CN111302665A - Regulating and controlling vacuum toughened glass plate with rolling support double-glue sealed glass spacing cavity - Google Patents

Regulating and controlling vacuum toughened glass plate with rolling support double-glue sealed glass spacing cavity Download PDF

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CN111302665A
CN111302665A CN201911255886.3A CN201911255886A CN111302665A CN 111302665 A CN111302665 A CN 111302665A CN 201911255886 A CN201911255886 A CN 201911255886A CN 111302665 A CN111302665 A CN 111302665A
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toughened glass
vacuum
glass plate
glass
sealing
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徐宝安
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C27/00Joining pieces of glass to pieces of other inorganic material; Joining glass to glass other than by fusing
    • C03C27/06Joining glass to glass by processes other than fusing
    • C03C27/08Joining glass to glass by processes other than fusing with the aid of intervening metal
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C27/00Joining pieces of glass to pieces of other inorganic material; Joining glass to glass other than by fusing
    • C03C27/06Joining glass to glass by processes other than fusing
    • C03C27/10Joining glass to glass by processes other than fusing with the aid of adhesive specially adapted for that purpose
    • EFIXED CONSTRUCTIONS
    • E06DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06BFIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B3/00Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
    • E06B3/66Units comprising two or more parallel glass or like panes permanently secured together
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A30/00Adapting or protecting infrastructure or their operation
    • Y02A30/24Structural elements or technologies for improving thermal insulation
    • Y02A30/249Glazing, e.g. vacuum glazing
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02BCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
    • Y02B80/00Architectural or constructional elements improving the thermal performance of buildings
    • Y02B80/22Glazing, e.g. vaccum glazing

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Joining Of Glass To Other Materials (AREA)

Abstract

According to the invention, the outer protective frame is utilized, high-humidity air is introduced into the vacuum furnace through double-glue sealing, and then air is exhausted from the hollow interlayer, so that double-glue sealing glass can be rapidly cured, and the rapid sealing and curing of the edge of the vacuum glass are realized. And a communicated sealing pipe fitting communicated with the two sides is arranged on the vacuum toughened glass plate. The invention realizes good glass metal bonding quality, solves the problem of tempering loss of the vacuum glass and solves the safety problem of the vacuum glass. The functional vacuum glass has simple manufacturing process, is widely applied to common toughened glass in material, greatly reduces the manufacturing cost, greatly improves the safety and the yield, and can be diversified in structural form. The toughened glass plate has the characteristics of thinness, light weight, high strength, safety, long service life, large size, high yield, strong functionality, low energy consumption, high efficiency, light transmission, safety, low manufacturing cost, condensation prevention, convenience for large-scale production and the like.

Description

Regulating and controlling vacuum toughened glass plate with rolling support double-glue sealed glass spacing cavity
Technical Field
The invention relates to a functional vacuum toughened glass plate which is manufactured by bonding and sealing glass and metal by using a vacuum bonding technology. Belongs to the field of glass building materials.
Background
At present, the mainstream of the functional glass is hollow glass and vacuum glass.
The heat insulation performance of the hollow glass is not ideal, and the two layers of glass are not mutually supported and cannot be mutually assisted, so that the wind pressure resistance of the glass is weak, and the glass is easy to break due to the resonance of the glass. Furthermore, there is a problem that the glass forms dew after the adhesive leaks.
The vacuum glass is made up by using two layers of glass plates and making them be sandwiched between them and supporting them, and using sealing adhesive to make adhesion, vacuumizing and sealing them. The vacuum glass is transparent vacuum glass with the best energy-saving effect at present, has a series of advantages of light weight, thin thickness, small heat transfer coefficient, good sound insulation effect and the like, and is an ideal energy-saving building material. But because of its expensive production cost and the inability to meet the safety requirements for toughened glass required by high-rise buildings, it has not been used on a large scale. Because the vacuum glass peripheral sealing adhesive is bonded by low-temperature glass sealing, the manufacturing process, the cost, the yield, the mechanical property and the size specification of the vacuum glass are greatly limited, and the tempering treatment of the glass plate is difficult to realize, so that the strength and the safety performance of the glass are influenced. Once the glass melt-edge sealing damages the vacuum leakage due to stress and the like, the whole vacuum glass loses good sound insulation and heat insulation performance.
The above disadvantages of the existing vacuum glass are caused by its design structure and production process. The existing vacuum glass, namely two original glass sheets are separated by a tiny support dot matrix, the periphery of the existing vacuum glass is sealed by fusing low-melting-point glass frit, and the vacuum glass is sealed after being exhausted through a glass exhaust tube, so that a vacuum layer with the air pressure lower than 0.1Pa and the thickness of only 0.1-0.2mm is formed. Therefore, the production of vacuum glass must be completed through a plurality of processes including: 1) drilling an air suction opening, 2) laying a support, 3) coating glass brazing material, 4) combining glass sheets, 5) performing high-temperature edge sealing/air suction opening brazing, 6) performing high-temperature air suction/sealing, and 7) unsealing a getter.
The applicant (Liu Weijie) applies for the application number CN200910188347.2 of low-cost toughened vacuum glass and a manufacturing method thereof
The application provides vacuum glass and a manufacturing method thereof, wherein the existing stainless steel support laying process is replaced by micro-convex point supports integrated with original glass sheets, the edge sealing is carried out by using a low-temperature metal tin brazing technology which cannot cause annealing of the original tempered glass sheets, and the traditional vacuum layer air extraction process and the edge sealing process are simply integrated into an air extraction and edge sealing integrated process.
Compared with the existing vacuum glass and the manufacturing process thereof, the application completes vacuumizing and brazing sealing at one time, and the safety reaches the use standard of high-rise buildings. However, because of the need of coating sintered molten gold, the low tin soldering temperature, the low heating temperature of the vacuum soldering furnace, the insufficient air release of glass and tin soldering material, the poor vacuum pumping effect, the low vacuum degree of the glass vacuum interlayer and the like, the heat preservation and sound insulation performance of the vacuum glass is unsatisfactory.
The technical proposal of the application No. CN200910234678.5 of glass and metal vacuum brazing process filed by the applicant (Nanjing university of industry), the surface of the glass needs to be treated by chemical electro-coppering metal surface on the basis of the original process. And after starting the heating system, heating the workpiece along with the furnace to 550 ℃, keeping the temperature until the vacuum degree in the furnace is 4 multiplied by 10 < -2 > Pa, so that the temperature of each part of the workpiece is uniform, continuously heating the brazing furnace to the brazing temperature, keeping the temperature for 10-30 min, stopping heating, slowly cooling along with the furnace, and keeping the tapping temperature of the vacuum glass below 50 ℃.
The high-temperature edge sealing process is the main reason that the conventional vacuum glass cannot reach the national safety standard of high-rise buildings. National standards require high-rise building glass components to be made from tempered glass. However, because the melting temperature of the existing high-temperature edge sealing glass brazing material exceeds 550 ℃ and is greatly higher than the annealing temperature of the conventional tempered glass of 388 ℃, the existing high-temperature edge sealing glass brazing material can be annealed into common glass in the edge sealing process even if the tempered glass is used for manufacturing vacuum glass.
The other vacuum regulating glass is formed through setting support in the middle interlayer between two glass plates, adhering the periphery with sealing adhesive, and intermittent or continuous vacuum pumping with vacuum pump to regulate and maintain the vacuum in the glass interlayer. The invention is a patent number of a sandwich flat glass curtain wall for regulating and controlling the vacuum degree of a cavity, which is previously applied by an applicant: 2010103000382.
although the prior application patent designs intermittent or continuous vacuum pumping through a vacuum pump, the vacuum heat preservation of the glass interlayer is realized. However, in practice, it has been found that it is difficult to achieve a high vacuum due to the unreasonable design and poor reliability of the apparatus. Meanwhile, when the adhesive is a sealant with a single-layer silicone structure, although the adhesive strength can be ensured, the airtightness is poor; when the single-layer airtight sealing agent is used for bonding, although the airtightness can be kept, the mechanical strength of the single-layer airtight sealing agent cannot be guaranteed; this makes it difficult to achieve a balance between the structural strength of the glass bond and the air-tight and weather-resistant properties. In both of these bonding methods, a large amount of air bubbles are present in the adhesive layer. And the vacuum glass is broken due to the fact that the glass corners are collided in the transportation and installation processes because the periphery of the vacuum glass is not provided with the protective frame.
Due to the problems, the vacuum interlayer which can be pumped by the vacuum pump is rough vacuum, and the problem of serious vacuum leakage exists. When the thickness of the vacuum interlayer is smaller, the heat insulation performance of the vacuum glass is poorer. Therefore, it is required to improve the thermal insulation effect of the vacuum layer by increasing the thickness of the hollow interlayer. But doing so makes the vacuum pump extremely energy intensive.
Disclosure of Invention
Under the background of the conventional process technology, the invention improves the quality of the welding surface between glass and metal by researching the basic theory and producing inspiration from practice and utilizing the vacuum electric heating brazing process and ensures that the performance of the toughened glass in the stainless steel protective frame is not changed.
In order to solve the problems, a brand new design scheme is adopted for the technology, the two pieces of glass are provided with a protective frame, an isolation support and a closed-loop sealing support frame, and are sealed by a temperature-resistant airtight sealant and a structural sealant; the vacuum regulation and control heat-preservation glass plate with the glass separation cavity is manufactured by arranging an airtight air inlet and outlet pipe fitting, a vacuum meter, a vacuum valve and a vacuum pump, and the heat preservation of the functional vacuum glass plate is realized by regulating and controlling the vacuum degree of the glass separation interlayer.
The vacuum glass manufactured by the process method has the characteristics of simple operation, high glass strength, safety, large size, low manufacturing cost, high yield, good thermal insulation performance, strong functionality, low energy consumption, good perspective effect, convenience for large-scale production and the like, and overcomes various problems of the existing functional vacuum glass. The method can obtain good metal glass brazing quality, solves the technical problem that the vacuum glass cannot be tempered and troubles people for a long time, and therefore, the invention obtains good economic benefit, environmental benefit and social benefit.
The technical scheme of the invention is realized as follows:
the rolling support double-glue sealed glass interval cavity is arranged for regulating and controlling the vacuum toughened glass plate, and comprises a toughened glass plate and a bonding sealant.
(A) Two toughened glass plates forming the interval interlayer cavity are mutually corresponding in outline shape and size, and one of the at least two toughened glass plates is provided with an embossed toughened glass plate which is integrated with the toughened glass plate and uniformly distributed with lattice raised support points and raised frame support bands; the height of the raised frame supporting belt is equal to that of the dot matrix raised supporting points; or a raised frame supporting belt which is processed and formed, has the complementary corresponding outline shape and size with the edges of the two toughened glass plates and has the height equal to the height of the relative supporting and superposing total height of the raised supporting points of the dot matrix is arranged between the edges of the two toughened glass plates; one of the two toughened glass plates is provided with a communicated sealing pipe fitting which is communicated with the two sides and is bonded and sealed by an airtight sealing glue and a structural sealing glue; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is bonded, sealed, screwed and locked by a connecting fastener and the airtight sealing glue; or a communicated sealing pipe fitting which is communicated with the two sides and is sealed by soldering through a low-melting-point metal soldering flux is arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is brazed, sealed and locked by a connecting fastener and a low-melting-point metal brazing flux;
the method comprises the following steps that two embossed toughened glass plates with mutually corresponding outline shapes and sizes and provided with lattice raised supporting points and raised frame supporting belts are subjected to complementary buckling, bonding and sealing after airtight sealant is coated on the raised frame supporting belts, or transparent glue is coated on the lattice raised supporting points and the airtight sealant is coated on the raised frame supporting belts;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a sealing rubber ring which is bonded with the bottom of the supporting band groove of the raised frame and the closed structures of the glass groove walls at two sides;
(B) or two toughened glass plates forming the interval interlayer cavity are mutually corresponding in outline shape and size, and one of the at least two toughened glass plates is provided with an embossed toughened glass plate of a dot matrix concave supporting point and a concave frame supporting belt which are formed by pressing and stretching by a mould; a concave frame supporting belt with the same height as the concave supporting points of the dot matrix is arranged between the edges of the two toughened glass plates; or the edges of the two toughened glass plates are provided with concave frame supporting bands, and the heights of the concave frame supporting bands are equal to the heights of the concave supporting points of the dot matrix; or the height of the concave frame supporting strip is as high as the total height of the opposite support superposition height of the concave supporting points of the dot matrix arranged at the edges of the two toughened glass plates;
one of the two toughened glass plates is provided with a communicated sealing pipe fitting which is communicated with the two sides and is bonded and sealed by an airtight sealing glue and a structural sealing glue; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is bonded, sealed, screwed and locked by a connecting fastener and the airtight sealing glue; or a communicated sealing pipe fitting which is communicated with the two sides and is sealed by soldering through a low-melting-point metal soldering flux is arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is brazed, sealed and locked by a connecting fastener and a low-melting-point metal brazing flux;
the method comprises the following steps of enabling two embossed toughened glass plates with mutually corresponding outline shapes and sizes and provided with lattice concave supporting points and concave frame supporting belts to be mutually matched, buckling, bonding and sealing the concave frame supporting belts of the two toughened glass plates after airtight sealant is coated on the concave frame supporting belts, or transparent adhesive is coated on the lattice concave supporting points and the airtight sealant is coated on the concave frame supporting belts;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a sealing rubber ring which is bonded with the bottom of a supporting band groove of the lower concave frame and a closed structure of the glass groove walls at two sides, so that a toughened glass plate blank is manufactured;
then, at least one tempered glass plate blank is sent into a vacuum furnace, and heating and vacuumizing are carried out; and then introducing humid air into the vacuum furnace, cooling, and opening the furnace to obtain the rolled support double-glue sealed glass interval cavity regulating and controlling vacuum toughened glass plate.
A method for manufacturing a vacuum tempered glass plate with a rolling support double-glue sealed glass interval cavity for regulating and controlling comprises a tempered glass plate, a bonding sealant and a vacuum furnace. Two communicated sealing pipe fittings which are provided with two communicated sides and are bonded and sealed by airtight sealing glue and structural sealant are arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is bonded, sealed, screwed and locked by a connecting fastener and the airtight sealing glue; or a communicated sealing pipe fitting which is communicated with the two sides and is sealed by soldering through a low-melting-point metal soldering flux is arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is brazed, sealed and locked by a connecting fastener and a low-melting-point metal brazing flux; the embossed toughened glass plates are provided with lattice support points and frame support belts, and after airtight sealant is coated on the frame support belts, or transparent adhesive is coated on the lattice support points and the airtight sealant is coated on the frame support belts, the frame support belts of the two toughened glass plates are complementarily buckled, bonded and sealed;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a groove bottom of a supporting band of the bonding frame and a sealing rubber ring of a closed structure of the glass groove walls at two sides, so that a toughened glass plate blank is manufactured;
then horizontally placing at least one hollow interlayer toughened glass plate blank into a vacuum furnace provided with a supporting base, a fixed supporting clamp or a tray; an ultrasonic transducer for improving the bonding quality of glass and glass, glass and metal is arranged on a glass tray of the vacuum furnace; closing the door of the vacuum furnace, and vacuumizing the blank of the hollow interlayer toughened glass plate in the vacuum furnace; the gas in the airtight sealant and the structural sealant is completely discharged;
when the vacuum degree is reached and the vacuum pumping time is set, introducing high-humidity air into the vacuum furnace, and instantly closing an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting; the air generates pressure, the stainless steel frame quickly compacts the softened airtight sealing glue and the structural sealing glue layer under the action of air pressure, and the airtight sealing glue and the structural sealing glue layer are bonded and solidified;
by the process, the bonding quality of the glass and the stainless steel through the airtight sealing glue and the structural sealing glue is improved; opening a vacuum furnace door to manufacture a heat-preservation toughened glass plate body provided with a hollow air inlet and outlet communicated sealing pipe fitting, wherein the periphery of the toughened glass plate body is provided with two annular sealing and bonding sealing belts, and the glass hollow interlayer is a heat-preservation lighting toughened glass plate with adjustable and controllable vacuum degree;
or horizontally placing at least one hollow interlayer toughened glass plate blank into a vacuum furnace provided with a supporting base, a fixed supporting clamp or a tray; closing the door of the vacuum furnace, and heating and vacuumizing the blank of the hollow interlayer toughened glass plate in the vacuum furnace; the gas in the hot-melt airtight sealant and the structural sealant is completely discharged;
when the heating temperature, the vacuum degree and the set vacuumizing time are reached, high-humidity air is introduced into the vacuum furnace, and an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting is closed instantly; the air absorbs heat, rises temperature and expands to generate pressure, the stainless steel frame quickly compacts the hot-melt airtight sealing adhesive and the structural sealing adhesive layer in a softened state under the action of air pressure, releases heat and solidifies, and then, or starts a cooling device arranged in the vacuum furnace to cool the vacuum furnace;
or introducing high-humidity air into the vacuum furnace, and instantly closing an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting; the air absorbs heat, the temperature rises and expands to generate pressure, the stainless steel frame rapidly compacts the hot-melt airtight sealing adhesive and the structural sealing adhesive layer in a softened state under the action of air pressure, the hot-melt airtight sealing adhesive and the structural sealing adhesive layer are made to release heat and solidify, then the vacuum furnace is cooled by releasing hot air and filling cold air, or a cooling device arranged in the vacuum furnace is started to cool the vacuum furnace, and the structural sealing adhesive in the stainless steel frame can be naturally cooled and solidified;
by the process, the bonding quality of the glass and the stainless steel through the hot-melt airtight sealing glue and the structural sealing glue is improved; when the temperature of the vacuum furnace is reduced to 50-55 ℃, the door of the vacuum furnace is opened to prepare the heat-insulating and lighting toughened glass plate with two annular sealing and bonding sealing belts and a stainless steel closed-loop protection frame on the periphery of the toughened glass plate body, wherein the vacuum degree of the glass hollow interlayer is adjustable.
The rolling support double-glue sealed glass interval cavity is arranged for regulating and controlling the vacuum toughened glass plate, and comprises a toughened glass plate and a bonding sealant.
(A) Two toughened glass plates forming the interval interlayer cavity are mutually corresponding in outline shape and size, and one of the at least two toughened glass plates is provided with an embossed toughened glass plate which is integrated with the toughened glass plate and uniformly distributed with lattice raised support points and raised frame support bands; the height of the raised frame supporting belt is equal to that of the dot matrix raised supporting points; or a raised frame supporting belt which is processed and formed, has the complementary corresponding outline shape and size with the edges of the two toughened glass plates and has the height equal to the height of the relative supporting and superposing total height of the raised supporting points of the dot matrix is arranged between the edges of the two toughened glass plates; one of the two toughened glass plates is provided with a communicated sealing pipe fitting which is communicated with the two sides and is bonded and sealed by an airtight sealing glue and a structural sealing glue; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is bonded, sealed, screwed and locked by a connecting fastener and the airtight sealing glue; or a communicated sealing pipe fitting which is communicated with the two sides and is sealed by soldering through a low-melting-point metal soldering flux is arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is brazed, sealed and locked by a connecting fastener and a low-melting-point metal brazing flux;
the method comprises the following steps that two embossed toughened glass plates with mutually corresponding outline shapes and sizes and provided with lattice raised supporting points and raised frame supporting belts are subjected to complementary buckling, bonding and sealing after airtight sealant is coated on the raised frame supporting belts, or transparent glue is coated on the lattice raised supporting points and the airtight sealant is coated on the raised frame supporting belts;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a sealing rubber ring which is bonded with the bottom of the supporting band groove of the raised frame and the closed structures of the glass groove walls at two sides; or a layer of metal thin belt with good plasticity is adhered to the periphery of the toughened glass plate which is adhered and sealed by the two toughened glass plate lamination sheets through airtight sealant to be used as an airtight sealing ring of the isolation sealing layer;
the outer side of the periphery of the hollow interlayer toughened glass plate body is wrapped with a closed-loop corrugated stainless steel frame with a U-shaped section, and structural sealant which does not generate chemical reaction with the airtight sealant is filled in a groove of the corrugated stainless steel frame; the U-shaped closed-loop corrugated stainless steel frame with the cross section is tightly attached and bonded with the outer side of the periphery of the hollow interlayer toughened glass plate body by utilizing the elasticity of the U-shaped closed-loop corrugated stainless steel frame and utilizing the self resilience of the closed-loop corrugated stainless steel frame;
or the outer side of the periphery of the hollow interlayer toughened glass plate body is wrapped with a protective frame of a hollow interlayer toughened glass plate structure, the upper section of the protective frame is L-shaped and reverse L-shaped, and the closed loop stainless steel frame coated with the structural sealant is buckled and sleeved to form the protective frame of the hollow interlayer toughened glass plate structure, so that a toughened glass plate blank is manufactured;
(B) or two toughened glass plates forming the interval interlayer cavity are mutually corresponding in outline shape and size, and one of the at least two toughened glass plates is provided with an embossed toughened glass plate of a dot matrix concave supporting point and a concave frame supporting belt which are formed by pressing and stretching by a mould; a concave frame supporting belt with the same height as the concave supporting points of the dot matrix is arranged between the edges of the two toughened glass plates; or the edges of the two toughened glass plates are provided with concave frame supporting bands, and the heights of the concave frame supporting bands are equal to the heights of the concave supporting points of the dot matrix; or the height of the concave frame supporting strip is as high as the total height of the opposite support superposition height of the concave supporting points of the dot matrix arranged at the edges of the two toughened glass plates;
one of the two toughened glass plates is provided with a communicated sealing pipe fitting which is communicated with the two sides and is bonded and sealed by an airtight sealing glue and a structural sealing glue; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is bonded, sealed, screwed and locked by a connecting fastener and the airtight sealing glue; or a communicated sealing pipe fitting which is communicated with the two sides and is sealed by soldering through a low-melting-point metal soldering flux is arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is brazed, sealed and locked by a connecting fastener and a low-melting-point metal brazing flux;
the method comprises the following steps of enabling two embossed toughened glass plates with mutually corresponding outline shapes and sizes and provided with lattice concave supporting points and concave frame supporting belts to be mutually matched, buckling, bonding and sealing the concave frame supporting belts of the two toughened glass plates after airtight sealant is coated on the concave frame supporting belts, or transparent adhesive is coated on the lattice concave supporting points and the airtight sealant is coated on the concave frame supporting belts;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a sealing rubber ring which is bonded with the bottom of a supporting band groove of the lower concave frame and a closed structure of the two side glass groove walls;
or a layer of metal thin belt with good plasticity is adhered to the periphery of the toughened glass plate which is adhered and sealed by the two toughened glass plate lamination sheets through airtight sealant to be used as an airtight sealing ring of the isolation sealing layer;
the outer side of the periphery of the hollow interlayer toughened glass plate body is wrapped with a closed-loop corrugated stainless steel frame with a U-shaped section, and structural sealant which does not generate chemical reaction with the airtight sealant is filled in a groove of the corrugated stainless steel frame; the U-shaped closed-loop corrugated stainless steel frame with the cross section is tightly attached and bonded with the outer side of the periphery of the hollow interlayer toughened glass plate body by utilizing the elasticity of the U-shaped closed-loop corrugated stainless steel frame and utilizing the self resilience of the closed-loop corrugated stainless steel frame;
or the outer side of the periphery of the hollow interlayer toughened glass plate body is wrapped with a protective frame of a hollow interlayer toughened glass plate structure, the upper section of the protective frame is L-shaped and reverse L-shaped, and the closed loop stainless steel frame coated with the structural sealant is buckled and sleeved to form the protective frame of the hollow interlayer toughened glass plate structure, so that a toughened glass plate blank is manufactured;
then, at least one tempered glass plate blank is sent into a vacuum furnace, and heating and vacuumizing are carried out; and then introducing humid air into the vacuum furnace, cooling, and opening the furnace to obtain the rolled support double-glue sealed glass interval cavity regulating and controlling vacuum toughened glass plate.
A method for manufacturing a vacuum tempered glass plate with a rolling support double-glue sealed glass interval cavity for regulating and controlling comprises a tempered glass plate, a bonding sealant and a vacuum furnace. Two communicated sealing pipe fittings which are provided with two communicated sides and are bonded and sealed by airtight sealing glue and structural sealant are arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is bonded, sealed, screwed and locked by a connecting fastener and the airtight sealing glue; or a communicated sealing pipe fitting which is communicated with the two sides and is sealed by soldering through a low-melting-point metal soldering flux is arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is brazed, sealed and locked by a connecting fastener and a low-melting-point metal brazing flux; the embossed toughened glass plates are provided with lattice support points and frame support belts, and after airtight sealant is coated on the frame support belts, or transparent adhesive is coated on the lattice support points and the airtight sealant is coated on the frame support belts, the frame support belts of the two toughened glass plates are complementarily buckled, bonded and sealed;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a groove bottom of a supporting band of the bonding frame and a sealing rubber ring of a closed structure of the glass groove walls at two sides, so that a toughened glass plate blank is manufactured;
then horizontally placing at least one hollow interlayer toughened glass plate blank into a vacuum furnace provided with a supporting base, a fixed supporting clamp or a tray; an ultrasonic transducer for improving the bonding quality of glass and glass, glass and metal is arranged on a glass tray of the vacuum furnace; closing the door of the vacuum furnace, and vacuumizing the blank of the hollow interlayer toughened glass plate in the vacuum furnace; the gas in the airtight sealant and the structural sealant is completely discharged; the airtight sealant, the bonding surface of the structural sealant and the glass and the bonding surface of the stainless steel are fully soaked and wetted under the action of self cohesion after gas is discharged by the airtight sealant and the structural sealant under the capillary action of contact gaps between the stainless steel and the glass, between the glass and between the stainless steel and the stainless steel, so that the bonding of the airtight sealant and the structural sealant to the glass and the stainless steel frames is realized;
meanwhile, the groove of the closed-loop stainless steel frame with the U-shaped section is designed to be deeper, so that the sealing glue layer of the closed-loop structure corresponding to the groove is also longer, and the formed bonding connection sealing layer is thicker, so that the bonding strength of the structural sealant and the glass and the stainless steel is high, and the airtight sealing performance is good;
when the vacuum degree is reached and the vacuum pumping time is set, introducing high-humidity air into the vacuum furnace, and instantly closing an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting; the air generates pressure, the stainless steel frame quickly compacts the softened airtight sealing glue and the structural sealing glue layer under the action of air pressure, and the airtight sealing glue and the structural sealing glue layer are bonded and solidified;
by the process, the bonding quality of the glass and the stainless steel through the airtight sealing glue and the structural sealing glue is improved; opening a vacuum furnace door to manufacture a heat-preservation toughened glass plate body provided with a hollow air inlet and outlet communicated sealing pipe fitting, wherein the periphery of the toughened glass plate body is provided with two annular closed bonding sealing belts and a stainless steel closed-loop protection frame, and the glass hollow interlayer is a heat-preservation lighting toughened glass plate with adjustable and controllable vacuum degree;
or horizontally placing at least one hollow interlayer toughened glass plate blank into a vacuum furnace provided with a supporting base, a fixed supporting clamp or a tray; closing the door of the vacuum furnace, and heating and vacuumizing the blank of the hollow interlayer toughened glass plate in the vacuum furnace; the gas in the hot-melt airtight sealant and the structural sealant is completely discharged; under the capillary action of contact gaps between stainless steel and glass, between glass and glass, between stainless steel and stainless steel, and under the action of self-cohesion after gas is discharged by the hot-melt airtight sealant and the structural sealant, the hot-melt airtight sealant, the bonding surface of the structural sealant and the glass, and the bonding surface of the stainless steel are fully soaked and wetted, so that the bonding of the hot-melt airtight sealant and the structural sealant to the glass and the stainless steel frame is realized;
meanwhile, the groove of the closed-loop stainless steel frame with the U-shaped section is designed to be deeper, so that the sealing glue layer of the closed-loop structure corresponding to the groove is also longer, and the formed bonding connection sealing layer is thicker, so that the bonding strength of the structural sealant and the glass and the stainless steel is high, and the airtight sealing performance is good;
when the heating temperature, the vacuum degree and the set vacuumizing time are reached, high-humidity air is introduced into the vacuum furnace, and an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting is closed instantly; the air absorbs heat, rises temperature and expands to generate pressure, the stainless steel frame quickly compacts the hot-melt airtight sealing adhesive and the structural sealing adhesive layer in a softened state under the action of air pressure, releases heat and solidifies, and then, or starts a cooling device arranged in the vacuum furnace to cool the vacuum furnace;
or introducing high-humidity air into the vacuum furnace, and instantly closing an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting; the air absorbs heat, the temperature rises and expands to generate pressure, the stainless steel frame rapidly compacts the hot-melt airtight sealing adhesive and the structural sealing adhesive layer in a softened state under the action of air pressure, the hot-melt airtight sealing adhesive and the structural sealing adhesive layer are made to release heat and solidify, then the vacuum furnace is cooled by releasing hot air and filling cold air, or a cooling device arranged in the vacuum furnace is started to cool the vacuum furnace, and the structural sealing adhesive in the stainless steel frame can be naturally cooled and solidified;
by the process, the bonding quality of the glass and the stainless steel through the hot-melt airtight sealing glue and the structural sealing glue is improved; when the temperature of the vacuum furnace is reduced to 50-55 ℃, the door of the vacuum furnace is opened to prepare the heat-insulating and lighting toughened glass plate with two annular sealing and bonding sealing belts and a stainless steel closed-loop protection frame on the periphery of the toughened glass plate body, wherein the vacuum degree of the glass hollow interlayer is adjustable.
The rolling support double-glue sealed glass interval cavity regulating and controlling vacuum toughened glass plate is arranged, the toughened glass plate comprises a glass original sheet, toughened glass, cloth-line glass, embossed glass, halogenated glass, frosted glass and coated glass, and functional films of the coated glass comprise an anti-reflection film, a metal film and a decorative film; the surface of the glass panel is compounded with the coating, so that the coating must be removed from the bonding surface of the glass panel; the toughened glass plate is double-layer or multi-layer laminated glass.
The rolling support double-glue sealed glass interval cavity is arranged to regulate and control the vacuum toughened glass plate, and the embossed toughened glass plate and the corrugated toughened glass plate are formed by hot-pressing and stretching the plate glass through corresponding dies or by blowing and stretching the plate glass through heating and positive and negative pressure of the corresponding dies; the convex point glass sheet is flat printed glass produced by adopting a rolling method, and a series of pits which are equal in shape and size and are arranged according to the dot matrix of the convex point support are engraved on the surface of a rolling roller of the glass rolling machine and are used as a printing mould of the convex points;
the embossed toughened glass plate with the convex points is formed by rolling the glass convex points on a proper temperature position in a glass tin bath by a glass rolling machine when a flat glass original sheet is produced; a series of pits which are uniform in shape and size and are arranged according to the dot matrix of the convex point supports are engraved on the surface of one calendering roller of the glass calender; cutting, edging and toughening the embossed toughened glass plate with the convex points;
or the embossed and toughened glass plate with the convex points is heated by a toughening furnace after edging and shaping a flat glass sheet, and is subjected to toughening treatment after rolling the convex points by a glass rolling mill and bending the supporting frame; a series of pits which are uniform in shape and size and are arranged according to the dot matrix of the convex point supports are engraved on the surface of one calendering roller of the glass calender;
or the convex-hull toughened glass plate or the corrugated toughened glass plate is rolled with glass concave points by a glass rolling machine at a proper temperature position in a glass tin bath when producing a flat glass sheet; the surface of a calendering roller on the used glass calender is engraved with a series of convex tips which are uniform in shape and size and are arranged according to the lattice of the concave point support; cutting, edging and toughening the concave embossed toughened glass plate;
or after edging and shaping the convex toughened glass plate or the corrugated toughened glass plate, heating the convex toughened glass plate or the corrugated toughened glass plate by a toughening furnace, stretching the convex points by a glass mold, bending the supporting frame, and after shaping, carrying out toughening treatment;
or the bump toughened glass plate is made by printing glass powder paste and sintering; firstly, printing low-temperature glass powder paste on a piece of plate glass according to the dot matrix arrangement pattern of the bump support, then sending the plate glass into a toughening sintering furnace, heating to a certain proper temperature of the melting point of the glass powder paste, converting a glass powder paste accumulation body into glass bumps fused with the surface of the plate glass, then bending a support frame, and carrying out toughening treatment;
the support is a support with at least one end coated with adhesive, and comprises a high-hardness glass support, a high-hardness metal support and a high-hardness ceramic support which are equal to or close to the height of the raised frame support band, and columnar, spherical or annular support lattices are arranged; or the support is a support heat insulation material pad with an aerogel heat insulation pad bonded on the end support surface, and the surfaces of the aerogel heat insulation pads at the two ends of the support heat insulation material pad are coated with hot melt adhesive, glass cement, ultraviolet curing cement or water glass cement.
Cutting flat glass with proper thickness according to the design size, edging and toughening the toughened glass panel, and using the toughened glass panel as a raw material; deoiling, cleaning and drying the glass bonding surface.
The regulating and controlling vacuum toughened glass plate is provided with a rolling supporting double-glue sealed glass interval cavity, wherein an opening on a hollow interlayer toughened glass plate body is arranged on a glass panel or arranged on a raised frame supporting belt and a raised frame supporting belt; the communicated sealing pipe fitting is a pipe fitting with a T-shaped section and a thread arranged on the outer wall of the pipe provided with a head blocking pipe, the thread of the pipe fitting is correspondingly provided with a tooth ridge at the root and an upward conical nut, the pipe fitting is screwed and sealed on the hollow interlayer toughened glass plate body through an airtight sealing glue and the nut, or the pipe fitting with the thread arranged on the outer wall of the pipe, the thread of the pipe fitting is correspondingly provided with a tooth ridge at the root and an upward conical nut, and the pipe fitting is screwed and sealed on the hollow interlayer toughened glass plate body through an airtight sealing glue and the nut; the communicated sealing pipe fitting is provided with a fastening sealing pipe fitting corresponding to the opening of the toughened glass plate, the air inlet and outlet pipe heads are locked and sealed by airtight sealing glue and the fastening sealing pipe fitting and are fixed on the opening of the air inlet and outlet pipe heads on the toughened glass plate, the section is T-shaped and is provided with a baffle head, the baffle head is provided with an air vent groove, and the outer wall of the pipe is provided with a threaded pipe fitting or is made of magnetic material.
The rolling support double-glue sealed glass spacing cavity regulating and controlling vacuum toughened glass plate is arranged, and a glass support frame is annularly sealed and is bonded through a first air-tight sealant; the first airtight sealant comprises butyl sealant, such as polyisobutylene rubber and hot melt butyl rubber; the second sealant is a curing weather-resistant structure sealant, and comprises elastic sealants for hollow glass, such as polysulfides, silicones and polyurethanes; the hot-melt structural sealant comprises hot-melt polyisobutylene rubber and hot-melt butyl rubber.
The method is characterized in that a rolling supporting double-glue sealed glass interval cavity is arranged to regulate and control a vacuum toughened glass plate, a raised frame supporting belt corresponding to the size of a glass panel is manufactured, the height of the raised frame supporting belt and the width of an airtight sealing glue bonding sealing surface are determined according to the design size; bonding the airtight sealant of the raised frame supporting band on the surface, and performing deoiling, cleaning and drying treatment; the raised frame supporting belt is a rectangular glass strip or a metal strip which has the same thickness as the heat-preservation and lighting toughened glass plate and is edged at the edge, and is adhered to the raised frame supporting belt formed on the edge of the toughened glass plate through airtight sealing glue; or the raised frame supporting strips are rectangular glass strips or metal strips and are bonded and formed by airtight sealing glue;
or the raised frame supporting belt is a U-shaped metal section with the outer width corresponding to the width of the edge of the toughened glass plate and is formed by hot melt welding and laser welding;
or the raised frame supporting belt is a U-shaped metal section with the outer width corresponding to the width of the edge of the toughened glass plate and is bonded and formed by airtight sealant; the section of the U-shaped section is arranged at the airtight sealing glue bonding position, and an airtight sealing glue bonding and splicing filling patch which enlarges the sealing connection surface and corresponds to the shape of the airtight sealing glue bonding position of the U-shaped section is arranged;
or the raised frame supporting belt is a T-shaped metal section with the outer width slightly larger than the width of the edge of the heat-preservation lighting toughened glass plate, and is bonded and formed by airtight sealant; corner joint parts of the T-shaped metal section bars are provided with corner-supplementing bonding patches;
the metal thin strip with good plasticity for prolonging the bonding thickness of the airtight sealant is an aluminum strip or a stainless steel strip.
The periphery of the hollow interlayer toughened glass plate body is wrapped with a closed-loop corrugated stainless steel frame with a U-shaped section; the U-shaped corrugated stainless steel channel section is formed by stamping and stretching a stainless steel strip through a die, or the U-shaped corrugated stainless steel channel section is formed by rolling the stainless steel strip through a rolling mill; the closed-loop corrugated stainless steel frame is a U-shaped corrugated stainless steel groove profile, and is made into an elastic closed-loop corrugated stainless steel frame by bending welding or cutting welding;
when the U-shaped closed-loop corrugated stainless steel frame groove is used, deoiling, cleaning and drying treatment are required;
the outer side of the periphery of the hollow interlayer toughened glass plate body is wrapped with a protective frame of a hollow interlayer toughened glass plate structure which is formed by buckling and sleeving a closed-loop stainless steel frame with an L-shaped and an inverted L-shaped section; the L-shaped stainless steel section is a stainless steel strip and is formed by stamping and stretching through a die, or the L-shaped stainless steel section is a stainless steel strip and is formed by rolling through a rolling mill; the closed loop 'L' -shaped stainless steel frame is an 'L' -shaped stainless steel section bar and is made into a stainless steel frame by bending welding or cutting welding;
when the L-shaped stainless steel section is used, deoiling, cleaning and drying treatment are required.
The use method of the regulating and controlling vacuum toughened glass plate provided with the rolling support double-glue sealed glass interval cavity comprises the steps that at least one glass frame supports and complementarily buckles an air inlet pipe and an air outlet pipe of double-glue bonded stainless steel frame vacuum regulating and controlling glass, or a vacuum gauge and a vacuum valve are arranged on the air inlet pipe and the air outlet pipe, wherein the vacuum gauge is an artificial intelligent vacuum gauge, and the vacuum valve is an artificial intelligent vacuum valve; the vacuum valve is connected with the main air inlet and outlet pipeline in a sealing and parallel way through a three-way or four-way pipe fitting in a mode of welding, bonding and bolting through a nut sealing pipe fitting;
the other interface of the main air inlet and outlet pipe tee joint or four-way pipe fitting is connected with a vacuum valve, the vacuum valve is connected with an interface of a dryer, and the dryer is provided with an electric heating dehumidification device and an air exhaust valve;
one of the interfaces of the dryer is respectively connected with a low-heat-conductivity gas steel cylinder comprising argon and carbon dioxide in parallel and in sealing connection through a main pipe, a three-way or four-way pipe fitting and a vacuum valve; meanwhile, the dryer is also connected with a steel cylinder containing high-heat-conductivity gas, such as hydrogen and helium, through a main pipe, a three-way or four-way pipe fitting and a vacuum valve respectively; the vacuum valve is also connected with an atmosphere air inlet pipe through a main pipe, a three-way or four-way pipe fitting and the vacuum valve; the main air inlet and outlet pipe is connected with a vacuum valve through another interface of a three-way or four-way pipe fitting, the vacuum valve is connected with a vacuum pump set through a pipeline, a vacuum meter is arranged on the main air inlet and outlet pipe, and the vacuum pump set is controlled to be opened and closed manually, automatically or intelligently; forming a glass frame support complementary buckling double-glue bonding stainless steel frame vacuum regulation glass system;
the vacuum pump set is provided with a rough pumping vacuum pump and a fine pumping vacuum pump which are connected in parallel, when the rough pumping vacuum pump pumps to set vacuum, the rough pumping vacuum pump is closed, the fine pumping vacuum pump is started, and the fine pumping vacuum pump is closed until the set vacuum is pumped; when the vacuum degree is reduced to a set value, the vacuum pump set is started again;
the vacuum degree of the glass frame support complementary buckling double-glue-bonded stainless steel frame vacuum regulation glass is reduced to a set value, then a vacuum valve is automatically closed, a vacuum pump measures the vacuum degree of the glass frame support complementary buckling double-glue-bonded stainless steel frame vacuum regulation glass cavity, whether the device leaks vacuum is judged, and the vacuum valve is automatically opened when the vacuum degree is reduced to the set value;
the glass frame support complementary buckling double-glue bonding stainless steel frame vacuum regulation and control glass system realizes good heat dissipation of the device by introducing hydrogen or helium of high-heat-conductivity-coefficient gas into the system according to design requirements;
the conventional heat dissipation of the device is realized by introducing air into the system;
the conventional heat preservation of the device is realized by introducing argon or carbon dioxide of low-heat-conductivity-coefficient gas into the system;
and the system is vacuumized, so that the good heat preservation of the device is realized.
The invention has the beneficial effects that:
the functional vacuum glass manufactured by the invention can realize the manufacture of glass and stainless steel frames by double-glue sealing and bonding. The glass bonding quality can be well realized, the problem of tempering loss of the vacuum glass is solved, the safety problem of the vacuum glass is solved, and the energy-saving requirements of facility agriculture and buildings are well met. The functional vacuum glass has simple manufacturing process, is widely applied to common toughened glass in material, greatly reduces the manufacturing cost, greatly improves the safety and the yield, and can be diversified in structural form. The toughened glass plate has the characteristics of thinness, light weight, high strength, safety, long service life, large size, high yield, strong functionality, low energy consumption, high efficiency, light transmission, safety, low manufacturing cost, condensation prevention, convenience for large-scale production and the like.
The invention relates to a vacuum regulating and controlling system for functional vacuum glass, which regulates and controls the vacuum degree of a glass isolation interlayer cavity by equipment comprising a vacuum pump set, an artificial intelligent control system, an airtight vacuum pipeline device, a vacuum valve, a vacuum meter, functional gas, a dryer and the like, and realizes the vacuum heat preservation, sound insulation and light transmission functions of the functional vacuum glass. The functional vacuum glass system can realize automatic remote control of artificial intelligence and reliable operation. The glass overcomes the defects that the prior hollow glass, vacuum glass and the prior application of the inventor are disclosed in the patent numbers: 2010103000382 laminated plate glass curtain wall for regulating and controlling vacuum degree of cavity. The adjustable heat-insulating property, the adjustable sound-insulating property and the good heat-insulating and sound-insulating properties are realized. Therefore, the invention has good economic benefit, environmental benefit and social benefit.
Drawings
The invention is further illustrated with reference to the following figures and examples.
FIG. 1 is a cross-sectional view of a toughened glass plate complementary combination sheet with lattice sintering support salient points compositely distributed on both sides and a U-shaped corrugated stainless steel channel section frame double-adhesive vacuum toughened glass plate;
FIG. 2 is a cross-sectional view of a toughened glass plate complementary combination sheet with lattice stretching support salient points compositely distributed on both sides and a U-shaped corrugated stainless steel channel section frame double-adhesive vacuum toughened glass plate;
FIG. 3 is a cross-sectional view of a toughened glass plate complementary combination sheet with lattice embossed support convex points compositely distributed on both sides and a U-shaped corrugated stainless steel channel profile frame double-adhesive vacuum toughened glass plate;
FIG. 4 is a cross-sectional view of a tempered glass plate complementary combination sheet with lattice sintering support salient points compositely distributed on both sides and a vacuum tempered glass plate which is bonded with a frame of a buckled L-shaped stainless steel groove profile by double glue;
FIG. 5 is a cross-sectional view of a tempered glass plate complementary sheet with lattice stretching support salient points compositely distributed on both sides and a vacuum tempered glass plate glued with a frame of a buckled L-shaped stainless steel channel profile;
FIG. 6 is a cross-sectional view of a tempered glass plate complementary combination sheet with lattice embossed support protrusions compositely distributed on both sides and a vacuum tempered glass plate glued with a frame of a buckled L-shaped stainless steel channel profile;
FIG. 7 is a cross-sectional view of a tempered glass plate with lattice embossed support protrusions compositely distributed on both sides, which is used for aligning the lamination sheets, and a U-shaped corrugated stainless steel channel profile frame double-adhesive vacuum tempered glass plate;
FIG. 8 is a cross-sectional view of a tempered glass plate with dot matrix stretching support bumps compositely distributed on both sides, which is used for aligning the lamination sheets, and a U-shaped corrugated stainless steel channel profile frame double-adhesive vacuum tempered glass plate;
FIG. 9 is a cross-sectional view of a tempered glass plate with lattice sintered support protrusions compositely distributed on both sides, which is used for aligning the lamination sheets, and a U-shaped corrugated stainless steel channel profile frame double-adhesive vacuum tempered glass plate;
FIG. 10 is a cross-sectional view of a tempered glass plate with lattice embossed support protrusions compositely distributed on both sides, which is aligned with the laminating sheet, and a vacuum tempered glass plate bonded with a frame of a buckled L-shaped stainless steel channel profile by double glue;
FIG. 11 is a cross-sectional view of a tempered glass plate with lattice stretching support bumps compositely distributed on both sides, which is aligned with the laminating sheet, and a vacuum tempered glass plate bonded with a frame of a buckled L-shaped stainless steel channel profile by double glue;
FIG. 12 is a cross-sectional view of a tempered glass plate with lattice sintered support protrusions compositely distributed on both sides, which is aligned with the lamination sheet, and a vacuum tempered glass plate bonded with a frame of a buckled L-shaped stainless steel channel profile by double glue;
fig. 13 and 14 are schematic connection views of the air inlet and outlet system of the glass curtain wall.
In the figure: 1 'U' -shaped stainless steel corrugated protective frame, 2 structural sealant, 3 lower side toughened plate glass, 4 vacuum interlayers, 5 upper side toughened plate glass, 6 sintered supporting salient points, 7 water glass, 8 stretched glass supporting frame, 9 air inlet and outlet pipes, 10 vacuum valves, 11 airtight sealant, 12 stretched supporting salient points, 13 embossed supporting salient points, 14 inner side 'L' -shaped stainless steel protective frame, 15 outer side 'L' -shaped stainless steel protective frame, 16 fine vacuum pump exhaust pipes, 17 fine vacuum pump, 18 artificial intelligent controller, 19 three-way pipe fittings, 20 drier, 21 vacuum meter, 22 drier exhaust valve, 23 carbon dioxide gas tank, 24 argon gas tank, 25 helium gas tank, 26 oxyhydrogen tank, 27 air inlet pipe, 28 coarse vacuum pump, 29 coarse vacuum pump exhaust pipes and 30 four-way pipe fittings.
Detailed Description
As shown in fig. 1: the stretching glass supporting frame 8 distributed with the toughened glass 5 on the upper side of the lattice sintering supporting salient points 6 and the toughened glass 3 on the lower side distributed with the lattice sintering supporting salient points 6 correspond to each other in outline shape and size and are buckled complementarily to form the vacuum interlayer 4 at intervals. A closed-loop U-shaped stainless steel corrugated protective frame 1 is bonded with a structural sealant 2 and an airtight sealant 11 to manufacture a tempered glass plate frame support complementary buckled stainless steel frame vacuum tempered glass plate.
As shown in fig. 2: lattice stretching support salient points 12 are distributed on the upper tempered glass 5 and the lower tempered glass 3, and the rest is equal to that in the figure 1.
As shown in fig. 3: dot matrix embossing supporting salient points 13 are distributed on the upper tempered glass 5 and the lower tempered glass 3, and the rest is equal to that in the figure 1.
As shown in fig. 4: the stretching glass supporting frame 8 distributed with the toughened glass 5 on the upper side of the lattice sintering supporting salient points 6 and the toughened glass 3 on the lower side distributed with the lattice sintering supporting salient points 6 correspond to each other in outline shape and size and are buckled complementarily to form the vacuum interlayer 4 at intervals. The buckled L-shaped stainless steel protective frame consisting of the inner L-shaped stainless steel protective frame 14 and the outer L-shaped stainless steel protective frame 15 is bonded with the structural sealant 2 and the airtight sealant 11 to manufacture the toughened glass plate edge frame for supporting the vacuum toughened glass plate with the complementarily buckled stainless steel edge frame.
As shown in fig. 5: lattice stretching support salient points 12 are distributed on the upper tempered glass 5 and the lower tempered glass 3, and the rest is equal to that in the figure 4.
As shown in fig. 6: dot matrix embossing supporting salient points 13 are distributed on the upper tempered glass 5 and the lower tempered glass 3, and the rest is equal to that in the figure 4.
As shown in fig. 7: the toughened glass plate composite metal solder with the dot matrix embossing support salient points 13 compositely distributed on the upper toughened glass 5 and the lower toughened glass 3 is opposite to the laminated sheet, and the others are equal to the graph 1.
As shown in fig. 8: the toughened glass plate composite metal solder with the lattice stretching support salient points 12 compositely distributed on the upper toughened glass 5 and the lower toughened glass 3 is opposite to the superposed sheets, and the others are equal to the graph 2.
As shown in fig. 9: the toughened glass plate composite metal solder with the dot matrix embossing support salient points 10 compositely distributed on the upper toughened glass 5 and the lower toughened glass 3 is opposite to the overlapping sheet, and the others are equal to the graph 3.
As shown in fig. 10: the toughened glass plate composite metal solder with the dot matrix embossing support salient points 13 compositely distributed on the upper toughened glass 5 and the lower toughened glass 3 is opposite to the laminated sheet, and the others are equal to the graph 4.
As shown in fig. 11: the toughened glass plate composite metal solder with the lattice stretching support salient points 12 compositely distributed on the upper toughened glass 5 and the lower toughened glass 3 is opposite to the superposed sheet, and the others are equal to the graph 5.
As shown in fig. 12: the toughened glass plate composite metal solder with the dot-matrix sintering support salient points 6 compositely distributed on the upper toughened glass 5 and the lower toughened glass 3 is opposite to the superposed sheet, and the others are equal to the graph 6.
As shown in fig. 13: the air inlet and exhaust pipe provided with the rolling support double-glue sealed glass interval cavity for regulating and controlling the vacuum toughened glass plate is connected with the air inlet and exhaust pipeline in a sealing and parallel way through a three-way pipe fitting 19 or a four-way pipe fitting 30 in a mode of welding, bonding and bolting a nut sealed pipe fitting. The air inlet and outlet pipeline is provided with a vacuum valve F3. The front vacuum meter 21 is arranged in front of the vacuum valve F3, and the rear vacuum meter 21 is arranged behind the vacuum valve F3. The air inlet and outlet pipeline is connected with a vacuum pump set through a pipe orifice at one end of the three-way pipe 19; the other end pipe orifice of the three-way pipe fitting 19 is connected with the functional gas tank group through a vacuum valve F2.
As shown in fig. 13, the roll-in supporting double-glue sealed glass interval cavity regulating and controlling vacuum toughened glass plate with the air inlet and outlet pipe fittings is composed of upper toughened glass 5 and lower toughened glass 3 distributed with lattice supporting salient points, which are mutually corresponding in outline shape and size and are complementarily buckled to form a hollow interlayer 4 at intervals. The periphery of the sealed glass is bonded by the structural sealant 1 and the airtight sealant 2 to manufacture the vacuum adjustable toughened glass plate. The vacuum toughened glass plate is provided with an air inlet and outlet pipe fitting 8.
The air inlet and outlet pipeline is hermetically connected with a vacuum pump set through a pipe orifice at one end of a three-way pipe 19, and the vacuum pump set is opened and closed through a numerical value standard set by a vacuum meter 21; or the variable frequency vacuum pump set can output power according to the numerical value standard set by the vacuum meter 21.
The vacuum pump set is provided with two groups of vacuum pumps, namely a rough vacuum pump 28 and a fine vacuum pump 17, when the rough vacuum pump 28 is vacuumized to a set vacuum, the rough vacuum pump 28 is closed, the fine vacuum pump 17 is started, and the fine vacuum pump 17 is closed until the set vacuum is pumped; when the vacuum degree is reduced to a set value, the vacuum pump set is started again; or the vacuum pump set is a continuously-operated variable-frequency vacuum pump set.
The vacuum pump group is provided with a rough pumping vacuum pump and a fine pumping vacuum pump which are connected in parallel, and the rapid vacuum pumping and the high vacuum pumping are realized by connecting two groups of vacuum pumps, namely the rough pumping vacuum pump 21 and the fine pumping vacuum pump 17 in parallel or in series.
If F4 and F18 are closed and opened, F5, F6, F7, F8 and F19 are opened, the rough vacuum pump 28 is started to vacuumize the system, and the gas passes through the rough vacuum pump 28 and the vacuum valve F19 and is exhausted through the exhaust pipe 18 of the rough vacuum pump 28.
After the vacuum degree of the functional gas pressure heat-preservation toughened glass plate with the sealed glass peripheral regulating and controlling interlayer is increased to a set value, the efficiency of the rough vacuum pump is greatly reduced. Closing vacuum valves F5, F6, F7, F8, F18 and F19, and closing the rough vacuum pump; and (3) starting the fine vacuum pump 17, starting vacuum valves F4, F9, F10, F16 and F17 until the set vacuum is pumped, closing vacuum valves F4, F9, F10, F16 and F17, and then, finely pumping the vacuum pump 17. When the vacuum degree is reduced to a set value, the vacuum pump set is started again;
or after the vacuum degree of the functional gas pressure heat-preservation toughened glass plate of the interlayer of the peripheral regulation and control of the sealed glass is increased to a set value, closing a vacuum valve F19, starting a fine vacuum pump 17, starting vacuum valves F18, F9, F10, F16 and F17, closing vacuum valves F5, F6, F7, F8, F18 and F19 and closing a rough vacuum pump until set vacuum is pumped; and then closing vacuum valves F4, F9, F10, F16 and F17, and finely pumping the vacuum pump 17. When the vacuum degree is reduced to a set value, the vacuum pump set is started again;
the air inlet and outlet pipeline is provided with a vacuum valve F2 connected with the other end pipe orifice of the tee pipe fitting 19. A functional gas inlet pipeline which is opened and closed by a vacuum valve F2; a dryer assembly 20 is arranged on the air inlet pipeline arranged in front of the vacuum valve F2; the drier component is provided with an electric heating dehumidification device and an air exhaust valve 22;
a plurality of groups of functional gas tanks containing air are arranged on the pipeline in front of the dryer 20; the functional gas tank group comprises a low-heat-conductivity-coefficient gas argon tank 24 and a carbon dioxide gas tank 23, and a high-heat-conductivity-coefficient gas comprises a hydrogen tank 26 and a helium tank 25;
according to design requirements, the heat-insulating heat-dissipating light-transmitting tempered glass plate is well heat-dissipating by introducing hydrogen or helium of gas with high heat conductivity coefficient into the heat-insulating heat-dissipating light-transmitting tempered glass plate;
the conventional heat dissipation of the heat-preservation heat-dissipation light-transmitting tempered glass plate is realized by introducing air into the heat-preservation heat-dissipation light-transmitting tempered glass plate;
the conventional heat preservation of the heat-preservation heat-dissipation light-transmitting tempered glass plate is realized by introducing argon or carbon dioxide of a gas with a low heat conductivity coefficient into the heat-preservation heat-dissipation light-transmitting tempered glass plate;
the good heat preservation of the heat-preservation heat-dissipation light-transmitting tempered glass plate is realized by vacuumizing the heat-preservation heat-dissipation light-transmitting tempered glass plate.
The vacuum meter 21 is a conventional vacuum meter, or an artificial intelligent vacuum meter, and the vacuum valve is a conventional vacuum valve, or an artificial intelligent vacuum valve.
As shown in fig. 14: the air inlet and exhaust pipe provided with the rolling support double-glue sealed glass interval cavity for regulating and controlling the vacuum toughened glass plate is provided with a vacuum meter
Figure DEST_PATH_IMAGE002
And a vacuum valve F16, vacuum gauge
Figure 280483DEST_PATH_IMAGE002
Or an artificial intelligent vacuum meter, a vacuum valve F16 or an artificial intelligent vacuum valve; the vacuum valve F16 is connected with the tee pipe 19 in a sealing and parallel way through a tee pipe or a four-way pipe in a way of welding, bonding and bolting a nut sealing pipe; the others are equivalent to fig. 13.

Claims (10)

1. Be equipped with roll-in and support two sealed glass interval cavity regulation and control vacuum toughened glass board of gluing, including toughened glass board, the sealed glue of bonding, characterized by: one of the two toughened glass plates is provided with a communicated sealing pipe fitting which is communicated with the two sides and is bonded and sealed by an airtight sealing glue and a structural sealing glue; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is bonded, sealed, screwed and locked by a connecting fastener and the airtight sealing glue; or a communicated sealing pipe fitting which is communicated with the two sides and is sealed by soldering through a low-melting-point metal soldering flux is arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is brazed, sealed and locked by a connecting fastener and a low-melting-point metal brazing flux;
(A) two toughened glass plates forming the interval interlayer cavity are mutually corresponding in outline shape and size, and one of the at least two toughened glass plates is provided with an embossed toughened glass plate which is integrated with the toughened glass plate and uniformly distributed with lattice raised support points and raised frame support bands; the height of the raised frame supporting belt is equal to that of the dot matrix raised supporting points; or a raised frame supporting belt which is processed and formed, has the complementary corresponding outline shape and size with the edges of the two toughened glass plates and has the height equal to the height of the relative supporting and superposing total height of the raised supporting points of the dot matrix is arranged between the edges of the two toughened glass plates;
the method comprises the following steps that two embossed toughened glass plates with mutually corresponding outline shapes and sizes and provided with lattice raised supporting points and raised frame supporting belts are subjected to complementary buckling, bonding and sealing after airtight sealant is coated on the raised frame supporting belts, or transparent glue is coated on the lattice raised supporting points and the airtight sealant is coated on the raised frame supporting belts;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a sealing rubber ring which is bonded with the bottom of the supporting band groove of the raised frame and the closed structures of the glass groove walls at two sides;
(B) or two toughened glass plates forming the interval interlayer cavity are mutually corresponding in outline shape and size, and one of the at least two toughened glass plates is provided with an embossed toughened glass plate of a dot matrix concave supporting point and a concave frame supporting belt which are formed by pressing and stretching by a mould; a concave frame supporting belt with the same height as the concave supporting points of the dot matrix is arranged between the edges of the two toughened glass plates; or the edges of the two toughened glass plates are provided with concave frame supporting bands, and the heights of the concave frame supporting bands are equal to the heights of the concave supporting points of the dot matrix; or the height of the concave frame supporting strip is as high as the total height of the opposite support superposition height of the concave supporting points of the dot matrix arranged at the edges of the two toughened glass plates;
the method comprises the following steps of enabling two embossed toughened glass plates with mutually corresponding outline shapes and sizes and provided with lattice concave supporting points and concave frame supporting belts to be mutually matched, buckling, bonding and sealing the concave frame supporting belts of the two toughened glass plates after airtight sealant is coated on the concave frame supporting belts, or transparent adhesive is coated on the lattice concave supporting points and the airtight sealant is coated on the concave frame supporting belts;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a sealing rubber ring which is bonded with the bottom of a supporting band groove of the lower concave frame and a closed structure of the glass groove walls at two sides, so that a toughened glass plate blank is manufactured;
then, at least one tempered glass plate blank is sent into a vacuum furnace, and heating and vacuumizing are carried out; and then introducing humid air into the vacuum furnace, cooling, and opening the furnace to obtain the rolled support double-glue sealed glass interval cavity regulating and controlling vacuum toughened glass plate.
2. A method for manufacturing a vacuum tempered glass plate with a rolling support double-glue sealed glass spacing cavity for regulating and controlling the vacuum tempered glass plate of the product of claim 1, which comprises the steps of tempering the glass plate, bonding the sealant and a vacuum furnace, and is characterized in that: two communicated sealing pipe fittings which are provided with two communicated sides and are bonded and sealed by airtight sealing glue and structural sealant are arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is bonded, sealed, screwed and locked by a connecting fastener and the airtight sealing glue; or a communicated sealing pipe fitting which is communicated with the two sides and is sealed by soldering through a low-melting-point metal soldering flux is arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is brazed, sealed and locked by a connecting fastener and a low-melting-point metal brazing flux; the embossed toughened glass plates are provided with lattice support points and frame support belts, and after airtight sealant is coated on the frame support belts, or transparent adhesive is coated on the lattice support points and the airtight sealant is coated on the frame support belts, the frame support belts of the two toughened glass plates are complementarily buckled, bonded and sealed;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a groove bottom of a supporting band of the bonding frame and a sealing rubber ring of a closed structure of the glass groove walls at two sides, so that a toughened glass plate blank is manufactured;
then horizontally placing at least one hollow interlayer toughened glass plate blank into a vacuum furnace provided with a supporting base, a fixed supporting clamp or a tray; an ultrasonic transducer for improving the bonding quality of glass and glass, glass and metal is arranged on a glass tray of the vacuum furnace; closing the door of the vacuum furnace, and vacuumizing the blank of the hollow interlayer toughened glass plate in the vacuum furnace; the gas in the airtight sealant and the structural sealant is completely discharged;
when the vacuum degree is reached and the vacuum pumping time is set, introducing high-humidity air into the vacuum furnace, and instantly closing an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting; the air generates pressure, the stainless steel frame quickly compacts the softened airtight sealing glue and the structural sealing glue layer under the action of air pressure, and the airtight sealing glue and the structural sealing glue layer are bonded and solidified;
by the process, the bonding quality of the glass and the stainless steel through the airtight sealing glue and the structural sealing glue is improved; opening a vacuum furnace door to manufacture a heat-preservation toughened glass plate body provided with a hollow air inlet and outlet communicated sealing pipe fitting, wherein the periphery of the toughened glass plate body is provided with two annular sealing and bonding sealing belts, and the glass hollow interlayer is a heat-preservation lighting toughened glass plate with adjustable and controllable vacuum degree;
or horizontally placing at least one hollow interlayer toughened glass plate blank into a vacuum furnace provided with a supporting base, a fixed supporting clamp or a tray; closing the door of the vacuum furnace, and heating and vacuumizing the blank of the hollow interlayer toughened glass plate in the vacuum furnace; the gas in the hot-melt airtight sealant and the structural sealant is completely discharged;
when the heating temperature, the vacuum degree and the set vacuumizing time are reached, high-humidity air is introduced into the vacuum furnace, and an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting is closed instantly; the air absorbs heat, rises temperature and expands to generate pressure, the stainless steel frame quickly compacts the hot-melt airtight sealing adhesive and the structural sealing adhesive layer in a softened state under the action of air pressure, releases heat and solidifies, and then, or starts a cooling device arranged in the vacuum furnace to cool the vacuum furnace;
or introducing high-humidity air into the vacuum furnace, and instantly closing an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting; the air absorbs heat, the temperature rises and expands to generate pressure, the stainless steel frame rapidly compacts the hot-melt airtight sealing adhesive and the structural sealing adhesive layer in a softened state under the action of air pressure, the hot-melt airtight sealing adhesive and the structural sealing adhesive layer are made to release heat and solidify, then the vacuum furnace is cooled by releasing hot air and filling cold air, or a cooling device arranged in the vacuum furnace is started to cool the vacuum furnace, and the structural sealing adhesive in the stainless steel frame can be naturally cooled and solidified;
by the process, the bonding quality of the glass and the stainless steel through the hot-melt airtight sealing glue and the structural sealing glue is improved; when the temperature of the vacuum furnace is reduced to 50-55 ℃, the door of the vacuum furnace is opened to prepare the heat-insulating and lighting toughened glass plate with two annular sealing and bonding sealing belts and a stainless steel closed-loop protection frame on the periphery of the toughened glass plate body, wherein the vacuum degree of the glass hollow interlayer is adjustable.
3. Be equipped with roll-in and support two sealed glass interval cavity regulation and control vacuum toughened glass board of gluing, including toughened glass board, the sealed glue of bonding, characterized by: one of the two toughened glass plates is provided with a communicated sealing pipe fitting which is communicated with the two sides and is bonded and sealed by an airtight sealing glue and a structural sealing glue; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is bonded, sealed, screwed and locked by a connecting fastener and the airtight sealing glue; or a communicated sealing pipe fitting which is communicated with the two sides and is sealed by soldering through a low-melting-point metal soldering flux is arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is brazed, sealed and locked by a connecting fastener and a low-melting-point metal brazing flux;
(A) two toughened glass plates forming the interval interlayer cavity are mutually corresponding in outline shape and size, and one of the at least two toughened glass plates is provided with an embossed toughened glass plate which is integrated with the toughened glass plate and uniformly distributed with lattice raised support points and raised frame support bands; the height of the raised frame supporting belt is equal to that of the dot matrix raised supporting points; or a raised frame supporting belt which is processed and formed, has the complementary corresponding outline shape and size with the edges of the two toughened glass plates and has the height equal to the height of the relative supporting and superposing total height of the raised supporting points of the dot matrix is arranged between the edges of the two toughened glass plates;
the method comprises the following steps that two embossed toughened glass plates with mutually corresponding outline shapes and sizes and provided with lattice raised supporting points and raised frame supporting belts are subjected to complementary buckling, bonding and sealing after airtight sealant is coated on the raised frame supporting belts, or transparent glue is coated on the lattice raised supporting points and the airtight sealant is coated on the raised frame supporting belts;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a sealing rubber ring which is bonded with the bottom of the supporting band groove of the raised frame and the closed structures of the glass groove walls at two sides; or a layer of metal thin belt with good plasticity is adhered to the periphery of the toughened glass plate which is adhered and sealed by the two toughened glass plate lamination sheets through airtight sealant to be used as an airtight sealing ring of the isolation sealing layer;
(B) or two toughened glass plates forming the interval interlayer cavity are mutually corresponding in outline shape and size, and one of the at least two toughened glass plates is provided with an embossed toughened glass plate of a dot matrix concave supporting point and a concave frame supporting belt which are formed by pressing and stretching by a mould; a concave frame supporting belt with the same height as the concave supporting points of the dot matrix is arranged between the edges of the two toughened glass plates; or the edges of the two toughened glass plates are provided with concave frame supporting bands, and the heights of the concave frame supporting bands are equal to the heights of the concave supporting points of the dot matrix; or the height of the concave frame supporting strip is as high as the total height of the opposite support superposition height of the concave supporting points of the dot matrix arranged at the edges of the two toughened glass plates;
the method comprises the following steps of enabling two embossed toughened glass plates with mutually corresponding outline shapes and sizes and provided with lattice concave supporting points and concave frame supporting belts to be mutually matched, buckling, bonding and sealing the concave frame supporting belts of the two toughened glass plates after airtight sealant is coated on the concave frame supporting belts, or transparent adhesive is coated on the lattice concave supporting points and the airtight sealant is coated on the concave frame supporting belts;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a sealing rubber ring which is bonded with the bottom of a supporting band groove of the lower concave frame and a closed structure of the two side glass groove walls;
or a layer of metal thin belt with good plasticity is adhered to the periphery of the toughened glass plate which is adhered and sealed by the two toughened glass plate lamination sheets through airtight sealant to be used as an airtight sealing ring of the isolation sealing layer;
the outer side of the periphery of the hollow interlayer toughened glass plate body is wrapped with a closed-loop corrugated stainless steel frame with a U-shaped section, and structural sealant which does not generate chemical reaction with the airtight sealant is filled in a groove of the corrugated stainless steel frame; the U-shaped closed-loop corrugated stainless steel frame with the cross section is tightly attached and bonded with the outer side of the periphery of the hollow interlayer toughened glass plate body by utilizing the elasticity of the U-shaped closed-loop corrugated stainless steel frame and utilizing the self resilience of the closed-loop corrugated stainless steel frame;
or the outer side of the periphery of the hollow interlayer toughened glass plate body is wrapped with a protective frame of a hollow interlayer toughened glass plate structure, the upper section of the protective frame is L-shaped and reverse L-shaped, and the closed loop stainless steel frame coated with the structural sealant is buckled and sleeved to form the protective frame of the hollow interlayer toughened glass plate structure, so that a toughened glass plate blank is manufactured;
then, at least one tempered glass plate blank is sent into a vacuum furnace, and heating and vacuumizing are carried out; and then introducing humid air into the vacuum furnace, cooling, and opening the furnace to obtain the rolled support double-glue sealed glass interval cavity regulating and controlling vacuum toughened glass plate.
4. A method for manufacturing a vacuum tempered glass plate with a rolling support double-glue sealed glass spacing cavity for regulating and controlling the vacuum tempered glass plate of the product of claim 1, which comprises the steps of tempering the glass plate, bonding the sealant and a vacuum furnace, and is characterized in that: two communicated sealing pipe fittings which are provided with two communicated sides and are bonded and sealed by airtight sealing glue and structural sealant are arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is bonded, sealed, screwed and locked by a connecting fastener and the airtight sealing glue; or a communicated sealing pipe fitting which is communicated with the two sides and is sealed by soldering through a low-melting-point metal soldering flux is arranged on one of the two toughened glass plates; or one of the two toughened glass plates is provided with a communicating sealing pipe fitting which is communicated with the two sides and is brazed, sealed and locked by a connecting fastener and a low-melting-point metal brazing flux; the embossed toughened glass plates are provided with lattice support points and frame support belts, and after airtight sealant is coated on the frame support belts, or transparent adhesive is coated on the lattice support points and the airtight sealant is coated on the frame support belts, the frame support belts of the two toughened glass plates are complementarily buckled, bonded and sealed;
structural sealant is filled in a peripheral groove of the hollow interlayer toughened glass plate body to form a groove bottom of a supporting band of the bonding frame and a sealing rubber ring of a closed structure of the glass groove walls at two sides, so that a toughened glass plate blank is manufactured;
then horizontally placing at least one hollow interlayer toughened glass plate blank into a vacuum furnace provided with a supporting base, a fixed supporting clamp or a tray; an ultrasonic transducer for improving the bonding quality of glass and glass, glass and metal is arranged on a glass tray of the vacuum furnace; closing the door of the vacuum furnace, and vacuumizing the blank of the hollow interlayer toughened glass plate in the vacuum furnace; the gas in the airtight sealant and the structural sealant is completely discharged; the airtight sealant, the bonding surface of the structural sealant and the glass and the bonding surface of the stainless steel are fully soaked and wetted under the action of self cohesion after gas is discharged by the airtight sealant and the structural sealant under the capillary action of contact gaps between the stainless steel and the glass, between the glass and between the stainless steel and the stainless steel, so that the bonding of the airtight sealant and the structural sealant to the glass and the stainless steel frames is realized;
meanwhile, the groove of the closed-loop stainless steel frame with the U-shaped section is designed to be deeper, so that the sealing glue layer of the closed-loop structure corresponding to the groove is also longer, and the formed bonding connection sealing layer is thicker, so that the bonding strength of the structural sealant and the glass and the stainless steel is high, and the airtight sealing performance is good;
when the vacuum degree is reached and the vacuum pumping time is set, introducing high-humidity air into the vacuum furnace, and instantly closing an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting; the air generates pressure, the stainless steel frame quickly compacts the softened airtight sealing glue and the structural sealing glue layer under the action of air pressure, and the airtight sealing glue and the structural sealing glue layer are bonded and solidified;
by the process, the bonding quality of the glass and the stainless steel through the airtight sealing glue and the structural sealing glue is improved; opening a vacuum furnace door to manufacture a heat-preservation toughened glass plate body provided with a hollow air inlet and outlet communicated sealing pipe fitting, wherein the periphery of the toughened glass plate body is provided with two annular closed bonding sealing belts and a stainless steel closed-loop protection frame, and the glass hollow interlayer is a heat-preservation lighting toughened glass plate with adjustable and controllable vacuum degree;
or horizontally placing at least one hollow interlayer toughened glass plate blank into a vacuum furnace provided with a supporting base, a fixed supporting clamp or a tray; closing the door of the vacuum furnace, and heating and vacuumizing the blank of the hollow interlayer toughened glass plate in the vacuum furnace; the gas in the hot-melt airtight sealant and the structural sealant is completely discharged; under the capillary action of contact gaps between stainless steel and glass, between glass and glass, between stainless steel and stainless steel, and under the action of self-cohesion after gas is discharged by the hot-melt airtight sealant and the structural sealant, the hot-melt airtight sealant, the bonding surface of the structural sealant and the glass, and the bonding surface of the stainless steel are fully soaked and wetted, so that the bonding of the hot-melt airtight sealant and the structural sealant to the glass and the stainless steel frame is realized;
meanwhile, the groove of the closed-loop stainless steel frame with the U-shaped section is designed to be deeper, so that the sealing glue layer of the closed-loop structure corresponding to the groove is also longer, and the formed bonding connection sealing layer is thicker, so that the bonding strength of the structural sealant and the glass and the stainless steel is high, and the airtight sealing performance is good;
when the heating temperature, the vacuum degree and the set vacuumizing time are reached, high-humidity air is introduced into the vacuum furnace, and an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting is closed instantly; the air absorbs heat, rises temperature and expands to generate pressure, the stainless steel frame quickly compacts the hot-melt airtight sealing adhesive and the structural sealing adhesive layer in a softened state under the action of air pressure, releases heat and solidifies, and then, or starts a cooling device arranged in the vacuum furnace to cool the vacuum furnace;
or introducing high-humidity air into the vacuum furnace, and instantly closing an exhaust vacuum valve arranged on the pipe orifice of the communicating sealing pipe fitting; the air absorbs heat, the temperature rises and expands to generate pressure, the stainless steel frame rapidly compacts the hot-melt airtight sealing adhesive and the structural sealing adhesive layer in a softened state under the action of air pressure, the hot-melt airtight sealing adhesive and the structural sealing adhesive layer are made to release heat and solidify, then the vacuum furnace is cooled by releasing hot air and filling cold air, or a cooling device arranged in the vacuum furnace is started to cool the vacuum furnace, and the structural sealing adhesive in the stainless steel frame can be naturally cooled and solidified;
by the process, the bonding quality of the glass and the stainless steel through the hot-melt airtight sealing glue and the structural sealing glue is improved; when the temperature of the vacuum furnace is reduced to 50-55 ℃, the door of the vacuum furnace is opened to prepare the heat-insulating and lighting toughened glass plate with two annular sealing and bonding sealing belts and a stainless steel closed-loop protection frame on the periphery of the toughened glass plate body, wherein the vacuum degree of the glass hollow interlayer is adjustable.
5. The regulated vacuum tempered glass plate with rolled supporting double-glue sealed glass spacing cavity as claimed in claim 1 or 2, wherein: the toughened glass plate comprises a glass original sheet, toughened glass, cloth-pattern glass, embossed glass, halogenated glass, frosted glass and coated glass, and functional films of the coated glass comprise an anti-reflection film, a metal film and a decorative film; the surface of the glass panel is compounded with the coating, so that the coating must be removed from the bonding surface of the glass panel; the toughened glass plate is double-layer or multi-layer laminated glass.
6. The regulated vacuum tempered glass plate with rolled supporting double-glue sealed glass spacing cavity as claimed in claim 1 or 2, wherein: the embossed toughened glass plate and the corrugated toughened glass plate are formed by hot-pressing and stretching the flat glass through corresponding dies or blow-stretching the flat glass through heating under positive and negative pressure of the corresponding dies; the convex point glass sheet is flat printed glass produced by adopting a rolling method, and a series of pits which are equal in shape and size and are arranged according to the dot matrix of the convex point support are engraved on the surface of a rolling roller of the glass rolling machine and are used as a printing mould of the convex points;
the embossed toughened glass plate with the convex points is formed by rolling the glass convex points on a proper temperature position in a glass tin bath by a glass rolling machine when a flat glass original sheet is produced; a series of pits which are uniform in shape and size and are arranged according to the dot matrix of the convex point supports are engraved on the surface of one calendering roller of the glass calender; cutting, edging and toughening the embossed toughened glass plate with the convex points;
or the embossed and toughened glass plate with the convex points is heated by a toughening furnace after edging and shaping a flat glass sheet, and is subjected to toughening treatment after rolling the convex points by a glass rolling mill and bending the supporting frame; a series of pits which are uniform in shape and size and are arranged according to the dot matrix of the convex point supports are engraved on the surface of one calendering roller of the glass calender;
or the convex-hull toughened glass plate or the corrugated toughened glass plate is rolled with glass concave points by a glass rolling machine at a proper temperature position in a glass tin bath when producing a flat glass sheet; the surface of a calendering roller on the used glass calender is engraved with a series of convex tips which are uniform in shape and size and are arranged according to the lattice of the concave point support; cutting, edging and toughening the concave embossed toughened glass plate;
or after edging and shaping the convex toughened glass plate or the corrugated toughened glass plate, heating the convex toughened glass plate or the corrugated toughened glass plate by a toughening furnace, stretching the convex points by a glass mold, bending the supporting frame, and after shaping, carrying out toughening treatment;
or the bump toughened glass plate is made by printing glass powder paste and sintering; firstly, printing low-temperature glass powder paste on a piece of plate glass according to the dot matrix arrangement pattern of the bump support, then sending the plate glass into a toughening sintering furnace, heating to a certain proper temperature of the melting point of the glass powder paste, converting a glass powder paste accumulation body into glass bumps fused with the surface of the plate glass, then bending a support frame, and carrying out toughening treatment;
the support is a support with at least one end coated with adhesive, and comprises a high-hardness glass support, a high-hardness metal support and a high-hardness ceramic support which are equal to or close to the height of the raised frame support band, and columnar, spherical or annular support lattices are arranged; or the support is a support heat insulation material pad with an aerogel heat insulation pad bonded on the end support surface, and the surfaces of the aerogel heat insulation pads at the two ends of the support heat insulation material pad are coated with hot melt adhesive, glass cement, ultraviolet curing cement or water glass cement;
cutting flat glass with proper thickness according to the design size, edging and toughening the toughened glass panel, and using the toughened glass panel as a raw material; deoiling, cleaning and drying the glass bonding surface.
7. The regulated vacuum tempered glass plate with rolled supporting double-glue sealed glass spacing cavity as claimed in claim 1 or 2, wherein: the holes on the hollow interlayer toughened glass plate body are arranged on the glass panel or on the raised frame supporting bands and the raised frame supporting bands; the communicated sealing pipe fitting is a pipe fitting with a T-shaped section and a thread arranged on the outer wall of the pipe provided with a head blocking pipe, the thread of the pipe fitting is correspondingly provided with a tooth ridge at the root and an upward conical nut, the pipe fitting is screwed and sealed on the hollow interlayer toughened glass plate body through an airtight sealing glue and the nut, or the pipe fitting with the thread arranged on the outer wall of the pipe, the thread of the pipe fitting is correspondingly provided with a tooth ridge at the root and an upward conical nut, and the pipe fitting is screwed and sealed on the hollow interlayer toughened glass plate body through an airtight sealing glue and the nut; the communicated sealing pipe fitting is provided with a fastening sealing pipe fitting corresponding to the opening of the toughened glass plate, the air inlet and outlet pipe heads are locked and sealed by airtight sealing glue and the fastening sealing pipe fitting and are fixed on the opening of the air inlet and outlet pipe heads on the toughened glass plate, the section is T-shaped and is provided with a baffle head, the baffle head is provided with an air vent groove, and the outer wall of the pipe is provided with a threaded pipe fitting or is made of magnetic material.
8. The regulated vacuum tempered glass plate with rolled supporting double-glue sealed glass spacing cavity as claimed in claim 1 or 2, wherein: the periphery of the annular closed glass or the annular closed glass supporting frame is sealed and bonded by airtight sealing glue and structural sealing glue which do not generate chemical reaction with each other; the sealant at the inner sides of the peripheries of the two pieces of glass is a first adhesive and is bonded by using airtight sealing glue; the first airtight sealant comprises butyl sealant, such as polyisobutylene rubber and hot melt butyl rubber; the sealant at the outer sides of the peripheries of the two pieces of glass is a second adhesive and is adhered by a structural sealant; the second sealant is a curing weather-resistant structure sealant, and comprises elastic sealants for glass, such as polysulfides, silicones and polyamines; the hot-melt structural sealant comprises hot-melt polyisobutylene rubber and hot-melt butyl rubber;
the metal thin strip with good plasticity for prolonging the bonding thickness of the airtight sealant comprises an aluminum strip, a copper strip and a stainless steel strip.
9. The regulated vacuum tempered glass plate with rolled supporting double-glue sealed glass spacing cavity as claimed in claim 1 or 2, wherein: manufacturing a raised frame supporting strip corresponding to the size of the glass panel, wherein the height of the raised frame supporting strip and the width of the airtight sealing glue bonding sealing surface are determined according to the design size; bonding the airtight sealant of the raised frame supporting band on the surface, and performing deoiling, cleaning and drying treatment; the raised frame supporting belt is a rectangular glass strip or a metal strip which has the same thickness as the heat-preservation and lighting toughened glass plate and is edged at the edge, and is adhered to the raised frame supporting belt formed on the edge of the toughened glass plate through airtight sealing glue; or the raised frame supporting strips are rectangular glass strips or metal strips and are bonded and formed by airtight sealing glue;
or the raised frame supporting belt is a U-shaped metal section with the outer width corresponding to the width of the edge of the toughened glass plate and is formed by hot melt welding and laser welding;
or the raised frame supporting belt is a U-shaped metal section with the outer width corresponding to the width of the edge of the toughened glass plate and is bonded and formed by airtight sealant; the section of the U-shaped section is arranged at the airtight sealing glue bonding position, and an airtight sealing glue bonding and splicing filling patch which enlarges the sealing connection surface and corresponds to the shape of the airtight sealing glue bonding position of the U-shaped section is arranged;
or the raised frame supporting belt is a T-shaped metal section with the outer width slightly larger than the width of the edge of the heat-preservation lighting toughened glass plate, and is bonded and formed by airtight sealant; corner joint parts of the T-shaped metal section bars are provided with corner-supplementing bonding patches;
the metal thin strip with good plasticity, which prolongs the bonding thickness of the airtight sealant, is an aluminum strip or a stainless steel strip;
the periphery of the hollow interlayer toughened glass plate body is wrapped with a closed-loop corrugated stainless steel frame with a U-shaped section; the U-shaped corrugated stainless steel channel section is formed by stamping and stretching a stainless steel strip through a die, or the U-shaped corrugated stainless steel channel section is formed by rolling the stainless steel strip through a rolling mill; the closed-loop corrugated stainless steel frame is a U-shaped corrugated stainless steel groove profile, and is made into an elastic closed-loop corrugated stainless steel frame by bending welding or cutting welding;
when the U-shaped closed-loop corrugated stainless steel frame groove is used, deoiling, cleaning and drying treatment are required;
the outer side of the periphery of the hollow interlayer toughened glass plate body is wrapped with a protective frame of a hollow interlayer toughened glass plate structure which is formed by buckling and sleeving a closed-loop stainless steel frame with an L-shaped and an inverted L-shaped section; the L-shaped stainless steel section is a stainless steel strip and is formed by stamping and stretching through a die, or the L-shaped stainless steel section is a stainless steel strip and is formed by rolling through a rolling mill; the closed loop 'L' -shaped stainless steel frame is an 'L' -shaped stainless steel section bar and is made into a stainless steel frame by bending welding or cutting welding;
when the L-shaped stainless steel section is used, deoiling, cleaning and drying treatment are required.
10. The system for regulating and controlling the vacuum tempered glass plate with the rolling-supported double-glue sealed glass interval cavity as claimed in claim 1 or 2, which comprises a tempered glass plate provided with an air inlet and outlet pipe fitting sealed glass peripheral regulating and controlling interval interlayer function gas pressure, a vacuum valve, a vacuum gauge, an air inlet and outlet pipeline and a vacuum pump set, and is characterized in that: at least one tempered glass plate provided with an air inlet and outlet pipe fitting, a sealed glass periphery and a function gas pressure regulating and controlling interlayer, wherein the air inlet and outlet pipe fitting is connected with an air inlet and outlet pipeline in parallel and in a sealing way by welding, bonding and bolting a nut sealed pipe fitting, and a vacuum meter is connected on the air inlet and outlet pipeline; the air inlet and outlet pipeline is hermetically connected with a vacuum pump set through a vacuum valve, and the vacuum pump set is opened and closed through a numerical value standard set by a vacuum meter; or the variable-frequency vacuum pump set is used for outputting power according to the numerical value standard set by the vacuum meter;
the gas inlet and outlet pipeline is connected and controlled by a vacuum valve, and a functional gas inlet pipeline is controlled to be opened and closed by a preposed vacuum valve; a dryer component is arranged on the air inlet pipeline arranged in front of the vacuum valve; the drier component is provided with an electric heating dehumidification device and an air exhaust valve;
a plurality of groups of functional gas tanks containing air are arranged on the pipeline before the dryer or are arranged on the pipeline; the functional gas tank group comprises a low-heat-conductivity-coefficient gas argon tank and a carbon dioxide gas tank, and the high-heat-conductivity-coefficient gas comprises a hydrogen tank and a helium tank;
the vacuum meter is a conventional vacuum meter or an artificial intelligent vacuum meter, and the vacuum valve is a conventional vacuum valve or an artificial intelligent vacuum valve;
the vacuum pump set is provided with two groups of vacuum pumps for rough pumping and fine pumping, and the two groups of vacuum pumps for rough pumping and fine pumping can run in parallel or in series; or after the rough vacuum pump is pumped to the set vacuum, the rough vacuum pump is closed, and the fine vacuum pump is started until the fine vacuum pump is closed after the rough vacuum pump is pumped to the set vacuum; when the vacuum degree is reduced to a set value, the vacuum pump set is started again; or the vacuum pump set is a continuously running variable-frequency vacuum pump set;
after the vacuum degree of the sealed glass peripheral regulation and control interlayer functional gas pressure heat-preservation toughened glass plate is reduced to a set value, or a vacuum valve arranged on a pipe fitting of the sealed glass peripheral regulation and control interlayer functional gas pressure heat-preservation toughened glass plate is automatically closed, a vacuum pump measures the vacuum degree in an interlayer of the sealed glass peripheral regulation and control interlayer functional gas pressure heat-preservation toughened glass plate, whether the heat-preservation heat-dissipation light-transmission toughened glass cover leaks vacuum is judged, and the vacuum valve is automatically opened and closed when the vacuum is increased to or reduced to the set;
according to design requirements, the heat-preservation heat-dissipation light-transmitting toughened glass cover of the heat-preservation heat-dissipation light-transmitting toughened glass plate is formed by regulating and controlling the air pressure of the functional gas at the periphery of the sealing glass and the interlayer, and good heat dissipation of the heat-preservation heat-dissipation light-transmitting toughened glass cover is realized by introducing hydrogen or helium of gas with high heat conductivity coefficient into the heat-preservation heat-dissipation light-transmitting toughened glass cover;
the conventional heat dissipation of the heat-preservation heat-dissipation light-transmitting toughened glass cover is realized by introducing air into the heat-preservation heat-dissipation light-transmitting toughened glass cover;
the conventional heat preservation of the heat preservation and radiation transparent toughened glass cover is realized by introducing argon or carbon dioxide of gas with low heat conductivity coefficient into the heat preservation and radiation transparent toughened glass cover;
through the evacuation to heat preservation heat dissipation printing opacity toughened glass cover, realize the good heat preservation of heat preservation heat dissipation printing opacity toughened glass cover.
CN201911255886.3A 2018-12-11 2019-12-10 Regulating and controlling vacuum toughened glass plate with rolling support double-glue sealed glass spacing cavity Pending CN111302665A (en)

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