CN111397986A - Horizontal type sample preparation and briquetting equipment - Google Patents
Horizontal type sample preparation and briquetting equipment Download PDFInfo
- Publication number
- CN111397986A CN111397986A CN202010295538.5A CN202010295538A CN111397986A CN 111397986 A CN111397986 A CN 111397986A CN 202010295538 A CN202010295538 A CN 202010295538A CN 111397986 A CN111397986 A CN 111397986A
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- China
- Prior art keywords
- sample preparation
- briquetting
- hydraulic cylinder
- limit sensor
- sample
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/286—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/36—Embedding or analogous mounting of samples
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N2001/2893—Preparing calibration standards
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/36—Embedding or analogous mounting of samples
- G01N2001/366—Moulds; Demoulding
Abstract
The invention discloses a horizontal sample preparation and briquetting device, which consists of a hydraulic system and a hardware mechanism, wherein an adjustable limit sensor is arranged at the mechanical structure part of the hardware, the sample preparation and briquetting device can be used for briquetting various powder materials, the density of a sample preparation and briquetting block is adjusted through hydraulic pressure setting, and the thickness of the sample preparation and briquetting block can be adjusted through adjusting the position of the adjustable limit sensor.
Description
Technical Field
The invention relates to a horizontal sample-making briquetting device, which presses powder or granules into regular sample blocks with smooth and flat surfaces.
Background
With the development of science and technology, the novel spectrum analyzer is highly regarded by the detection field, is widely applied to the metal detection field at present, and accurately displays the measurement result in real time for the measurement of metal element components and element content. The method has a small application range in the non-metal field, the spectral analysis instrument has strict requirements on the surface of a detected substance, and the smoother and smoother the surface of the detected substance, the more accurate the detection data. Therefore, the application of the spectrum analyzer in non-material detection is important for making a uniform standard sample block for the detected material.
The spectrum analyzer is based on the principle that the characteristic spectrum of an element to be measured, which is emitted from a light source, is absorbed by ground state atoms of the element to be measured in vapor of a sample, and the emission spectrum is attenuated, thereby determining the content of the element to be measured in the sample, which conforms to the lambert-beer law a = -lg I/I o = -L gT = KC L, where I is the transmitted light intensity, I0 is the emitted light intensity, T is the transmittance, and L is the optical path length L of the atomizer, so that the atoms of any element are composed of nuclei and electrons moving around the nuclei, and the electrons outside the nuclei are distributed in different levels according to the high and low levels of their energies, so that one nucleus may have multiple energy level states.
Emission spectrum analysis process:
1. the sample is vaporized and atomized (converted into gaseous atoms) under the action of energy, and the outer electrons of the gaseous atoms are excited to a high energy state. When transitioning from a higher energy level to a lower energy level, the atoms will release excess energy and emit characteristic lines. This process, known as evaporation, atomization and excitation, is achieved by means of an excitation light source.
2. The radiation generated by atoms is dispersed and split, and recorded on the light-sensitive plate according to the wavelength sequence, so that regular spectral lines, namely a spectrogram can be presented. Is realized by means of a light splitting and detecting device of a spectrograph.
3. And carrying out qualitative identification or quantitative analysis according to the obtained spectrogram. Because the atomic structures of different elements are different, the wavelengths of the emitted light lines are different after being excited, namely, each element has the characteristic wavelength, so that the existence of the elements can be accurately identified according to the characteristic spectrums of the elements (qualitative analysis), and the intensities of the spectral lines are related to the content of the elements in a sample, so that the content of the elements can be determined by using the intensities of the spectral lines (quantitative analysis).
Advantages of the spectroscopic analyzer:
1. the sampling mode is flexible, and the loss caused by sampling can be saved for the detection and analysis of rare and precious metals.
2. The test speed is high, multi-channel instant multi-point acquisition can be set, and real-time output is realized through a calculator.
3. The nondestructive testing can be carried out on some mechanical parts without damaging samples, and the nondestructive testing is convenient.
4. The analysis speed is fast, and the method is more suitable for stokehold analysis or field analysis, thereby achieving fast detection.
5. The accuracy of the analysis results is based on the chemical analysis standards.
Disclosure of Invention
The invention mainly solves the technical problem of providing a horizontal sample preparation briquetting device for detecting non-metallic substances by a spectrum analyzer, and the device has the following main advantages:
1. the pressure adjusting range is large, and the pressure adjustment is flexible;
2. the sample block has a large thickness adjusting range and flexible thickness adjustment;
3. automatic operation can be realized by matching with a P L C controller;
in order to solve the technical problem, the invention adopts a technical scheme that the system comprises: 1. a hydraulic cylinder; 2. a movable articulation joint; 3. a limit sensor; 4. a limiting baffle plate; 5. a left ejector rod; 6. a mold; 7. a material receiving plate; 8. a limiting baffle plate; 9. a limit sensor; 10. a movable articulation joint; 11. a hydraulic cylinder; 12. a right side bracket; 13. a right side mandril; 14. a fixing plate; 15. a left side bracket; 16. and a hydraulic station.
The invention has the beneficial effects that: the press forming device has the advantages of smooth and flat surface for pressing and forming powder or particles of non-metallic substances, adjustable pressure and thickness for different materials, convenient and flexible use and wide application range.
Drawings
FIG. 1 is a schematic view of a three-dimensional structure of a horizontal type sample preparation and briquetting device.
FIG. 2 is a schematic diagram illustrating the structure of a horizontal sample-making and briquetting apparatus according to the present invention.
FIG. 3 is a schematic diagram of the working process of the horizontal type sample preparation and briquetting equipment.
FIG. 4 is a schematic diagram of the working process of the horizontal type sample preparation and briquetting equipment.
FIG. 5 is a schematic diagram of the working process of the horizontal type sample preparation and briquetting equipment.
FIG. 6 is a schematic diagram of the working process of the horizontal type sample preparation and briquetting equipment.
FIG. 7 is a schematic diagram of the working process of the horizontal type sample preparation and briquetting equipment.
FIG. 8 is a schematic diagram of the working process of the horizontal type sample preparation and briquetting equipment.
The components in fig. 2 are labeled as follows: 1. a hydraulic cylinder; 2. a movable articulation joint; 3. a limit sensor; 4. a limiting baffle plate; 5. a left ejector rod; 6. a mold; 7. a material receiving plate; 8. a limiting baffle plate; 9. a limit sensor; 10. a movable articulation joint; 11. a hydraulic cylinder; 12. a right side bracket; 13. a right side mandril; 14. a fixing plate; 15. a left side bracket; 16. and a hydraulic station.
Detailed Description
The following detailed description of the present invention is provided in conjunction with the accompanying drawings so that the advantages and features of the present invention will be readily understood by those skilled in the art, and the scope of the present invention will be clearly and clearly defined.
Referring to fig. 2, the components in the embodiment of the present invention include: 1. a hydraulic cylinder; 2. a movable articulation joint; 3. a limit sensor; 4. a limiting baffle plate; 5. a left ejector rod; 6. a mold; 7. a material receiving plate; 8. a limiting baffle plate; 9. a limit sensor; 10. a movable articulation joint; 11. a hydraulic cylinder; 12. a right side bracket; 13. a right side mandril; 14. a fixing plate; 15. and a left bracket.
Referring to fig. 3, fig. 4, fig. 5, fig. 6, fig. 7 and fig. 8, a schematic diagram of a work flow of a horizontal type sample-making briquetting apparatus according to the present invention is shown.
The invention relates to a horizontal sample preparation and briquetting device working process which comprises the following steps:
1. as shown in figure 3, the hydraulic cylinder of the part 11 is started, the push rod on the right side of the pushing part 13 moves leftwards, the push rod on the right side of the part 13 enters the die of the part 6, the limit blocking piece of the part 8 contacts the limit sensor of the part 9, the limit sensor of the part 9 sends a signal, and the hydraulic cylinder of the part 11 stops moving forwards.
2. As shown in fig. 4, the powder enters the die cavity from the die upper opening of the part 6.
3. As shown in figure 5, the hydraulic cylinder of the part 1 is started, the push rod on the left side of the pushing part 5 moves rightwards, the hydraulic cylinder of the part 11 and the push rod on the right side of the part 13 keep the original position unchanged, the material is pressed into a cake sample block under the action of the push rod on the left side of the part 5 and the push rod under the part 13, the hydraulic cylinder of the part 1 and the hydraulic cylinder of the part 11 maintain pressure for 10 seconds, the density of the cake sample block of the pressed material is uniform, the surface is smoother, and redundant material is extruded to other parts of.
4. As shown in figure 6, when the push rod on the side of the hydraulic cylinder driving part 13 of the part 11 retracts, the limit stop sheet of the part 8 contacts the limit sensor of the part 9, the limit sensor of the part 9 sends out a signal, and the hydraulic cylinder of the part 11 stops retracting.
5. As shown in fig. 7, the hydraulic cylinder of the part 1 starts to drive the ejector rod on the left side of the part 5 to move rightwards, so that the material cake sample block is pushed, when the limiting blocking piece of the part 4 contacts the limiting sensor of the part 3, the limiting sensor of the part 3 sends a signal, the hydraulic cylinder of the part 1 stops, the material cake sample block is pushed out of the mold cavity of the part 6, and the material cake sample block falls on the material receiving plate of the part 7, so that the sample preparation process is completed.
6. As shown in fig. 8, in the second sample preparation operation, the hydraulic cylinder of the part 1 drives the left ejector rod of the part 5 to move back, when the limit blocking piece of the part 4 contacts the limit sensor of the part 3, the limit sensor of the part 3 sends a signal, the part 1 stops moving, and simultaneously, the hydraulic cylinder of the part 11 drives the right ejector rod of the part 13 to push to the left, and when the limit blocking piece of the part 8 contacts the limit sensor of the part 9, the hydraulic cylinder of the part 9 sends a signal, the part 11 stops moving, and the next first sample preparation process is started.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all modifications of equivalent structures and equivalent processes performed by the present specification and drawings, or directly or indirectly applied to other related technical fields, are included in the scope of the present invention.
Claims (3)
1. A horizontal sample-making briquetting device is a powder and particle sample-making briquetting device.
2. The device is used in cooperation with a spectral analysis instrument to sample and press the non-metallic substances to be detected.
3. The equipment comprises: 1. a hydraulic cylinder; 2. a movable articulation joint; 3. a limit sensor; 4. a limiting baffle plate; 5. a left ejector rod; 6. a mold; 7. a material receiving plate; 8. a limiting baffle plate; 9. a limit sensor; 10. a movable articulation joint; 11. a hydraulic cylinder; 12. a right side bracket; 13. a right side mandril; 14. a fixing plate; 15. a left side bracket; 16. and a hydraulic station.
Priority Applications (1)
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CN202010295538.5A CN111397986A (en) | 2020-04-15 | 2020-04-15 | Horizontal type sample preparation and briquetting equipment |
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CN202010295538.5A CN111397986A (en) | 2020-04-15 | 2020-04-15 | Horizontal type sample preparation and briquetting equipment |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112067406A (en) * | 2020-10-10 | 2020-12-11 | 北京华泰美景科技发展有限公司 | System appearance briquetting equipment |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5035845A (en) * | 1988-05-13 | 1991-07-30 | Kzk Powder Technologies Corporation | Powder pressing method |
JPH06213787A (en) * | 1993-01-21 | 1994-08-05 | Nippon Saamonikusu Kk | Method and apparatus for molding powder sample |
CN101629880A (en) * | 2009-08-05 | 2010-01-20 | 中国地质大学(武汉) | Horizontally push-type bidirectional sample preparation instrument |
CN101863073A (en) * | 2010-05-21 | 2010-10-20 | 中国地质大学(武汉) | Multifunctional joint sampling instrument for undisturbed soil |
CN106501047A (en) * | 2016-12-06 | 2017-03-15 | 铜陵有色金属集团股份有限公司金冠铜业分公司 | A kind of pelletized powder samples method for xrf analysis |
CN107328802A (en) * | 2017-07-26 | 2017-11-07 | 瑞绅葆分析技术(上海)有限公司 | X ray fluorescence spectrometry sample preparation device |
CN110567777A (en) * | 2019-10-08 | 2019-12-13 | 宁夏大学 | hollow cylinder remolded soil sample bidirectional sample pressing device and method |
CN110954387A (en) * | 2020-02-14 | 2020-04-03 | 北京华泰美景科技发展有限公司 | System appearance briquetting equipment |
-
2020
- 2020-04-15 CN CN202010295538.5A patent/CN111397986A/en active Pending
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5035845A (en) * | 1988-05-13 | 1991-07-30 | Kzk Powder Technologies Corporation | Powder pressing method |
JPH06213787A (en) * | 1993-01-21 | 1994-08-05 | Nippon Saamonikusu Kk | Method and apparatus for molding powder sample |
CN101629880A (en) * | 2009-08-05 | 2010-01-20 | 中国地质大学(武汉) | Horizontally push-type bidirectional sample preparation instrument |
CN101863073A (en) * | 2010-05-21 | 2010-10-20 | 中国地质大学(武汉) | Multifunctional joint sampling instrument for undisturbed soil |
CN106501047A (en) * | 2016-12-06 | 2017-03-15 | 铜陵有色金属集团股份有限公司金冠铜业分公司 | A kind of pelletized powder samples method for xrf analysis |
CN107328802A (en) * | 2017-07-26 | 2017-11-07 | 瑞绅葆分析技术(上海)有限公司 | X ray fluorescence spectrometry sample preparation device |
CN110567777A (en) * | 2019-10-08 | 2019-12-13 | 宁夏大学 | hollow cylinder remolded soil sample bidirectional sample pressing device and method |
CN110954387A (en) * | 2020-02-14 | 2020-04-03 | 北京华泰美景科技发展有限公司 | System appearance briquetting equipment |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112067406A (en) * | 2020-10-10 | 2020-12-11 | 北京华泰美景科技发展有限公司 | System appearance briquetting equipment |
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