncle furuncle, unknown Pyogenic infections, insect-bite;The root of gansui, is all right rich in several mineral materials with good the effect of going miliaria function, also anti-aging The beneficial mineral matter of skin, water pouring drink, breaks accumulation, leads to two just, controls oedema turgor, stays drink, and accumulation of pathogens in chest, dysentery epilepsy is dysphagic, Disorder lumps in the abdomen product It is poly-, constipation and anuresis;Cocculus trilobus extract has an antioxidation, suppresses lipid peroxide to be formed, can delaying skin aging, dispel Wind pain relieving, inducing diuresis to remove edema, removing toxic substances is hypotensive.For rheumatic arthritis, intercostal neuralgia, acute nephritis, urinary tract infections, high blood Venomous snake bite is controlled in pressure disease, rheumatic heart disease, oedema, external application;Balsamiferou Blumea Herb has elimination grease, moisturizing, the effect of skin care, Wind-dispelling is subsided a swelling, promoting blood circulation to remove blood stasis, and for catching a cold, traumatic injury, boil carbuncle are controlled in rheumatic arthritis, cold after delivery pain, dysmenorrhoea, external application It is swollen, eczema, dermatitis;The antimicrobial components such as the chlorogenic acid contained in Spiny Amarauth Herb or Root, with extremely strong antibacterial and anti-inflammation functions, astringing to arrest bleeding The effects such as dysentery, antibacterial, anti-inflammatory, detumescence;Chinese coriaria root, can play nourishing, skin whitening effect, control rheumatic numbness, acute toothache, phlegm Drink, lump in the abdomen, scrofula, injury from falling down, acute conjunctivitis, burn.
Glycerine has extremely strong hygroscopicity, and skin moisturizing, softness, isolation air can be kept to invade, and is difficult moisture of skin Evaporation, can carry out skin care with the moisture in absorption air, effectively prevent chapped skin.
Vitamin E, is natural antioxidant, and energy effective protection cell membrane adds from the oxidative damage of free radical from interior Gu the natural protective barrier of skin, and can effectively eliminate the excessive oxygen freedom that the external world such as ultraviolet, air pollution key element is formed Base, plays a part of delay skin aging, sunburn, while, moreover it is possible to it is wrinkle resistant effectively to smooth microgroove, skin-active, pins moisture of skin, protects Hold the smooth of skin, water profit.
Beneficial effects of the present invention:One kind of the present invention has spent miliaria shower cream with a smile, without any chemical addition agent, adopts Pure plant is filled a prescription, and fully extracts Michelia figo elite, and chooses kinds of traditional Chinese medicines material and its compatibility, while being aided with glycerine and Wei Sheng Plain E, while cleaning skin dirt, moreover it is possible to effectively remove miliaria, with good miliaria effect is gone, and skin will not be caused sensitive, Applicable crowd extensively, is particularly suited for infant's skin.
The technological advantage of the present invention:In operation, Michelia figo water is extracted using the way of distillation, without the need for adding any chemistry examination Agent, effectively prevent chemical agent residue stimulates skin;Secondly, using the method for microwave abstracting, with equipment is simple, extraction effect Rate is high, time saving and energy saving, pollute little advantage;Using ultrasonic extraction, the active ingredient in Chinese medicine is extracted, Chinese medicine can be promoted In active ingredient be fully dissolved out, and avoid chemical reagent extracting method, chemical agent residue affects product pure natural property And the situation of product quality occurs;In addition, choosing high-quality propolis, using ultrasonic extraction, honey Essence is extracted, with saving time Laborsaving, energy consumption is low, the advantage that extraction efficiency is high, and extraction temperature is low, the natural sex composition that will not be destroyed in product, and grasps Make simple and safe;Additionally, the present invention is not added with from natural plants and Chinese herbal medicine in wide material sources, and product processing Chemical reagent and essence, effect is gentle, and product quality is higher.
Specific embodiment
The present invention is described in further detail with reference to specific embodiment.
Embodiment 1
One kind has spent with a smile miliaria shower cream, described to have spent miliaria shower cream with a smile, with Michelia figo extract as major ingredient, with traditional Chinese medicine extraction Liquid, Mel extract, glycerine are auxiliary material, add vitamin E to make, and its preparation process is:
(1)Prepare Michelia figo extract:
A. distill:By weight, high-quality, fresh Michelia figo are chosen, after cleaning stalk, is placed in boiler, injection water steams Gas, distillation processes to obtain Michelia figo distillate;
B. microwave abstracting:Take Michelia figo distillate to be placed in Microwave Extraction Apparatus, microwave treatment 10-15min, filter Michelia figo carries Take liquid;
(2)Prepare Chinese medicine extract:
A. ultrasonic extraction:By weight, the water intaking tuber of pinellia, the root of gansui, Cocculus trilobus, Balsamiferou Blumea Herb, Spiny Amarauth Herb or Root, Chinese coriaria root, after cleaning, Section or silk, add 3-5 times of distilled water, after immersion 3-5h, are placed in ultrasonic extraction instrument, add 1-2 times of distilled water, ultrasonic wave 20-40min is processed, Chinese medicine extract is filtered to obtain;
B. concentrate:Chinese medicine extract is taken, moisture is concentrated in vacuo to below 15%, Chinese medicine extract is obtained;
(3)Prepare honey Essence:
By weight, high-quality propolis is taken, 80-100 mesh sieves is crossed after crushing, obtain bee glue powder, and 3-5 times of the addition into bee glue powder Distillation water termostat stirring, as solubility > 90%, is placed in ultrasonic extraction instrument, using ultrasonication 15- of 400-600W After 30min, moisture is concentrated in vacuo to below 8%, obtain honey Essence;
(4)Mixing, sterilizing:
By weight, Michelia figo extract, Chinese medicine extract, honey Essence are taken, glycerine, vitamin E is added, mixing is placed in After being well mixed in machine, Jing after sterilization processing, packaging gets product.
The step(1)The temperature that process is distilled in preparation Michelia figo extract is 85-100 DEG C, distills the time for processing For 2-3h;The temperature of microwave treatment is 60-70 DEG C, and the microwave power of microwave treatment is 300-450W.
The step(2)The temperature for preparing ultrasonication in Chinese medicine extract is 40-65 DEG C, the ultrasound of ultrasonication Wave power is 300-800W.
The step(3)The temperature for preparing constant temperature stirring in honey Essence is 40-50 DEG C, and the time of constant temperature stirring is 2- 3h。
The step(4)In mixing, sterilizing the sterilization mode that adopts of sterilization processing can for ultraviolet disinfection, pasteurization, Any one in high-temperature short-time sterilization.
It is described it is a kind of spent miliaria shower cream with a smile, the Michelia figo extract, Chinese medicine extract, Mel extract, glycerine, The weight proportion of composing of vitamin E is 10:3-5:2-4:1-3:0.5-1;
The Chinese medicine extract is made up of raw material by following parts by weight, RHIZOMA TYPHONII FLAGELLIFORMIS 3-4 parts, root of gansui 2-3 parts, Cocculus trilobus 1-3 parts, Balsamiferou Blumea Herb 1-2.5 parts, Spiny Amarauth Herb or Root 1-1.5 parts, Chinese coriaria root 0.5-1.5 parts.
The Michelia figo extract, Chinese medicine extract, Mel extract, glycerine, the optimum weight proportion of composing of vitamin E For 10:4:3:1:0.8.
Raw material presses optimum weight number, 3 parts of RHIZOMA TYPHONII FLAGELLIFORMIS, 2.5 parts of the root of gansui, 2 parts of Cocculus trilobus, strong wind in the Chinese medicine extract 1.4 parts of Chinese mugwort, 1.25 parts of Spiny Amarauth Herb or Root, 0.8 part of Chinese coriaria root.
Embodiment 2
Further, technical scheme steps described in embodiment 1(1)The microwave assisted extraction methods prepared in Michelia figo extract can be adopted Ultrasonic extraction method is substituted, and during from ultrasonic extraction, the temperature of ultrasonic extraction is 45-55 DEG C, the ultrasonic extraction time For 15-25min, the power of ultrasonic extraction is 400-600W.
Embodiment 3
Further, technical scheme steps described in embodiment 1(2)Preparing ultrasonic processing method in Chinese medicine extract can adopt micro- Ripple extracting process is substituted, and during from microwave abstracting, the temperature of microwave abstracting is 50-60 DEG C, and the time of microwave abstracting is 15- 25min, the power of microwave abstracting is 450-650W.
Embodiment 4
Prepare the experiment of single factor of Michelia figo extract:
Efficient the referring to of Michelia figo extract have a smile on one's face in the Michelia figo extract for extracting flower essential oil and its fragrance ingredient content Summation.
(1)To prepare the vapo(u)rizing temperature of Michelia figo extract as experiment of single factor and experimental result:
The vapo(u)rizing temperature for preparing Michelia figo extract is 85 DEG C, 90 DEG C, 95 DEG C, 100 DEG C when, distillation time is 2.5h, microwave extraction Take time 13min, microwave abstracting power 380W, 65 DEG C of microwave abstracting temperature, experimental result is shown in Table 1:
The Michelia figo extract obtained under the different vapo(u)rizing temperatures of table 1 it is efficient
Vapo(u)rizing temperature With a smile rare colored extract is efficient(%)
85℃ 14.24
90℃ 14.87
95℃ 14.61
100℃ 14.47
As shown in Table 1, when vapo(u)rizing temperature is 90 DEG C, the efficient highest of Michelia figo extract.
(2)To prepare the distillation time of Michelia figo extract as experiment of single factor and experimental result:
When the distillation time for preparing Michelia figo extract is 2h, 2.5h, 3h, the temperature of distillation is 95 DEG C, the microwave abstracting time 13min, microwave abstracting power 380W, 65 DEG C of microwave abstracting temperature, experimental result is shown in Table 2:
The Michelia figo extract obtained under the different distillation times of table 2 it is efficient
Distillation time Michelia figo extract it is efficient(%)
2h 17.18
2.5h 16.85
3h 16.63
As shown in Table 2, when distillation time is 2h, the efficient highest of Michelia figo extract.
(3)To prepare the microwave abstracting time of Michelia figo extract as experiment of single factor and experimental result:
When the microwave abstracting time for preparing Michelia figo extract is 10min, 12min, 13min, 15min, distillation time is 2.5h, Vapo(u)rizing temperature is 95 DEG C, microwave abstracting power 380W, 65 DEG C of microwave abstracting temperature, and experimental result is shown in Table 3:
The Michelia figo extract that table 3 is obtained under the different microwave abstracting times it is efficient
The microwave abstracting time Michelia figo extract it is efficient(%)
10min 17.82
12min 18.61
13min 18.87
15min 18.42
As shown in Table 3, when the microwave abstracting time being 13min, the efficient highest of Michelia figo extract.
(4)To prepare the microwave abstracting power of Michelia figo extract as experiment of single factor and experimental result:
When the microwave abstracting power for preparing Michelia figo extract is 300W, 350 W, 450 W, distillation time is 2.5h, distillation temperature Spend for 95 DEG C, microwave abstracting time 13min, 65 DEG C of microwave abstracting temperature, experimental result is shown in Table 4:
The Michelia figo extract obtained under the different microwave abstracting powers of table 4 it is efficient
Microwave abstracting power Michelia figo extract it is efficient(%)
300W 18.87
350W 19.23
380 W 19.49
450 W 18.76
As shown in Table 4, when microwave abstracting power is 380W, the efficient highest of Michelia figo extract.
(5)To prepare the microwave abstracting temperature of Michelia figo extract as experiment of single factor and experimental result:
The microwave abstracting temperature for preparing Michelia figo extract is 60 DEG C, 65 DEG C, 70 DEG C when, distillation time is 2.5h, vapo(u)rizing temperature For 95 DEG C, microwave abstracting time 13min, microwave abstracting power 380W, experimental result is shown in Table 5:
The Michelia figo extract obtained at a temperature of the different microwave abstractings of table 5 it is efficient
Microwave abstracting power Michelia figo extract it is efficient(%)
60℃ 19.39
65℃ 19.96
70℃ 19.42
As shown in Table 5, when microwave abstracting temperature is 65 DEG C, the efficient highest of Michelia figo extract.
In sum, when vapo(u)rizing temperature be 90 DEG C, distillation time be 2h, the microwave abstracting time be 13min, microwave abstracting work( When rate is 380W, microwave abstracting temperature is 65 DEG C, the efficient highest of Michelia figo extract;Therefore, Michelia figo extract is prepared When, vapo(u)rizing temperature is 90 DEG C, distillation time is 2h, the microwave abstracting time is 13min, microwave abstracting power is 380W, microwave extraction It is optimal preparation scheme that temperature is taken for 65 DEG C.

Claims (9)

  1. It is 1. a kind of to have spent miliaria shower cream with a smile, it is characterised in that:It is described to have spent miliaria shower cream with a smile, based on Michelia figo extract Material, with Chinese medicine extract, Mel extract, glycerine as auxiliary material, adds vitamin E to make, and its preparation process is:
    (1)Prepare Michelia figo extract:
    A. distill:By weight, high-quality, fresh Michelia figo are chosen, after cleaning stalk, is placed in boiler, injection water steams Gas, distillation processes to obtain Michelia figo distillate;
    B. microwave abstracting:Take Michelia figo distillate to be placed in Microwave Extraction Apparatus, microwave treatment 10-15min, filter Michelia figo carries Take liquid;
    (2)Prepare Chinese medicine extract:
    A. ultrasonic extraction:By weight, the water intaking tuber of pinellia, the root of gansui, Cocculus trilobus, Balsamiferou Blumea Herb, Spiny Amarauth Herb or Root, Chinese coriaria root, after cleaning, Section or silk, add 3-5 times of distilled water, after immersion 3-5h, are placed in ultrasonic extraction instrument, add 1-2 times of distilled water, ultrasonic wave 20-40min is processed, Chinese medicine extract is filtered to obtain;
    B. concentrate:Chinese medicine extract is taken, moisture is concentrated in vacuo to below 15%, Chinese medicine extract is obtained;
    (3)Prepare honey Essence:
    By weight, high-quality propolis is taken, 80-100 mesh sieves is crossed after crushing, obtain bee glue powder, and 3-5 times of the addition into bee glue powder Distillation water termostat stirring, as solubility > 90%, is placed in ultrasonic extraction instrument, using ultrasonication 15- of 400-600W After 30min, moisture is concentrated in vacuo to below 8%, obtain honey Essence;
    (4)Mixing, sterilizing:
    By weight, Michelia figo extract, Chinese medicine extract, honey Essence are taken, glycerine, vitamin E is added, mixing is placed in After being well mixed in machine, Jing after sterilization processing, packaging gets product.
  2. It is 2. a kind of according to claim 1 to have spent miliaria shower cream with a smile, it is characterised in that:The step(1)Prepare Michelia figo The temperature that process is distilled in extract is 85-100 DEG C, and the time for distilling process is 2-3h;The temperature of microwave treatment is 60-70 DEG C, the microwave power of microwave treatment is 300-450W.
  3. It is 3. a kind of according to claim 1 to have spent miliaria shower cream with a smile, it is characterised in that:The step(2)Prepare Chinese medicine to carry The temperature for taking ultrasonication in liquid is 40-65 DEG C, and the ultrasonic power of ultrasonication is 300-800W.
  4. It is 4. a kind of according to claim 1 to have spent miliaria shower cream with a smile, it is characterised in that:The step(3)Prepare honey essence The temperature of constant temperature stirring is 40-50 DEG C in magnificent liquid, and the time of constant temperature stirring is 2-3h.
  5. It is 5. a kind of according to claim 1 to have spent miliaria shower cream with a smile, it is characterised in that:The step(4)In mixing, sterilizing The sterilization mode that sterilization processing is adopted can be any one in ultraviolet disinfection, pasteurization, high-temperature short-time sterilization.
  6. It is 6. a kind of according to claim 1 to have spent miliaria shower cream with a smile, it is characterised in that:The Michelia figo extract, Chinese medicine Extract, Mel extract, glycerine, the weight proportion of composing of vitamin E are 10:3-5:2-4:1-3:0.5-1.
  7. 7. Chinese medicine extract described in is made up of raw material by following parts by weight, RHIZOMA TYPHONII FLAGELLIFORMIS 3-4 parts, root of gansui 2-3 parts, Cocculus trilobus 1-3 Part, Balsamiferou Blumea Herb 1-2.5 parts, Spiny Amarauth Herb or Root 1-1.5 parts, Chinese coriaria root 0.5-1.5 parts.
  8. It is 8. a kind of according to claim 6 to have spent miliaria shower cream with a smile, it is characterised in that:The Michelia figo extract, Chinese medicine Extract, Mel extract, glycerine, the optimum weight proportion of composing of vitamin E are 10:4:3:1:0.8.
  9. It is 9. a kind of according to claim 6 to have spent miliaria shower cream with a smile, it is characterised in that:Raw material is pressed in the Chinese medicine extract Optimum weight number, 3 parts of RHIZOMA TYPHONII FLAGELLIFORMIS, 2.5 parts of the root of gansui, 2 parts of Cocculus trilobus, 1.4 parts of Balsamiferou Blumea Herb, 1.25 parts of Spiny Amarauth Herb or Root, Chinese coriaria root 0.8 Part.
CN201611174125.1A 2016-12-19 2016-12-19 Magnolia figo prickly-heat-removing shower gel and preparation method thereof Withdrawn CN106619456A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP4000689A1 (en) * 2020-11-17 2022-05-25 Fethiann Molecule Applied Co., Ltd. Magnolia figo extract for use in reducing epidermal desquamation and promoting wound healing

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106074330A (en) * 2016-06-30 2016-11-09 义乌市庆鹏化妆品有限公司 A kind of rose bath gel

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106074330A (en) * 2016-06-30 2016-11-09 义乌市庆鹏化妆品有限公司 A kind of rose bath gel

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP4000689A1 (en) * 2020-11-17 2022-05-25 Fethiann Molecule Applied Co., Ltd. Magnolia figo extract for use in reducing epidermal desquamation and promoting wound healing

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