CN111551792A - Dielectric infinite high frequency relative dielectric constant measuring principle - Google Patents

Dielectric infinite high frequency relative dielectric constant measuring principle Download PDF

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CN111551792A
CN111551792A CN202010461190.2A CN202010461190A CN111551792A CN 111551792 A CN111551792 A CN 111551792A CN 202010461190 A CN202010461190 A CN 202010461190A CN 111551792 A CN111551792 A CN 111551792A
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potential
dielectric constant
high frequency
dielectric
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CN111551792B (en
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索长友
李忠华
陈宇
郭文敏
郑欢
韩永森
孙云龙
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Harbin University of Science and Technology
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Harbin University of Science and Technology
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    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R27/00Arrangements for measuring resistance, reactance, impedance, or electric characteristics derived therefrom
    • G01R27/02Measuring real or complex resistance, reactance, impedance, or other two-pole characteristics derived therefrom, e.g. time constant
    • G01R27/26Measuring inductance or capacitance; Measuring quality factor, e.g. by using the resonance method; Measuring loss factor; Measuring dielectric constants ; Measuring impedance or related variables
    • G01R27/2617Measuring dielectric properties, e.g. constants

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Abstract

The invention discloses a dielectric medium infinite high frequency relative dielectric constant measuring principle, which solves the technical problem that the dielectric medium infinite high frequency relative dielectric constant cannot be accurately measured. The basic principle of the invention is as follows: the method comprises the steps of polarizing a tested dielectric by adopting a high-voltage direct-current power supply, then realizing acquisition and recording of a short-circuit current and a replying potential time domain spectrum of the tested insulating dielectric by adopting an acquisition system consisting of an electrometer, an electrostatic voltmeter and a computer, accurately acquiring the change rate of the replying potential at the initial moment by least square fitting, and acquiring the change rate of the replying potential at the initial moment by the change rate of the replying potential at the initial moment
Figure DDA0002510967960000011
And short-circuit current Id(t1‑) By the formula
Figure DDA0002510967960000012
Realizing the achievement of infinite high frequency relative dielectric constantThe measurement of (2).

Description

Dielectric infinite high frequency relative dielectric constant measuring principle
Technical Field
The invention relates to the field of dielectric parameter measurement of insulating dielectrics, in particular to an infinite high-frequency relative dielectric constant measurement principle of the insulating dielectrics.
Background
Insulating dielectrics are materials that make up the insulation of electronic devices and electrical equipment and serve as electrical insulation, mechanical support, and external encapsulation. Relative dielectric constant at a given frequency: (r) Is one of the important technical indexes for expressing the insulation performance of an insulating dielectric medium under the action of a determined frequency electric field, and is defined as the dielectric constant of the insulating dielectric medium and the dielectric constant in vacuum under a given frequency (0) In which the vacuum dielectric constant: (0) Is a constant, and is also a unit conversion coefficient. Dielectric physics establishes the relative permittivity of an insulating dielectric at a given frequency for a particular insulating dielectric (satisfying a single Debye relaxation polarization mechanism) ((r) And relative dielectric constant of infinite high frequency: () Static relative dielectric constant: (s) And frequency (f). Wherein, the relative dielectric constant of infinite high frequency is the appearance of instantaneous displacement polarization; static relative dielectric constant: (s) The external manifestation after polarization is fully established under the action of a direct current electric field is the sum of instantaneous displacement polarization and all relaxation polarization. Theoretically for a particular insulating dielectric, the relative permittivity at known infinite frequency of () And static relative dielectric constant: (s) The relative permittivity at any given frequency can be calculated under the conditions. All insulating dielectrics inevitably generate instantaneous displacement polarization under the action of an electric field, and the research on the polarization mechanism is based on the instantaneous displacement polarization behavior, so that the measurement and the conjecture of the infinite high-frequency relative dielectric constant have important theoretical significance and engineering significance.
For gas, transparent liquid and transparent solid insulating dielectric medium, the refractive index (n) of light can be measured, and then the relative dielectric constant (n) can be calculated according to the infinite high frequency) Relation to the photorefractive coefficient n (=n2) Realizing the relative dielectric constant of infinite high frequency: () The measurement of (2). For insulating dielectrics that fail optical testing,the infinite high frequency relative permittivity can generally be achieved by measuring and inferring the high frequency relative permittivity(s) ((s))) Presumably, e.g. Novocontrol Concept80 model broadband dielectrophoresis tests up to 107Measurement of relative permittivity at Hz frequency. For neutral insulating dielectrics, there is no relaxation polarization, and the infinite high frequency relative permittivity can be obtained relatively accurately by measuring the high frequency relative permittivity () And (4) information. For dielectric materials containing relaxed polarization, a higher frequency relative permittivity measurement is required to obtain the infinite high frequency relative permittivity (R) ((R))) More precise speculation, e.g. using hundreds of GHz (10)9Hz) was measured with a vector analyzer. Using hundreds of GHz (10)9Hz) is relatively expensive and the measured result is not truly infinite high frequency relative permittivity.
SUMMARY OF THE PATENT FOR INVENTION
In order to overcome the technical problem that the infinite high frequency relative dielectric constant of the insulating dielectric medium cannot be accurately measured, the invention provides a measuring principle of the infinite high frequency relative dielectric constant of the insulating dielectric medium, and aims to conveniently and accurately measure the infinite high frequency relative dielectric constant.
The above purpose is realized by the following technical scheme:
the principle is characterized in that a measuring switch is switched from a short-circuit state to a surface potential test state, the short-circuit current before the switch acts and the recovery potential after the switch acts are recorded, and the change rate of the recovery potential at the initial moment is measured
Figure BDA0002510967940000021
And short-circuit current Id(t1-) By the formula
Figure BDA0002510967940000022
Calculating to obtain infinite high-frequency relative dielectric constantThe test results of (1).
Further, the influence of noise on the return potential measurement is eliminated through a least square fitting method, and the change rate of the return potential of the insulating dielectric medium at the initial moment is obtained through a fitting function.
Further, under the action of direct current voltage, the short-circuit current and the time domain spectrum of the return potential of the insulation dielectric medium to be detected are collected and recorded through an electrometer, an electrostatic voltmeter and a computer collection system.
Compared with the prior art, the invention has the following beneficial effects: the invention fully utilizes the information contained in the time domain spectrum of the polarization, short circuit depolarization current and the time domain spectrum of the return potential of the insulating dielectric medium to calculate and obtain the infinite high-frequency relative dielectric constantThe dielectric constant measurement method has the advantages that the dielectric constant measurement method realizes the measurement of the infinite high frequency relative dielectric constant and the displacement polarizability of the insulating dielectric for the first time, compared with the traditional method of extrapolating the dielectric spectrum test result to obtain the infinite high frequency relative dielectric constant result, the test method is simple, convenient and feasible, the test equipment is relatively low in manufacturing cost, and a research means is provided for the dielectric mechanism research of the insulating dielectric.
Drawings
FIG. 1 is a schematic diagram of a short circuit current and surface potential time domain spectroscopy joint test system for insulating dielectrics;
FIG. 2 is a test result of the insulating dielectric short-circuit current time domain spectrum in the example;
FIG. 3 shows the time domain spectrum test result of the insulation dielectric in the embodiment.
In the figure: 1-a direct current high voltage power supply; 2-a switch; 3-measured insulating dielectric; 4-a high voltage electrode; 5-a guard electrode; 6-a measuring electrode; 7-high voltage electrostatic measuring probe; 8-an electrostatic voltmeter; 9-data communication line 1 connected to computer; 10-an electrometer; 11-a data communication line 2 connected to a computer;
Detailed Description
The present invention will be described in detail with reference to the following embodiments and examples. It should be emphasized that this summary is intended to be illustrative, and not limiting, of the invention.
Detailed description of the invention
The dielectric infinite high frequency relative dielectric constant measuring principle includes switching the measuring switch from short circuit state to surface potential test state and recording the switch motionShort-circuit current before operation and recovery potential after operation, from initial time change rate of recovery potential
Figure BDA0002510967940000031
And short-circuit current Id(t1-) By the formula
Figure BDA0002510967940000032
Calculating to obtain infinite high-frequency relative dielectric constantThe test results of (1).
Detailed description of the invention
On the basis of the first embodiment, specifically, the initial time rate of change of the return potential of the insulating dielectric is obtained from the fitting function.
Detailed description of the invention
On the basis of the first specific embodiment, specifically, the short-circuit current and the time domain spectrum of the return potential of the insulating dielectric medium to be tested are collected and recorded by an electrometer, an electrostatic voltmeter and a computer collection system under the action of the direct-current voltage.
Detailed description of the invention
Based on the first embodiment, the rate of change of the recovery potential of the tested insulating dielectric causes the current Ihd(t) is calculated by the formula
Figure BDA0002510967940000033
In particular, C in said formulaIs an infinite high-frequency capacitor, and is,is a relative dielectric constant of an infinite high frequency,0s is the area of the insulating dielectric and d is the thickness of the insulating dielectric, for a vacuum dielectric constant.
Detailed description of the invention
In the first and fifth embodiments, the short circuit is switched to the open circuit instant (time t ═ t)1) Short-circuit current I flowing through the measured insulating dielectricd(t1-) And rate of change of return potential dU (t)1+) The equivalent relation of current caused by dt is
Figure BDA0002510967940000034
Detailed description of the invention
Based on the first embodiment and the sixth embodiment, in particular, the infinite high frequency relative permittivity of the measured insulating dielectricIs calculated by the formula
Figure BDA0002510967940000035
Detailed description of the invention
On the basis of the second embodiment, specifically, the least square fitting formula of the reply potential is
U(t)=A0+A1exp(-t/τ1)-A2exp(-t/τ2)+A3exp(-t/τ3)-A4exp(-t/τ4)
Specifically, the parameter A in the fitting formula0、A1、A2、A3And A4Are respectively constant, parameter tau1、τ2、τ3And τ4Respectively the relaxation time constant
Detailed description of the invention
On the basis of the third specific embodiment, specifically, the direct-current voltage is generated by a direct-current voltage-stabilizing high-voltage direct-current power supply, the electrometer is provided with a data interface communicated with a computer, the input end of the electrostatic voltmeter is connected with the high-voltage electrostatic probe, and the output end of the electrostatic voltmeter is connected with the computer.
Examples
The insulating dielectric of this example is a 10 wt% silicon carbide/polyethylene composite insulating dielectric, and the electrode area S is 452.16mm2And the thickness d is 0.2mm, and a direct-current high voltage of 5kV is applied to the tested insulating dielectric by using a polarization current spectrum testing system shown in FIG. 1. After 1800s the samples were short-circuited and the short-circuit current through the tested dielectric was recorded by a Keithley6517B electrometer, as shown in fig. 2Shown in the figure. The short circuit obtained in this embodiment is switched to the open circuit time (t)11811s) of short-circuit depolarized current I (t) flowing through the insulating dielectric to be tested1-)=422.32pA。
After the short circuit is switched to the open circuit, the measured time domain spectrum of the insulation dielectric return potential obtained in the example is shown in FIG. 3, and the fitting parameter A0=140.52V,A1=-34.40V,A2=37.50V,A3=-35.14V,A4=31.84V,τ1=767.14s,τ2=3.65s,τ3=129.96s,τ420.96s, short circuit transitions to open circuit time (t)11810s) rate of change dU (t) of the return potential of the measured insulating dielectric1+) (dt) ═ 12.13V/s, relative dielectric constant at high frequencyIs 2.18.

Claims (3)

1. The principle is characterized in that a measuring switch is switched from a short-circuit state to a surface potential test state, the short-circuit current before the switch acts and the recovery potential after the switch acts are recorded, and the change rate of the recovery potential at the initial moment is measured
Figure FDA0002510967930000011
And short-circuit current Id(t1-) By the formula
Figure FDA0002510967930000012
Calculating to obtain infinite high-frequency relative dielectric constantThe test results of (1).
2. In claim 1, the influence of noise on the measurement of the return potential is removed by a least square fitting method, and the rate of change of the return potential of the insulating dielectric at the initial time is obtained from a fitting function.
3. The method of claim 1, wherein the short-circuit current and the time domain spectrum of the back potential of the insulating dielectric to be measured under the action of the direct-current voltage are collected and recorded by an electrometer, an electrostatic voltmeter and a computer collection system.
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