CN111330319A - Device and method for reducing refined brine suspended matters - Google Patents

Device and method for reducing refined brine suspended matters Download PDF

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Publication number
CN111330319A
CN111330319A CN202010339350.6A CN202010339350A CN111330319A CN 111330319 A CN111330319 A CN 111330319A CN 202010339350 A CN202010339350 A CN 202010339350A CN 111330319 A CN111330319 A CN 111330319A
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China
Prior art keywords
refined brine
barrel
refined
reducing
brine
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Pending
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CN202010339350.6A
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Chinese (zh)
Inventor
吴剑超
钱浩
吴冬冬
朱海东
徐坤
刘绍云
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Hunan Xiangheng Salt Chemical Co ltd
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Hunan Xiangheng Salt Chemical Co ltd
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Priority to CN202010339350.6A priority Critical patent/CN111330319A/en
Publication of CN111330319A publication Critical patent/CN111330319A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D21/00Separation of suspended solid particles from liquids by sedimentation
    • B01D21/02Settling tanks with single outlets for the separated liquid

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatment Of Sludge (AREA)

Abstract

The device comprises a first refined brine barrel, the lower part of the first refined brine barrel is of a cone structure, and a feed inlet of the first refined brine barrel is arranged below the water level line of the first refined brine barrel in height. The invention also includes a method for reducing fine halogen suspended matter. The invention can greatly reduce the SS content in the refined brine and improve the quality of the refined brine, thereby ensuring the product quality and reducing the energy consumption cost of manual mud cleaning and salt making.

Description

Device and method for reducing refined brine suspended matters
Technical Field
The invention relates to the technical field of brine purification, in particular to a device and a method for reducing fine brine suspended matters.
Background
During brine purification in the salt production industry, a large amount of calcium-magnesium mud sediment is generated, and after a period of clarification, part of solid suspended substances still remain in refined brine. The solid suspended matter has important influence on the quality of salt products, particularly on the downstream chemical industry, the content of water insoluble matters in the salt products is a key index, and the quality and consumption of the downstream products are directly restricted; in the salt production process, the excessive suspended solid matters in the refined brine can cause the refined brine to scale in an evaporation device, so that the energy consumption of the product is increased. At present, when refined brine is transferred from a reaction barrel to a refined brine barrel, the refined brine barrel is influenced by relevant factors such as barrel body design, material transferring water body disturbance, sludge discharge and the like, so that the SS value (solid suspended substances) in the refined brine is relatively high and unstable, the quality of the refined brine is greatly influenced, and the quality of salt and mirabilite is influenced.
Prior art carries out artifical clearance mostly through opening the manhole door to reduce the barrel head and deposit the material and get into in the middle of the smart steamed again, however this mode clearance frequency is limited, can't accomplish real-time guarantee to the brine quality.
The existing step of separating the refined brine generally comprises two refined brine barrels, the refined brine enters a first refined brine barrel through a refined brine inlet pipe, the refined brine clear solution enters a second refined brine barrel through a communicating pipe, suspended matters in the refined brine are left in the first refined brine barrel through natural sedimentation, and after a period of continuous production, the suspended matters form sediment in the first refined brine barrel and are then pumped and discharged. However, the existing refined brine barrel has the following defects: (1) the bottom of the existing refined brine barrel is designed to be flat, and precipitates at the lower part are not easy to be discharged; the sediment can be cleaned manually every year, and part of sediment is sucked by the material transferring port and is brought to salt making; when the secondary reaction barrel transfers materials, the material transferring port can bring partial sludge at the bottom of the refined brine barrel and on the blades into the refined brine barrel; (2) the feeding pipe of the refined brine barrel is unreasonably arranged, and the refined brine enters the refined brine barrel, so that the water in the barrel is greatly disturbed; (3) the discharging pipe of the refined brine barrel is too low, and bottom sediments are possibly stirred up in the material transferring process and are brought into the next working procedure along with refined brine.
Based on the influence of the factors, the SS content in refined brine is extremely unstable, and great influence is caused on links such as product quality, labor cost, production consumption and the like.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provide the device and the method for reducing the refined brine suspended matters, which have the advantages of simple structure and low cost, can effectively reduce the SS content in the refined brine, improve the quality of the refined brine, ensure the product quality and reduce the energy consumption cost of manual mud cleaning and salt making.
The technical scheme of the invention is as follows:
the device for reducing refined brine suspended matters comprises a first refined brine barrel, wherein the lower part of the first refined brine barrel is of a cone structure, and a feed inlet of the first refined brine barrel is arranged below the water level of the first refined brine barrel in height.
Further, the height of the discharge hole of the first refined brine barrel is arranged above the water level line of the first refined brine barrel.
Furthermore, a pumping device for pumping sediment is arranged at the cone structure.
Furthermore, the first refined brine barrel is connected with the original refined brine barrel through a pipeline.
Furthermore, the part of the discharge hole of the refined brine barrel positioned at the tail end and positioned in the barrel is provided with an elbow bent upwards.
Further, the original refined brine barrel comprises a second refined brine barrel and a third refined brine barrel, and the first refined brine barrel is communicated with the second refined brine barrel through a communicating pipe; the second refined brine barrel is communicated with the third refined brine barrel through a communicating pipe.
Further, the height of the feeding hole of the second refined brine barrel is higher than that of the discharging hole of the second refined brine barrel.
Further, a feed inlet of the first refined brine barrel is connected with the reaction barrel; the lower part of the first refined brine barrel is provided with a slag discharge pipeline which is connected with the other reaction barrel through the pumping device.
Furthermore, the second refined brine barrel and the third refined brine barrel adopt original barrels, and the first refined brine barrel is additionally arranged on the original barrels.
The invention relates to a method for reducing refined brine suspended matters, which comprises the following steps:
s1: a refined brine barrel with a cone structure is additionally arranged on the basis of the original refined brine barrel, and the feeding and discharging modes of the refined brine barrel with the cone structure are that the material inlet and the material outlet are arranged in a low-inlet and high-outlet mode;
s2: refined brine enters the refined brine barrel with the cone structure, refined brine clear liquid enters the next original refined brine barrel, suspended matters in the refined brine are left in the refined brine barrel with the cone structure through natural sedimentation, and after the refined brine barrel is continuously produced for a period of time, the suspended matters form sediment in the refined brine barrel with the cone structure and are pumped and discharged.
Further, the number of the original refined brine barrels is 1-2.
The invention has the beneficial effects that:
(1) compared with the flat bottom design of the original refined brine barrel, the cone design of the invention is more beneficial to mud sedimentation and pumping drainage;
(2) compared with the prior manual sludge cleaning, the invention adopts the pumping device to pump and discharge more efficiently and more economically;
(3) compared with the original design of the communicating pipe with high inlet and high outlet of the refined brine barrel, the design of the communicating pipe with low inlet and high outlet is more beneficial to reducing the disturbance of the material transferring process to the water body;
(4) compared with the original design that the discharge port of the tail end refined brine barrel is in a direct insertion type and is positioned at the bottom of the barrel, the lifting device can effectively reduce the carrying of bottom sediment in the material transferring process after the discharge port of the tail end refined brine barrel is lifted.
Drawings
Fig. 1 is a schematic structural diagram of an embodiment of the present invention.
Detailed Description
The invention will be described in further detail below with reference to the drawings and specific examples.
As shown in fig. 1: a device for reducing refined brine suspended matters comprises a first refined brine barrel, wherein the lower part of the first refined brine barrel is of a cone structure, and a pumping device for pumping and draining sediments is arranged at the cone structure; the height of the feeding hole of the first refined brine barrel is lower than that of the discharging hole of the first refined brine barrel.
The scheme has the following advantages: the lower part of the first refined brine barrel is of a cone structure, so that mud is precipitated and pumped and discharged; the pumping device is arranged, so that sediments collected by the cone part can be periodically pumped; the feeding hole of the first refined brine barrel is designed to be lower than the discharging hole of the first refined brine barrel, so that the feeding and discharging modes of the refined brine barrel are low in feeding and high out, the water disturbance during feeding can be reduced, and sediments at the bottom of the barrel are prevented from being carried away during discharging.
Specifically, the height of the feed inlet of the first refined brine barrel is arranged below the water level line of the first refined brine barrel. The water level line is the lowest water level line in the refined brine barrel, so that the disturbance to the water body in the material transferring process can be reduced.
The discharge port height of the first refined brine barrel is arranged above the water level line of the first refined brine barrel. The water level line is the lowest water level line in the refined brine barrel. Higher than the water level line, can avoid the discharge gate to take away barrel bottom deposit suction when the refined brine ejection of compact.
In this embodiment, the first refined brine barrel is newly added on the basis of the original refined brine barrel, rather than completely changing the original structure, that is, two refined brine barrels are usually adopted to separate refined brine in the prior art, that is, the second refined brine barrel and the third refined brine barrel; the second refined brine barrel is communicated with the third refined brine barrel through a communicating pipe. The feed inlet of the first refined brine barrel is connected with the reaction barrel; the lower part of the first refined brine barrel is provided with a slag discharge pipeline which is connected with the other reaction barrel through the pumping device. Because the first refined brine barrel is in a lower-in and higher-out mode, the height of the feeding hole of the second refined brine barrel is higher than that of the discharging hole of the second refined brine barrel, namely the position of a communicating pipe between the second refined brine barrel and the first refined brine barrel is not improved.
In this embodiment, the discharge port of the refined brine barrel at the end is provided with an upward-curved elbow at the part located in the barrel, that is, the third refined brine barrel of this embodiment is located at the end, and therefore an upward-curved elbow is provided at the part of the discharge port located in the barrel. The discharge gate of current terminal smart steamed bucket is the formula of cuting straightly usually, in the pipeline direct access bucket, is the vertical state with the ladle body promptly, now need lifting the height of ejection of compact pipeline in the bucket to the realization changes the disturbance of material process to the barrel head sediment material. Therefore, on the basis of not changing the position of the original discharge hole, the part of the original discharge pipe in the barrel is welded with a 90-degree elbow, and pipelines with different lengths can be welded on the basis of the elbow according to actual needs. Therefore, the lifting can be realized on the basis of not changing the position of the original discharge hole, so that the disturbance of the material transferring process on the sediment at the bottom of the barrel is realized.
A method for reducing fine halogen suspension comprising the steps of:
s101: the refined brine barrel with the cone structure is additionally arranged on the basis of the original refined brine barrel, and the feeding and discharging modes of the refined brine barrel with the cone structure are low in feeding and high out feeding.
Specifically, newly increase first smart steamed bucket on the basis of second smart steamed bucket and third smart steamed bucket, design for the cone structure, the feed inlet and the reaction barrel pipe connection of first smart steamed bucket, the row's of first smart steamed bucket cinder notch is through arranging the sediment pipeline and connecting another reaction barrel through pump drainage device. The three refined brine barrels are sequentially communicated through a communicating pipe, and a discharge port of the first refined brine barrel is connected with salt making equipment. The pumping device of this embodiment is a sludge pump, and is used for discharging the precipitate to the reaction barrel. Preferably, the first refined brine bucket of this embodiment upper portion is the cylinder, and the lower part is the centrum, and the feed inlet is located on the inclined plane of centrum to reduce the disturbance to the water among the material transfer process.
S102: refined brine enters the first refined brine barrel, refined brine clear liquid enters the next original refined brine barrel, suspended matters in the refined brine are left in the refined brine barrel with the cone structure through natural sedimentation, and after the refined brine barrel is continuously produced for a period of time, the suspended matters form sediment in the refined brine barrel with the cone structure and are pumped and discharged.
Specifically, refined brine in the reaction barrel enters the first refined brine barrel through the feed inlet, refined brine clear liquid is generated in the first refined brine barrel, and the liquid level of the refined brine clear liquid is above the feed inlet. The smart steamed clear liquid of production is gone into in the smart steamed bucket of second through discharge gate and communicating pipe by the pump, the smart steamed bucket of second filters the sediment once more, because the discharge gate height of first smart steamed bucket is higher, can not inhale the smart steamed bucket of second with the precipitate, consequently, the smart steamed clear liquid that gets into the smart steamed bucket of second deposits the back once more in the smart steamed bucket of second, its precipitate is few almost, the scale deposit is few, very easily get rid of, consequently, the smart steamed bucket of second still adopts flat structure in the past, and the feed inlet and the discharge gate position of the smart steamed bucket of second also need not to improve, greatly reduced cost. And (3) the refined brine clear liquid after being filtered and clarified in the second refined brine barrel enters a third refined brine barrel to finally obtain clean refined brine clear liquid, and then the obtained refined brine clear liquid is conveyed to salt making equipment to enter a salt making process. In addition, the sediment collected by the cone at the lower part of the first refined brine barrel is automatically pumped and drained by the pumping and draining device every two days.
It is understood that the present invention may also be used with only two fine-marinating drums, for example, with the second drum eliminated, and still obtain a higher quality clear fine-marinated liquor.
In conclusion, the invention greatly reduces the SS content in the refined brine and improves the quality of the refined brine by the cone design of the refined brine barrel, the improvement of the feed inlet and the discharge outlet and the combination of the pumping device for discharging the mud, thereby ensuring the product quality and reducing the energy consumption cost of manual mud cleaning and salt making.

Claims (10)

1. A device for reducing refined brine suspended matters comprises a first refined brine barrel, wherein a feed inlet and a discharge outlet are formed in the first refined brine barrel; the device is characterized in that the lower part of the first refined brine barrel is of a cone structure, and the feed inlet of the first refined brine barrel is arranged below the water level line of the first refined brine barrel in height.
2. An apparatus for reducing suspended matter in refined brine according to claim 1, wherein the outlet of the first refined brine tank is positioned at a height above the water level of the first refined brine tank.
3. An apparatus for reducing fine halogen suspension according to claim 2, characterized in that the cone structure is provided with pumping means for pumping sediment.
4. An apparatus for reducing concentrate suspension according to claim 1, 2 or 3, characterized in that the first concentrate tank is piped to the original concentrate tank.
5. An apparatus for reducing suspended matter of refined brine according to claim 4, wherein the outlet of the refined brine tank at the end is provided with an elbow bent upward at a portion located inside the tank.
6. The apparatus for reducing suspended matters of refined brine according to claim 4, wherein the original refined brine bucket comprises a second refined brine bucket and a third refined brine bucket, and the first refined brine bucket is communicated with the second refined brine bucket through a communicating pipe; the second refined brine barrel is communicated with the third refined brine barrel through a communicating pipe.
7. An apparatus for reducing refined brine suspension as claimed in claim 4, wherein the height of the inlet of the second refined brine tank is higher than the height of the outlet of the second refined brine tank.
8. An apparatus for reducing fine halogen suspension according to claim 1, 2 or 3, wherein the feed inlet of the first fine halogen barrel is connected to the reaction barrel; the lower part of the first refined brine barrel is provided with a slag discharge pipeline which is connected with the other reaction barrel through the pumping device.
9. A method for reducing fine halogen suspension, comprising the steps of:
s1: a refined brine barrel with a cone structure is additionally arranged on the basis of the original refined brine barrel, and the feeding and discharging modes of the refined brine barrel with the cone structure are that the material inlet and the material outlet are arranged in a low-inlet and high-outlet mode;
s2: refined brine enters the refined brine barrel with the cone structure, refined brine clear liquid enters the next original refined brine barrel, suspended matters in the refined brine are left in the refined brine barrel with the cone structure through natural sedimentation, and after the refined brine barrel is continuously produced for a period of time, the suspended matters form sediment in the refined brine barrel with the cone structure and are pumped and discharged.
10. The method for reducing refined brine suspension as claimed in claim 9, wherein the number of original refined brine barrels is 1-2.
CN202010339350.6A 2020-04-26 2020-04-26 Device and method for reducing refined brine suspended matters Pending CN111330319A (en)

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Application Number Priority Date Filing Date Title
CN202010339350.6A CN111330319A (en) 2020-04-26 2020-04-26 Device and method for reducing refined brine suspended matters

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Application Number Priority Date Filing Date Title
CN202010339350.6A CN111330319A (en) 2020-04-26 2020-04-26 Device and method for reducing refined brine suspended matters

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CN206881214U (en) * 2017-04-06 2018-01-16 青海锦泰锂业有限公司 A kind of low-grade salt lake lithium carbonate extraction settling tank
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CN209596617U (en) * 2019-01-11 2019-11-08 武汉市武钢丹斯克科技磁材有限公司 A kind of sedimentation basin for material recycle
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CN212039146U (en) * 2020-04-26 2020-12-01 湖南省湘衡盐化有限责任公司 Device for reducing refined bittern suspended matter

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5362407A (en) * 1993-04-15 1994-11-08 Modern Welding Company, Inc. Circular gravity clarifier and method
RU13326U1 (en) * 1999-12-14 2000-04-10 Общество С Ограниченной Ответственностью "Лукойл-Пермнефть" DEVICE FOR CLEANING LIQUID FROM MECHANICAL IMPURITIES
JP2001334107A (en) * 2000-05-25 2001-12-04 Vision:Kk Apparatus for separating slurry
JP2004154690A (en) * 2002-11-06 2004-06-03 Masanori Enai Precipitation and floatation separation structure for suspension, suspension separation system, and precipitate collection block for suspension separation system
JP2005007311A (en) * 2003-06-19 2005-01-13 Kazuya Sasaki Multitank continuous purifying facility for dirty and turbid water
US20060086676A1 (en) * 2004-10-22 2006-04-27 Bos Rentals Ltd. Settling tank and method for separating a solids containing material
JP2007000792A (en) * 2005-06-24 2007-01-11 Nippon Steel Corp Treating method of suspended matter in steel manufacturing degassing drain
US20080121589A1 (en) * 2006-11-27 2008-05-29 Scott Blair Godlien Fluid clarification system, method, and apparatus
JP2011025188A (en) * 2009-07-28 2011-02-10 Homei Kyo Water treatment apparatus
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CN212039146U (en) * 2020-04-26 2020-12-01 湖南省湘衡盐化有限责任公司 Device for reducing refined bittern suspended matter

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