CN111624137A - Device for testing viscosity of granular sticky explosive and using method - Google Patents

Device for testing viscosity of granular sticky explosive and using method Download PDF

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Publication number
CN111624137A
CN111624137A CN201911172954.XA CN201911172954A CN111624137A CN 111624137 A CN111624137 A CN 111624137A CN 201911172954 A CN201911172954 A CN 201911172954A CN 111624137 A CN111624137 A CN 111624137A
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China
Prior art keywords
viscosity
explosive
granular
scale
quantitative
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CN201911172954.XA
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Chinese (zh)
Inventor
霍勇
祝贺
杨永军
王高宏
李建民
原国虎
张爱娜
杨亚军
王东
刘杰
史志军
赵建智
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Shanxi Jiangyang Xing'an Civil Explosive Apparatus Co ltd
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Shanxi Jiangyang Xing'an Civil Explosive Apparatus Co ltd
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Priority to CN201911172954.XA priority Critical patent/CN111624137A/en
Publication of CN111624137A publication Critical patent/CN111624137A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • G01N11/02Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material

Abstract

The invention relates to a device for testing the viscosity of granular sticky explosive and a using method thereof, belonging to the technical field of civil explosive equipment, aiming at solving the technical problem of providing a device for measuring the viscosity of the granular sticky explosive, and adopting the technical scheme that: the quantitative barrel is a conical barrel with openings at the upper end and the lower end, the measuring disc is arranged below the quantitative barrel, the circle center of the measuring disc is superposed with the axis of the quantitative barrel, the measuring disc is concentrically provided with a positioning ring, the outer diameter of the lower end of the quantitative barrel is superposed with the positioning ring, the measuring disc is concentrically and uniformly provided with circular scale marks, the positioning ring is superposed with a zero scale mark, and the scale of the scale mark is gradually increased from the zero scale mark to the direction far away from the quantitative barrel; the device and the method designed by the invention are convenient and fast to operate, simple and understandable, and the viscosity of the granular sticky explosive is accurately measured.

Description

Device for testing viscosity of granular sticky explosive and using method
Technical Field
The invention belongs to the technical field of civil explosive equipment, and particularly relates to a device for testing viscosity of granular sticky explosive and a using method thereof.
Background
The viscous explosive is mainly applied to top hole charging of mine pumping, and in the top hole charging blasting operation process, the required explosive has the characteristics of low mechanical sensitivity, safe operation process, small top hole charging return amount, large explosion power, higher water resistance and the like. If viscosity is too big, easily cause charge ware pumping pressure too big, have potential safety hazard and the problem of powder charge inefficiency, easily cause the jam of powder charge pipeline when powder charge in the pit to not only influence the powder charge, still increased the danger of powder charge process simultaneously. If the viscosity is too low, a large amount of explosive return of blast holes after charging is easily caused, so that the problems of unrealized charging and insufficient charging amount are caused, and greater potential safety hazards exist on site.
The granular sticky explosive needs to have moderate viscosity, namely, both cohesiveness and free-running property, and in the explosive charging process, certain cohesiveness can avoid the phenomenon of explosive return, and certain free-running property is also beneficial to preventing hole blockage in the explosive charging process. However, the existing viscosity measuring method can only measure the viscosity of liquid substances generally, and for finished products formed by mixing solid granular components such as granular sticky explosives, liquid oil phases and adhesives, no related viscosity measuring method exists. At present, the method for testing viscosity generally depends on the experience of technicians, and the method comprises the steps of picking a product by using an instrument, visually observing the wire drawing condition, and then judging whether the viscosity is proper or not by years of experience. Therefore, the method can not be used for judging the product performance in a standardized way and can not ensure the continuity of knowledge. Meanwhile, the viscosity requirement of different users is also differentiated experience judgment, the viscosity range of differentiated products cannot be described more accurately, the viscosity is also the main performance index of the granular sticky explosive, and the use effect of the users is directly related.
Disclosure of Invention
The device and the use method for measuring the viscosity of the granular sticky explosive overcome the defects in the prior art, are convenient and fast to operate, simple and easy to understand, are accurate in viscosity measurement of the granular sticky explosive, and can accurately provide the required product according to different customers through measured viscosity data.
In order to solve the technical problems, the invention adopts the technical scheme that: a granular viscous explosive viscosity test apparatus comprising: the quantitative barrel is a conical barrel body with an upper end and a lower end being open, the weighing plate is arranged below the quantitative barrel, the circle center of the weighing plate coincides with the axis of the quantitative barrel, the positioning ring is concentrically arranged on the weighing plate, the lower end of the outer diameter of the quantitative barrel coincides with the positioning ring, the weighing plate is concentrically and uniformly provided with circular scale marks, the positioning ring coincides with zero scale marks, namely the outer diameter of the lower end of the quantitative barrel coincides with the diameter of the positioning ring, the positioning ring coincides with the zero scale marks, the quantitative barrel is accurately positioned on the weighing plate, and the scales of the scale marks are located away from the zero scale marks and gradually increase in the direction of the quantitative barrel.
The number of the scale marks is 2-20.
The diameter of the upper end of the quantitative barrel 1 is smaller than that of the lower end of the quantitative barrel, and the taper of the quantitative barrel is 10-30 degrees, so that uniform accumulation and rapid dispersion of granular sticky explosives are facilitated.
The distance between two adjacent graduation marks is 10 mm.
The diameter of the upper end opening of the quantitative barrel is 120mm, the diameter of the lower end opening of the quantitative barrel is 200mm, and the height of the quantitative barrel is 200 mm.
For more accurate reading of the scale, a mark line for dividing 5 equal parts of the adjacent two scale lines is marked between the adjacent two scale lines.
Two handles are fixed on the quantitative barrel, and the handles are convenient for operators to lift the quantitative barrel.
A method for using a granular viscous explosive viscosity testing device comprises the following steps:
1) horizontally placing the measuring disc, and placing the quantitative cylinder on a zero scale mark of the measuring disc;
2) slowly filling a quantitative viscous granular explosive with viscosity to be measured into a quantitative cylinder;
3) an operator holds the handle, and slowly and vertically lifts the quantitative cylinder to enable the viscous granular explosive to spread on the weighing disc by means of self gravity;
4) standing for 5 minutes, comparing the spreading surface of the viscous granular explosive with the scale of the weighing disc, and reading the scale value Ri at the edge of the spreading surface;
5) and (4) judging a result: by the formula
Figure RE-GDA0002603399330000021
Calculating the average value of the crossed scales of the spreading surface and the scale marks, wherein n is the number of the scale marks, RiThe scale value is read out by intersecting the spreading surface with the ith scale mark; assuming a numerical range Ra~RbProducts consistently needed by the customer if
Figure RE-GDA0002603399330000022
The viscosity of the sample to be measured is qualified, if so
Figure RE-GDA0002603399330000023
The viscosity of the sample to be tested is too high, if so
Figure RE-GDA0002603399330000024
The viscosity of the sample to be measured is too low.
Compared with the prior art, the invention has the following beneficial effects.
Firstly, the viscosity of the viscous granular explosive required by a customer is numerically and quantitatively described through the device, so that the problem of deviation caused by judgment by the experience of workers in the past is solved, the continuation of the technical experience is facilitated, and larger errors caused by different workers are avoided.
Secondly, the viscosity testing device for the granular sticky explosive designed by the invention can identify products required by specific customers according to the viscosity required by different customers, and can determine the viscosity ranges (R) of the products required by different customers according to years of technical experience and different user tests under the conditions of quantification and timinga~RbAnd (d) to determine whether the viscosity of the sample is appropriate based on the viscosity range data. If the spreading surface is qualified within the designated range, otherwise, the spreading surface is unqualified, the viscosity is too high when the spreading surface is smaller than the designated range, and the viscosity is too low when the spreading surface is larger than the designated range.
Drawings
The invention is further described below with reference to the accompanying drawings.
FIG. 1 is a cross-sectional view of a granular viscous explosive viscosity testing apparatus according to the present invention.
Fig. 2 is a cross-sectional view of a dosing cartridge according to the present invention.
FIG. 3 is a cross-sectional view of a metering disc of the present invention.
FIG. 4 is a top view of a metering disc of the present invention.
FIG. 5 is an enlarged view of the invention at A.
FIG. 6 is an enlarged view of the invention at B.
In the figure: 1 is a quantitative barrel, 2 is a weighing plate, 3 is a handle, 4 is a scale mark, 5 is a scale mark, and 6 is a positioning ring.
Detailed Description
The following is a further description with reference to specific examples.
A granular viscous explosive viscosity test apparatus comprising: quantitative bucket 1, measure dish 2, scale mark 4, scale 5 and position circle 6, quantitative bucket 1 is the conical barrel of the equal open-ended of upper end, lower extreme, the scale dish 2 set up in the below of quantitative bucket 1, the centre of a circle of scale dish 2 with the axle center coincidence of quantitative bucket 1, be provided with one heart on the scale dish 2 the position circle 6, the lower extreme of 1 external diameter of quantitative bucket with the position circle 6 coincidence, it is circular that the concentricity evenly is provided with on the scale dish 2 scale mark 4, position circle 6 and zero scale mark coincidence, promptly the outer diameter of 1 lower extreme of quantitative bucket with the diameter of position circle 6 is unanimous, and is convenient like this quantitative bucket 1 accurate positioning is in on the scale dish 2, the scale 5 of scale mark 4 follows the zero scale mark is kept away from the direction of quantitative bucket 1 increases gradually.
The number of the scale marks 4 is 20, and the distance between two adjacent scale marks 4 is 10 mm.
The diameter of the upper port of the quantitative barrel 1 is 120mm, the diameter of the lower port of the quantitative barrel 1 is 200mm, and the height of the quantitative barrel 1 is 200mm, so that the granular sticky explosive is favorably and uniformly stacked and rapidly dispersed.
For more accurate reading of the scale, two adjacent graduation marks 4 are marked with a marking line between them that divides them 5 equally.
Two handles 3 are fixed on the quantitative barrel 1, and the handles 3 are convenient for an operator to lift the quantitative barrel 1.
The user of a certain user needs the viscous explosive of a company, the viscosity required by the user is high, and through years of experience and field tests of the user, the viscous explosive with the reading of a measuring disc between 100mm and 130mm is suitable. The company produces a new batch of viscous explosives, and to determine whether the viscosity of the new batch is suitable, the following determinations are made:
the first step is as follows: horizontally placing the measuring disc, and placing the quantifying cylinder on the positioning ring of the measuring disc;
the second step is that: slowly loading a new batch of viscous granular explosive to be tested into the quantitative cylinder;
the third step: an operator holds the handle, slowly and vertically lifts the quantitative cylinder, and the viscous granular explosive is spread on the weighing disc by means of dead weight;
the fourth step: standing for 5 minutes, visually observing the viscous granular explosiveOpening the surface, comparing the scale lines of the measuring disc, reading the opening surface and the scale values R, R1=118mm,R2=120mm,R3=120mm,R4=118mm;
The fifth step: the results describe:
Figure RE-GDA0002603399330000041
by means of the calculation, the user can select,
Figure RE-GDA0002603399330000042
known as Ra=100mm,Rb130 mm; therefore, it is not only easy to use
Figure RE-GDA0002603399330000043
And obtaining the viscosity of the new batch of viscous explosive products meeting the user requirement.
The above embodiments are merely illustrative of the principles of the present invention and its effects, and do not limit the present invention. It will be apparent to those skilled in the art that modifications and improvements can be made to the above-described embodiments without departing from the spirit and scope of the invention. Accordingly, it is intended that all equivalent modifications or changes be made by those skilled in the art without departing from the spirit and technical spirit of the present invention, and be covered by the claims of the present invention.

Claims (8)

1. A device for testing the viscosity of a granular viscous explosive, comprising: ration bucket (1), balance dish (2), scale mark (4), scale (5) and position circle (6), ration bucket (1) is the equal open-ended conical barrel of upper end, lower extreme, balance dish (2) set up in the below of ration bucket (1), the centre of a circle of balance dish (2) with the axle center coincidence of ration bucket (1), be provided with one heart on balance dish (2) position circle (6), the external diameter of ration bucket (1) lower extreme with position circle (6) coincidence, be provided with the circularity on balance dish (2) with one heart evenly scale mark (4), position circle (6) and zero scale mark coincidence, scale (5) of scale mark (4) are followed zero scale mark is kept away from the direction of ration bucket (1) increases gradually.
2. A granular viscous explosive viscosity test device according to claim 1, wherein the number of the graduation marks (4) is 2-20.
3. A granular viscous explosive viscosity test apparatus according to claim 2, wherein the diameter of the upper end of the quantitative barrel (1) is smaller than that of the lower end thereof, and the taper of the quantitative barrel (1) is 10 ° to 30 °.
4. A granular viscous explosive viscosity testing apparatus according to claim 3, wherein the distance between two adjacent graduation marks (4) is 10 mm.
5. A granular viscous explosive viscosity test device according to claim 4, wherein the diameter of the upper end opening of the quantitative barrel (1) is 120mm, the diameter of the lower end opening of the quantitative barrel (1) is 200mm, and the height of the quantitative barrel (1) is 200 mm.
6. A granular viscous explosive viscosity test apparatus according to claim 5, wherein the adjacent graduation marks (4) are marked with a mark line for dividing the graduation mark by 5.
7. A granular viscous explosive viscosity test device according to claim 6, wherein two handles (3) are fixed on the quantitative barrel (1).
8. A method of using the apparatus for testing the viscosity of a granular viscous explosive according to any one of claims 1 to 7, comprising the steps of:
1) horizontally placing the measuring disc, and placing the quantitative cylinder on a zero scale mark of the measuring disc;
2) slowly filling a quantitative viscous granular explosive with viscosity to be measured into a quantitative cylinder;
3) an operator holds the handle, and slowly and vertically lifts the quantitative cylinder to enable the viscous granular explosive to spread on the weighing disc by means of self gravity;
4) standing for 5 min, comparing the spreading surface of the viscous granular explosive with the scale of the weighing plate, and reading the scale value R at the edge of the spreading surfacei
5) And (4) judging a result: by the formula
Figure RE-RE-DEST_PATH_IMAGE002
Calculating the average value of the scale of the spreading surface intersected with the scale line
Figure RE-RE-DEST_PATH_IMAGE004
Where n is the number of graduation marks, RiThe scale value is read out by intersecting the spreading surface with the ith scale mark; assuming a numerical range Ra~RbProducts required by the customer, if Ra
Figure RE-DEST_PATH_IMAGE006
≤RbThe viscosity of the sample to be tested is qualified, if so
Figure RE-DEST_PATH_IMAGE008
<RaThe viscosity of the sample to be tested is too high, if so
Figure RE-DEST_PATH_IMAGE010
>RbThe viscosity of the sample to be measured is too low.
CN201911172954.XA 2019-11-26 2019-11-26 Device for testing viscosity of granular sticky explosive and using method Pending CN111624137A (en)

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Citations (7)

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Publication number Priority date Publication date Assignee Title
RU2439481C1 (en) * 2010-08-02 2012-01-10 Сергей Михайлович Мужичек Method to estimate completeness of explosive charge detonation and device for its realisation
CN103936533A (en) * 2014-04-21 2014-07-23 中国工程物理研究院化工材料研究所 High-viscosity PBX (Polymer Bonded Explosive) injection-compression molding method and device
CN104803814A (en) * 2015-04-22 2015-07-29 长沙亦川机电设备科技有限责任公司 Intermediate-temperature-sensitized emulsion explosive and preparation method thereof
CN205643082U (en) * 2016-05-19 2016-10-12 科之杰新材料集团有限公司 Concrete viscosity measurement device
CN108440222A (en) * 2018-03-01 2018-08-24 中国葛洲坝集团易普力股份有限公司 Sticky ammonium nitrate-fuel oil mixture mixed charge machine
CN208505837U (en) * 2018-08-13 2019-02-15 常州工程职业技术学院 A kind of gravity flowing levelling mortar fluidity test panel
CN211553665U (en) * 2019-11-26 2020-09-22 山西江阳兴安民爆器材有限公司 Device for testing viscosity of granular sticky explosive

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2439481C1 (en) * 2010-08-02 2012-01-10 Сергей Михайлович Мужичек Method to estimate completeness of explosive charge detonation and device for its realisation
CN103936533A (en) * 2014-04-21 2014-07-23 中国工程物理研究院化工材料研究所 High-viscosity PBX (Polymer Bonded Explosive) injection-compression molding method and device
CN104803814A (en) * 2015-04-22 2015-07-29 长沙亦川机电设备科技有限责任公司 Intermediate-temperature-sensitized emulsion explosive and preparation method thereof
CN205643082U (en) * 2016-05-19 2016-10-12 科之杰新材料集团有限公司 Concrete viscosity measurement device
CN108440222A (en) * 2018-03-01 2018-08-24 中国葛洲坝集团易普力股份有限公司 Sticky ammonium nitrate-fuel oil mixture mixed charge machine
CN208505837U (en) * 2018-08-13 2019-02-15 常州工程职业技术学院 A kind of gravity flowing levelling mortar fluidity test panel
CN211553665U (en) * 2019-11-26 2020-09-22 山西江阳兴安民爆器材有限公司 Device for testing viscosity of granular sticky explosive

Non-Patent Citations (1)

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Title
李鹤群 等: "DNTF/TNT/HMX基熔铸炸药流变性能研究", 中北大学学报(自然科学版), vol. 35, no. 06, 15 December 2014 (2014-12-15), pages 720 - 723 *

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