CN111643398A

CN111643398A - Preparation method of hyaluronic acid skin care product

Info

Publication number: CN111643398A
Application number: CN202010708142.9A
Authority: CN
Inventors: 宋如心; 杨帅
Original assignee: Individual
Current assignee: Individual
Priority date: 2020-07-21
Filing date: 2020-07-21
Publication date: 2020-09-11

Abstract

The invention relates to the field of skin care product preparation, in particular to a hyaluronic acid skin care product preparation method which comprises a mounting frame, a stirrer, a driving mechanism, a pushing mechanism, a piston mechanism and a splash-proof mechanism, wherein a shell is fixedly arranged on the inner bottom wall of the mounting frame, an inner container is arranged in the shell, the stirrer is arranged in the inner container, the stirrer comprises a rotating cylinder, an inner tube, a spiral plate and through holes, the inner tube is coaxially arranged in the rotating cylinder, the inner tube is fixedly connected with the inner wall of the rotating cylinder through the spiral plate, the rotating cylinder is provided with a plurality of uniformly distributed through holes, the driving mechanism for driving the stirrer to rotate is arranged on the mounting frame, and the pushing mechanism for pushing the inner container to move up and down along the inner part of the shell is arranged in the shell. The hyaluronic acid skin care product preparation device provided by the invention has the advantage of improving the stirring effect.

Description

Preparation method of hyaluronic acid skin care product

Technical Field

The invention relates to the field of skin care product preparation, in particular to a preparation method of a hyaluronic acid skin care product.

Background

Hyaluronic acid is also called hyaluronic acid, the basic structure of which is composed of two disaccharide units, namely D-glucuronic acid and N-acetylglucosamine, and the hyaluronic molecule of the hyaluronic acid can carry over 500 times of water, is the best moisture-preserving component recognized at present and is widely applied to maintenance products and cosmetics. The hyaluronic acid facial mask mainly comprises deionized water, hyaluronic acid and cactus juice, can rapidly enter deep skin, repair skin injury, aging and wrinkles, and deeply supplement water, and can maintain oil-water balance of skin and delay aging after being used.

In the process of preparing hyaluronic acid, the cockscomb fragments are added into acetone in the early stage, soaked overnight until the cockscomb is dehydrated and hardened, then placed in a porcelain plate for drying, and crushed into powder by a crusher after drying. In pouring the cockscomb powder into enamel tank, add 6 ~ 7 times of distilled water, the stirring is even, because the volatility of traditional device stirring is not big, leads to work efficiency not high. Therefore, it is necessary to provide a preparation method of hyaluronic acid skin care products to solve the above technical problems.

Disclosure of Invention

Aiming at the problems in the prior art, the invention provides a preparation method of a hyaluronic acid skin care product.

The technical scheme adopted by the invention for solving the technical problems is as follows: a hyaluronic acid skin care product is prepared from deionized water, hyaluronic acid, radix et caulis Opuntiae Dillenii juice, and facial mask matrix;

the preparation method comprises the following steps:

s1: putting fresh cockscombs for preparing hyaluronic acid into a reaction kettle, adding sufficient acetone liquid into the reaction kettle, completely immersing the fresh cockscombs below the liquid level by the added acetone liquid, then sealing the reaction kettle, soaking for 24 hours in a constant temperature state, and dehydrating and hardening the soaked cockscombs;

s2: dehydrating and drying the cockscomb processed in the step S1 in a low-temperature reduced-pressure drying mode, putting the cockscombs into a grinder to be ground after drying, and screening by using a 50-mesh screen after grinding to obtain cockscomb powder;

s3: putting the cockscomb powder obtained in the step S2 into a preparation device, adding deionized distilled water with the volume equal to 6-7 times of the volume of the cockscomb powder, keeping the temperature in the preparation device at 130 ℃ and the pressure at 5-8MPa, stirring and extracting, and filtering to obtain an extraction liquid;

s4: putting the filtrate obtained in the step S3 into a freeze spray drying device for freeze spray drying to obtain hyaluronic acid freeze-dried powder;

s5: dissolving the prepared hyaluronic acid freeze-dried powder in deionized water, then adding the cactus juice into the deionized water to obtain a mixed solution, and then infiltrating the mixed solution onto a mask substrate to obtain a finished product of the skin care mask;

the preparation device in the step S3 comprises a mounting rack, a stirrer, a driving mechanism, a pushing mechanism, a piston mechanism and a splash-proof mechanism, wherein a shell is fixedly arranged on the inner bottom wall of the mounting rack, and an inner container is arranged in the shell; the stirrer is arranged in the inner container and comprises a rotating cylinder, an inner pipe, a spiral plate and through holes, the inner pipe which is coaxial with the rotating cylinder is arranged in the rotating cylinder, the inner pipe is fixedly connected with the inner wall of the rotating cylinder through the spiral plate, and the rotating cylinder is provided with a plurality of uniformly distributed through holes; the driving mechanism for driving the stirrer to rotate is arranged on the mounting frame; the pushing mechanism for pushing the inner container to move up and down along the inside of the shell is arranged in the shell; the piston mechanism is arranged in the inner container; the two splash-proof mechanisms with the same specification are symmetrically arranged in the inner container.

Preferably, actuating mechanism includes that driving motor, first rotation wheel, axis of rotation, second rotate wheel and belt, driving motor fixed mounting is on the lateral wall of mounting bracket, and driving motor's output fixed mounting has first rotation wheel, the one end of axis of rotation is passed through the bearing and is connected with the interior roof rotation of mounting bracket, and the other end of axis of rotation extend to in the inner bag and with the top fixed connection who rotates a section of thick bamboo, the second rotates the fixed cup joint of wheel in the axis of rotation, and the second rotates the wheel and is connected with first rotation wheel transmission through the belt.

Preferably, the pushing mechanism comprises a mounting seat, a mounting cavity, a threaded rod, threaded connecting blocks, first rotating rods, second rotating rods and a rotating motor, the mounting seat is fixedly mounted on the inner bottom wall of the shell, the mounting cavity is arranged in the mounting seat, two ends of the threaded rod are rotatably connected with the inner walls of two sides of the mounting cavity through bearings, one end of the threaded rod extends out of the shell and is fixedly connected with the output end of the rotating motor, the rotating motor is fixedly mounted on the inner bottom wall of the mounting seat, two sections of opposite threads are arranged on the threaded rod, each section of threads is sleeved with the threaded connecting block in threaded connection, the two threaded connecting blocks are symmetrically arranged with each other, the two threaded connecting blocks are slidably connected with the inner side wall of the mounting cavity, the two first rotating rods are respectively hinged with two sides of the upper surface of the mounting seat, and the other ends of the two first rotating rods are hinged, two the upper surface of threaded connection piece all articulates there is the second dwang, and the other end of two second dwangs is articulated with the interlude of adjacent first dwang respectively.

Preferably, the piston mechanism comprises a piston rod and a piston, the piston rod is fixedly installed on the inner bottom wall of the inner container and is vertically arranged, the top of the piston rod extends into the inner tube on the stirrer, and the piston is fixedly installed at the extending end of the piston rod.

Preferably, splashproof mechanism includes arc board and spring, the inner wall that the one end and the inner bag of arc board are close to the top is articulated, and the outer wall fixed mounting that the arc board is close to the other end has the spring, the other end of spring and the interior diapire fixed connection of casing.

Preferably, the top fixed mounting of casing has the inlet pipe, and in the inlet pipe extends to the inner bag, fixed mounting has row material pipe on the lateral wall that the casing is close to the bottom, and arranges the liquid inlet of material pipe and the liquid outlet fixed connection of inner bag, equal fixed mounting has the valve on inlet pipe and the row material pipe, and arranges that the material pipe adopts the elasticity plastic tubing.

Compared with the related technology, the preparation method of the hyaluronic acid skin care product provided by the invention has the following beneficial effects:

(1) according to the hyaluronic acid skin care product preparation method, the stirrer is driven by the driving mechanism to rotate at a high speed, so that liquid medicine input into the stirrer from the feeding pipe slides down along the rotating cylinder along with the spiral plate, and meanwhile, the liquid medicine is thrown into the inner container from through holes with different heights under the action of centrifugal force, and the stirring effect of the stirrer is enhanced.

(2) According to the preparation method of the hyaluronic acid skin care product, the inner container continuously slides up and down along the shell through the pushing mechanism, so that the liquid medicine in the inner container can be stirred to a greater extent, and meanwhile, when the inner container continuously slides up and down along the shell, the piston rod pushes the piston to slide up and down along the inner tube, so that the liquid medicine in the inner tube is continuously taken out of the inner tube, and the volatility of the liquid medicine in the inner container is further improved.

Drawings

FIG. 1 is a schematic structural diagram of a preferred embodiment of a method for preparing a hyaluronic acid skin care product according to the present invention;

FIG. 2 is a schematic view of the agitator shown in FIG. 1;

FIG. 3 is an enlarged schematic view of the structure shown at A in FIG. 1;

FIG. 4 is a flow chart of the method of the present invention.

Reference numbers in the figures: 1. mounting frame, 2, casing, 3, inner bag, 4, agitator, 41, rotary cylinder, 42, inner tube, 43, spiral board, 44, through-hole, 5, actuating mechanism, 51, driving motor, 52, first runner, 53, axis of rotation, 54, second runner, 55, belt, 6, pushing mechanism, 61, mount pad, 62, installation cavity, 63, threaded rod, 64, threaded connection piece, 65, first runner, 66, second runner, 67, rotation motor, 7, piston mechanism, 71, piston rod, 72, piston, 8, splashproof mechanism, 81, arc board, 82, spring, 9, inlet pipe, 9a, row of material pipe.

Detailed Description

The invention is further described with reference to the following figures and embodiments.

Referring to fig. 1, fig. 2, fig. 3 and fig. 4, a method for preparing hyaluronic acid skin care product includes deionized water, hyaluronic acid, cactus juice, and mask base;

the preparation method comprises the following steps:

the preparation device in the step S3 includes an installation frame 1, a stirrer 4, a driving mechanism 5, a pushing mechanism 6, a piston mechanism 7 and a splash-proof mechanism 8, wherein a casing 2 is fixedly installed on an inner bottom wall of the installation frame 1, a liner 3 is arranged in the casing 2, the stirrer 4 is installed in the liner 3, the stirrer 4 includes a rotation cylinder 41, an inner tube 42, a spiral plate 43 and through holes 44, the rotation cylinder 41 is internally provided with the inner tube 42 coaxial with the rotation cylinder 41, the inner tube 42 is fixedly connected with the inner wall of the rotation cylinder 41 through the spiral plate 43, and the rotation cylinder 41 is provided with a plurality of through holes 44 uniformly distributed; the stirrer 4 is driven by the driving mechanism 5 to rotate at a high speed, so that the liquid medicine input into the stirrer 4 from the feeding pipe 9 slides down along the rotating cylinder 41 along with the spiral plate 43, and simultaneously, the liquid medicine is thrown into the inner container 3 from the through holes 44 with different heights under the action of centrifugal force, thereby enhancing the stirring effect of the stirrer 4.

Referring to fig. 1 and 2, the driving mechanism 5 for driving the stirrer 4 to rotate is installed on the installation frame 1, the driving mechanism 5 includes a driving motor 51, a first rotating wheel 52, a rotating shaft 53, a second rotating wheel 54 and a belt 55, the driving motor 51 is fixedly installed on the side wall of the installation frame 1, the first rotating wheel 52 is fixedly installed at the output end of the driving motor 51, one end of the rotating shaft 53 is rotatably connected with the inner top wall of the installation frame 1 through a bearing, the other end of the rotating shaft 53 extends into the inner container 3 and is fixedly connected with the top of the rotating cylinder 41, the second rotating wheel 54 is fixedly sleeved on the rotating shaft 53, and the second rotating wheel 54 is in transmission connection with the first rotating wheel 52 through the belt 55; the drive motor 51 is turned on to rotate the first rotating wheel 52, and the agitator 4 rotates because the first rotating wheel 52 is drivingly connected to the second rotating wheel 54 through the belt 55.

Referring to fig. 1 and 3, the pushing mechanism 6 for pushing the inner container 3 to move up and down along the inside of the casing 2 is installed inside the casing 2, the pushing mechanism 6 includes an installation seat 61, an installation cavity 62, a threaded rod 63, a threaded connection block 64, a first rotating rod 65, a second rotating rod 66 and a rotating motor 67, the installation seat 61 is fixedly installed on the inner bottom wall of the casing 2, the installation cavity 62 is opened in the installation seat 61, both ends of the threaded rod 63 are rotatably connected with the inner walls of both sides of the installation cavity 62 through bearings, one end of the threaded rod 63 extends out of the casing 2 and is fixedly connected with the output end of the rotating motor 67, the rotating motor 67 is fixedly installed on the inner bottom wall of the installation seat 1, two opposite threads are arranged on the threaded rod 63, the threaded connection block 64 of threaded connection is sleeved on each section of the threads, and the threaded connection blocks 64 are symmetrically arranged, the two threaded connecting blocks 64 are slidably connected with the inner side wall of the mounting cavity 62, the two first rotating rods 65 are respectively hinged with two sides of the upper surface of the mounting seat 61, the other ends of the two first rotating rods 65 are hinged with the lower surface of the inner container 3, the upper surfaces of the two threaded connecting blocks 64 are respectively hinged with second rotating rods 66, and the other ends of the two second rotating rods 66 are respectively hinged with the middle sections of the adjacent first rotating rods 65; when agitator 4 mixes the medicine in to inner bag 3, open and rotate motor 67 and drive the continuous corotation and the reversal of threaded rod 63, thereby two threaded connection piece 64 along the continuous motion in opposite directions or the back of the body motion of threaded rod 63, when two threaded connection piece 64 move in opposite directions, second dwang 66 drives first dwang 65 and rotates to threaded rod 63 direction, thereby inner bag 3 glides along casing 2, when two threaded connection piece 64 move in opposite directions, second dwang 66 drives first dwang 65 and rotates to keeping away from threaded rod 63 direction, thereby inner bag 3 slides along casing 2, inner bag 3 is continuous to slide from top to bottom along casing 2 and makes the liquid medicine in the inner bag 3 can the stirring of bigger degree.

Referring to fig. 1, the piston mechanism 7 is installed in the inner container 3, the piston mechanism 7 includes a piston rod 71 and a piston 72, the piston rod 71 is fixedly installed on the inner bottom wall of the inner container 3, the piston rod 71 is vertically disposed, the top of the piston rod 71 extends into the inner tube 42 on the stirrer 4, the piston 72 is fixedly installed at the extending end of the piston rod 71, when the inner container 3 continuously slides up and down along the housing 2, the piston rod 71 pushes the piston 72 to slide up and down along the inner tube 42, so that the liquid medicine in the inner tube 42 is continuously taken out of the inner tube 42, and the volatility of the liquid medicine in the inner container 3 is further improved.

Referring to fig. 1, two specifications are the same the splashproof mechanism 8 symmetry is installed in inner bag 3, splashproof mechanism 8 includes arc board 81 and spring 82, the one end of arc board 81 is articulated with the inner wall that inner bag 3 is close to the top, and the outer wall fixed mounting that arc board 81 is close to the other end has spring 82, the other end of spring 82 and the interior diapire fixed connection of casing 2, the effectual liquid medicine that has reduced to throw away in the agitator 4 of arc board 81 drenches spill inner bag 3.

Referring to fig. 1, the top fixed mounting of casing 2 has inlet pipe 9, and inlet pipe 9 extends to in the inner bag 3, casing 2 is close to fixed mounting on the lateral wall of bottom and arranges material pipe 9a, and arranges the inlet of material pipe 9a and the liquid outlet fixed connection of inner bag 3, inlet pipe 9 with arrange equal fixed mounting has the valve on the material pipe 9a, and arrange material pipe 9a and adopt the elasticity plastic tubing, be convenient for input or export the mixed liquid medicine in the inner bag 3.

The working principle of the preparation device provided by the invention is as follows: when the hyaluronic acid skin care product containing hyaluronic acid and other liquid medicine components is manufactured, hyaluronic acid and the required liquid medicine components are sequentially input into the inner container 3 from the feeding pipe 9, the driving motor 51 is started to drive the first rotating wheel 52 to rotate, the stirrer 4 rotates along with the first rotating wheel 52 which is in transmission connection with the second rotating wheel 54 through the belt 55, the stirrer 4 is driven by the driving mechanism 5 to rotate at a high speed, so that the liquid medicine input into the stirrer 4 from the feeding pipe 9 slides down along the rotating cylinder 41 along with the spiral plate 43, meanwhile, the liquid medicine is thrown into the inner container 3 from the through holes 44 with different heights under the action of centrifugal force, the stirring effect of the stirrer 4 is enhanced, the mixing degree of the hyaluronic acid and the other liquid medicine is improved, when the stirrer 4 mixes the medicine in the inner container 3, the rotating motor 67 is started to drive the threaded rod 63 to rotate forwards and backwards continuously, therefore, the two threaded connecting blocks 64 move or move back and forth continuously along the threaded rod 63, when the two threaded connecting blocks 64 move back and forth, the second rotating rod 66 drives the first rotating rod 65 to rotate towards the threaded rod 63, so that the liner 3 slides down along the shell 2, when the two threaded connecting blocks 64 move back and forth, the second rotating rod 66 drives the first rotating rod 65 to rotate towards the direction away from the threaded rod 63, so that the liner 3 slides upwards along the shell 2, the liner 3 continuously slides upwards and downwards along the shell 2 to stir the liquid medicine in the liner 3 to a greater extent, when the liner 3 continuously slides upwards and downwards along the shell 2, the piston rod 71 pushes the piston 72 to slide upwards and downwards along the inner tube 42, so that the liquid medicine in the inner tube 42 is continuously taken out of the inner tube 42, the liquid medicine is mixed through the fluidity of gas, and meanwhile, the stirrer 4 can be prevented from deviating, and then the volatility of the liquid medicine of the inner container 3 is improved, and the arc plate 81 in the anti-splash mechanism 8 effectively reduces the liquid medicine thrown out of the stirrer 4 from splashing out of the inner container 3 and reduces the splashing of the liquid medicine on the inner wall of the shell 2.

The foregoing illustrates and describes the principles, general features, and advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the embodiments and descriptions given above are only illustrative of the principles of the present invention, and various changes and modifications may be made without departing from the spirit and scope of the invention, which fall within the scope of the claims. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims

1. A preparation method of hyaluronic acid skin care product is characterized by comprising deionized water, hyaluronic acid, cactus juice and a mask matrix;

the preparation method comprises the following steps:

the preparation device in the S3 step comprises a mounting rack (1), a stirrer (4), a driving mechanism (5), a pushing mechanism (6), a piston mechanism (7) and a splash-proof mechanism (8), wherein a shell (2) is fixedly installed on the inner bottom wall of the mounting rack (1), and an inner container (3) is arranged in the shell (2); the stirrer (4) is arranged in the inner container (3), the stirrer (4) comprises a rotating cylinder (41), an inner tube (42), a spiral plate (43) and through holes (44), the inner tube (42) coaxial with the rotating cylinder (41) is arranged in the rotating cylinder (41), the inner tube (42) is fixedly connected with the inner wall of the rotating cylinder (41) through the spiral plate (43), and the rotating cylinder (41) is provided with a plurality of uniformly distributed through holes (44); the driving mechanism (5) for driving the stirrer (4) to rotate is arranged on the mounting frame (1); the pushing mechanism (6) for pushing the inner container (3) to move up and down along the inside of the shell (2) is arranged inside the shell (2); the piston mechanism (7) is arranged in the inner container (3); the two splash-proof mechanisms (8) with the same specification are symmetrically arranged in the inner container (3).

2. The preparation method of the hyaluronic acid skin care product according to claim 1, wherein the driving mechanism (5) comprises a driving motor (51), a first rotating wheel (52), a rotating shaft (53), a second rotating wheel (54) and a belt (55), the driving motor (51) is fixedly installed on the side wall of the installation frame (1), the first rotating wheel (52) is fixedly installed at the output end of the driving motor (51), one end of the rotating shaft (53) is rotatably connected with the inner top wall of the installation frame (1) through a bearing, the other end of the rotating shaft (53) extends into the inner container (3) and is fixedly connected with the top of the rotating cylinder (41), the second rotating wheel (54) is fixedly sleeved on the rotating shaft (53), and the second rotating wheel (54) is in transmission connection with the first rotating wheel (52) through the belt (55).

3. The preparation method of the hyaluronic acid skin care product according to claim 1, wherein the pushing mechanism (6) comprises an installation seat (61), an installation cavity (62), a threaded rod (63), a threaded connection block (64), a first rotating rod (65), a second rotating rod (66) and a rotating motor (67), the installation seat (61) is fixedly installed on the inner bottom wall of the shell (2), the installation cavity (62) is arranged in the installation seat (61), two ends of the threaded rod (63) are rotatably connected with the inner walls of two sides of the installation cavity (62) through bearings, one end of the threaded rod (63) extends out of the shell (2) and is fixedly connected with the output end of the rotating motor (67), the rotating motor (67) is fixedly installed on the inner bottom wall of the installation frame (1), two opposite threads are arranged on the threaded rod (63), and the threaded connection block (64) in threaded connection is sleeved on each thread, two threaded connection piece (64) symmetry each other sets up, and the inside wall sliding connection of two threaded connection piece (64) and installation cavity (62), two first dwang (65) are articulated with the both sides of mount pad (61) upper surface respectively, and the other end of two first dwang (65) all is articulated with the lower surface of inner bag (3), two the upper surface of threaded connection piece (64) all articulates there is second dwang (66), and the other end of two second dwang (66) is articulated with the interlude of adjacent first dwang (65) respectively.

4. The preparation method of hyaluronic acid skin care product according to claim 1, wherein the piston mechanism (7) comprises a piston rod (71) and a piston (72), the piston rod (71) is fixedly installed on the inner bottom wall of the inner container (3), the piston rod (71) is vertically arranged, the top of the piston rod (71) extends into the inner tube (42) on the stirrer (4), and the piston (72) is fixedly installed at the extending end of the piston rod (71).

5. The preparation method of the hyaluronic acid skin care product according to claim 1, wherein the anti-splash mechanism (8) comprises an arc plate (81) and a spring (82), one end of the arc plate (81) is hinged to the inner wall of the inner container (3) close to the top, the spring (82) is fixedly installed on the outer wall of the arc plate (81) close to the other end, and the other end of the spring (82) is fixedly connected with the inner bottom wall of the shell (2).

6. The preparation method of the hyaluronic acid skin care product according to claim 1, wherein a feeding pipe (9) is fixedly installed at the top of the shell (2), the feeding pipe (9) extends into the inner container (3), a discharging pipe (9a) is fixedly installed on the side wall of the shell (2) close to the bottom, a liquid inlet of the discharging pipe (9a) is fixedly connected with a liquid outlet of the inner container (3), valves are fixedly installed on the feeding pipe (9) and the discharging pipe (9a), and the discharging pipe (9a) is made of an elastic plastic pipe.