CN111374908A - Cosmetic of organosilicon elastic powder composition and preparation method thereof - Google Patents

Cosmetic of organosilicon elastic powder composition and preparation method thereof Download PDF

Info

Publication number
CN111374908A
CN111374908A CN202010204126.6A CN202010204126A CN111374908A CN 111374908 A CN111374908 A CN 111374908A CN 202010204126 A CN202010204126 A CN 202010204126A CN 111374908 A CN111374908 A CN 111374908A
Authority
CN
China
Prior art keywords
weight
parts
homogenizer
stirring
silicone
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202010204126.6A
Other languages
Chinese (zh)
Inventor
田勇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiaxing Huasheng Cosmetics Co ltd
Original Assignee
Jiaxing Huasheng Cosmetics Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiaxing Huasheng Cosmetics Co ltd filed Critical Jiaxing Huasheng Cosmetics Co ltd
Priority to CN202010204126.6A priority Critical patent/CN111374908A/en
Publication of CN111374908A publication Critical patent/CN111374908A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/895Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55Phosphorus compounds
    • A61K8/556Derivatives containing from 2 to 10 oxyalkylene groups
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8188Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bonds, and at least one being terminated by a bond to sulfur or by a hertocyclic ring containing sulfur; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/12Face or body powders for grooming, adorning or absorbing
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a preparation method of a cosmetic composition of organosilicon elastic powder, which comprises the following steps: a first step of stirring 82.75% of purified water and 5% of butanediol with a homogenizer at 2500 rpm; secondly, adding 10 percent of organosilicon elastic powder composition into the result of the first step, and then stirring for 5 minutes by a homogenizer at the rotating speed of 3000 rpm; thirdly, adding 0.25 percent of hydroxyethyl acrylate/sodium acryloyl dimethyl taurate copolymer into the result of the second step, and stirring for 5 minutes at 4000rpm by a homogenizer; and fourthly, cooling the result obtained in the step 3 to 45-50 ℃, adding 2% of 1, 2-hexanediol, stirring for 1 minute at 2500rpm by using a homogenizer, and cooling to below 30 ℃, thus finishing the process. The present invention can temporarily improve wrinkles and does not block skin pores by wrapping the continuous phase with a water-soluble material, thus causing no skin irritation inflammation.

Description

Cosmetic of organosilicon elastic powder composition and preparation method thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a cosmetic of an organosilicon elastic powder composition and a preparation method thereof.
Background
Skin wrinkles are known to have several factors. The most important factor is sunlight. When continuously exposed to sunlight, degeneration of collagen fibers and elastic fibers of the dermis is caused, and skin aging occurs as the skin dries. As a result, wrinkles may occur. Facial expressions also affect wrinkle formation. As the muscles continue to contract, skin wrinkles appear, often deeper than those caused by other causes. Gravity also affects it, which can cause the skin to stretch downward, causing it to sag. The dryness of the skin also affects wrinkles, and as the skin ages, the function of the glands that retain the moisture of the skin decreases, the skin becomes dry, and the dry skin becomes rough, elastic and wrinkled.
In addition, cigarette, genetic predisposition and skin tone (fair people are more prone to wrinkles as they are more prone to sunburn).
The prior art documents are: in korean patent laid-open No. 10-2011-; in korean patent laid-open No. 10-2014-0132371, a super absorbent polymer and a silicone elastomer for a skin care composition; in korean patent laid-open No. 10-2006-.
In conclusion, it is similar in that it is a cosmetic composition using a silicone polymer, but in the prior art documents, there is no description of a method for temporarily improving wrinkles by wrapping a continuous phase with a water-soluble material without blocking skin pores.
Disclosure of Invention
The invention provides a non-volatile silicone oil cosmetic composition and a preparation method thereof. For solving the above-mentioned prior art problems.
In order to solve the technical problem, the invention aims to realize that:
a silicone elastomeric powder composition comprising the following components and weights: 40-80 parts by weight of one or more organosilicon elastic powders of polydimethylsiloxane/vinyl dimethyl siloxane cross-linked polymer and vinyl dimethyl siloxane/polymethylsiloxane silsesquioxane cross-linked polymer; 10-50 parts by weight of one or more of phenyl trimethyl silicone oil, diphenyl dimethyl silicone oil, phenyl trimethyl siloxy diphenyl siloxane, diphenyl dimethyl silicone oil and diphenyl methyl diphenyl trisiloxane; at least one component of polyglycerol-4 stearate, polyglycerol-4 oleate, polyglycerol-6 myristate, polyglycerol-10 isostearate and polyglycerol-10 stearate is 10 parts by weight; further comprising 30-40 parts by weight of a mixture of glycerin, maltitol and purified water as a continuous phase in a weight ratio of 40:30: 30.
A method of preparing a silicone elastomeric powder composition comprising the steps of: a first step of stirring 40 parts by weight of a polydimethylsiloxane/vinyldimethylsiloxane crosspolymer powder having a diameter of 1 to 10 μm and a specific gravity of 1.01 or less, and 20 parts by weight of phenyl trimethicone oil for 5 minutes using a homogenizer at 2000 rpm; a second step of dissolving 10 parts by weight of polyglycerol-4 oleate at 60 ℃ or higher in the first step and stirring at 2000rpm for 5 minutes using a homogenizer; and step three, adding 30 parts by weight of glycerol, maltitol and purified water in the step two, wherein the ratio of the mixture to the total weight of the mixture is 4: 3: 3 weight ratio of the mixture was used as a continuous phase to produce a water-in-oil emulsion, and the mixture was stirred using a homogenizer at 3000rpm for 5 minutes.
A cosmetic composition of a silicone elastic powder composition comprising the following components: an organosilicon elastomeric powder composition; butanediol; hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and 1, 2-hexanediol.
On the basis of the above scheme and as a preferable scheme of the scheme: 0 part by weight of an organosilicon elastic powder composition; 5 parts by weight of butanediol; 0.25 parts by weight of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and 2 parts by weight of 1, 2-hexanediol.
A method for preparing a cosmetic composition of silicone elastic powder, comprising the steps of: a first step of stirring 82.75% of purified water and 5% of butanediol with a homogenizer at 2500 rpm;
secondly, adding 10 percent of organosilicon elastic powder composition into the result of the first step, and then stirring for 5 minutes by a homogenizer at the rotating speed of 3000 rpm;
thirdly, adding 0.25 percent of hydroxyethyl acrylate/sodium acryloyl dimethyl taurate copolymer into the result of the second step, and stirring for 5 minutes at 4000rpm by a homogenizer;
and fourthly, cooling the result obtained in the step 3 to 45-50 ℃, adding 2% of 1, 2-hexanediol, stirring for 1 minute at 2500rpm by using a homogenizer, and cooling to below 30 ℃, thus finishing the process.
A cosmetic composition containing organosilicon elastic powder is prepared by the above preparation method.
Compared with the prior art, the invention has the outstanding and beneficial technical effects that:
the present invention can temporarily improve wrinkles and does not block skin pores by wrapping the continuous phase with a water-soluble material, thus causing no skin irritation inflammation.
Drawings
The left side of figure 1 is a photograph of example 1 and the right side of figure 1 is a photograph of the particles of example 2.
Fig. 2 shows the photographs of the particles of example 3 and example 4 on the left and on the right in table 1.
Fig. 3 shows the photographs of the particles of example 5 and example 6 on the left and in table 1.
On the left side of FIG. 4 is a photograph of the particles of example 7 in Table 1.
Fig. 5 shows the particle photographs of comparative example 1 and comparative example 2 on the left in table 1.
Fig. 6 shows on the left before and after the application of the skin wrinkles.
Detailed Description
Hereinafter, embodiments of the present invention will be described in detail to facilitate understanding of the present invention. However, the embodiment according to the present invention may be modified into various other forms, and the scope of the present invention should not be construed as being limited to the following embodiments. The embodiments of the present invention are provided to enable those skilled in the art to more clearly understand the present invention.
Preparation example 1 Silicone elastomeric powder composition
The silicone elastic powder composition of the present invention,
silicone elastomer powder of one or more of polydimethylsiloxane/vinyldimethylsiloxane crosspolymer and vinyldimethylsiloxane/polymethylsiloxane silsesquioxane crosspolymer;
one or more components of phenyl trimethyl silicone oil, diphenyl dimethyl silicone oil, phenyl trimethyl siloxy diphenyl siloxane, diphenyl dimethyl silicone oil and diphenyl methyl diphenyl trisiloxane;
at least one component selected from semi-solid polyglycerin-4 stearate, polyglycerin-4 oleate, polyglycerin-6 myristate, polyglycerin-10 isostearate and polyglycerin-10 stearate among components having HLB value of 10 or more in the polyglycerin emulsifier for improving adsorption ability;
and a suitable mixture of glycerol, maltitol and purified water as a continuous phase for reducing the prevention of pore clogging of the silicone elastic powder;
in addition, the silicone elastic powder composition of the present invention,
40-80 parts by weight of one or more organosilicon elastic powders of polydimethylsiloxane/vinyl dimethyl siloxane cross-linked polymer and vinyl dimethyl siloxane/polymethylsiloxane silsesquioxane cross-linked polymer;
10-50 parts by weight of one or more of phenyl trimethyl silicone oil, diphenyl dimethyl silicone oil, phenyl trimethyl siloxy diphenyl siloxane, diphenyl dimethyl silicone oil and diphenyl methyl diphenyl trisiloxane;
at least one component of polyglycerol-4 stearate, polyglycerol-4 oleate, polyglycerol-6 myristate, polyglycerol-10 isostearate and polyglycerol-10 stearate is 10 parts by weight;
further comprising 30-40 parts by weight of a mixture of glycerin, maltitol and purified water as a continuous phase in a weight ratio of 40:30:30 to prevent the phenomenon of pore clogging of silicon powder.
Preparation example 2 Process for producing Silicone elastic powder composition
An example of a method for producing the silicone elastic powder composition of preparation example 1 is as follows. The following values may be adjusted within an appropriate range according to design conditions.
A first step of stirring 40 parts by weight of a polydimethylsiloxane/vinyldimethylsiloxane crosspolymer powder having a diameter of 1 to 10 μm and a specific gravity of 1.01 or less, and 20 parts by weight of phenyl trimethicone oil for 5 minutes using a homogenizer at 2000 rpm;
a second step of dissolving 10 parts by weight of polyglycerol-4 oleate at 60 ℃ or higher in the first step and stirring at 2000rpm for 5 minutes using a homogenizer;
and step three, adding 30 parts by weight of glycerol, maltitol and purified water in the step two, wherein the ratio of the mixture to the total weight of the mixture is 4: 3: 3 weight ratio of the mixture as a continuous phase to produce a water-in-oil emulsion and stirring the mixture for 5 minutes at 3000rpm using a homogenizer;
preparation example 3 cosmetic composition Using Silicone elastic powder composition
An example of the composition of a cosmetic composition to which the silicone elastic powder composition of preparation example 1 was applied is as follows.
An organosilicon elastomeric powder composition; butanediol; hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and 1, 2-hexanediol;
preferably, 10 parts by weight of an organosilicon elastomeric powder composition; 5 parts by weight of butanediol; 0.25 parts by weight of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and 2 parts by weight of 1, 2-hexanediol.
Preparation example 4 method for producing cosmetic composition Using Silicone elastic powder composition
An example of a method for producing the cosmetic composition of preparation example 3 is as follows. The following values may be adjusted to some extent within an appropriate range according to design conditions.
A first step of stirring 82.75% of purified water and 5% of butanediol with a homogenizer at 2500 rpm;
secondly, adding 10 percent of organosilicon elastic powder composition into the result of the first step, and then stirring for 5 minutes by a homogenizer at the rotating speed of 3000 rpm;
thirdly, adding 0.25 percent of hydroxyethyl acrylate/sodium acryloyl dimethyl taurate copolymer into the result of the second step, and stirring for 5 minutes at 4000rpm by a homogenizer;
and fourthly, cooling the result obtained in the step 3 to 45-50 ℃, adding 2% of 1, 2-hexanediol, stirring for 1 minute at 2500rpm by using a homogenizer, and cooling to below 30 ℃, thus finishing the process.
Experimental example 1, verification of the composition for preparing column 1 and the method for preparing column 2
[ Experimental method ]
Silicone elastomeric powder compositions of examples consisting of the ingredients and amounts described in table 1 were prepared as follows.
Phase a was stirred using a homogenizer at 2000rpm for 5 minutes, then phase B was added to phase a, dissolved to 60 ℃, and stirred at the same rpm for 5 minutes. Next, phase C was added and stirred with a homogenizer at 3000rpm for 5 minutes.
TABLE 1
Figure BDA0002418558660000071
[ Performance evaluation 1]
As shown in Table 2 below, in order to determine the adhesion between wrinkles upon coating of examples and comparative examples, the adhesion was measured using CT3TA-SF of Brookfield under the following conditions: target value: 10.0 mm; triggering load: 1.0 g; testing speed: 1.0mm/s, sample temperature: 25 +/-3 ℃.
In addition, as shown in fig. 1 to 5, particle observation was performed to measure the degree of coalescence of the silicone elastic powders of examples and comparative examples. In the particle observation and the particle measurement, observation was performed using an olympus BX43 microscope at a magnification of 400 times the polarization mode.
TABLE 2
Figure BDA0002418558660000072
Figure BDA0002418558660000081
From the results, it can be seen that when the content of the polydimethylsiloxane/vinyldimethylsiloxane crosspolymer is 50% or more, the coalescence phenomenon is remarkable and the dispersibility is poor; a dimethicone/vinyl dimethicone crosspolymer content of from 20 to 30. The performance is good, but the distribution of spherical silicon powder is small, or the particle size of the composite material is increased.
As can be seen from the adhesive strength, examples 3 and 5 have the best adhesion.
Thus, example 5, which contains 40% of a polydimethylsiloxane/vinyldimethylsiloxane crosspolymer, can be judged to have excellent adhesion, and can be judged to have a fairly stable particle size distribution and a uniform size.
[ Performance evaluation 2]
The silicone elastic powder has the property of absorbing oil, and when applied to the skin, can be absorbed and fixed by the oil of the human body. Therefore, general cleaning methods are often difficult to remove, or require thorough cleaning, and substances that are not easy to clean are present in pores, wrinkles, etc., thereby causing skin inflammation or acne.
Therefore, in order to prevent pore clogging, the water solubility of the examples and comparative examples was evaluated to confirm that the continuous phase was an aqueous phase, as shown in table 3.
Referring to fig. 6, it can be seen that when the composition is aqueous in the continuous phase before and after coating, a temporary anti-wrinkle effect is produced.
To measure the water solubility, 95% purified water was added to examples and comparative examples having a content of 10%, and the water solubility was measured after stirring at 1000rpm for 5 minutes in a homogenizer.
TABLE 3
Figure BDA0002418558660000091
◎ very stable, ○ stable, △ normal, X unstable
The water solubility of example 5 was evaluated to be excellent.
However, it can be seen that the water solubility of example 7 and comparative example 2 is very stable, but this is due to the polydimethylsiloxane/vinyldimethylsiloxane crosspolymer being less than 10%.
Experimental example 2, verifying the composition of preparation example 3 and the method of preparation example 4
As shown in Table 4, water-in-oil cosmetic examples 8, 9 and 10 were prepared using examples 1, 3 and 5, some of which were expected to have the best performance. In addition, comparative example 3 was prepared by performing comparison using comparative example 1.
For a more objective evaluation, only a minimum of raw materials is used.
The manufacturing method is as follows.
Phase a was stirred at 2500RPM for 5 minutes at room temperature using a homogenizer, then phase B was added to phase a and stirred at 3000RPM for 5 minutes using a homogenizer. After confirming successful dispersion, phase C was placed into phase a and then stirred using a homogenizer at 4000RPM for 5 minutes. Thereafter, phase D was added and the mixture was stirred for 1 minute at 2500RPM using a homogenizer and the process was terminated.
TABLE 4
Figure BDA0002418558660000092
Figure BDA0002418558660000101
[ Performance evaluation ]
As shown in table 5, the stability of the formulation in a high temperature chamber at 50 ℃ and the surface stability of the formulation within 1 month, which are long-term problems of the spherical silicone powder, floating on the surface with time, were used to evaluate the high temperature stability in the water system. Evaluate it for the desired properties-and perform a sensory evaluation of spreadability and wrinkles after skin application.
TABLE 5
Figure BDA0002418558660000102
Figure BDA0002418558660000111
◎ good, ○ general, △ deficient and X bad
It can be seen that example 10, to which example 5 was applied as described above, exhibited significantly improved properties in various aspects such as raw material stability, sensory evaluation and volatilization, for example. In other words, it can be said that the performances of examples 5 and 10 prepared using preparation examples 1 to 4 were confirmed to be excellent.
The above description is merely an example of the technical idea of the present invention, and those skilled in the art to which the present invention pertains may make various modifications and variations without departing from the essential features of the present invention.
Therefore, the embodiments disclosed in the present invention are not intended to limit the technical spirit of the present invention but are intended to cause blindness, and the scope of the technical idea of the present invention is not limited by these embodiments. The scope of the present invention should be construed in accordance with the following claims, and all technical ideas within the scope of equivalents thereof should be construed to be included in the scope of the present invention.

Claims (6)

1. A silicone elastomeric powder composition characterized by: comprises the following components by weight:
40-80 parts by weight of one or more organosilicon elastic powders of polydimethylsiloxane/vinyl dimethyl siloxane cross-linked polymer and vinyl dimethyl siloxane/polymethylsiloxane silsesquioxane cross-linked polymer;
10-50 parts by weight of one or more of phenyl trimethyl silicone oil, diphenyl dimethyl silicone oil, phenyl trimethyl siloxy diphenyl siloxane, diphenyl dimethyl silicone oil and diphenyl methyl diphenyl trisiloxane;
at least one component of polyglycerol-4 stearate, polyglycerol-4 oleate, polyglycerol-6 myristate, polyglycerol-10 isostearate and polyglycerol-10 stearate is 10 parts by weight;
further comprising 30-40 parts by weight of a mixture of glycerin, maltitol and purified water as a continuous phase in a weight ratio of 40:30: 30.
2. A method for preparing an elastomeric powder composition of silicone, characterized by: the method comprises the following steps:
a first step of stirring 40 parts by weight of a polydimethylsiloxane/vinyldimethylsiloxane crosspolymer powder having a diameter of 1 to 10 μm and a specific gravity of 1.01 or less, and 20 parts by weight of phenyl trimethicone oil for 5 minutes using a homogenizer at 2000 rpm;
a second step of dissolving 10 parts by weight of polyglycerol-4 oleate at 60 ℃ or higher in the first step and stirring at 2000rpm for 5 minutes using a homogenizer;
and step three, adding 30 parts by weight of glycerol, maltitol and purified water in the step two, wherein the ratio of the mixture to the total weight of the mixture is 4: 3: 3 weight ratio of the mixture was used as a continuous phase to produce a water-in-oil emulsion, and the mixture was stirred using a homogenizer at 3000rpm for 5 minutes.
3. A cosmetic composition of a silicone elastic powder composition characterized by: comprises the following components: an organosilicon elastomeric powder composition; butanediol; hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and 1, 2-hexanediol.
4. A cosmetic composition of silicone elastic powder composition according to claim 3, characterized in that: 10 parts by weight of an organosilicon elastic powder composition; 5 parts by weight of butanediol; 0.25 parts by weight of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and 2 parts by weight of 1, 2-hexanediol.
5. A process for the preparation of a cosmetic composition of silicone elastic powder, characterized in that: the method comprises the following steps:
a first step of stirring 82.75% of purified water and 5% of butanediol with a homogenizer at 2500 rpm;
secondly, adding 10 percent of organosilicon elastic powder composition into the result of the first step, and then stirring for 5 minutes by a homogenizer at the rotating speed of 3000 rpm;
thirdly, adding 0.25 percent of hydroxyethyl acrylate/sodium acryloyl dimethyl taurate copolymer into the result of the second step, and stirring for 5 minutes at 4000rpm by a homogenizer;
and fourthly, cooling the result obtained in the step 3 to 45-50 ℃, adding 2% of 1, 2-hexanediol, stirring for 1 minute at 2500rpm by using a homogenizer, and cooling to below 30 ℃, thus finishing the process.
6. A cosmetic composition of silicone elastic powder characterized by: prepared by the preparation process of claim 5.
CN202010204126.6A 2020-03-20 2020-03-20 Cosmetic of organosilicon elastic powder composition and preparation method thereof Pending CN111374908A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010204126.6A CN111374908A (en) 2020-03-20 2020-03-20 Cosmetic of organosilicon elastic powder composition and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202010204126.6A CN111374908A (en) 2020-03-20 2020-03-20 Cosmetic of organosilicon elastic powder composition and preparation method thereof

Publications (1)

Publication Number Publication Date
CN111374908A true CN111374908A (en) 2020-07-07

Family

ID=71215458

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202010204126.6A Pending CN111374908A (en) 2020-03-20 2020-03-20 Cosmetic of organosilicon elastic powder composition and preparation method thereof

Country Status (1)

Country Link
CN (1) CN111374908A (en)

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1902704A1 (en) * 2006-08-31 2008-03-26 Henkel KGaA Cosmetic compositions containing a combination of silicon-elastomers
EP2382961A2 (en) * 2010-04-28 2011-11-02 Henkel AG & Co. KGaA Cosmetic compound for optical concealing of wrinkles
CN103998018A (en) * 2011-12-19 2014-08-20 株式会社资生堂 Oil-in-water emulsion composition
JP2016074660A (en) * 2014-10-08 2016-05-12 堺化学工業株式会社 Oil-in-water emulsion cosmetic and production method thereof
CN109464334A (en) * 2018-12-10 2019-03-15 苏州绿叶日用品有限公司 Powder packet oil-in-water type anti-apolexis composition and its preparation method and application
CN110200853A (en) * 2019-07-12 2019-09-06 瑞希(重庆)生物科技有限公司 A kind of oil-in-water emulsion and its preparation method and application
JP2019178079A (en) * 2018-03-30 2019-10-17 株式会社マンダム Gel-like cosmetic

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1902704A1 (en) * 2006-08-31 2008-03-26 Henkel KGaA Cosmetic compositions containing a combination of silicon-elastomers
EP2382961A2 (en) * 2010-04-28 2011-11-02 Henkel AG & Co. KGaA Cosmetic compound for optical concealing of wrinkles
CN103998018A (en) * 2011-12-19 2014-08-20 株式会社资生堂 Oil-in-water emulsion composition
US20150005396A1 (en) * 2011-12-19 2015-01-01 Shiseido Company, Ltd. Oil-in-water emulsion composition
JP2016074660A (en) * 2014-10-08 2016-05-12 堺化学工業株式会社 Oil-in-water emulsion cosmetic and production method thereof
JP2019178079A (en) * 2018-03-30 2019-10-17 株式会社マンダム Gel-like cosmetic
CN109464334A (en) * 2018-12-10 2019-03-15 苏州绿叶日用品有限公司 Powder packet oil-in-water type anti-apolexis composition and its preparation method and application
CN110200853A (en) * 2019-07-12 2019-09-06 瑞希(重庆)生物科技有限公司 A kind of oil-in-water emulsion and its preparation method and application

Similar Documents

Publication Publication Date Title
DE69925669T2 (en) Latex emulsions of hydrophilic siloxanes
DE69014358T2 (en) Cosmetic preparation.
JP4647045B2 (en) Emulsion of silicone and non-aqueous hydroxyl solvent
DE69911312T2 (en) Compositions with iron oxide nanopigments for the artificial coloring of the skin and uses
CN114793419A (en) Composition comprising hyaluronic acid-based polyion composite particles
DE69816526T2 (en) Film forming polysiloxane composition and toilet products containing these compositions
EP0829253B1 (en) Method for the preparation of improved water-base toiletry composition
CN109223597B (en) Base liquid of powder for holding dressing
KR101158281B1 (en) Water Immediate Release Highly Hydrous Water-in-Oil Type Foundation Composition And Manufacturing Method Thereof
CA2301812C (en) Make-up or care composition containing an oxyalkylene group cross-linked organopolysiloxane
CN111249200B (en) Makeup powder and preparation method and application thereof
KR102260054B1 (en) Emulsified cosmetic composition comprising amphiphilic clay mineral
CN113350228B (en) Makeup pre-emulsion capable of improving darkness of foundation makeup
CN115052664A (en) Ultra-long lasting make-up foundation
CN113262178A (en) Moistened satin gloss lip glaze and preparation method thereof
WO2005053633A1 (en) Water in oil form cosmetic composition
EP0105657B1 (en) Cosmetic compositions containing glycerine
JP2018528225A (en) Skin care formulation comprising copolymer, inorganic metal oxide particles, and silicone
KR101070819B1 (en) Water-in-silicone and silicone-in-water emulsion type using the poly-ionic complex
CN115429705A (en) Skin-nourishing and beautifying sun screen and preparation process thereof
KR102086315B1 (en) Wax-free typed cosmetic composition for eye makeup
CN112641669B (en) Composition with skin moisturizing and tightening functions and application thereof
KR102003278B1 (en) Cosmetic composition containing silicon elasticity powder with temporary anti-wrinkles, and manufacturing method thereof
JP5989962B2 (en) Styling cosmetics
CN111374908A (en) Cosmetic of organosilicon elastic powder composition and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20200707

RJ01 Rejection of invention patent application after publication