CN111607104A - Sucrose with low human body absorption and preparation method thereof - Google Patents

Sucrose with low human body absorption and preparation method thereof Download PDF

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Publication number
CN111607104A
CN111607104A CN202010447091.9A CN202010447091A CN111607104A CN 111607104 A CN111607104 A CN 111607104A CN 202010447091 A CN202010447091 A CN 202010447091A CN 111607104 A CN111607104 A CN 111607104A
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Prior art keywords
sugar
sucrose
cane
solution
water
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Inventor
周庆余
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Shanghai Zhongdao Sugar Industry Ltd By Share Ltd
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Shanghai Zhongdao Sugar Industry Ltd By Share Ltd
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H8/00—Macromolecular compounds derived from lignocellulosic materials
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/20—Reducing nutritive value; Dietetic products with reduced nutritive value
    • A23L33/21—Addition of substantially indigestible substances, e.g. dietary fibres
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention discloses cane sugar with low human body absorption and a preparation method thereof. Because the sugarcane fibers are combined with the sucrose molecules, the absorption of the human body to the sucrose is reduced due to the macromolecular effect of the sugarcane fibers, the sugar intake of the human body is effectively reduced, and the sugarcane is novel healthy sucrose. In addition, the invention utilizes the bagasse which is produced in a large amount in the sugar manufacturing process, thereby playing a role of environmental protection.

Description

Sucrose with low human body absorption and preparation method thereof
Technical Field
The invention relates to the field of food, in particular to the field of edible sucrose.
Background
With the better life quality of people, the intake of sugar becomes more and more, which leads to the increasing proportion of the obese people at present.
In recent years there has been an increasing interest in health, and many alternatives to sucrose, such as sugarless colas, such as sweeteners, have emerged. However, the taste of sugar-free products is obviously not satisfactory for users, and sweeteners such as aspartame can be decomposed into methanol, aspartic acid and phenylalanine in human bodies, and researches show that the levels of formic acid (formicacid) and alanine (alanine, an amino acid) in urine of people with hypertension are higher. One possible explanation is that these people drink large quantities of soda containing aspartame, causing hypertension and high levels of aspartame metabolites.
Therefore, people need to develop a product which keeps the taste of the cane sugar and is completely harmless to human bodies.
Disclosure of Invention
In order to solve the problems, the invention discloses a low human body absorption sucrose. The invention modifies the bagasse, combines the fiber and the cane sugar molecules in a certain way, thereby reducing the absorption of human body to cane sugar.
The whole preparation process comprises three steps of (1) preparing the sugarcane fiber velvet; (2) bridging of sugarcane fiber flock and sucrose molecules; (3) and (5) crystallizing sucrose to prepare.
(1) Preparing the sucrose fiber velvet:
the preparation method comprises adding 10g bagasse into a reactor containing 30g-1000g and 30% hydrogen peroxide, stirring for 3-5 hr, and filtering to remove filtrate.
The product of the first step is added to a reactor containing 30-1000g of 10% aqueous sodium hydroxide solution, stirred for 3-5 hours, and filtered to remove the filtrate.
The product of the previous step was filtered repeatedly with water until the solution PH = 7. Distilling to remove most of water under ultrasonic condition, and vacuum lyophilizing to obtain the final product. FDS-2000 from Tokyo physicochemical instruments was used as a freeze dryer.
(2) Sugarcane fiber flock and sucrose molecular bridging:
adding 1g of the treated sugarcane fiber velvet into 200g of anhydrous cyclohexanone, starting stirring, adding 0.2-0.5g of adipic anhydride, and reacting for 3 hours until the anhydride reaction is complete.
0.05g of trifluoromethanesulfonic acid and 10-20g of sucrose were added to the reactor, and the reaction was continued until the carboxylic acid reaction was complete.
(3) And (3) sucrose crystallization preparation:
adding 400g of deionized water into the solution, shaking for layering, collecting a water phase, washing an organic phase for 3 times, and finally combining the 3 times of water phases to obtain the bridged solution containing the sugarcane fiber velvet and the sucrose.
Adding the solution containing the sugarcane fiber velvet and the cane sugar which are bridged into a reactor, keeping the temperature at 60-80 ℃, stirring at the speed of 20-40 r/min, keeping ultrasonic oscillation, crystallizing the cane sugar solution after evaporating most of water, and finally separating and drying the crystals to obtain the product.
In the scheme, the invention modifies the bagasse which is a byproduct in the sucrose industry to form small-size sugarcane fiber velvet. This can reduce sucrose absorption without affecting the appearance.
In the second step, adipic anhydride is used for bridging, mainly because adipic anhydride is a domestic allowable food additive, and even if residue exists, the adipic anhydride does not cause harmful damage to human bodies. The bridging ratio of the sugarcane fiber velvet and the sucrose is 1:10-1:20, when the proportion of the sugarcane fiber velvet is too large, a turbid phenomenon can obviously occur in a system, the appearance is influenced, and the sweetness is reduced too much due to the fact that the bridging ratio is too large. When the ratio is too small, the effect of reducing sucrose absorption is not significant.
In the third step of crystallization process, ultrasonic oscillation must be kept, the phenomenon of agglomeration of the sugarcane fiber velvet is prevented, and in addition, because the sugarcane fiber velvet is added, the sucrose is easier to crystallize, and the production efficiency is improved.
The technical scheme provided by the embodiment of the invention has the following beneficial effects:
the sucrose obtained by the synthesis method provided by the embodiment of the invention is connected with the sucrose by using adipic anhydride, and the sucrose cannot be absorbed by human body due to the characteristics of the fiber, so that the sugar intake is reduced.
Meanwhile, the health-care food is rich in dietary fibers, so that the health-care food can mechanically stimulate the intestinal peristalsis and accelerate the intestinal digestion function, and has a health-care effect.
Detailed description of the invention
The present invention will be further described below by way of specific examples.
In the following examples, those whose operations are not subject to the conditions indicated, are carried out according to the conventional conditions or conditions recommended by the manufacturer. The raw materials are conventional products which can be obtained commercially by manufacturers and specifications.
Example 1
10g of bagasse was added to a reactor containing 30g of 30% hydrogen peroxide, stirred for 5 hours, and the filtrate was removed by filtration.
The first step product was added to a reactor containing 30g of 10% aqueous sodium hydroxide solution, stirred for 5 hours, and the filtrate was removed by filtration.
The second product was filtered repeatedly with water until the solution PH = 7. Distilling to remove most of water under ultrasonic condition, and vacuum lyophilizing to obtain the final product. FDS-2000 from Tokyo physicochemical instruments was used as a freeze dryer.
And (3) adding 1g of the sugarcane fiber velvet into 200g of anhydrous cyclohexanone, starting stirring, adding 0.2g of adipic anhydride, and reacting for 3 hours until the anhydride completely reacts.
0.05g of trifluoromethanesulfonic acid and 20g of sucrose were added to the reactor, and the reaction was continued until the carboxylic acid was completely reacted.
Adding 400g of deionized water into the solution, shaking for layering, collecting a water phase, washing an organic phase for 3 times, and finally combining the 3 times of water phases to obtain a bridged solution containing the sugarcane fibers and the sucrose.
Adding the solution containing the sugarcane fibers and the cane sugar which are bridged into a reactor, keeping the temperature at 60 ℃, stirring at the speed of 20 r/min, keeping ultrasonic oscillation, crystallizing the cane sugar solution after evaporating most of water, and finally separating and drying crystals to obtain the product.
Example 2
10g of bagasse was added to a reactor containing 200g of 30% hydrogen peroxide, stirred for 4 hours, and the filtrate was removed by filtration.
The first step product was added to a reactor containing 200g of 10% aqueous sodium hydroxide solution, stirred for 4 hours, and filtered to remove the filtrate.
The second product was filtered repeatedly with water until the solution PH = 7. Distilling to remove most of water under ultrasonic condition, and vacuum lyophilizing to obtain the final product. FDS-2000 from Tokyo physicochemical instruments was used as a freeze dryer.
And (3) adding 1g of the sugarcane fiber velvet into 200g of anhydrous cyclohexanone, starting stirring, adding 0.4g of adipic anhydride, and reacting for 3 hours until the anhydride completely reacts.
0.05g of trifluoromethanesulfonic acid and 12g of sucrose were added to the reactor, and the reaction was continued until the carboxylic acid was completely reacted.
Adding 400g of deionized water into the solution, shaking for layering, collecting a water phase, washing an organic phase for 3 times, and finally combining the 3 times of water phases to obtain a bridged solution containing the sugarcane fibers and the sucrose.
Adding the solution containing the sugarcane fibers and the cane sugar which are bridged into a reactor, keeping the temperature at 80 ℃, stirring at the speed of 40 r/min, keeping ultrasonic oscillation, crystallizing the cane sugar solution after evaporating most of water, and finally separating and drying crystals to obtain the product.
Example 3
10g of bagasse was added to a reactor containing 500g of 30% hydrogen peroxide, stirred for 4 hours, and the filtrate was removed by filtration.
The first step product was added to a reactor containing 500g of 10% aqueous sodium hydroxide solution, stirred for 4 hours, and filtered to remove the filtrate.
The second product was filtered repeatedly with water until the solution PH = 7. Distilling to remove most of water under ultrasonic condition, and vacuum lyophilizing to obtain the final product. FDS-2000 from Tokyo physicochemical instruments was used as a freeze dryer.
And (3) adding 1g of the sugarcane fiber velvet into 200g of anhydrous cyclohexanone, starting stirring, adding 0.3g of adipic anhydride, and reacting for 3 hours until the anhydride completely reacts.
0.05g of trifluoromethanesulfonic acid and 13g of sucrose were added to the reactor, and the reaction was continued until the carboxylic acid was completely reacted.
Adding 400g of deionized water into the solution, shaking for layering, collecting a water phase, washing an organic phase for 3 times, and finally combining the 3 times of water phases to obtain a bridged solution containing the sugarcane fibers and the sucrose.
Adding the solution containing the sugarcane fibers and the cane sugar which are bridged into a reactor, keeping the temperature at 70 ℃, stirring at the speed of 30 r/min, keeping ultrasonic oscillation, crystallizing the cane sugar solution after evaporating most of water, and finally separating and drying crystals to obtain the product.
Example 4
10g of bagasse was added to a reactor containing 1000g of 30% hydrogen peroxide, stirred for 3 hours, and the filtrate was removed by filtration.
The first step product was added to a reactor containing 1000g of 10% aqueous sodium hydroxide solution, stirred for 3 hours, and the filtrate was removed by filtration.
The second product was filtered repeatedly with water until the solution PH = 7. Distilling to remove most of water under ultrasonic condition, and vacuum lyophilizing to obtain the final product. FDS-2000 from Tokyo physicochemical instruments was used as a freeze dryer.
And (3) adding 1g of the sugarcane fiber velvet into 200g of anhydrous cyclohexanone, starting stirring, adding 0.4g of adipic anhydride, and reacting for 3 hours until the anhydride completely reacts.
0.05g of trifluoromethanesulfonic acid and 10g of sucrose were added to the reactor, and the reaction was continued until the carboxylic acid was completely reacted.
Adding 400g of deionized water into the solution, shaking for layering, collecting a water phase, washing an organic phase for 3 times, and finally combining the 3 times of water phases to obtain a bridged solution containing the sugarcane fibers and the sucrose.
Adding the solution containing the sugarcane fibers and the cane sugar which are bridged into a reactor, keeping the temperature at 60 ℃, stirring at the speed of 20 r/min, keeping ultrasonic oscillation, crystallizing the cane sugar solution after evaporating most of water, and finally separating and drying crystals to obtain the product.
Example 5
10g of bagasse was added to a reactor containing 500g of 30% hydrogen peroxide, stirred for 4 hours, and the filtrate was removed by filtration.
The first step product was added to a reactor containing 500g of 10% aqueous sodium hydroxide solution, stirred for 4 hours, and filtered to remove the filtrate.
The second product was filtered repeatedly with water until the solution PH = 7. Distilling to remove most of water under ultrasonic condition, and vacuum lyophilizing to obtain the final product. FDS-2000 from Tokyo physicochemical instruments was used as a freeze dryer.
And (3) adding 1g of the sugarcane fiber velvet into 200g of anhydrous cyclohexanone, starting stirring, adding 0.2g of adipic anhydride, and reacting for 3 hours until the anhydride completely reacts.
0.05g of trifluoromethanesulfonic acid and 15g of sucrose were added to the reactor, and the reaction was continued until the carboxylic acid was completely reacted.
Adding 400g of deionized water into the solution, shaking for layering, collecting a water phase, washing an organic phase for 3 times, and finally combining the 3 times of water phases to obtain a bridged solution containing the sugarcane fibers and the sucrose.
Adding the solution containing the sugarcane fibers and the cane sugar which are bridged into a reactor, keeping the temperature at 80 ℃, stirring at the speed of 40 r/min, keeping ultrasonic oscillation, crystallizing the cane sugar solution after evaporating most of water, and finally separating and drying crystals to obtain the product.
Example 6
10g of bagasse was added to a reactor containing 700g of 30% hydrogen peroxide, stirred for 3 hours, and filtered to remove the filtrate.
The first step product was added to a reactor containing 700g of a 10% aqueous solution of sodium hydroxide, stirred for 3 hours, and the filtrate was removed by filtration.
The second product was filtered repeatedly with water until the solution PH = 7. Distilling to remove most of water under ultrasonic condition, and vacuum lyophilizing to obtain the final product. FDS-2000 from Tokyo physicochemical instruments was used as a freeze dryer.
And (3) adding 1g of the sugarcane fiber velvet into 200g of anhydrous cyclohexanone, starting stirring, adding 0.4g of adipic anhydride, and reacting for 3 hours until the anhydride completely reacts.
0.05g of trifluoromethanesulfonic acid and 15g of sucrose were added to the reactor, and the reaction was continued until the carboxylic acid was completely reacted.
Adding 400g of deionized water into the solution, shaking for layering, collecting a water phase, washing an organic phase for 3 times, and finally combining the 3 times of water phases to obtain a bridged solution containing the sugarcane fibers and the sucrose.
Adding the solution containing the sugarcane fibers and the cane sugar which are bridged into a reactor, keeping the temperature at 70 ℃, stirring at the speed of 30 r/min, keeping ultrasonic oscillation, crystallizing the cane sugar solution after evaporating most of water, and finally separating and drying crystals to obtain the product.
Example 7
10g of bagasse was added to a reactor containing 200g of 30% hydrogen peroxide, stirred for 5 hours, and the filtrate was removed by filtration.
The first step product was added to a reactor containing 200g of 10% aqueous sodium hydroxide solution, stirred for 5 hours, and the filtrate was removed by filtration.
The second product was filtered repeatedly with water until the solution PH = 7. Distilling to remove most of water under ultrasonic condition, and vacuum lyophilizing to obtain the final product. FDS-2000 from Tokyo physicochemical instruments was used as a freeze dryer.
And (3) adding 1g of the sugarcane fiber velvet into 200g of anhydrous cyclohexanone, starting stirring, adding 0.2g of adipic anhydride, and reacting for 3 hours until the anhydride completely reacts.
0.05g of trifluoromethanesulfonic acid and 17g of sucrose were added to the reactor and the reaction was continued until the carboxylic acid was completely reacted.
Adding 400g of deionized water into the solution, shaking for layering, collecting a water phase, washing an organic phase for 3 times, and finally combining the 3 times of water phases to obtain a bridged solution containing the sugarcane fibers and the sucrose.
Adding the solution containing the sugarcane fibers and the cane sugar which are bridged into a reactor, keeping the temperature at 60 ℃, stirring at the speed of 20 r/min, keeping ultrasonic oscillation, crystallizing the cane sugar solution after evaporating most of water, and finally separating and drying crystals to obtain the product.
Example 8
10g of bagasse was added to a reactor containing 1000g of 30% hydrogen peroxide, stirred for 3 hours, and the filtrate was removed by filtration.
The first step product was added to a reactor containing 1000g of 10% aqueous sodium hydroxide solution, stirred for 3 hours, and the filtrate was removed by filtration.
The second product was filtered repeatedly with water until the solution PH = 7. Distilling to remove most of water under ultrasonic condition, and vacuum lyophilizing to obtain the final product. FDS-2000 from Tokyo physicochemical instruments was used as a freeze dryer.
And (3) adding 1g of the sugarcane fiber velvet into 200g of anhydrous cyclohexanone, starting stirring, adding 0.5g of adipic anhydride, and reacting for 3 hours until the anhydride completely reacts.
0.05g of trifluoromethanesulfonic acid and 13g of sucrose were added to the reactor, and the reaction was continued until the carboxylic acid was completely reacted.
Adding 400g of deionized water into the solution, shaking for layering, collecting a water phase, washing an organic phase for 3 times, and finally combining the 3 times of water phases to obtain a bridged solution containing the sugarcane fibers and the sucrose.
Adding the solution containing the sugarcane fibers and the cane sugar which are bridged into a reactor, keeping the temperature at 80 ℃, stirring at the speed of 40 r/min, keeping ultrasonic oscillation, crystallizing the cane sugar solution after evaporating most of water, and finally separating and drying crystals to obtain the product.
The above description is only exemplary of the present invention and should not be taken as limiting the scope of the present invention, as any modifications, equivalents, improvements and the like made within the spirit and principle of the present invention should be included in the scope of the present invention.
The main function of the invention is to reduce the absorption of human body to cane sugar, so the blood sugar rise value after eating is detected.
The test method comprises the following steps:
5 subjects, A/B/C/D/E, were selected, wherein A, B was female, C, D, E was male, A, C was lean and B, E was fat, respectively. 75g of the sucrose of the present invention and the comparative example were administered for 9 days, respectively, and blood glucose values were measured after 1 hour after each day of administration. The final average was taken as the conclusion, the comparative example was commercial sucrose.
Figure 825268DEST_PATH_IMAGE002
The combination of all the data shows that the sugar absorption of human body is obviously reduced on the premise of keeping the taste of the sucrose, and the maximum sugar absorption is reduced by 32.72%.

Claims (7)

1. The invention relates to a cane sugar with low human body absorption, which is characterized in that modified cane fiber is used, and cane fiber and cane sugar molecules are combined in a certain mode, so that the absorption of a human body to cane sugar can be reduced.
2. A method according to claim 1, wherein the sugar cane fibres used in the method of the invention are sugar cane fibre flock.
3. The method for synthesizing the sugarcane fiber velvet according to claim 2, wherein the sugarcane bagasse is treated under 30% hydrogen peroxide water, then treated with 10% sodium hydroxide aqueous solution, repeatedly washed with water until the solution is neutral, then subjected to reduced pressure distillation to remove part of water, ultrasonically dispersed, and subjected to vacuum freeze-drying treatment to finally obtain the sugarcane fiber velvet.
4. A method according to claim 1, wherein the method of combining sugar cane fiber and sucrose molecules used in the present invention is bridging using adipic anhydride.
5. According to claim 1, the mass ratio of the sugar cane fiber and the cane sugar used in the invention is 1:10 to 1: 20.
6. The method for preparing sucrose with low human body absorption according to claim 1, wherein the solution containing cane fiber and sucrose bridged by adipic anhydride is added into a reactor, the temperature is kept at 60-80 ℃, the stirring speed is 20-40 r/min, ultrasonic oscillation is kept, most of water is evaporated, the sucrose solution is crystallized, and finally the crystallization is separated and dried to obtain the product.
7. The sugar solution of claim 1, which is not limited to sucrose solution, can be white sugar, brown sugar, powdered sugar, etc.
CN202010447091.9A 2020-05-25 2020-05-25 Sucrose with low human body absorption and preparation method thereof Pending CN111607104A (en)

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Publication number Priority date Publication date Assignee Title
CN1887293A (en) * 2005-06-28 2007-01-03 牛蓉 Slimming composition with cross-linked monosaccharide/disaccharide and dietary fiber
CN104664383A (en) * 2015-03-10 2015-06-03 天津桂发祥十八街麻花食品股份有限公司 Stuffed fried dough twist being capable of lowering fasting blood-glucose and increasing glucose tolerance and having glycose metabolism regulating function as well as production method thereof
CN105839440A (en) * 2016-05-31 2016-08-10 华南理工大学 Preparation method of bagasse nanocellulose
CN109170429A (en) * 2018-09-06 2019-01-11 山东禹王生态食业有限公司 A kind of preparation method of modified bean dregs dietary fiber beverage
CN112175405A (en) * 2020-09-11 2021-01-05 刘喜文 High-strength wood-plastic composite board and preparation method thereof
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CN1887293A (en) * 2005-06-28 2007-01-03 牛蓉 Slimming composition with cross-linked monosaccharide/disaccharide and dietary fiber
CN104664383A (en) * 2015-03-10 2015-06-03 天津桂发祥十八街麻花食品股份有限公司 Stuffed fried dough twist being capable of lowering fasting blood-glucose and increasing glucose tolerance and having glycose metabolism regulating function as well as production method thereof
CN105839440A (en) * 2016-05-31 2016-08-10 华南理工大学 Preparation method of bagasse nanocellulose
CN109170429A (en) * 2018-09-06 2019-01-11 山东禹王生态食业有限公司 A kind of preparation method of modified bean dregs dietary fiber beverage
CN112175405A (en) * 2020-09-11 2021-01-05 刘喜文 High-strength wood-plastic composite board and preparation method thereof
CN112403442A (en) * 2020-10-30 2021-02-26 广西大学 Preparation method of modified bagasse cellulose-based composite adsorbent

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Application publication date: 20200901